Conditions | Yield |
---|---|
With water; sodium hydroxide In ethanol at 10 - 20℃; for 1.08333h; | 100% |
With iodine; aluminium In acetonitrile at 80℃; for 18h; | 99% |
1-(2-bromophenyl)-4,4,4-trifluorobutane-1,3-dione
2-bromobenzoic-acid
Conditions | Yield |
---|---|
With oxygen; sodium hydrogencarbonate In acetonitrile for 4h; Molecular sieve; Irradiation; | 96% |
Conditions | Yield |
---|---|
With ruthenium trichloride; sodium hypochlorite; tetrabutylammomium bromide In 1,2-dichloro-ethane at 25℃; for 2h; | 95% |
With ruthenium trichloride; sodium hypochlorite; tetrabutylammomium bromide In 1,2-dichloro-ethane at 25℃; for 2h; Rate constant; pH 9; | 95% |
With potassium acetate In water | 93.2% |
Conditions | Yield |
---|---|
With oxygen; Langlois reagent In acetonitrile at 25℃; under 760.051 Torr; for 12h; Irradiation; Green chemistry; | 95% |
With tert.-butylhydroperoxide; potassium tert-butylate In water at 60℃; for 5h; | 90% |
With oxygen at 120℃; for 5h; Neat (no solvent); | 85% |
o-bromobenzyl alcohol
2-bromobenzoic-acid
Conditions | Yield |
---|---|
With sodium bromate; sodium hydrogen sulfate In acetonitrile for 20h; Heating; | 95% |
With Langlois reagent In acetonitrile at 25℃; for 12h; Irradiation; Sealed tube; | 91% |
With 3,5-Lutidine; 4-acetylamino-2,2,6,6-tetramethylpiperidine-N-oxyl; sodium persulfate; tris(2,2'‐bipyridine)ruthenium(II) hexafluorophosphate In water; acetonitrile at 20℃; for 48h; Sealed tube; Irradiation; | 75% |
Conditions | Yield |
---|---|
Stage #1: 2-bromostyrene With tert.-butylhydroperoxide; iron(III) chloride hexahydrate; sodium hydroxide In water at 80℃; for 10h; Stage #2: With hydrogenchloride In water at 20℃; | 95% |
With Oxone; 2-iodo-3,4,5,6-tetramethylbenzoic acid In water; acetonitrile for 24h; | 81% |
With Oxone In water; acetonitrile for 24h; Reflux; | 77% |
2-bromobenzoic-acid
Conditions | Yield |
---|---|
With tert.-butylhydroperoxide; potassium tert-butylate In water at 80℃; for 8h; | 94% |
Conditions | Yield |
---|---|
With potassium bromide; potassium acetate | 92.7% |
2-bromobenzoic-acid
Conditions | Yield |
---|---|
With iodine; dimethyl sulfoxide at 180℃; for 0.0833333h; Inert atmosphere; Microwave irradiation; | 92% |
2-bromobenzoic-acid
Conditions | Yield |
---|---|
With sodium hydroxide In water at 100℃; for 9h; Reflux; chemoselective reaction; | 92% |
Conditions | Yield |
---|---|
Stage #1: ortho-bromobenzaldehyde With potassium hydroxide for 0.0833333h; Cannizzaro Reaction; Milling; Inert atmosphere; Sealed tube; Green chemistry; Stage #2: With hydrogenchloride In water for 0.0833333h; Green chemistry; | A 91% B 90% |
5-[(2-bromophenyl)methylene]-2,2-dimethyl-1,3-dioxane-4,6-dione
2-bromobenzoic-acid
Conditions | Yield |
---|---|
With oxone In water for 16h; Reflux; | 91% |
2-bromo-N,N-diisopropylbenzamide
2-bromobenzoic-acid
Conditions | Yield |
---|---|
With hydrogenchloride; zinc(II) chloride at 160℃; for 72h; | 90% |
2-bromobenzoic-acid
Conditions | Yield |
---|---|
With hydrogenchloride In water at 145℃; for 48h; Schlenk technique; | 89% |
With hydrogenchloride; water at 145℃; for 48h; | 80% |
Conditions | Yield |
---|---|
With Oxone; trifluoroacetic acid In 1,4-dioxane for 10h; Reflux; Green chemistry; | 88% |
With hydroxylamine hydrochloride; iodine In dimethyl sulfoxide at 100℃; for 5h; | 58% |
Conditions | Yield |
---|---|
With C22H28Br2N4Pd; water; potassium carbonate In tetrahydrofuran at 100℃; under 750.075 Torr; for 24h; Autoclave; | 86% |
With water; palladium diacetate; potassium carbonate at 20℃; under 760.051 Torr; for 12h; | 84% |
With water; palladium diacetate; triethylamine; triphenylphosphine In 1,4-dioxane at 110℃; under 11251.1 Torr; for 2h; Flow reactor; | 70% |
2-(2-bromophenyl)-2-hydroxyacetonitrile
A
ortho-bromobenzaldehyde
B
2-bromobenzoic-acid
Conditions | Yield |
---|---|
Stage #1: 2-(2-bromophenyl)-2-hydroxyacetonitrile With (η(6)-benzene)chloro[1,2-bis(diphenylphosphino)ethane]ruthenium(II) chloride In benzene at 120℃; for 24h; Inert atmosphere; Schlenk technique; Stage #2: With water In dichloromethane; ethyl acetate; benzene for 24h; | A 81% B 17% |
Conditions | Yield |
---|---|
With Oxone In water; acetonitrile for 24h; Reflux; | 80% |
2,5-dibromobenzoic acid
A
m-bromobenzoic acid
B
benzoic acid
C
2-bromobenzoic-acid
Conditions | Yield |
---|---|
With n-butyllithium In tetrahydrofuran | A 78% B 13% C 2% |
2-methylphenyl bromide
A
1-Bromo-2-bromomethyl-benzene
B
2-bromobenzoic-acid
Conditions | Yield |
---|---|
With tert.-butylhydroperoxide; copper(ll) bromide In acetic anhydride | A 77% B 10% |
1-(Bis-tert-butylperoxy-methyl)-2-bromo-benzene
2-bromobenzoic-acid
Conditions | Yield |
---|---|
With piperidine In water at 90℃; for 3h; | 76% |
2-bromobenzoic-acid
Conditions | Yield |
---|---|
Stage #1: 2-b romo-N-(quinolin-8-yl)benzamide With ozone In dichloromethane at -78℃; Inert atmosphere; Stage #2: With lithium hydroxide monohydrate; dihydrogen peroxide In tetrahydrofuran; water at 20℃; for 24h; Inert atmosphere; | 66% |
Conditions | Yield |
---|---|
Stage #1: With [bis(acetoxy)iodo]benzene; iodine In 1,2-dichloro-ethane at 20℃; for 1h; Stage #2: benzoic acid With tetrabutylammomium bromide; palladium diacetate In 1,2-dichloro-ethane at 100℃; for 24h; | A n/a B 65% |
Conditions | Yield |
---|---|
With chloro[1,3-bis(2,6-di-i-propylphenyl)imidazol-2-ylidene]copper(I); potassium methanolate In N,N-dimethyl acetamide at 70℃; for 24h; Schlenk technique; Sealed tube; | 65% |
Conditions | Yield |
---|---|
With tert.-butylhydroperoxide; [O-Cu4(triethanolamine)4(BOH)4][BF4]2 In acetonitrile at 69.84℃; for 6h; | A 61.8% B n/a |
With 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; Ir(4,4'-di-tert-butyl-2,2'-bipyridyl)(2-phenylpyridine)2(PF6); tetrabutyl-ammonium chloride; oxygen; sodium hydrogencarbonate In dichloromethane; water at 20℃; for 48h; Reagent/catalyst; Solvent; Irradiation; Green chemistry; chemoselective reaction; | A > 99 %Chromat. B 9% |
With oxygen; potassium carbonate In water at 80℃; for 48h; |
4-(2-bromophenyl)but-3-en-2-one
2-bromobenzoic-acid
Conditions | Yield |
---|---|
With hydroxylamine hydrochloride; iodine In dimethyl sulfoxide at 100℃; for 6h; | 60% |
1-Bromo-2-iodobenzene
diphenylmethylsilanecarboxylic acid
2-bromobenzoic-acid
Conditions | Yield |
---|---|
With potassium trimethylsilonate; 4,5-bis(diphenylphos4,5-bis(diphenylphosphino)-9,9-dimethylxanthenephino)-9,9-dimethylxanthene; bis(dibenzylideneacetone)-palladium(0) In 1,4-dioxane at 60℃; Sealed tube; | 60% |
Conditions | Yield |
---|---|
With 1,2-dibromo-1,1,2,2-tetrachloroethane; N,N,N,N,-tetramethylethylenediamine; sec.-butyllithium In tetrahydrofuran; hexane; cyclohexane 1.) -90 deg C, 60 min, 2.) -78 deg C; | 55% |
With 1,2-dibromo-1,1,2,2-tetrachloroethane; N,N,N,N,-tetramethylethylenediamine; sec.-butyllithium In tetrahydrofuran 1.) -90 deg C, 30 min, 2.) -78 deg C; | 55% |
With chlorosulfonic acid; bromine at 10℃; for 2.5h; Temperature; Inert atmosphere; |
1-Bromo-2-iodobenzene
carbon monoxide
phenylboronic acid
A
o-bromobenzophenone
B
2-bromobenzoic-acid
Conditions | Yield |
---|---|
With C57H43IP2Pd; potassium carbonate In 1,4-dioxane at 90℃; under 3750.38 Torr; for 12h; carbonylative Suzuki coupling; Autoclave; | A 50% B n/a |
1-(2-bromophenyl)-butane-1,3-dione
2-bromobenzoic-acid
Conditions | Yield |
---|---|
With oxygen; sodium hydrogencarbonate In acetonitrile for 4h; Molecular sieve; Irradiation; | 50% |
Conditions | Yield |
---|---|
With thionyl chloride; N,N-dimethyl-formamide In dichloromethane at 20℃; for 3h; | 100% |
Stage #1: 2-bromobenzoic-acid With oxalyl dichloride In dichloromethane at 20℃; for 0.0833333h; Stage #2: With N,N-dimethyl-formamide In dichloromethane at 20℃; for 5h; | 100% |
With thionyl chloride In N,N-dimethyl-formamide at 70℃; Inert atmosphere; | 100% |
2-bromobenzoic-acid
2-bromobenzoic anhydride
Conditions | Yield |
---|---|
With trimethylsilylethoxyacetylene In dichloromethane at 20℃; for 3h; | 100% |
With potassium carbonate In dichloromethane at 20℃; for 0.583333h; | 91% |
With potassium carbonate; p-toluenesulfonyl chloride In acetonitrile at 20℃; for 2h; | 70% |
Conditions | Yield |
---|---|
With copper(I) oxide; copper; potassium carbonate In N,N-dimethyl-formamide at 130℃; for 20h; Inert atmosphere; | 100% |
With copper; potassium carbonate; copper(II) oxide In N,N-dimethyl-formamide at 130℃; for 20h; | 94% |
With copper; potassium carbonate In N,N-dimethyl-formamide Jourdan-Ullmann reaction; Inert atmosphere; Reflux; | 91% |
2-amino-3-methoxybenzoic acid
2-bromobenzoic-acid
2-(2-carboxyphenylamino)-3-methoxybenzoic acid
Conditions | Yield |
---|---|
With copper; potassium carbonate In ethanol for 1h; Reflux; Inert atmosphere; | 100% |
With copper; potassium carbonate In ethanol for 1.5h; Reflux; | 5.07 g |
With copper; potassium carbonate In ethanol for 1.5h; Reflux; |
Conditions | Yield |
---|---|
With dibromoisocyanuric acid In dichloromethane at 20℃; for 24h; Reagent/catalyst; Solvent; Temperature; UV-irradiation; | 100% |
Conditions | Yield |
---|---|
With sulfuric acid Reflux; Inert atmosphere; | 99% |
With sulfuric acid Reflux; | 99% |
With sulfuric acid at 0℃; for 20.25h; Fischer-Speier Esterification; Reflux; | 96% |
Conditions | Yield |
---|---|
With trans-[PdBr2(1-n-butyl-3-(1-O-methyl-6-deoxy-α-D-glucopyrano-6-yl)imidazol-2-ylidene)2]; sodium methylate In water at 100℃; for 15h; Suzuki coupling; | 99% |
With potassium carbonate In water at 50℃; for 1.5h; Suzuki Coupling; | 98% |
With magnesium hydroxide; potassium hydroxide; barium(II) hydroxide; calcium hydroxide In water at 20℃; for 15h; Suzuki Coupling; | 98% |
1,3-cylohexanedione
2-bromobenzoic-acid
2-bromo-benzoic acid 3-oxo-cyclohex-1-enyl ester
Conditions | Yield |
---|---|
With 2-chloro-1-methyl-pyridinium iodide; triethylamine In tetrahydrofuran at 20℃; Acylation; | 99% |
With 2-chloro-1-methyl-pyridinium iodide; triethylamine In tetrahydrofuran at 20℃; for 10h; | 99% |
4-Methoxybenzenethiol
2-bromobenzoic-acid
2-<(4-methoxyphenyl)thio>benzoic acid
Conditions | Yield |
---|---|
With copper(I) oxide; copper; potassium carbonate In 2-ethoxy-ethanol at 130℃; for 4h; | 99% |
Conditions | Yield |
---|---|
With copper(I) oxide; copper; potassium carbonate In 2-ethoxy-ethanol at 130℃; for 12h; | 99% |
Conditions | Yield |
---|---|
With copper(I) oxide; copper; potassium carbonate In 2-ethoxy-ethanol at 130℃; for 4h; | 99% |
With tetra(n-butyl)ammonium hydroxide In water at 80℃; for 48h; Inert atmosphere; Sealed tube; chemoselective reaction; | 87% |
With copper(I) oxide; copper; potassium carbonate In 2-ethoxy-ethanol at 130℃; for 4h; | 76% |
benzamidine monohydrochloride
2-bromobenzoic-acid
2-phenyl-4(3H)-quinazolinone
Conditions | Yield |
---|---|
With C26H24Cu2N8(2+)*2F6P(1-); caesium carbonate In N,N-dimethyl-formamide at 70℃; for 6h; Inert atmosphere; Sealed tube; | 99% |
With caesium carbonate In N,N-dimethyl-formamide at 20℃; for 10h; Inert atmosphere; Sealed tube; | 95% |
With copper(l) iodide; caesium carbonate In N,N-dimethyl-formamide at 25℃; for 12h; Inert atmosphere; | 85% |
Conditions | Yield |
---|---|
Stage #1: 2-bromobenzoic-acid With oxalyl dichloride; N,N-dimethyl-formamide In dichloromethane for 20h; Inert atmosphere; Cooling with ice; Stage #2: 3-nitro-aniline With pyridine In dichloromethane at 45℃; for 1h; Inert atmosphere; | 99% |
Stage #1: 2-bromobenzoic-acid With oxalyl dichloride In dichloromethane; N,N-dimethyl-formamide for 20h; Sealed tube; Inert atmosphere; Cooling with ice; Stage #2: 3-nitro-aniline With pyridine In dichloromethane; N,N-dimethyl-formamide at 45℃; for 1h; | 99% |
Conditions | Yield |
---|---|
With bis-triphenylphosphine-palladium(II) chloride; potassium hydroxide In neat (no solvent) at 110℃; for 24h; Suzuki-Miyaura Coupling; Schlenk technique; Inert atmosphere; | 99% |
4-iodoanisol
bicyclo[2.2.1]hepta-2,5-diene
2-bromobenzoic-acid
1-methoxyphenanthrene
Conditions | Yield |
---|---|
With palladium diacetate; caesium carbonate; tricyclohexylphosphine In 1,4-dioxane at 130℃; for 18h; Schlenk technique; Sealed tube; Inert atmosphere; | 99% |
bicyclo[2.2.1]hepta-2,5-diene
1-iodo-2-(trifluoromethoxy)benzene
2-bromobenzoic-acid
Conditions | Yield |
---|---|
With palladium diacetate; caesium carbonate; tricyclohexylphosphine In 1,4-dioxane at 130℃; for 18h; Schlenk technique; Sealed tube; Inert atmosphere; | 99% |
1-Fluoro-2-iodobenzene
bicyclo[2.2.1]hepta-2,5-diene
2-bromobenzoic-acid
1-fluorophenanthrene
Conditions | Yield |
---|---|
With palladium diacetate; caesium carbonate; tricyclohexylphosphine In 1,4-dioxane at 130℃; for 18h; Schlenk technique; Sealed tube; Inert atmosphere; | 99% |
ethyl 5-(2-iodophenoxy)pentanoic acid
bicyclo[2.2.1]hepta-2,5-diene
2-bromobenzoic-acid
Conditions | Yield |
---|---|
With palladium diacetate; caesium carbonate; tricyclohexylphosphine In 1,4-dioxane at 130℃; for 18h; Schlenk technique; Sealed tube; Inert atmosphere; | 99% |
4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane
2-bromobenzoic-acid
Conditions | Yield |
---|---|
In neat (no solvent) at 30℃; Inert atmosphere; Schlenk technique; Glovebox; chemoselective reaction; | 99% |
With [ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2 In neat (no solvent) at 60℃; for 24h; | |
With (4-Me)Triaz(NHPiPr2)2Mn(CO)2Br In toluene at 25℃; for 6h; Catalytic behavior; Inert atmosphere; chemoselective reaction; | > 99 %Spectr. |
2-bromobenzoic-acid
9-methyl-9H-dibenzo[a,c]carbazole
Conditions | Yield |
---|---|
With bis-triphenylphosphine-palladium(II) chloride; potassium carbonate; p-benzoquinone In dimethyl sulfoxide at 140℃; for 9h; Schlenk technique; Inert atmosphere; | 99% |
Conditions | Yield |
---|---|
With norborn-2-ene; bis-triphenylphosphine-palladium(II) chloride; potassium carbonate; p-benzoquinone In dimethyl sulfoxide at 140℃; for 3h; Schlenk technique; Inert atmosphere; | 99% |
ethyl acetoacetate
2-bromobenzoic-acid
2-(ethoxycarbonylmethyl)benzoic acid
Conditions | Yield |
---|---|
Stage #1: ethyl acetoacetate With sodium ethanolate In ethanol at 20℃; for 0.166667h; Inert atmosphere; Stage #2: 2-bromobenzoic-acid With copper(I) bromide In ethanol at 80℃; for 16h; Inert atmosphere; | 98% |
With sodium ethanolate; copper |
Conditions | Yield |
---|---|
With dmap; dicyclohexyl-carbodiimide In tetrahydrofuran Ambient temperature; | 98% |
Conditions | Yield |
---|---|
With potassium carbonate; copper In water at 130 - 140℃; for 3h; Product distribution / selectivity; Ullmann Condensation; | 98% |
With copper; potassium carbonate In water at 130 - 140℃; for 3h; | 96% |
With potassium carbonate In water | 52.8 g (97%) |
Conditions | Yield |
---|---|
Stage #1: 2-bromobenzoic-acid With water; sodium carbonate for 1h; Heating / reflux; Stage #2: With water; trans-N,N'-dimethyl-1,2-cyclohexyldiamine; copper(ll) bromide at 80℃; for 1h; Stage #3: With hydrogenchloride In water at 25℃; Product distribution / selectivity; | 98% |
Stage #1: 2-bromobenzoic-acid With water; sodium carbonate for 1h; Heating / reflux; Stage #2: trans-N,N'-dimethyl-1,2-cyclohexyldiamine; copper(I) bromide In acetonitrile at 80℃; for 2h; Stage #3: With hydrogenchloride In water; acetonitrile at 25℃; Product distribution / selectivity; | 98% |
Stage #1: 2-bromobenzoic-acid With water; sodium carbonate at 80℃; Stage #2: With water; trans-N,N'-dimethyl-1,2-cyclohexyldiamine; copper(I) bromide In water; acetonitrile at 80℃; for 3h; Stage #3: With hydrogenchloride In water; acetonitrile at 20℃; Product distribution / selectivity; | 96% |
Conditions | Yield |
---|---|
With dmap; dicyclohexyl-carbodiimide In dichloromethane at 0 - 20℃; | 98% |
[3-(methoxycarbonyl)phenyl]boronic acid
2-bromobenzoic-acid
3'-(methoxycarbonyl)-[1,1'-biphenyl]-2-carboxylic acid
Conditions | Yield |
---|---|
With palladium bis[bis(diphenylphosphino)ferrocene] dichloride; potassium carbonate In chloroform; water at 80 - 100℃; for 0.25h; Suzuki Coupling; | 98% |
With PdCl2-[5-(naphth-1-yl)isoxazole-3-carbaldehyde oxime]; potassium carbonate In methanol; water at 100℃; for 0.166667h; Suzuki Coupling; | 97% |
ortho-methylphenyl iodide
bicyclo[2.2.1]hepta-2,5-diene
2-bromobenzoic-acid
1-methylphenanthrene
Conditions | Yield |
---|---|
With palladium diacetate; caesium carbonate; tricyclohexylphosphine In 1,4-dioxane at 130℃; for 18h; Catalytic behavior; Reagent/catalyst; Solvent; Schlenk technique; Sealed tube; Inert atmosphere; | 98% |
2-iodo-5-methylthiophene
bicyclo[2.2.1]hepta-2,5-diene
2-bromobenzoic-acid
2-methylnaphtho[2,1-b]thiophene
Conditions | Yield |
---|---|
With palladium diacetate; caesium carbonate; tricyclohexylphosphine In 1,4-dioxane at 130℃; for 18h; Schlenk technique; Sealed tube; Inert atmosphere; | 98% |
The IUPAC name of this chemical is 2-bromobenzoic acid. With the CAS registry number 88-65-3, it is also named as Benzoic acid, 2-bromo-. The product's categories are Aromatic Compounds; Aromatic Carboxylic Acids, Amides, Anilides, Anhydrides & Salts; Benzoic Acid; Organic Acids; Acids & Esters; Bromine Compounds; C7; Carbonyl Compounds; Carboxylic Acids. It is white to light yellow crystal powder which is soluble in alcohol, ether, acetone, chloroform and hot water, slightly soluble in cold water. When heated to decomposition it emits toxic vapors of Br−. Additionally, this chemical should be sealed in the container.
The other characteristics of this product can be summarized as: (1)ACD/LogP: 2.15; (2)# of Rule of 5 Violations: 0; (3)ACD/LogD (pH 5.5): -0.38; (4)ACD/LogD (pH 7.4): -0.98; (5)ACD/BCF (pH 5.5): 1; (6)ACD/BCF (pH 7.4): 1; (7)ACD/KOC (pH 5.5): 1.04; (8)ACD/KOC (pH 7.4): 1; (9)#H bond acceptors: 2; (10)#H bond donors: 1; (11)#Freely Rotating Bonds: 1; (12)Index of Refraction: 1.608; (13)Molar Refractivity: 40.87 cm3; (14)Molar Volume: 118.1 cm3; (15)Polarizability: 16.2×10-24 cm3; (16)Surface Tension: 53.7 dyne/cm; (17)Enthalpy of Vaporization: 56.62 kJ/mol; (18)Vapour Pressure: 0.000649 mmHg at 25°C; (19)Rotatable Bond Count: 1; (20)Exact Mass: 199.947292; (21)MonoIsotopic Mass: 199.947292; (22)Topological Polar Surface Area: 37.3; (23)Heavy Atom Count: 10; (24)Complexity: 136.
Preparation of 2-Bromobenzoic acid: It can be obtained by 1-bromo-2-methyl-benzene. This reaction should react at 350 °C.
Uses of 2-Bromobenzoic acid: It is used in organic synthesis. For example: it can react with 1-(4-amino-phenyl)-ethanone to get N-(4-acetyl-phenyl)-anthranilic acid. This reaction needs reagent potassium carbonate, copper(I) chloride, catalytic agent copper powder and solvent dimethylformamide at temperature of 140-145 °C. The reaction time is 6 hours. The yield is 76%.
When you are using this chemical, please be cautious about it as the following:
It is irritating to eyes, respiratory system and skin, so people should avoid contact with skin and eyes. In case of contact with eyes, rinse immediately with plenty of water and seek medical advice. If you want to contact this product, you must wear suitable protective clothing, gloves and eye/face protection.
People can use the following data to convert to the molecule structure.
1. SMILES:O=C(O)c1ccccc1Br
2. InChI:InChI=1/C7H5BrO2/c8-6-4-2-1-3-5(6)7(9)10/h1-4H,(H,9,10)
3. InChIKey:XRXMNWGCKISMOH-UHFFFAOYAG
The following are the toxicity data which has been tested.
Organism | Test Type | Route | Reported Dose (Normalized Dose) | Effect | Source |
---|---|---|---|---|---|
rat | LD | oral | > 500mg/kg (500mg/kg) | National Academy of Sciences, National Research Council, Chemical-Biological Coordination Center, Review. Vol. 5, Pg. 7, 1953. |
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