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Dayang Chem (Hangzhou) Co.,Ltd.

Dayangchem's R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantities

7-Methoxy-1-tetralone Manufacturer/High quality/Best price/In stock

Cas:6836-19-7

Min.Order:1 Kilogram

FOB Price: $3.0

Type:Lab/Research institutions

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Simagchem Corporation

Welcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our

High quality 7-Methoxy-1-Tetralone supplier in China

Cas:6836-19-7

Min.Order:1 Kilogram

Negotiable

Type:Manufacturers

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Jinan Finer Chemical Co., Ltd

Product Description Product website: http://www.finerchem.com/pro01en/id/882.html Product Name 7-Methoxy-1-tetralone CAS No. 6836-19-7

7-Methoxy-1-tetralone

Cas:6836-19-7

Min.Order:1 Gram

FOB Price: $45.0

Type:Lab/Research institutions

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Wuhan Fortuna Chemical Co.,Ltd

High purity 7-Methoxy-1-tetralone CAS 6836-19-7 with prompt service Company profile Wuhan Fortuna Chemical Co.,Ltd established in 2006, is a big integrative chemical enterprise being engaged in Pharmaceutical & its intermediates, Food/Feed a

High purity 7-Methoxy-1-tetralone CAS 6836-19-7 with prompt service

Cas:6836-19-7

Min.Order:1 Kilogram

FOB Price: $50.0

Type:Trading Company

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Hangzhou Think Chemical Co. Ltd

7-methoxy-1-tetralone CAS No.:6836-19-7 Name 7-Methoxy-1-tetralone Molecular Structure Molecular Formula C11H12O2 Molecular Weight 176.21 CAS Registry Number 6836-19-7 EINECS 229-916-0 Appearance:de

7-methoxy-1-tetralone CAS No.:6836-19-7

Cas:6836-19-7

Min.Order:1 Kilogram

FOB Price: $2.0

Type:Other

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Henan Allgreen Chemical Co.,Ltd

high quality Appearance:Colorless liquid Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea Port:shanghai

7-Methoxy-1-tetralone

Cas:6836-19-7

Min.Order:1 Gram

Negotiable

Type:Manufacturers

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Ality Chemical Corporation

The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi

Factory Supply 7-methoxy-1,2,3,4-tetrahydronaphthalen-1-one

Cas:6836-19-7

Min.Order:1

Negotiable

Type:Other

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Xi'an Xszo Chem Co., Ltd.

1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s

Large Stock 99.0% 7-Methoxy-1-tetralone 6836-19-7 Producer

Cas:6836-19-7

Min.Order:1 Gram

FOB Price: $0.1

Type:Manufacturers

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Chemwill Asia Co., Ltd.

Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block

7-Methoxy-1-tetralone

Cas:6836-19-7

Min.Order:5 Kiloliter

FOB Price: $1.2 / 5.0

Type:Manufacturers

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Hubei DiBo chemical co., LTD

Name: 7-methoxy-1-tetralone CAS NO:6836-19-7 Grade:Used as pharmaceutical raw materials and intermediates; Agomelatine intermediate Product Quality 12 years of chemical raw materials Mature operation of the industry System stability Data stor

7-methoxy-1-tetralone CAS:6836-19-7 Chinese manufacturers high-quality

Cas:6836-19-7

Min.Order:25 Kilogram

FOB Price: $1.0 / 2.0

Type:Other

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Henan Tianfu Chemical Co., Ltd.

Competitive Price High Quality Fast Delivery custom-made Welcome to Henan Tianfu Chemical Co., Ltd. website. Our company engages in Sodium Tripolyphosphate (STPP) and Sodium Hexametabphosphate (SHMP) production; development of noble me

7-Methoxy-1-tetralone 6836-19-7

Cas:6836-19-7

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

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Hebei Nengqian Chemical Import and Export Co., LTD

With our good experience, we offer detailed technical support and advice to assist customers. We communicate closely with customers to establish their quality requirements. Consistent Quality Our plant has strict quality control in each manufacturin

7-Methoxy-1-tetralone CAS 6836-19-7

Cas:6836-19-7

Min.Order:1 Kilogram

FOB Price: $70.0 / 90.0

Type:Trading Company

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Sinoway Industrial Co., Ltd.

Why is SINOWAY: 1) Specialized in pharmaceutical and healthcare industrial for 34 years. 2) ISO 9001:2015 & SGS audited supplier . 3) Accept various payment terms : T.T 30-60 days. 4) We have warehouse in USA with quickly shipment . 5) We c

Agomelatine intermediate/7-Methoxy-1-tetralone CAS 6836-19-7

Cas:6836-19-7

Min.Order:25 Kilogram

FOB Price: $100.0

Type:Trading Company

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Zhuozhou Wenxi import and Export Co., Ltd

WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et

Wholesale price CAS 6836-19-7 with best price

Cas:6836-19-7

Min.Order:1 Kilogram

FOB Price: $139.0 / 210.0

Type:Trading Company

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LIDE PHARMACEUTICALS LIMITED

Advantage : LIDE PHARMACEUTICALS LTD. is a mid-small manufacturing-type enterprise, engaged in pharmaceutical intermediates of R&D, custom-made and production, and also involving trading chemicals for export. We have established the R&amp

7-Methoxy-1-tetralone/ LIDE PHARMA- Factory supply / Best price

Cas:6836-19-7

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Henan Sinotech Import&Export Corporation

Name: 7-methoxy-1-tetralone Synonyms: 7-methoxy-1,2,3,4-tetrahydronaphthalen-1-one CAS: 6836-19-7 MF: C11H12O2 Appearance:White powder Storage:Store in cool and dry place, away from sun light. Package:25kg/drum Application:Chemical materials Trans

7-methoxy-1-tetralone

Cas:6836-19-7

Min.Order:1 Kilogram

FOB Price: $1.0

Type:Other

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Hubei Langyou International Trading Co., Ltd

Advantages: Hubei XinRunde Chemical Co., Ltd is a renowned pharmaceutical manufacturer. We can offer high quality products at competitive price in quick delivery with 100% custom pass guaranteed. Never stop striving to offer our best s

Agomelatine Intermediate 99%min 7-Methoxy-1-tetralone

Cas:6836-19-7

Min.Order:10 Gram

Negotiable

Type:Other

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HANWAYS CHEMPHARM CO.,LIMITED

Hanways chempharm is a specialized company concentrating on the R&D, production, marketing and technical service of APIs and pharmaceutical intermediates. The marketing department is located in Wuhan. We have two GMP facilities in Hubei Pr

Agomelatine Intermediate 7-Methoxy-1-tetralone CAS 6836-19-7 with high purity and factory price

Cas:6836-19-7

Min.Order:1 Kilogram

FOB Price: $20.0 / 40.0

Type:Trading Company

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Shanghai Upbio Tech Co.,Ltd

1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized

7-Methoxy-1-tetralone 6836-19-7

Cas:6836-19-7

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

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Baoji Guokang Healthchem co.,ltd

Our company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At prese

7-Methoxy-1-tetralone

Cas:6836-19-7

Min.Order:1 Kilogram

FOB Price: $76.0 / 85.0

Type:Trading Company

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Qingdao Beluga Import and Export Co., LTD

7-Methoxy-1-tetralone CAS:6836-19-7 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic inte

7-Methoxy-1-tetralone CAS:6836-19-7

Cas:6836-19-7

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

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Shandong Hanjiang Chemical Co., Ltd.

Hello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai

7-Methoxy-1-tetralone

Cas:6836-19-7

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

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Henan Wentao Chemical Product Co., Ltd.

Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

CAS NO.:6836-19-7

Cas:6836-19-7

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Hebei Mojin Biotechnology Co.,Ltd

Hebei Mojin Biotechnology Co., Ltd, Our company is a professional chemical raw materials and chemical reagents research and development production enterprises. We have several production line,So we can control the lowest price. We also have several

7-Methoxy-1-tetralone cas:6836-19-7

Cas:6836-19-7

Min.Order:25 Gram

FOB Price: $90.0 / 100.0

Type:Trading Company

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Triumph International Development Limilted

Appearance:Off-white to white solid powder Storage:Store in a cool,dry place and keep away from direct strong light Package:As customer request Application:Intermediate Transportation:By Sea/Air/Courier Port:Qingdao\Shanghai,China

7-Methoxy-1-tetralone 6836-19-7

Cas:6836-19-7

Min.Order:0 Metric Ton

Negotiable

Type:Lab/Research institutions

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Afine Chemicals Limited

Our Services 1. New Molecules R&D 2. Own test center HPLC NMR GC LC-MS 3. API and Intermediates from China reputed manufacturers 4. Documents support COA MOA MSDS DMF open part Our advantages 1. Government awarded company. Top 100 enter

7-Methoxy-1-tetralone

Cas:6836-19-7

Min.Order:0 Metric Ton

Negotiable

Type:Lab/Research institutions

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Wuhan Han Sheng New Material Technology Co.,Ltd

Our Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We

7-Methoxy-1-tetralone Pharmaceutical Raw Materials Agomelatine Intermediate

Cas:6836-19-7

Min.Order:10 Kilogram

Negotiable

Type:Trading Company

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Hangzhou Keyingchem Co.,Ltd

Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det

7-Methoxy-1-tetralone

Cas:6836-19-7

Min.Order:0 Metric Ton

Negotiable

Type:Lab/Research institutions

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SHANGHAI T&W PHARMACEUTICAL CO., LTD.

A substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc

7-Methoxytetralone

Cas:6836-19-7

Min.Order:4 Kilogram

Negotiable

Type:Lab/Research institutions

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Hangzhou Lingrui Chemical Co.,Ltd.

Our advantages: 1, High quality with competitive price: 1) Standard:BP/USP/EP/Enterprise standard 2) All Purity≥99% 3) We are manufacturer and can provide high quality products with factory price. 2, Fast and safe delivery 1) Parcel can be

Manufacturer/High quality 7-Methoxy-1-tetralone 6836-19-7

Cas:6836-19-7

Min.Order:1 Gram

Negotiable

Type:Other

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Synthetic route

4-(4-methoxyphenyl) butanoyl chloride
6836-18-6

4-(4-methoxyphenyl) butanoyl chloride

7-Methoxy-1-tetralone
6836-19-7

7-Methoxy-1-tetralone

Conditions
ConditionsYield
With Fe-Al-MCM-41 molecular sieve In toluene at 60℃; for 18h; Green chemistry;98.4%
unter vermindertem Druck;
With aluminium trichloride; 1,1,2,2-tetrachloroethane at -5℃;
7-methoxy-1,2,3,4-tetrahydro-1-naphthol
32820-10-3

7-methoxy-1,2,3,4-tetrahydro-1-naphthol

7-Methoxy-1-tetralone
6836-19-7

7-Methoxy-1-tetralone

Conditions
ConditionsYield
With acetone In toluene at 80℃; for 0.25h; Flow reactor;96%
4-(4-Methoxyphenyl)butyric acid
4521-28-2

4-(4-Methoxyphenyl)butyric acid

7-Methoxy-1-tetralone
6836-19-7

7-Methoxy-1-tetralone

Conditions
ConditionsYield
With phosphoric acid; phosphorus pentoxide at 70 - 80℃; for 2h;94%
With trifluoroacetic anhydride In 1,2-dichloro-ethane at 0 - 20℃; Friedel-Crafts acylation;94%
With trichloroacetic acid anhydride at 70℃; Friedel Crafts acylation; Neat (no solvent);92%
(7-Methoxy-1,2,3,4-tetrahydro-naphthalen-1-yl)-methanol
106336-27-0

(7-Methoxy-1,2,3,4-tetrahydro-naphthalen-1-yl)-methanol

7-Methoxy-1-tetralone
6836-19-7

7-Methoxy-1-tetralone

Conditions
ConditionsYield
With dipyridinium dichromate; Celite In dichloromethane at 25℃; for 24h;79%
dimethyl 1,2-dihydro-4-hydroxy-6-methoxynaphthalene-1,3-dicarboxylate
666177-27-1

dimethyl 1,2-dihydro-4-hydroxy-6-methoxynaphthalene-1,3-dicarboxylate

7-Methoxy-1-tetralone
6836-19-7

7-Methoxy-1-tetralone

Conditions
ConditionsYield
With sodium chloride In dimethyl sulfoxide at 200℃;65%
4-(4-Methoxy-phenyl)-butyryl azide

4-(4-Methoxy-phenyl)-butyryl azide

7-Methoxy-1-tetralone
6836-19-7

7-Methoxy-1-tetralone

Conditions
ConditionsYield
64%
7-methoxy-8a-methyl-1,2,3,4,6,8a-hexahydro-naphthalen-1-one
65128-90-7

7-methoxy-8a-methyl-1,2,3,4,6,8a-hexahydro-naphthalen-1-one

A

7-Methoxy-1-tetralone
6836-19-7

7-Methoxy-1-tetralone

(6S,8aS)-6-Hydroxy-7-methoxy-8a-methyl-3,4,6,8a-tetrahydro-2H-naphthalen-1-one

(6S,8aS)-6-Hydroxy-7-methoxy-8a-methyl-3,4,6,8a-tetrahydro-2H-naphthalen-1-one

(6R,8aS)-6-Hydroxy-7-methoxy-8a-methyl-3,4,6,8a-tetrahydro-2H-naphthalen-1-one

(6R,8aS)-6-Hydroxy-7-methoxy-8a-methyl-3,4,6,8a-tetrahydro-2H-naphthalen-1-one

Conditions
ConditionsYield
With sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid In dichloromethane at 4℃; pH=8.3;A 63%
B 20%
C 12%
1,1-(1,2-Benzenediyldithio)-7-methoxy-1,2,3,4-tetrahydronaphthalene
87543-05-3

1,1-(1,2-Benzenediyldithio)-7-methoxy-1,2,3,4-tetrahydronaphthalene

7-Methoxy-1-tetralone
6836-19-7

7-Methoxy-1-tetralone

Conditions
ConditionsYield
With boron trifluoride diethyl etherate; mercury(II) oxide In tetrahydrofuran; water62%
With tetrahydrofuran; mercury(II) oxide; boron trifluoride diethyl etherate56%
1-(3-methoxyphenyl)cyclobutan-1-ol
1202643-83-1

1-(3-methoxyphenyl)cyclobutan-1-ol

7-Methoxy-1-tetralone
6836-19-7

7-Methoxy-1-tetralone

Conditions
ConditionsYield
With potassium carbonate; copper(II) sulfate; Selectfluor In water; acetonitrile at 60℃; for 5h;59%
8a-allyl-7-methoxy-1,2,3,4,6,8a-hexahydro-naphthalen-1-one
310897-19-9

8a-allyl-7-methoxy-1,2,3,4,6,8a-hexahydro-naphthalen-1-one

A

7-Methoxy-1-tetralone
6836-19-7

7-Methoxy-1-tetralone

(6S,8aS)-8a-Allyl-6-hydroxy-7-methoxy-3,4,6,8a-tetrahydro-2H-naphthalen-1-one

(6S,8aS)-8a-Allyl-6-hydroxy-7-methoxy-3,4,6,8a-tetrahydro-2H-naphthalen-1-one

(6R,8aS)-8a-Allyl-6-hydroxy-7-methoxy-3,4,6,8a-tetrahydro-2H-naphthalen-1-one

(6R,8aS)-8a-Allyl-6-hydroxy-7-methoxy-3,4,6,8a-tetrahydro-2H-naphthalen-1-one

Conditions
ConditionsYield
With sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid In dichloromethane at 4℃; pH=8.3;A 54%
B 22.5%
C 12.5%
tert.-butylhydroperoxide
75-91-2

tert.-butylhydroperoxide

6-methoxy-1,2,3,4-tetrahydronaphthalene
1730-48-9

6-methoxy-1,2,3,4-tetrahydronaphthalene

A

7-Methoxy-1-tetralone
6836-19-7

7-Methoxy-1-tetralone

B

6-methoxy-2,3-dihydronaphthalene-1,4-dione

6-methoxy-2,3-dihydronaphthalene-1,4-dione

C

1-tert-butylperoxy-6-methoxytetralin

1-tert-butylperoxy-6-methoxytetralin

D

1-tert-butylperoxy-7-methoxytetralin

1-tert-butylperoxy-7-methoxytetralin

E

6-methoxy-3,4-dihydro-1(2H)-naphthalenone
1078-19-9

6-methoxy-3,4-dihydro-1(2H)-naphthalenone

Conditions
ConditionsYield
With copper(II) choride dihydrate; tetrabutyl-ammonium chloride; sodium carbonate; 2,2′‐biquinoline‐4,4′‐dicarboxylic acid dipotassium salt In water at 20℃; for 17h; Green chemistry;A 8%
B 12%
C n/a
D n/a
E 50%
7-methoxy-1,2,3,4-tetrahydro-1-naphthol
32820-10-3

7-methoxy-1,2,3,4-tetrahydro-1-naphthol

A

7-Methoxy-1-tetralone
6836-19-7

7-Methoxy-1-tetralone

B

(+)-(S)-7-Methoxy-1-tetralol
182965-69-1

(+)-(S)-7-Methoxy-1-tetralol

C

(-)-(R)-7-Methoxy-1-tetralol

(-)-(R)-7-Methoxy-1-tetralol

Conditions
ConditionsYield
With 4-vinylbenzyl chloride; [N,N'-bis(2-cyclohexyloxycarbonyl-3-oxobutylidene)-(1S,2S)-dimesitylethylenediaminato]cobalt(II); oxygen In tert-butyl alcohol at 20 - 50℃; for 12h; Resolution of racemate; optical yield given as %ee;A 41.9%
B n/a
C n/a
tert.-butylhydroperoxide
75-91-2

tert.-butylhydroperoxide

6-methoxy-1,2,3,4-tetrahydronaphthalene
1730-48-9

6-methoxy-1,2,3,4-tetrahydronaphthalene

A

7-methoxy-1,2,3,4-tetrahydro-1-naphthol
32820-10-3

7-methoxy-1,2,3,4-tetrahydro-1-naphthol

B

7-Methoxy-1-tetralone
6836-19-7

7-Methoxy-1-tetralone

C

6-methoxy-1,2,3,4-tetrahydronaphthalen-1-ol
16821-32-2

6-methoxy-1,2,3,4-tetrahydronaphthalen-1-ol

D

1-tert-butylperoxy-6-methoxytetralin

1-tert-butylperoxy-6-methoxytetralin

E

1-tert-butylperoxy-7-methoxytetralin

1-tert-butylperoxy-7-methoxytetralin

F

6-methoxy-3,4-dihydro-1(2H)-naphthalenone
1078-19-9

6-methoxy-3,4-dihydro-1(2H)-naphthalenone

Conditions
ConditionsYield
With copper(II) choride dihydrate; tetrabutyl-ammonium chloride; sodium carbonate; 2,2′‐biquinoline‐4,4′‐dicarboxylic acid dipotassium salt In water at 20℃; for 17h; Green chemistry;A n/a
B 17%
C n/a
D n/a
E n/a
F 39%
6-methoxy-1,2,3,4-tetrahydronaphthalene
1730-48-9

6-methoxy-1,2,3,4-tetrahydronaphthalene

A

7-Methoxy-1-tetralone
6836-19-7

7-Methoxy-1-tetralone

B

6-methoxy-3,4-dihydro-1(2H)-naphthalenone
1078-19-9

6-methoxy-3,4-dihydro-1(2H)-naphthalenone

Conditions
ConditionsYield
With tert.-butylhydroperoxide; chromium(VI) oxide In dichloromethane for 9h; Ambient temperature;A 17%
B 36%
With tert.-butylhydroperoxide; bis-(tributyltin oxide) dioxochromium(VI) In dichloromethane at 40℃; for 7.5h;A 15%
B 32%
With tert.-butylhydroperoxide; 2,4-dimethyl-2,4-pentanediol cyclic Cr(VI) ester In tetrachloromethane; dichloromethane at 0℃; for 8h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
With potassium permanganate; copper(II) sulfate In dichloromethane for 72h; Heating;A 5 % Chromat.
B 85 % Chromat.
6-methoxy-1,2,3,4-tetrahydronaphthalene
1730-48-9

6-methoxy-1,2,3,4-tetrahydronaphthalene

A

7-Methoxy-1-tetralone
6836-19-7

7-Methoxy-1-tetralone

B

6-methoxy-2,3-dihydronaphthalene-1,4-dione

6-methoxy-2,3-dihydronaphthalene-1,4-dione

C

6-methoxy-3,4-dihydro-1(2H)-naphthalenone
1078-19-9

6-methoxy-3,4-dihydro-1(2H)-naphthalenone

Conditions
ConditionsYield
With tert.-butylhydroperoxide; sodium hydrogencarbonate; dirhodium(II) tetrakis(caprolactam) In decane; 1,2-dichloro-ethane at 20℃; for 16h; Title compound not separated from byproducts;A n/a
B 29%
C n/a
7-hydroxy-1-tetralone
22009-38-7

7-hydroxy-1-tetralone

dimethyl sulfate
77-78-1

dimethyl sulfate

7-Methoxy-1-tetralone
6836-19-7

7-Methoxy-1-tetralone

Conditions
ConditionsYield
With potassium carbonate In acetone for 2.5h; Heating; Yield given;
dimethyl sulfate
77-78-1

dimethyl sulfate

7-hydroxy-1-oxo-tetralin

7-hydroxy-1-oxo-tetralin

7-Methoxy-1-tetralone
6836-19-7

7-Methoxy-1-tetralone

Conditions
ConditionsYield
With sodium hydroxide
7-methoxy-3,4-dihydro-2H-<1-14C>naphthalen-1-one

7-methoxy-3,4-dihydro-2H-<1-14C>naphthalen-1-one

7-Methoxy-1-tetralone
6836-19-7

7-Methoxy-1-tetralone

Conditions
ConditionsYield
Herstellung;
methoxybenzene
100-66-3

methoxybenzene

(+-)-propylsuccinic acid-anhydride

(+-)-propylsuccinic acid-anhydride

7-Methoxy-1-tetralone
6836-19-7

7-Methoxy-1-tetralone

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: 73.4 percent / AlCl3 / nitromethane / 12 h / 0 - 25 °C
2: 95 percent / NH2NH2*H2O; KOH / bis-(2-hydroxy-ethyl) ether / 7 h / 130 - 195 °C
3: 87.7 percent / H3PO4; P2O5 / 3 h / 70 - 80 °C
View Scheme
Multi-step reaction with 3 steps
1: Zn; HCl / toluene
2: PPA
View Scheme
4-(4-methoxy-phenyl)-4-oxo-butyric acid
3153-44-4

4-(4-methoxy-phenyl)-4-oxo-butyric acid

7-Methoxy-1-tetralone
6836-19-7

7-Methoxy-1-tetralone

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 95 percent / NH2NH2*H2O; KOH / bis-(2-hydroxy-ethyl) ether / 7 h / 130 - 195 °C
2: 87.7 percent / H3PO4; P2O5 / 3 h / 70 - 80 °C
View Scheme
Multi-step reaction with 2 steps
1: Zn; HCl / toluene
2: PPA
View Scheme
Multi-step reaction with 2 steps
1: Zn/HCl
2: CF3COOH, (CF3COO)2O
View Scheme
4-(4-methoxyphenyl)-3-butenoic acid
91142-97-1

4-(4-methoxyphenyl)-3-butenoic acid

7-Methoxy-1-tetralone
6836-19-7

7-Methoxy-1-tetralone

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: hydrogen / Pd/C / tetrahydrofuran / 3 h / 20 °C / 760.21 Torr
2: 94 percent / trifluoroacetic anhydride / 1,2-dichloro-ethane / 0 - 20 °C
View Scheme
C23H38O3Sn

C23H38O3Sn

7-Methoxy-1-tetralone
6836-19-7

7-Methoxy-1-tetralone

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: hydrochloric acid / H2O / 0.25 h / 20 °C
2: hydrogen / Pd/C / tetrahydrofuran / 3 h / 20 °C / 760.21 Torr
3: 94 percent / trifluoroacetic anhydride / 1,2-dichloro-ethane / 0 - 20 °C
View Scheme
methoxybenzene
100-66-3

methoxybenzene

(+-)-hept-2t(?)-en-4-ol

(+-)-hept-2t(?)-en-4-ol

7-Methoxy-1-tetralone
6836-19-7

7-Methoxy-1-tetralone

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: AlCl3
2: Zn/HCl
3: CF3COOH, (CF3COO)2O
View Scheme
methoxybenzene
100-66-3

methoxybenzene

7-Methoxy-1-tetralone
6836-19-7

7-Methoxy-1-tetralone

Conditions
ConditionsYield
Multi-step reaction with 2 steps
2: 85 percent / polyphosphoric acid / 90 °C
View Scheme
Multi-step reaction with 3 steps
1: 72 percent / AlCl3 / nitrobenzene / Ambient temperature
2: 87 percent / Zn, conc. HCl, HgCl2 / H2O; toluene / 24 h / Heating
3: 94 percent / P2O5, H3PO4 / 2 h / 70 - 80 °C
View Scheme
Multi-step reaction with 3 steps
1.1: aluminum (III) chloride / nitrobenzene / 0.5 h / 20 °C
1.2: 60 °C
2.1: palladium 10% on activated carbon; hydrogen / acetic acid / 70 °C
3.1: polyphosphoric acid / 90 °C
View Scheme
1-<4,4-(1,2-Benzenediyldithio)but-3-enyl>-4-methoxybenzene
87543-11-1

1-<4,4-(1,2-Benzenediyldithio)but-3-enyl>-4-methoxybenzene

7-Methoxy-1-tetralone
6836-19-7

7-Methoxy-1-tetralone

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 74 percent / p-toluenesulfonic acid / acetonitrile / 24 h / 0 °C
2: 56 percent / HgO, aq. THF / BF3.Et2O
View Scheme
Multi-step reaction with 2 steps
1: 74 percent / p-toluenesulfonic acid monohydrate / acetonitrile / 40 - 50 °C
2: 62 percent / mercury(II) oxide, BF3*Et2O / tetrahydrofuran; H2O
View Scheme
7-Oxa-bicyclo[4.1.0]heptan-2-one oxime
58008-75-6

7-Oxa-bicyclo[4.1.0]heptan-2-one oxime

7-Methoxy-1-tetralone
6836-19-7

7-Methoxy-1-tetralone

Conditions
ConditionsYield
Multi-step reaction with 5 steps
1: 72 percent / NaHCO3, CF3CO3H, urea / acetonitrile / 1.42 h / 0 °C
2: 85 percent / pyridinium chlorochromate / CH2Cl2 / 3.2 h / 23 °C
3: toluene / 19 h / 80 °C
4: 1.) hydrochloric acid 2.)DBN / 1.) THF, 0 deg C, 30 min, 2.) 0 deg C, 1 h
5: K2CO3 / acetone / 2.5 h / Heating
View Scheme
3-nitro-2-cyclopenten-1-one
77970-17-3

3-nitro-2-cyclopenten-1-one

7-Methoxy-1-tetralone
6836-19-7

7-Methoxy-1-tetralone

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: toluene / 19 h / 80 °C
2: 1.) hydrochloric acid 2.)DBN / 1.) THF, 0 deg C, 30 min, 2.) 0 deg C, 1 h
3: K2CO3 / acetone / 2.5 h / Heating
View Scheme
3-nitro-2-cyclohexen-1-ol
67730-57-8

3-nitro-2-cyclohexen-1-ol

7-Methoxy-1-tetralone
6836-19-7

7-Methoxy-1-tetralone

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: 85 percent / pyridinium chlorochromate / CH2Cl2 / 3.2 h / 23 °C
2: toluene / 19 h / 80 °C
3: 1.) hydrochloric acid 2.)DBN / 1.) THF, 0 deg C, 30 min, 2.) 0 deg C, 1 h
4: K2CO3 / acetone / 2.5 h / Heating
View Scheme
5-Methoxy-4a-nitro-7-trimethylsilanyloxy-3,4,4a,5,8,8a-hexahydro-2H-naphthalen-1-one

5-Methoxy-4a-nitro-7-trimethylsilanyloxy-3,4,4a,5,8,8a-hexahydro-2H-naphthalen-1-one

7-Methoxy-1-tetralone
6836-19-7

7-Methoxy-1-tetralone

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 1.) hydrochloric acid 2.)DBN / 1.) THF, 0 deg C, 30 min, 2.) 0 deg C, 1 h
2: K2CO3 / acetone / 2.5 h / Heating
View Scheme
7-Methoxy-1-tetralone
6836-19-7

7-Methoxy-1-tetralone

7-methoxy-3,4-dihydronaphthalen-1(2H)-one oxime
20175-97-7

7-methoxy-3,4-dihydronaphthalen-1(2H)-one oxime

Conditions
ConditionsYield
With hydroxylamine hydrochloride; potassium carbonate In methanol for 16h; Reflux;100%
With pyridine; hydroxylamine hydrochloride at 25℃; for 3h; Inert atmosphere;94%
With hydroxylamine hydrochloride; potassium carbonate In methanol; water for 3h; Heating;92%
diethyl 1-cyanomethylphosphonate
2537-48-6

diethyl 1-cyanomethylphosphonate

7-Methoxy-1-tetralone
6836-19-7

7-Methoxy-1-tetralone

(7-methoxy-3,4-dihydro-2H-naphthalene-1-ylidene)acetonitrile
127299-26-7

(7-methoxy-3,4-dihydro-2H-naphthalene-1-ylidene)acetonitrile

Conditions
ConditionsYield
With sodium methylate In methanol at -20 - -10℃; for 24h; Reagent/catalyst; Wittig Rearrangement;100%
Stage #1: diethyl 1-cyanomethylphosphonate With potassium hydroxide In dimethyl sulfoxide at 15 - 25℃; for 1h; Industry scale;
Stage #2: 7-Methoxy-1-tetralone In tetrahydrofuran; dimethyl sulfoxide at 15 - 25℃; for 2.5h; Product distribution / selectivity;
95%
Stage #1: 7-Methoxy-1-tetralone With sodium hydride In 1,2-dimethoxyethane at 15℃; for 0.5h;
Stage #2: diethyl 1-cyanomethylphosphonate In monoethylene glycol diethyl ether at 10 - 15℃;
89%
N,N-phenylbistrifluoromethane-sulfonimide
37595-74-7

N,N-phenylbistrifluoromethane-sulfonimide

7-Methoxy-1-tetralone
6836-19-7

7-Methoxy-1-tetralone

trifluoromethanesulfonic acid 7-methoxy-3,4-dihydronaphthalen-1-yl ester
724707-85-1

trifluoromethanesulfonic acid 7-methoxy-3,4-dihydronaphthalen-1-yl ester

Conditions
ConditionsYield
Stage #1: 7-Methoxy-1-tetralone With lithium hexamethyldisilazane In tetrahydrofuran at -79℃; for 0.75h;
Stage #2: N,N-phenylbistrifluoromethane-sulfonimide In tetrahydrofuran at -78 - 0℃; for 3h;
100%
With potassium hexamethylsilazane In tetrahydrofuran at -78℃; for 1h;96%
With potassium hexamethylsilazane In tetrahydrofuran at -78℃; for 1.5h;96%
7-Methoxy-1-tetralone
6836-19-7

7-Methoxy-1-tetralone

7-methoxy-1,2,3,4-tetrahydro-1-naphthol
32820-10-3

7-methoxy-1,2,3,4-tetrahydro-1-naphthol

Conditions
ConditionsYield
With Tetrahydrofurfuryl alcohol; sodium tetrahydroborate; ethanol; (S,S)-(β-oxoaldiminato)cobalt(II) In chloroform at -20℃; for 12h;99%
With sodium tetrahydroborate In ethanol at 20℃; Inert atmosphere;99%
With methanol; sodium tetrahydroborate at 20℃;98%
7-Methoxy-1-tetralone
6836-19-7

7-Methoxy-1-tetralone

2-chloro-7-methoxy-3,4-dihydronaphthalen-1(2H)-one
85299-01-0

2-chloro-7-methoxy-3,4-dihydronaphthalen-1(2H)-one

Conditions
ConditionsYield
With 2,2,3,4,5,6-hexachloro-cyclohexa-2,4-dien-1-one In ethanol for 4h; Reflux;99%
With 2,2,3,4,5,6-hexachloro-cyclohexa-2,4-dien-1-one In ethanol for 4h; Heating;76%
Stage #1: 7-Methoxy-1-tetralone With lithium diisopropyl amide In tetrahydrofuran at -78℃; for 0.5h;
Stage #2: With p-toluenesulfonyl chloride In tetrahydrofuran at -78 - 20℃; for 1.33333h;
With N-chloro-succinimide; thiourea In methanol at 35℃; for 2h; Inert atmosphere;
7-Methoxy-1-tetralone
6836-19-7

7-Methoxy-1-tetralone

8-bromo-7-methoxy-1,2,3,4-tetrahydronaphthalen-1-one
61362-78-5

8-bromo-7-methoxy-1,2,3,4-tetrahydronaphthalen-1-one

Conditions
ConditionsYield
With iron(III) chloride; N-Bromosuccinimide In acetonitrile at 20℃; for 4h;99%
With iron(III) chloride; N-Bromosuccinimide In acetonitrile at 20℃; for 10h;98%
With N-Bromosuccinimide In acetonitrile at 20℃;96%
7-Methoxy-1-tetralone
6836-19-7

7-Methoxy-1-tetralone

(-)-(R)-7-Methoxy-1-tetralol

(-)-(R)-7-Methoxy-1-tetralol

Conditions
ConditionsYield
With C32H39BrMnN2O2P; potassium tert-butylate; hydrogen In methanol at 20℃; under 22502.3 Torr; for 16h; Glovebox; Autoclave; enantioselective reaction;99%
With potassium tert-butylate; hydrogen; trans-RuCl2[(S)-XylBINAP][(R)-IPHAN] In isopropyl alcohol; tert-butyl alcohol at 25℃; under 6840 Torr; for 8h;95%
With bis(1,5-cyclooctadiene)diiridium(I) dichloride; C49H64FeNOP; hydrogen; sodium t-butanolate In isopropyl alcohol at 25 - 30℃; under 38002.6 Torr; for 12h; Autoclave; enantioselective reaction;95%
7-Methoxy-1-tetralone
6836-19-7

7-Methoxy-1-tetralone

1-methylene-7-methoxy-1,2,3,4-tetrahydronaphthalene
107727-34-4

1-methylene-7-methoxy-1,2,3,4-tetrahydronaphthalene

Conditions
ConditionsYield
With (bromomethyl)triphenyl-λ5-phosphane; potassium tert-butylate In tetrahydrofuran at 20 - 50℃; for 1h; Wittig Olefination; Inert atmosphere;99%
7-Methoxy-1-tetralone
6836-19-7

7-Methoxy-1-tetralone

2-(3,4,5-trimethoxybenzylidene)malononitrile
5688-82-4

2-(3,4,5-trimethoxybenzylidene)malononitrile

2-amino-5,6-dihydro-9-methoxy-4-(3,4,5-trimethoxyphenyl)benzo[h]quinoline-3-carbonitrile

2-amino-5,6-dihydro-9-methoxy-4-(3,4,5-trimethoxyphenyl)benzo[h]quinoline-3-carbonitrile

Conditions
ConditionsYield
With ammonium acetate; acetic acid In ethanol for 12h; Reflux;99%
7-Methoxy-1-tetralone
6836-19-7

7-Methoxy-1-tetralone

acetonitrile
75-05-8

acetonitrile

2-(1-hydroxyl-7-methoxy-1,2,3,4-tetrahydro-naphthalen-1-yl)-acetonitrile
59081-65-1

2-(1-hydroxyl-7-methoxy-1,2,3,4-tetrahydro-naphthalen-1-yl)-acetonitrile

Conditions
ConditionsYield
Stage #1: acetonitrile With n-butyllithium In tetrahydrofuran; hexane at -70℃; for 0.5h;
Stage #2: 7-Methoxy-1-tetralone In tetrahydrofuran; hexane at -70℃; for 1h;
Stage #3: With ammonium chloride In tetrahydrofuran; hexane; water Product distribution / selectivity;
98.4%
Stage #1: acetonitrile With n-butyllithium In tetrahydrofuran; hexane at -70℃; for 0.5h; Cooling with ethanol-dry ice;
Stage #2: 7-Methoxy-1-tetralone In tetrahydrofuran; hexane at -70℃; for 1h; Concentration; Cooling with ether-dry ice;
98.4%
With n-butyllithium In tetrahydrofuran; hexane at -78℃; for 1h;95%
Stage #1: 7-Methoxy-1-tetralone; acetonitrile With sodium hexamethyldisilazane In tetrahydrofuran at -80 - -70℃; for 0.75h; Inert atmosphere;
Stage #2: With ammonium chloride In tetrahydrofuran
7-Methoxy-1-tetralone
6836-19-7

7-Methoxy-1-tetralone

N,N-dimethyl-formamide
68-12-2, 33513-42-7

N,N-dimethyl-formamide

1-chloro-7-methoxy-3,4-dihydronaphthalene-2-carboxaldehyde
77664-95-0

1-chloro-7-methoxy-3,4-dihydronaphthalene-2-carboxaldehyde

Conditions
ConditionsYield
Stage #1: N,N-dimethyl-formamide With trichlorophosphate for 0.5h; Cooling with ice;
Stage #2: 7-Methoxy-1-tetralone at 20 - 70℃; for 2h;
98.1%
Stage #1: N,N-dimethyl-formamide With trichlorophosphate at -10℃; Vilsmeier-Haack reaction; Reflux;
Stage #2: 7-Methoxy-1-tetralone In N,N-dimethyl-formamide for 2h; Vilsmeier-Haack reaction; Reflux;
Stage #3: With water; sodium acetate In N,N-dimethyl-formamide Vilsmeier-Haack reaction;
93%
With trichlorophosphate at 0 - 90℃; Vilsmeier-Haack Formylation;91%
Stage #1: N,N-dimethyl-formamide With trichlorophosphate at 0 - 20℃;
Stage #2: 7-Methoxy-1-tetralone at 0 - 20℃; for 6h;
90%
With trichlorophosphate 1.) CH2Cl2, 27 deg C, 2 h, 2.) CH2Cl2, 27 deg C, 8 h; Yield given. Multistep reaction;
7-Methoxy-1-tetralone
6836-19-7

7-Methoxy-1-tetralone

7-hydroxy-1-tetralone
22009-38-7

7-hydroxy-1-tetralone

Conditions
ConditionsYield
With hydrogen bromide; acetic acid In water at 120℃;98%
Stage #1: 7-Methoxy-1-tetralone With aluminum (III) chloride In toluene at 20 - 65℃; for 2.6h;
Stage #2: In toluene at 0 - 65℃; for 1.5h; Temperature;
96.4%
With aluminium trichloride In toluene Heating;95%
trimethylsilyl cyanide
7677-24-9

trimethylsilyl cyanide

7-Methoxy-1-tetralone
6836-19-7

7-Methoxy-1-tetralone

7-methoxy-1-(trimethylsilyloxy)-1,2,3,4-tetrahydronaphthalene-1-carbonitrile
182621-29-0

7-methoxy-1-(trimethylsilyloxy)-1,2,3,4-tetrahydronaphthalene-1-carbonitrile

Conditions
ConditionsYield
With zinc(II) iodide In acetonitrile at 20℃; for 48h; Addition;98%
With zinc(II) iodide In dichloromethane at 25℃; for 24h;
With zinc(II) iodide
With zinc(II) iodide In dichloromethane at 20℃;
With zinc(II) iodide In nitromethane at 0 - 20℃; for 96h; Inert atmosphere;
7-Methoxy-1-tetralone
6836-19-7

7-Methoxy-1-tetralone

(+)-(S)-7-Methoxy-1-tetralol
182965-69-1

(+)-(S)-7-Methoxy-1-tetralol

Conditions
ConditionsYield
With chloro[(1S,2S)-N-(p-toluenesulfonyl)-1,2-diphenylethylenediamine]-(mesitylene) ruthenium (II); formic acid; triethylamine In dichloromethane at 0 - 20℃; for 72h; Inert atmosphere; Schlenk technique; enantioselective reaction;98%
With chloro[(1S,2S)-N-(p-toluenesulfonyl)-1,2-diphenylethylenediamine]-(mesitylene) ruthenium (II); formic acid; triethylamine In dichloromethane at 23℃; for 48h; Inert atmosphere; Cooling with ice; Schlenk technique;98%
With formic acid; C29H38N3O2RuS; triethylamine at 60℃; for 4h; Inert atmosphere; enantioselective reaction;96%
3-bromo-1-(4-ethylpiperazin-1-yl)isoquinoline
223552-79-2

3-bromo-1-(4-ethylpiperazin-1-yl)isoquinoline

7-Methoxy-1-tetralone
6836-19-7

7-Methoxy-1-tetralone

3-(6-methoxy-1,2-dihydronaphthalen-4-yl)-1-(4-ethylpiperazin-1-yl)isoquinoline

3-(6-methoxy-1,2-dihydronaphthalen-4-yl)-1-(4-ethylpiperazin-1-yl)isoquinoline

Conditions
ConditionsYield
98%
methyl magnesium iodide
917-64-6

methyl magnesium iodide

7-Methoxy-1-tetralone
6836-19-7

7-Methoxy-1-tetralone

1,2-dihydro-6-methoxy-4-methylnaphthalene
30021-91-1

1,2-dihydro-6-methoxy-4-methylnaphthalene

Conditions
ConditionsYield
Stage #1: methyl magnesium iodide; 7-Methoxy-1-tetralone In diethyl ether at 20℃; for 3h;
Stage #2: With hydrogenchloride In water at 40℃; for 3h; pH=5;
97%
With diethyl ether Erhitzen des nach der Hydrolyse erhaltenen Reaktionsprodukts unter Normaldruck auf 100-110grad;
With diethyl ether Erhitzen des nach der Hydrolyse erhaltenen Reaktionsprodukts unter vermindertem Druck auf 120-160grad;
7-Methoxy-1-tetralone
6836-19-7

7-Methoxy-1-tetralone

7-methoxy-1-d-1,2,3,4-tetrahydro-1-naphthol
199442-41-6

7-methoxy-1-d-1,2,3,4-tetrahydro-1-naphthol

Conditions
ConditionsYield
With sodium borodeuteride In methanol for 1.5h;97%
With sodium borodeuteride
7-Methoxy-1-tetralone
6836-19-7

7-Methoxy-1-tetralone

allyl bromide
106-95-6

allyl bromide

A

8a-allyl-7-methoxy-1,2,3,4,6,8a-hexahydro-naphthalen-1-one
310897-19-9

8a-allyl-7-methoxy-1,2,3,4,6,8a-hexahydro-naphthalen-1-one

B

2,8a-diallyl-7-methoxy-3,4,6,8a-tetrahydro-2H-naphthalen-1-one

2,8a-diallyl-7-methoxy-3,4,6,8a-tetrahydro-2H-naphthalen-1-one

Conditions
ConditionsYield
Stage #1: 7-Methoxy-1-tetralone With ammonia; potassium In diethyl ether; tert-butyl alcohol at -78℃; for 0.25h; Reduction;
Stage #2: With lithium bromide In diethyl ether; tert-butyl alcohol at -78℃; for 0.5h; deprotonation;
Stage #3: allyl bromide In diethyl ether; tert-butyl alcohol at -78 - 20℃; Alkylation; Birch reductive alkylation;
A 97%
B n/a
7-Methoxy-1-tetralone
6836-19-7

7-Methoxy-1-tetralone

phenyl trifluoromethanesulfonamide
456-64-4

phenyl trifluoromethanesulfonamide

trifluoromethanesulfonic acid 7-methoxy-3,4-dihydronaphthalen-1-yl ester
724707-85-1

trifluoromethanesulfonic acid 7-methoxy-3,4-dihydronaphthalen-1-yl ester

Conditions
ConditionsYield
Stage #1: 7-Methoxy-1-tetralone With 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; lithium diisopropyl amide In tetrahydrofuran at -78℃; for 2h;
Stage #2: phenyl trifluoromethanesulfonamide In tetrahydrofuran at 0℃; for 9h;
97%
7-Methoxy-1-tetralone
6836-19-7

7-Methoxy-1-tetralone

1-((allyloxy)carbonyl)-1H-imidazole
83395-39-5

1-((allyloxy)carbonyl)-1H-imidazole

allyl 7-methoxy-3,4-dihydronaphthalen-1-yl carbonate

allyl 7-methoxy-3,4-dihydronaphthalen-1-yl carbonate

Conditions
ConditionsYield
Stage #1: 7-Methoxy-1-tetralone With sodium hexamethyldisilazane In 1,2-dimethoxyethane at -78℃; for 1h; Inert atmosphere;
Stage #2: 1-((allyloxy)carbonyl)-1H-imidazole With boron trifluoride diethyl etherate In 1,2-dimethoxyethane at -78℃; for 2.16667h; Inert atmosphere;
97%
7-Methoxy-1-tetralone
6836-19-7

7-Methoxy-1-tetralone

oxalic acid diethyl ester
95-92-1

oxalic acid diethyl ester

ethyl 2-(1-hydroxy-7-methoxy-3,4-dihydronaphthalen-2-yl)-2-oxoacetate
1417448-97-5

ethyl 2-(1-hydroxy-7-methoxy-3,4-dihydronaphthalen-2-yl)-2-oxoacetate

Conditions
ConditionsYield
With lithium tert-butoxide In tetrahydrofuran at 0 - 20℃; for 4h; Claisen Condensation; Inert atmosphere;97%
7-Methoxy-1-tetralone
6836-19-7

7-Methoxy-1-tetralone

cyanoacetic acid
372-09-8

cyanoacetic acid

2-(7-methoxy-3,4-dihydronaphthalen-1-yl)acetonitrile
861960-34-1

2-(7-methoxy-3,4-dihydronaphthalen-1-yl)acetonitrile

Conditions
ConditionsYield
With oenanthic acid; benzylamine In toluene at 140℃; for 48h;96.3%
With oenanthic acid; benzylamine In toluene Product distribution / selectivity; Heating / reflux;90%
With oenanthic acid; benzylamine In toluene Product distribution / selectivity; Heating / reflux;90%
7-methoxy-1,2,3,4-tetrahydro-1-naphthol
32820-10-3

7-methoxy-1,2,3,4-tetrahydro-1-naphthol

7-Methoxy-1-tetralone
6836-19-7

7-Methoxy-1-tetralone

7-methoxy-3,4-dihydronaphthalene
60573-58-2

7-methoxy-3,4-dihydronaphthalene

Conditions
ConditionsYield
96%
7-Methoxy-1-tetralone
6836-19-7

7-Methoxy-1-tetralone

salicylaldehyde
90-02-8

salicylaldehyde

2-methoxy-7H-benzo[c]xanthene
1289414-86-3

2-methoxy-7H-benzo[c]xanthene

Conditions
ConditionsYield
With scandium tris(trifluoromethanesulfonate) In chlorobenzene at 180℃; for 0.5h; Microwave irradiation;96%
7-Methoxy-1-tetralone
6836-19-7

7-Methoxy-1-tetralone

N-methoxylamine hydrochloride
593-56-6

N-methoxylamine hydrochloride

C12H15NO2

C12H15NO2

Conditions
ConditionsYield
With pyridine In ethanol for 1h; Inert atmosphere; Reflux;96%
7-Methoxy-1-tetralone
6836-19-7

7-Methoxy-1-tetralone

3,4,5-trimethoxy-benzaldehyde
86-81-7

3,4,5-trimethoxy-benzaldehyde

(E)-2-(3,4,5-trimethoxybenzylidene)-7-methoxy-3,4-dihydronaphthalen-1(2H)-one

(E)-2-(3,4,5-trimethoxybenzylidene)-7-methoxy-3,4-dihydronaphthalen-1(2H)-one

Conditions
ConditionsYield
With sodium methylate In methanol at 20℃;96%
With sodium hydroxide In ethanol
7-Methoxy-1-tetralone
6836-19-7

7-Methoxy-1-tetralone

6-methoxy-1,2,3,4-tetrahydronaphthalene
1730-48-9

6-methoxy-1,2,3,4-tetrahydronaphthalene

Conditions
ConditionsYield
With palladium dichloride In methanol at 40℃; for 24h; Inert atmosphere; Green chemistry;95%
With potassium hydroxide; hydrazine hydrate In diethylene glycol for 0.333333h; Wolff-Kishner reduction; Irradiation;87%
With hydrazine hydrate; sodium hydroxide In methanol at 200℃; under 37503.8 Torr; Wolff-Kishner Reduction; Microwave irradiation;81%
With copper oxide-chromium oxide at 125 - 200℃; under 154457 Torr; Hydrogenolyse;
With hydrogenchloride; amalgamated zinc
7-Methoxy-1-tetralone
6836-19-7

7-Methoxy-1-tetralone

ethyl bromoacetate
105-36-2

ethyl bromoacetate

ethyl 1-hydroxy-7-methoxy-1,2,3,4-tetrahydro-1-naphthaleneacetate
99416-97-4

ethyl 1-hydroxy-7-methoxy-1,2,3,4-tetrahydro-1-naphthaleneacetate

Conditions
ConditionsYield
Stage #1: 7-Methoxy-1-tetralone; ethyl bromoacetate With zinc In tert-butyl methyl ether at 55 - 60℃; Reformatsky Reaction;
Stage #2: With hydrogenchloride; water at 10 - 15℃;
95%
With toluene; zinc
With iodine; zinc In benzene for 2.5h; Reformatsky reaction; Heating;
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