As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem’s R&D center offer custom synthesis according to the contract research and development services for
Cas:621-23-8
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inquiryItems Standard Result Assay 99.9%min 99.9% Hangzhou Dingyan Chem is a leading manufacturer and supplier of che
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inquiryProduct Description Product website: http://www.finerchem.com Product Name Phloroglucinol trimethyl ether CAS No. 621-23-8 Appearan
Cas:621-23-8
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inquiryUnique advantages Guaranteed purity High quality & competitive price Quality control Fast feedback Prompt shipment Appearance:White or almost white crystalline powder Storage:cool dry place Package:1kg/foil bag;25kg/drum Application:pharma
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inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
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inquiryCangzhou Enke Pharma Tech Co.,ltd. is located in Cangzhou City, Hebei province ,where is a famous petroleum chemical industry city in China. Enke Pharma a high-tech enterprise ,and we are dedicated to developing and manufacturing new ap
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inquiryShanghai Seasonsgreen Chemical is a high-tech research and development, production, sale and custom synthesis set in one high-tech chemical products enterprises. Our sales and marketing division is located in Shanghai, serving international pharmaceu
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inquiry1,3,5-Trimethoxybenzene 621-23-8 1,3,5-Trimethoxybenzene Basic information Product Name: 1,3,5-Trimethoxybenzene Synonyms: PHLOROGLUCINOL TRIMETHYL ETHER;TRISMETHOXYBENZENE;1,3,5-trime
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inquiryOur advantages: 1. All inquiries will be replied within 12 hours. 2. Dedication to quality, supply & service. 3. Strictly on selecting raw materials. 4. Reasonable & competitive price, fast lead time. 5. Sample is available for your eva
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inquiryOur Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We
Cas:621-23-8
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inquiryName: Phloroglucinol trimethyl ether CAS NO.:621-23-8 Molecular formula: C9H12O3 Molecular weight: 168.19 Appearance:White or off-white crystal Storage:Store in cool and dry place, away from sun light. Package:25kg Application:Medicinal (eg,
Advantages: Hubei XinRunde Chemical Co., Ltd is a renowned pharmaceutical manufacturer. We can offer high quality products at competitive price in quick delivery with 100% custom pass guaranteed. Never stop striving to offer our best service is
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inquiry1,3,5-Trimethoxybenzene CAS: 621-23-8 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic in
Cas:621-23-8
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inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
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Type:Trading Company
inquiryBest quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia
Product Name: 1,3,5-Trimethoxybenzene Synonyms: 1,3,5-trimethoxy-benzen;1,3,5-Trimethyoxybenzene;Benzene, 1,3,5-trimethoxy-;3,5-DIMETHOXYANISOLE;1,3,5-TRIMETHOXYBENZENE;1,3,5-Trimethoxybenzene/Phloroglucinol trimethyl ether;O,O,O-1,3,5-trimethyl
Cas:621-23-8
Min.Order:100 Gram
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inquiryAppearance:White to cream crystalline powder Storage:Store below +30°C. Package:As customer request Transportation:As customer request Port:Qingdao,China
Cas:621-23-8
Min.Order:100 Gram
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Type:Lab/Research institutions
inquiry1. Timely and efficient service to ensure communication with customers 2. Produce products of different specifications and sizes according to your requirements. 3. Quality procedures and standards recognized by SGS. Advanced plant equipment ensures
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inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
Cas:621-23-8
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inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
Our Services 1. New Molecules R&D 2. Own test center HPLC NMR GC LC-MS 3. API and Intermediates from China reputed manufacturers 4. Documents support COA MOA MSDS DMF open part Our advantages 1. Government awarded company. Top 100 enter
Conditions | Yield |
---|---|
With tris-(dibenzylideneacetone)dipalladium(0); tert-butyl XPhos In N,N-dimethyl-formamide at 100℃; Inert atmosphere; | 100% |
Conditions | Yield |
---|---|
Stage #1: methanol; 1,3,5-trisbromobenzene In toluene at 135℃; under 5320.36 Torr; for 0.75h; Stage #2: With triethylamine In toluene at 165℃; under 8360.56 Torr; for 11h; Temperature; | 99.5% |
With sodium methylate; copper(l) chloride In N,N-dimethyl-formamide at 100 - 110℃; for 6h; | 90% |
Conditions | Yield |
---|---|
With potassium carbonate In acetone for 3h; Reflux; | 99% |
With potassium carbonate In acetone for 6h; Reflux; | 80% |
With methanol man troepfelt methylalkoholische Natriummethylatloesung hinzu; |
Conditions | Yield |
---|---|
With palladium(II) trifluoroacetate; trifluoroacetic acid In dimethyl sulfoxide; N,N-dimethyl-formamide at 70℃; for 24h; | 99% |
With [Rh(OH)(cod)]2; 1,3-bis-(diphenylphosphino)propane; water; sodium hydroxide In toluene at 120℃; for 18h; Inert atmosphere; | 85% |
With sodium persulfate; ethanol at 60℃; for 18h; Temperature; Time; Sealed tube; Green chemistry; | 85% |
With C40H42NO7PPdS In dichloromethane at 20℃; Schlenk technique; |
Conditions | Yield |
---|---|
With trifluoroacetic acid In water at 80℃; for 0.5h; Diels-Alder Cycloaddition; | A n/a B 99% |
1,3,5-trimethoxybenzene-2,4,6-d3
1,2,3-trimethoxybenzene
Conditions | Yield |
---|---|
With tris(pentafluorophenyl)borate; water In chloroform at 80℃; for 24h; Sealed tube; | 98% |
With acetic acid In hexane at 24.9℃; Kinetics; Thermodynamic data; Rate constant; other solvents; ΔH(activ.); -ΔS(activ.); ΔF(activ.).; |
Conditions | Yield |
---|---|
With methanol; Methyl formate; copper(l) chloride at 115℃; for 2h; Autoclave; Green chemistry; | 98% |
With copper(I) chloride In N,N-dimethyl-formamide at 130℃; for 6h; | 91% |
A
1,2,3-trimethoxybenzene
Conditions | Yield |
---|---|
With trifluoroacetic acid In water at 80℃; for 0.5h; Diels-Alder Cycloaddition; | A n/a B 98% |
A
1,2,3-trimethoxybenzene
Conditions | Yield |
---|---|
With trifluoroacetic acid In water at 80℃; for 0.5h; Diels-Alder Cycloaddition; | A n/a B 97% |
2-trimethylsilyl-1,3,5-trimethoxybenzene
1,2,3-trimethoxybenzene
Conditions | Yield |
---|---|
With chloro-trimethyl-silane; water; potassium iodide In acetonitrile at 20℃; for 0.1h; | 96% |
1,2,3-trimethoxybenzene
Conditions | Yield |
---|---|
With trifluoroacetic acid at 120℃; | 96% |
Conditions | Yield |
---|---|
With N,N'-dimethylimidazolium-2-carboxylate In acetonitrile at 160℃; for 1.33333h; Microwave irradiation; Green chemistry; | 96% |
Conditions | Yield |
---|---|
With sodium; copper(I) iodide In N-methyl-acetamide; methanol | 95% |
1,3,5-trimethoxy-2-(buta-1,3-dienyl)benzene
1,2,3-trimethoxybenzene
Conditions | Yield |
---|---|
With trifluoroacetic acid at 120℃; | 95% |
ethyl 3-(2,4,6-trimethoxy phenyl)acrylate
1,2,3-trimethoxybenzene
Conditions | Yield |
---|---|
With trifluoroacetic acid at 120℃; | 95% |
Conditions | Yield |
---|---|
rhodium(III) chloride; 1,3-bis-(diphenylphosphino)propane In diethylene glycol dimethyl ether for 40h; Heating; | 94% |
With hydrogen In cyclohexane at 165℃; under 15001.5 - 26252.6 Torr; for 4h; Solvent; Autoclave; | 90.9% |
With bis(1,5-cyclooctadiene)diiridium(I) dichloride; air; triphenylphosphine In 1,4-dioxane for 48h; Heating; | 78% |
With methanol; scandium tris(trifluoromethanesulfonate) Mechanism; other aromatic aldehydes; |
1,2,3-trimethoxybenzene
Conditions | Yield |
---|---|
With trifluoroacetic acid at 120℃; | 94% |
Conditions | Yield |
---|---|
With trifluoroacetic acid In water at 80℃; for 0.5h; Solvent; Temperature; Time; Diels-Alder Cycloaddition; | A n/a B 94% |
A
1,2,3-trimethoxybenzene
Conditions | Yield |
---|---|
With trifluoroacetic acid In water at 80℃; for 0.5h; Diels-Alder Cycloaddition; | A n/a B 93% |
Conditions | Yield |
---|---|
With potassium carbonate In acetone | 92% |
With potassium carbonate In acetone for 48h; Reflux; | 92% |
With potassium carbonate In acetone for 0.0666667h; Heating; Microwave irradiation; | 91% |
1,3,5-trimethoxy 2-vinyl benzene
1,2,3-trimethoxybenzene
Conditions | Yield |
---|---|
With trifluoroacetic acid at 120℃; | 92% |
A
1,2,3-trimethoxybenzene
B
7-methyl-2-(4-methylphenyl)naphthalene
Conditions | Yield |
---|---|
With trifluoroacetic acid In water at 80℃; for 0.5h; Diels-Alder Cycloaddition; | A n/a B 92% |
A
1,2,3-trimethoxybenzene
Conditions | Yield |
---|---|
With trifluoroacetic acid In water at 80℃; for 0.5h; Diels-Alder Cycloaddition; | A n/a B 92% |
A
1,2,3-trimethoxybenzene
B
2-(4'-bromophenyl)-7-bromonaphthalene
Conditions | Yield |
---|---|
With trifluoroacetic acid In water at 80℃; for 0.5h; Diels-Alder Cycloaddition; | A n/a B 92% |
1,2,3-trimethoxybenzene
Conditions | Yield |
---|---|
With Octanethiol; trifluorormethanesulfonic acid In dichloromethane at 23℃; for 12h; | 91% |
Conditions | Yield |
---|---|
With tin(IV) chloride In 1,2-dichloro-ethane Heating; | 90% |
1,2,3-trimethoxybenzene
Conditions | Yield |
---|---|
With trifluoroacetic acid at 120℃; | 90% |
Conditions | Yield |
---|---|
With trifluoroacetic acid In water at 80℃; for 0.5h; Diels-Alder Cycloaddition; | A n/a B 90% |
A
1,2,3-trimethoxybenzene
Conditions | Yield |
---|---|
With trifluoroacetic acid In water at 80℃; for 0.5h; Diels-Alder Cycloaddition; | A n/a B 90% |
A
1,2,3-trimethoxybenzene
Conditions | Yield |
---|---|
With trifluoroacetic acid In water at 80℃; for 0.5h; Diels-Alder Cycloaddition; | A n/a B 90% |
Conditions | Yield |
---|---|
With N-Bromosuccinimide In tetrachloromethane for 3h; Heating; | 100% |
With ammonium metavanadate; oxygen; aluminium bromide In diethyl ether at 20℃; for 18h; | 99% |
With perchloric acid; C34H45MoNO5; tetrabutylammomium bromide; dihydrogen peroxide In d7-N,N-dimethylformamide at 28℃; for 0.4h; | 99% |
Conditions | Yield |
---|---|
With ammonium metavanadate; oxygen; aluminium bromide In 1,4-dioxane at 80℃; for 4h; | 100% |
With hydrogen bromide; dimethyl sulfoxide In water; ethyl acetate at 60℃; for 2h; | 94% |
With oxygen; lithium bromide; copper(ll) bromide In acetic acid at 60℃; under 760.051 Torr; regioselective reaction; | 93% |
1,2,3-trimethoxybenzene
Conditions | Yield |
---|---|
With dinitrogen tetraoxide; Nitrogen dioxide In dichloromethane Nitration; | 100% |
Conditions | Yield |
---|---|
With hydrogenchloride; tin(IV) chloride In benzene | 100% |
1,2,3-trimethoxybenzene
9-benzyl-6-chloro-9H-purine
6-(1,3,5-trimethoxyphen-4-yl)-9-phenylmethyl-9H-purine
Conditions | Yield |
---|---|
With trifluorormethanesulfonic acid; 1,1,1,3',3',3'-hexafluoro-propanol at 60℃; for 24h; | 100% |
With aluminum (III) chloride In 1,2-dichloro-ethane for 0.5h; Reflux; | 95% |
1,2,3-trimethoxybenzene
tert-butyl ((ethylthio)(phenyl)methyl)carbamate
tert-butyl N-[phenyl(2,4,6-trimethoxyphenyl)methyl]carbamate
Conditions | Yield |
---|---|
With N-iodo-succinimide In dichloromethane at -78℃; for 0.0833333h; Solvent; Temperature; Reagent/catalyst; Friedel-Crafts Alkylation; Sealed tube; Inert atmosphere; chemoselective reaction; | 100% |
1,2,3-trimethoxybenzene
Conditions | Yield |
---|---|
With iron(III) chloride In dichloromethane at 20℃; for 0.166667h; Inert atmosphere; regioselective reaction; | 100% |
Conditions | Yield |
---|---|
With iron(III) chloride In dichloromethane at 20℃; for 0.166667h; Inert atmosphere; regioselective reaction; | 100% |
1,2,3-trimethoxybenzene
dimethyl 2-(p-methylphenyl)cyclopropane-1,1-dicarboxylate
Conditions | Yield |
---|---|
With trifluorormethanesulfonic acid at 20℃; for 3h; | 100% |
With ytterbium(III) triflate In 1,2-dichloro-ethane at 20 - 65℃; Catalytic behavior; Inert atmosphere; | 95% |
Conditions | Yield |
---|---|
In 2,2,2-trifluoroethanol at 0 - 20℃; for 1h; Inert atmosphere; | 100% |
1,2,3-trimethoxybenzene
dimethyl 2-(2-fluorophenyl)cyclopropane-1,1-dicarboxylate
Conditions | Yield |
---|---|
With trifluorormethanesulfonic acid at 40℃; for 4h; | 100% |
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid In 1,2-dichloro-ethane at 100℃; for 4h; Sealed tube; | 100% |
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid In 1,2-dichloro-ethane at 100℃; for 4h; Sealed tube; | 100% |
1,2,3-trimethoxybenzene
SS-morpholino 4-toluene(dithioperoxo)sulfonate
Conditions | Yield |
---|---|
With trifluoroacetic acid In dichloromethane at 20℃; for 16h; Inert atmosphere; | 100% |
Multi-step reaction with 2 steps 1: trifluoroacetic acid; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical / dichloromethane / 1 h / 20 °C / Inert atmosphere 2: trifluoroacetic acid / dichloromethane / 16 h / 20 °C / Inert atmosphere View Scheme |
1,2,3-trimethoxybenzene
methyl vinyl ketone
4-(2,4,6-trimethoxy-phenyl)-butan-2-one
Conditions | Yield |
---|---|
gold(III) chloride; silver trifluoromethanesulfonate In 1,2-dichloro-ethane at 20℃; | 99% |
gold(III) chloride In acetonitrile at 20℃; for 24h; | 99.5% |
With boron trifluoride diethyl etherate In dichloromethane at 20℃; for 0.0333333h; Michael Addition; Green chemistry; | 93% |
With dichloro bis(acetonitrile) palladium(II); tin(ll) chloride In acetonitrile at 30℃; for 2h; Kinetics; Reagent/catalyst; Time; Solvent; Michael Addition; Inert atmosphere; Schlenk technique; | 92% |
With boron trifluoride diethyl etherate |
1,2,3-trimethoxybenzene
9-phenyl-fluoren-9-ol
9-phenyl-9-(2,4,6-trimethoxyphenyl)-9H-fluorene
Conditions | Yield |
---|---|
With scandium tris(trifluoromethanesulfonate) In dichloromethane at 60℃; for 4h; Sealed tube; | 99% |
With perchloric acid; nitromethane |
1,2,3-trimethoxybenzene
1,3,5-tribromo-2,4,6-trimethoxybenzene
Conditions | Yield |
---|---|
With N-Bromosuccinimide In acetonitrile at 20℃; for 144h; | 99% |
With bromine excess of reagent; | 80% |
With bromine; iron(III) chloride In 1,2-dichloro-ethane Heating; | 70% |
With bromine |
1,2,3-trimethoxybenzene
benzaldehyde
2,2'-(phenylmethylene)bis(1,3,5-trimethoxybenzene)
Conditions | Yield |
---|---|
With chloro-trimethyl-silane; bismuth(III) sulfate at 20℃; for 1h; | 99% |
With boron trifluoride diethyl etherate In dichloromethane at 20℃; for 0.0833333h; Friedel-Crafts Alkylation; | 96% |
With PEG-400 at 50 - 60℃; for 2h; Friedel-Crafts Alkylation; Green chemistry; | 92% |
1,2,3-trimethoxybenzene
acetyl chloride
1-(2,4,6-trimethoxyphenyl)ethanone
Conditions | Yield |
---|---|
Stage #1: 1,2,3-trimethoxybenzene In dichloromethane at 0℃; for 0.166667h; Stage #2: acetyl chloride With aluminum (III) chloride In dichloromethane for 2h; Friedel-Crafts Acylation; | 99% |
With zinc(II) chloride | 98% |
With 1,1,1,3',3',3'-hexafluoro-propanol at 20℃; for 5h; Friedel-Crafts Acylation; Inert atmosphere; | 92% |
1,2,3-trimethoxybenzene
2,3,4,6-tetra-O-benzyl-1-O-(trifluoroacetyl)-α-D-glucopyranose
1-deoxy-1-(C-2',4',6'-trimethoxyphenyl) 2,3,4,6-tetra-O-benzyl-β-D-glucopyranoside
Conditions | Yield |
---|---|
With boron trifluoride diethyl etherate In dichloromethane for 0.0833333h; Ambient temperature; | 99% |
With boron trifluoride diethyl etherate In dichloromethane for 0.0833333h; Product distribution; Ambient temperature; var. Lewis acids and aryl ethers;; | 99% |
Conditions | Yield |
---|---|
With orcinol; Acetobacterium dehalogenans veratrol-O-demethylase; Desulfitobacterium hafniense methyltransferase dhaf4611 In aq. buffer at 25℃; for 24h; pH=6.5; Inert atmosphere; Enzymatic reaction; regioselective reaction; | 99% |
With N,N,N,N,N,N-hexamethylphosphoric triamide; sodium hydride; N-methylaniline In diethyl ether; xylene at 95℃; for 9h; | 85% |
With 2-(diethylamino)ethanethiol hydrochloride; sodium t-butanolate In N,N-dimethyl-formamide for 2h; Heating; | 84% |
1,2,3-trimethoxybenzene
acetic anhydride
1-(2,4,6-trimethoxyphenyl)ethanone
Conditions | Yield |
---|---|
With scandium tris(trifluoromethanesulfonate) In acetonitrile for 0.5h; Time; Friedel-Crafts Acylation; Inert atmosphere; Microwave irradiation; Heating; Green chemistry; | 99% |
With trifluoroacetic acid at 20℃; for 1.5h; Friedel-Crafts Acylation; | 95% |
With boron trifluoride diethyl etherate In ethyl acetate at 20℃; for 2h; Friedel-Crafts Acylation; | 93% |
1,2,3-trimethoxybenzene
4-nitrobenzaldehdye
(4-nitrophenyl)-bis-(2,4,6-trimethoxyphenyl)methane
Conditions | Yield |
---|---|
With tin(IV) chloride; bis(1,5-cyclooctadiene)diiridium(I) dichloride at 90℃; for 1h; | 99% |
With air; iodine In toluene at 60℃; for 24h; Friedel Crafts alkylation; | 93% |
With [1,2,3,4,5-pentamethylcyclopentadiene Ir(SnCl3)2{SnCl2(H2O)2}] In 1,2-dichloro-ethane at 80℃; for 1h; | 90% |
1,2,3-trimethoxybenzene
2,3,5,6-tetramethyl-4-oxo-1-phenylthiocyclohexa-2,5-dienyl 2-chloroacetate
A
1,3,5-trimethoxy-2-(phenylsulfanyl)benzene
Conditions | Yield |
---|---|
With trimethylsilyl trifluoromethanesulfonate In acetonitrile for 0.166667h; Yields of byproduct given; | A 99% B n/a |
1,2,3-trimethoxybenzene
2,3,5,6-tetramethyl-4-oxo-1-phenylthiocyclohexa-2,5-dienyl 2-chloroacetate
1,3,5-trimethoxy-2-(phenylsulfanyl)benzene
Conditions | Yield |
---|---|
With trimethylsilyl trifluoromethanesulfonate In acetonitrile at -30 - 20℃; for 0.166667h; | 99% |
1,2,3-trimethoxybenzene
1-(2,3,4,5,6-pentafluorophenylthio)-2,3,5,6-tetramethyl-4-oxocyclohexa-2,5-dienyl 2-chloroacetate
Conditions | Yield |
---|---|
With trimethylsilyl trifluoromethanesulfonate In acetonitrile at -30 - 0℃; for 0.166667h; | A n/a B 99% |
Conditions | Yield |
---|---|
With aluminium trichloride In 1,2-dichloro-ethane at 75℃; for 3.5h; Friedel-Crafts reaction; | 99% |
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