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Cas:102-36-3
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Cas:102-36-3
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inquiryhigh quality Appearance:White or off-white Solid Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea Port:shanghai
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inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
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inquiryNow we would like to update our product list for you, kindly check the below information: 1. Catalyst series ( such as Noble Metal Catalyst, Phosphorous ligand, etc ) 2. Pharmaceutical Intermediate ( such as diabtes series, Anti
Product Name 3,4-Dichlorophenyl isocyanate Synonyms 4-Dichlorophenyl isocyanate;2-Dichloro-4-phenyl isocyanate CAS: 102-36-3 MF: C19H22FN3O4 MW:
Cas:102-36-3
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inquiry3,4-Dichlorophenyl isocyanate CAS: 102-36-3 Specification Product Name 3,4-Dichlorophenyl isocyanate Synonyms 4-Dichlorophenyl isocyanate;2-Dichloro-4-phenyl isocyanate CAS: 102-36-3 MF: C19H22FN3O4
Cas:102-36-3
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inquiryMassive Chemical is certified with ISO9001 and ISO14001 manufacturer for this product. We will offer all documents as requirement for the materials which includes, Certificate of Analysis, Material Safety Data Sheet, and Method of Analysis and
Cas:102-36-3
Min.Order:1 Gram
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inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
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3,4-dichlorophenyl isocyanateAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air
ISO/factory/goodqualityAppearance:off white Storage:Dry,cool place Package:drum Application:active pharmaceutical ingredients Transportation:by air/sea/express Port:shenzhen/shanghai
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Cas:102-36-3
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inquiryJinhua huayi chemical co., ltd. is dedicated to the development, production and marketing of chemicals. On the basis of equality and mutual benefit, and under the principle of customer first, credit first, quality first, we are ready to join hands
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Min.Order:100 Gram
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Product Description Description & Specification Category Pharmaceutical Raw Materials, Fine Chemicals, Bulk drug Standard Medical standard
Cas:102-36-3
Min.Order:1 Kilogram
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inquiryAmoychem is committed to providing the top-quality chemical products and services Internationally. We offer our customers with friendly, professional service and reliable, high performance products that have been manufactured according to the accredi
Isocyanic acid 3,4-dichlorophenyl ester/High quality/Best price Application:Isocyanic acid 3,4-dichlorophenyl ester/High quality/Best price
Cas:102-36-3
Min.Order:0
Negotiable
Type:Other
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inquirybis(trichloromethyl) carbonate
m,p-dichloroaniline
3,4-dichlorophenylisocyanate
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 0 - 20℃; | 96% |
In 1,2-dichloro-ethane at 70 - 83℃; | 91.9% |
With triethylamine In benzene for 3h; Heating; |
Conditions | Yield |
---|---|
With bis(trichloromethyl) carbonate at 80℃; for 3.3h; Temperature; | 94% |
With ethyl acetate | |
With sodium hydrogencarbonate In dichloromethane; water; toluene at 0 - 20℃; |
Conditions | Yield |
---|---|
With pyridine; rhodium(III) chloride; bis(acetylacetonate)oxovanadium; 1-methyl-4-nitrobenzene; Azobenzene In chlorobenzene at 175℃; under 60004.8 Torr; for 1h; Product distribution; other reagents; | |
With pyridine; palladium dichloride In chlorobenzene at 160℃; under 76000 Torr; for 1h; Product distribution; other temperature, effects of adding Fe, V, Mo compounds and other additives on the conversion and selectivity of reaction; | |
With N,N-diphenylaminobenzene; palladium dichloride at 200℃; under 76000 Torr; Product distribution; selectivity of reaction, combined carbonylation with 3-chloronitrobenzene and azobenzene, influence of bases, salts; |
Conditions | Yield |
---|---|
at 170 - 220℃; Thermodynamic data; ΔH; heat of dissociation; | |
With hydrogenchloride; potassium chloride at 60.1℃; Kinetics; Further Variations:; Reagents; pH-values; |
3-Methyl-pyrazole-1-carboxylic acid (3,4-dichloro-phenyl)-amide
A
3-Methylpyrazole
B
3,4-dichlorophenylisocyanate
Conditions | Yield |
---|---|
With dibutylamine In tetrachloromethane at 40℃; Rate constant; | |
In 1,4-dioxane at 40℃; Rate constant; var. aprotic solvents; |
Conditions | Yield |
---|---|
With boron trichloride; triethylamine In benzene for 0.5h; Heating; | 97 % Chromat. |
Conditions | Yield |
---|---|
With boron trichloride; triethylamine In benzene for 0.5h; Heating; | 87 % Chromat. |
1-Butyl-3-(3,4-dichlorophenyl)-1-methylurea
A
N-n-butyl-N-methylamine
B
3,4-dichlorophenylisocyanate
Conditions | Yield |
---|---|
With hydrogenchloride; potassium chloride at 60.1℃; Kinetics; Further Variations:; Reagents; |
Conditions | Yield |
---|---|
With sodium azide In toluene for 1h; Heating; | |
Multi-step reaction with 2 steps 1: sodium azide / acetone / 0.5 h / 0 °C 2: toluene / 1 h / 100 °C / Reflux View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: thionyl chloride 2: sodium azide / toluene / 1 h / Heating View Scheme |
Conditions | Yield |
---|---|
In toluene at 100℃; for 1h; Reflux; |
bis(2-trimethylsilyloxylethyl)amine
3,4-dichlorophenylisocyanate
Conditions | Yield |
---|---|
In benzene for 1h; Heating; | 100% |
2-(trimethylsiloxy)-N-(trimethylsilyl)ethylamine
3,4-dichlorophenylisocyanate
Conditions | Yield |
---|---|
In benzene Heating; | 100% |
3,4-dichlorophenylisocyanate
6,7-dimethoxy-4-(1-piperazinyl)quinazoline
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide at 20℃; | 100% |
(3S)-3-aminomethyl-4-(4-[3-(2-methoxybenzyloxy)propoxy]phenyl)-5-oxopiperazine-1-carboxylic acid tert-butyl ester
3,4-dichlorophenylisocyanate
(3S)-3-[3-(3,4-dichlorophenyl)ureidomethyl]-(4-[3-(2-methoxybenzyloxy)propoxy]phenyl)-5-oxopiperazine-1-carboxylic acid tert-butyl ester
Conditions | Yield |
---|---|
In dichloromethane at 20℃; for 18h; | 100% |
3,4-dichlorophenylisocyanate
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In dichloromethane; N,N-dimethyl-formamide for 0.166667h; | 100% |
3,4-dichlorophenylisocyanate
Conditions | Yield |
---|---|
With tetrabutylammonium phthalimide-N-oxyl at 50℃; for 0.00833333h; Neat (no solvent); | 99% |
With potassium phthalimide N-oxide at 70℃; for 0.0666667h; | 97% |
With 1,5,7-triazabicyclo[4.4.0]dec-5-enium acetate at 50℃; for 0.00388889h; | 95% |
ethyl 4,5,6,7-tetrahydroisoxazolo[4,5-c]pyridine-3-carboxylate
3,4-dichlorophenylisocyanate
ethyl 5-(3,4-dichlorophenylcarbamoyl)-4,5,6,7-tetrahydroisoxazolo[4,5-c]pyridine-3-carboxylate
Conditions | Yield |
---|---|
In toluene for 2h; Reflux; | 99% |
Conditions | Yield |
---|---|
In toluene for 15h; Inert atmosphere; Reflux; | 99% |
In 1,4-dioxane for 15h; Reflux; | 69% |
Conditions | Yield |
---|---|
In toluene at 5 - 12℃; Temperature; Inert atmosphere; Green chemistry; | 98.3% |
1,2,3,4-thiatriazole-5-amine
3,4-dichlorophenylisocyanate
1-(3,4-Dichloro-phenyl)-3-[2-(3,4-dichloro-phenyl)-3-oxo-2,3-dihydro-[1,2,4]thiadiazol-5-yl]-urea
Conditions | Yield |
---|---|
In pyridine at 10 - 15℃; for 24h; | 98% |
3,4-dichlorophenylisocyanate
Conditions | Yield |
---|---|
Stage #1: 3,4-dichlorophenylisocyanate; (R)-2-(4-Methoxy-benzylamino)-propionic acid 4,4,5,5,6,6,7,7,8,8,9,9,10,10,11,11,11-heptadecafluoro-undecyl ester With triethylamine In dichloromethane at 25℃; for 2h; Stage #2: With Amberlite G-50 ion-exchange resin; fluorous reverse-phase silica In dichloromethane | 98% |
3,4-dichlorophenylisocyanate
methyl N-[5(6)-(4-aminophenylsulfanyl)benzimidazol-2-yl]carbamate
(5-{4-[3-(3,4-dichloro-phenyl)-ureido]-phenylsulfanyl}-1H-benzoimidazol-2-yl)-carbamic acid methyl ester
Conditions | Yield |
---|---|
In dimethyl sulfoxide at 20℃; | 98% |
3,4-dichlorophenylisocyanate
(2E)-4-{[(tert-butyl)diphenylsilyl]oxy}-3-methylbut-2-en-1-ol
(2E)-4-(tert-butyl(diphenyl)silyloxy)-3-methylbut-2-en-1-yl (3,4-dichlorophenyl)carbamate
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 20℃; | 98% |
3-aminoindazole
3,4-dichlorophenylisocyanate
N-(3,4-dichlorophenyl)-3-(([(3,4-dichlorophenyl)amino]carbonyl)amino)-1H-indazole-1-carboxamide
Conditions | Yield |
---|---|
In tetrahydrofuran at 20℃; Reflux; | 98% |
(4-Thiazolidin-2-yl-phenyl)-carbamic acid ethyl ester
3,4-dichlorophenylisocyanate
{4-[3-(3,4-Dichloro-phenylcarbamoyl)-thiazolidin-2-yl]-phenyl}-carbamic acid ethyl ester
Conditions | Yield |
---|---|
In benzene for 1h; Heating; | 97.5% |
3,4-dichlorophenylisocyanate
methyl N-[5(6)-(4-aminophenylsulfanyl)benzimidazol-2-yl]carbamate
Conditions | Yield |
---|---|
In dimethyl sulfoxide at 70 - 80℃; for 3h; | 97.1% |
methyl 3-(2-amino-6-nitroquinazolin-4ylamino)propanoate
3,4-dichlorophenylisocyanate
methyl 3-(2-(3-(3,4-dichlorophenyl)ureido)-6-nitroquinazolin-4-ylamino)propanoate
Conditions | Yield |
---|---|
In 1,4-dioxane at 120℃; for 0.0833333h; Microwave irradiation; | 97% |
tert-butyl 3-((pyridin-3-yloxy)methyl)piperazine-1-carboxylate
3,4-dichlorophenylisocyanate
C22H26Cl2N4O4
Conditions | Yield |
---|---|
In dichloromethane for 1h; | 97% |
2-methyl-2-methylaminopropionaldoxime
3,4-dichlorophenylisocyanate
1-(3,4-Dichloro-phenyl)-5-hydroxyamino-3,4,4-trimethyl-imidazolidin-2-one
Conditions | Yield |
---|---|
With sodium hydroxide In water Heating; | 96% |
3,4-dichlorophenylisocyanate
5-hydroxy-3-methylpyrazole
5-Hydroxy-3-methyl-pyrazole-1-carboxylic acid (3,4-dichloro-phenyl)-amide
Conditions | Yield |
---|---|
In chloroform for 15h; Ambient temperature; | 96% |
Conditions | Yield |
---|---|
for 0.0333333h; microwave irradiation; | 96% |
at 20℃; for 0.5h; | 96% |
Conditions | Yield |
---|---|
Stage #1: pyridine; 3,4-dichlorophenylisocyanate In dichloromethane Stage #2: dimethyl acetylenedicarboxylate In dichloromethane at -5℃; for 0.166667h; Stage #3: In dichloromethane at 20℃; for 2h; Further stages.; | 96% |
Conditions | Yield |
---|---|
With 1,4-diaza-bicyclo[2.2.2]octane In tetrahydrofuran at 20℃; | 96% |
3,4-dichlorophenylisocyanate
5-amino-3-benzylthio-4-ethoxycarbonyl-1H-pyrazol
5-Amino-3-benzylsulfanyl-1-(3,4-dichloro-phenylcarbamoyl)-1H-pyrazole-4-carboxylic acid ethyl ester
Conditions | Yield |
---|---|
In tetrahydrofuran Ambient temperature; | 95.1% |
(hydroxy-phenyl-methyl)-phosphonic acid diisopropyl ester
3,4-dichlorophenylisocyanate
Conditions | Yield |
---|---|
With triethylamine In benzene at 50 - 60℃; | 95% |
(Z)-trimethylsilyl N-trimethylsilylacetimidate
3,4-dichlorophenylisocyanate
1,3-Bis(3,4-dichlorphenyl)-6-methyl-5-trimethylsilyl-6-trimethylsilyloxy-1,3,5-triazinan-2,4-dion
Conditions | Yield |
---|---|
In cyclohexane for 16h; Ambient temperature; | 95% |
1,5,5-trimethyl-3-phenyl-4-hydroxylaminoimidazolidin-2-one
3,4-dichlorophenylisocyanate
C19H20Cl2N4O3
Conditions | Yield |
---|---|
In acetone | 95% |
2-Amino-9,10-dimethoxy-1,3,4,6,7,11b-hexahydrobenzoquinolizine-2-carbonitrile
3,4-dichlorophenylisocyanate
(+/-)-2R*,11bS*-N-(2-Cyano-9,10-dimethoxy-1,3,4,6,7,11b-hexahydrobenzoquinolizin-2-yl)-N'-(3",4"-dichlorophenyl)urea
Conditions | Yield |
---|---|
In benzene for 2h; Ambient temperature; | 95% |
2-Amino-9,10-dimethoxy-1,3,4,6,7,11b-hexahydrobenzoquinolizine-2-carbonitrile
3,4-dichlorophenylisocyanate
(+/-)-2R*,11bS*-3'-(3",4"-Dichlorophenyl)-4'-imino-9,10-dimethoxy-1,3,4,6,7,11b-hexahydrospiroquinolizin-2,5'-imidazolidin>-2'-one
Conditions | Yield |
---|---|
With triethylamine In benzene for 3h; Ambient temperature; sonication; | 95% |
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