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inquiryN,N-Dimethylbenzamide Chemical Properties Melting point 43-45 °C (lit.) Boiling point 132-133 °C/15 mmHg (lit.) density 1.0753 (rough estimate) refractive index 1.5279 (estimate) Fp >230 °F pka -1.14±0.70(
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benzoic acid methyl ester
methylchloroaluminum N,N-dimethylamide
N,N-dimethylbenzamide
Conditions | Yield |
---|---|
In benzene for 12h; Heating; | 100% |
N,N-dimethylthiobenzamide
N,N-dimethylbenzamide
Conditions | Yield |
---|---|
With 6H(1+)*Mo9O40PV3(6-); oxygen In acetonitrile at 90℃; under 760.051 Torr; for 2h; Inert atmosphere; Glovebox; | 99% |
With hydrogenchloride; N-nitrosopiperidine; potassium iodide In dichloromethane; water at 22℃; for 50h; | 94% |
With hydrogenchloride; sodium nitrite In water at 20℃; for 0.5h; | 94% |
Conditions | Yield |
---|---|
With tert.-butylhydroperoxide In acetonitrile at 80℃; for 24h; | 99% |
Conditions | Yield |
---|---|
With tert.-butylhydroperoxide; copper(II) oxide In water at 80℃; for 20h; Catalytic behavior; | 99% |
With tert.-butylhydroperoxide; copper(II) perchlorate hexahydrate at 100℃; for 15h; | 90% |
With trichlorophosphate at 120℃; for 1h; Sealed tube; | 90% |
Conditions | Yield |
---|---|
In 5,5-dimethyl-1,3-cyclohexadiene for 12h; Reflux; | 99% |
benzoyl chloride
A
2,4,6-Triphenyl-thiopyrylium-chlorid
B
N,N-dimethylbenzamide
Conditions | Yield |
---|---|
With 2-Dimethylamino-2,4,6-triphenyl-2H-thiopyran In diethyl ether for 1h; Heating; | A 98% B 40% |
2-Dimethylamino-2,4,6-triphenyl-2H-thiopyran
A
2,4,6-Triphenyl-thiopyrylium-chlorid
B
N,N-dimethylbenzamide
Conditions | Yield |
---|---|
With benzoyl chloride In diethyl ether for 1h; Heating; | A 98% B 40% |
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine; (bis-(2-methoxyethyl)amino)sulfur trufluoride In dichloromethane at 0℃; for 0.5h; | 98% |
With tetrabutylammomium bromide; iodine; potassium hydroxide In water at 20℃; for 2.5h; Irradiation; | 75% |
With dichloro(dimethylglyoxime)(dimethylglyoximato)cobalt(III); [4,4′-bis(1,1-dimethylethyl)-2,2′-bipyridine-N1,N1′]bis{3,5-difluoro-2-[5-(trifluoromethyl)-2-pyridinyl-κN]phenyl-κC}iridium(III) hexafluorophosphate; triphenylphosphine In dichloromethane at 20℃; for 12h; Inert atmosphere; Sealed tube; Irradiation; | 74% |
Stage #1: dimethyl amine; benzoic acid at 60℃; Autoclave; Cooling with dry ice; Stage #2: at 290℃; under 22502.3 Torr; for 0.0136111h; Microwave irradiation; |
Conditions | Yield |
---|---|
With sodium methylate; nickel diacetate In 1,4-dioxane at 110℃; | 98% |
Stage #1: N,N-dimethyl-formamide With 1,3,5-trichloro-2,4,6-triazine at 20℃; for 1h; Stage #2: bromobenzene With 1,1'-bis-(diphenylphosphino)ferrocene; palladium diacetate In N,N-dimethyl-formamide at 120℃; for 6h; | 81% |
With palladium diacetate; 4,5-bis(diphenylphos4,5-bis(diphenylphosphino)-9,9-dimethylxanthenephino)-9,9-dimethylxanthene; trichlorophosphate at 165℃; for 24h; Inert atmosphere; | 72% |
Conditions | Yield |
---|---|
With Pd nanoparticles supported on reduced graphene oxide nanosheets at 200℃; for 6h; Temperature; Concentration; Autoclave; | 98% |
With palladium diacetate; 4,5-bis(diphenylphos4,5-bis(diphenylphosphino)-9,9-dimethylxanthenephino)-9,9-dimethylxanthene; trichlorophosphate at 135℃; for 6h; Inert atmosphere; | 93% |
Stage #1: N,N-dimethyl-formamide With tungsten(VI) chloride at 20℃; for 0.25h; Inert atmosphere; Stage #2: iodobenzene With palladium dichloride at 140℃; for 5h; Catalytic behavior; Reagent/catalyst; Temperature; Inert atmosphere; | 93% |
N,N-dimethylbenzamide dimethyl acetal
B
N,N-dimethylbenzamide
Conditions | Yield |
---|---|
With trichloroacetamidine In tetrahydrofuran at 40 - 50℃; for 3h; Title compound not separated from byproducts; | A 96% B 5% |
N,N-dimethylbenzamide dimethyl acetal
trichloroacetamidine
B
N,N-dimethylbenzamide
Conditions | Yield |
---|---|
In tetrahydrofuran at 40 - 50℃; for 3h; Title compound not separated from byproducts; | A 96% B 5% |
tert-butyl benzoyl(phenyl)carbamate
dimethyl amine
N,N-dimethylbenzamide
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 23℃; for 15h; Inert atmosphere; Schlenk technique; | 96% |
1,3-diphenylpropanedione
N,N-dimethyl-formamide
N,N-dimethylbenzamide
Conditions | Yield |
---|---|
With iodosylbenzene at 25℃; for 24h; | 96% |
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 20℃; Inert atmosphere; | 95% |
With triethylamine In dichloromethane at 0 - 20℃; | 93% |
With dmap; triethylamine In tetrahydrofuran; dichloromethane at 0 - 20℃; for 12h; | 91% |
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 23℃; for 15h; Inert atmosphere; Schlenk technique; | 95% |
N,N-phenyl-p-toluenesulfonylbenzamide
dimethyl amine
N,N-dimethylbenzamide
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 23℃; for 15h; Inert atmosphere; Schlenk technique; | 94% |
2-bromo-N,N-dimethyl benzamide
N,N-dimethylbenzamide
Conditions | Yield |
---|---|
With [ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2; potassium tert-butylate; isopropyl alcohol at 100℃; Schlenk technique; Inert atmosphere; | 93% |
Conditions | Yield |
---|---|
In chloroform for 1h; | 92% |
Conditions | Yield |
---|---|
With sodium iodide In dimethyl sulfoxide at 20℃; for 6h; Solvent; Reagent/catalyst; Electrochemical reaction; | 92% |
Conditions | Yield |
---|---|
With dysprosium at 20℃; for 0.333333h; Inert atmosphere; | 91% |
Stage #1: N,N-dimethyl-formamide With potassium tert-butylate In tetrahydrofuran at 20℃; for 0.25h; Schlenk technique; Stage #2: benzoyl chloride In tetrahydrofuran at 50℃; for 12h; | 84% |
benzoyl chloride
2-Dimethylamino-3-methyl-2,4,6-triphenyl-2H-pyran
A
3-Methyl-2,4,6-triphenylpyryliumchlorid
B
N,N-dimethylbenzamide
Conditions | Yield |
---|---|
In diethyl ether for 1h; Heating; | A 91% B 54% |
2-Dimethylamino-3-methyl-2,4,6-triphenyl-2H-pyran
A
3-Methyl-2,4,6-triphenylpyryliumchlorid
B
N,N-dimethylbenzamide
Conditions | Yield |
---|---|
With benzoyl chloride In diethyl ether for 1h; Heating; | A 91% B 54% |
Conditions | Yield |
---|---|
With oxygen; sodium hydroxide In water at 25℃; for 24h; Green chemistry; | 91% |
With oxygen; sodium hydroxide In water at 25℃; for 24h; | 90% |
With tert.-butylhydroperoxide; [bis(acetoxy)iodo]benzene In acetonitrile Reagent/catalyst; Solvent; Reflux; | 86% |
Conditions | Yield |
---|---|
With tert.-butylhydroperoxide; iodine at 70 - 80℃; for 24h; | 91% |
With hydrogenchloride; tert.-butylhydroperoxide; iodine In cyclohexane; water at 80℃; | 88% |
With tert.-butylhydroperoxide; tetra-(n-butyl)ammonium iodide at 80℃; for 24h; | 85% |
N,N-dimethylbenzamide
Conditions | Yield |
---|---|
With (R)-(+)-2,2'-bis[bis(3,5-dimethylphenyl)phosphino]-1,1'-binaphthyl; bis(1,5-cyclooctadiene)iridium(I) tetrakis[3,5-bis(trifluoromethyl)phenyl]borate In tetrahydrofuran at 135℃; for 24h; Reagent/catalyst; Sealed tube; Inert atmosphere; | 91% |
Conditions | Yield |
---|---|
bis(di-tert-butylphosphinous acid)PdCl2 In acetonitrile at 25℃; for 24h; | 90% |
Conditions | Yield |
---|---|
In methanol at 20℃; for 3h; UV-irradiation; | 90% |
Conditions | Yield |
---|---|
In toluene at 100℃; for 12h; | 90% |
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide | 88% |
N,N-dimethylbenzamide
Conditions | Yield |
---|---|
In n-heptane soln. was refluxed for 5 h, after cooling, heptane was removed under vac.; elem.anal.; | 100% |
Conditions | Yield |
---|---|
With C37H46FeN4; diphenylsilane In tetrahydrofuran at 70℃; for 24h; Schlenk technique; Inert atmosphere; | 99% |
With Pt(ItBu)(divinyltetramethyldisiloxane); diphenylsilane In tetrahydrofuran; Hexadecane at 40℃; for 1h; Reagent/catalyst; Solvent; Schlenk technique; Inert atmosphere; | 99% |
With triethyl borane; phenylsilane; sodium hydroxide In tetrahydrofuran; tert-butyl methyl ether at 20℃; Reagent/catalyst; Solvent; Inert atmosphere; Schlenk technique; Sealed tube; chemoselective reaction; | 99% |
N,N-dimethylbenzamide
N,N-dimethylthiobenzamide
Conditions | Yield |
---|---|
With thiophosphorylated amine resin In toluene at 90℃; for 30h; | 99% |
With tetraphosphorus decasulfide In dichloromethane for 0.25h; Inert atmosphere; Reflux; | 99% |
With tetraphosphorus decasulfide; sodium carbonate In tetrahydrofuran at 25℃; for 4h; | 90% |
Conditions | Yield |
---|---|
With silver hexafluoroantimonate; copper diacetate; C46H44I4Ir2N2O4 In 1,4-dioxane at 100℃; for 24h; Glovebox; Inert atmosphere; | 99% |
N-Bromosuccinimide
N,N-dimethylbenzamide
N-methyl-N-succinimidomethylbenzamide
Conditions | Yield |
---|---|
With dibenzoyl peroxide In tetrachloromethane Product distribution; Heating; succinimidation by N-bromosuccinimide of N,N-dimethylamides and N,N-dimethylamines; | 98% |
With dibenzoyl peroxide In tetrachloromethane Heating; | 98% |
Conditions | Yield |
---|---|
With n-butyllithium; borane-THF; diisopropylamine at 25℃; | 98% |
With diisobutylaluminum borohydride In tetrahydrofuran at 0 - 25℃; Inert atmosphere; | 98% |
With diisobutylaluminum borohydride In tetrahydrofuran at 25℃; for 1h; Inert atmosphere; | 98% |
acrylic acid n-butyl ester
N,N-dimethylbenzamide
N,N-dimethyl-2-[(E)-(n-butoxycarbonyl)ethenyl]benzamide
Conditions | Yield |
---|---|
With [ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2; Ag(1+)*(x)F6Sb; copper(II) acetate monohydrate In tert-Amyl alcohol at 100℃; for 4h; Inert atmosphere; regioselective reaction; | 98% |
With silver hexafluoroantimonate; tris(2,2-bipyridine)ruthenium(II) hexafluorophosphate; dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer In chlorobenzene at 80℃; for 16h; Heck Reaction; Irradiation; | 91% |
Conditions | Yield |
---|---|
With lithium diisobutylmorpholinoaluminum hydride In tetrahydrofuran; hexane at 0℃; for 0.5h; Concentration; Time; | 97% |
Stage #1: N,N-dimethylbenzamide With chloromagnesium dimethylaminoborohydride In tetrahydrofuran at 25℃; for 0.5h; Inert atmosphere; Stage #2: With acetaldehyde; acetic acid In tetrahydrofuran; pentane for 5h; Inert atmosphere; | 74% |
With diethyl ether; diisobutylaluminium hydride |
Conditions | Yield |
---|---|
With trichlorophosphate at 30 - 40℃; Microwave irradiation; | 97% |
4-Methoxyphenethylamine
N,N-dimethylbenzamide
N-[2-(4-methoxyphenyl)ethyl]benzamide
Conditions | Yield |
---|---|
With Imidazole hydrochloride at 150℃; for 3h; Sealed tube; | 97% |
Li{(CH2)(CH2)P(C6H5)2}
N,N-dimethylbenzamide
A
Methyl-diphenyl-phenacyl-phosphonium
B
acetophenone
C
diphenyl(methyl)phosphine oxide
Conditions | Yield |
---|---|
With HX In water 1.) 2 h, -55 deg C; 2.) 13 h, 21 deg C; | A 96% B 20% C 20% |
With HX In water 1.) 2 h, -55 deg C; 2.) 13 h, 21 deg C; | A 80% B 20% C 20% |
N,N-dimethylbenzamide
Conditions | Yield |
---|---|
With C34H43IrN3(1+)*F6P(1-); deuterium In dichloromethane at -78℃; for 16h; Reagent/catalyst; Inert atmosphere; | 96% |
With Crabtree's catalyst; water-d2; deuterium In dichloromethane at 20℃; | |
With silver tetrafluoroborate; bis(1,5-cyclooctadiene)diiridium(I) dichloride; deuterium; triphenylphosphine In dichloromethane at 20℃; | 2 mg |
With water-d2; Ir(cod)(hfac) In N,N-dimethyl acetamide at 160℃; for 0.0333333h; microwave irradiation; | |
With 2,6-(2,6-iPr2-C6H3-4,5-H2-imidazol-2-ylidene)2C5H3NFe(N2)2; deuterium In tetrahydrofuran at 45℃; under 3040.2 Torr; for 24h; |
tris(1,3-diphenyl-1,3-propanedionato)aquoeuropium(III)
N,N-dimethylbenzamide
Conditions | Yield |
---|---|
In acetone Eu complex in acetone reacted with dimethylbenzamide; solvent evapd., ppt. washed with water, vac. dried; elem. anal.; | 96% |
1H-imidazole
N,N-dimethylbenzamide
N-((1H-imidazol-1-yl)methyl)-N-methylbenzamide
Conditions | Yield |
---|---|
With di-tert-butyl peroxide; iron(II) chloride In chlorobenzene at 120℃; for 3h; Inert atmosphere; Schlenk technique; | 96% |
Conditions | Yield |
---|---|
With dipotassium peroxodisulfate; potassium iodide at 80℃; for 6h; Schlenk technique; | 96% |
Conditions | Yield |
---|---|
Stage #1: C54H62N6; N,N-dimethylbenzamide With trichlorophosphate In 1,2-dichloro-ethane at 20 - 40℃; for 2h; Vilsmeier-Haack Formylation; Inert atmosphere; Stage #2: With potassium hexafluorophosphate; sodium hydrogencarbonate In water | 96% |
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