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Cas:10238-21-8
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inquiryItems Standard Result Assay (Ursolic acid) 98%min 98.22% ----------------------------------------------------------------
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inquiryDescription Glibenclamide CAS No: 10238-21-8 MF: C23H28ClN3O5 Appreance:White crystalline powder Introduction Glyburide (Glibenclamide) i
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inquiryUnique advantages for Glibenclamide Cas 10238-21-8 Guaranteed purity High quality & competitive price Quality control Fast feedback Prompt shipment Appearance:White crystalline powder Storage:N/A Package:1kg/foil bag;25kg/drum Applic
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inquiryXi’an Quanao Biotech Co., Ltd. with 18 years experience in plant extract filed. Product grade: Medicine, Health care product, Cosmetics, Food, Beverage, Feed. Hot selling market: Europe, North America, South America, Middle East, Asia Pacifi
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inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
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inquiryOur main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
Name:Glibenclamide CAS NO: 10238-21-8 Grade:Medical scientific research and export Molecular formula:C23H28ClN3O5S Molecular weight:494.01 Product Quality 12 years of chemical raw materials Mature operation of the industry System stability
Cas:10238-21-8
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inquiryOur Advantage Rich Experience Our products are sold all over Europe,North&South America, Sino-East, Asia and pacific area as well as Africa,we establish long term. Quality service Company cooperates with research institutes. We strictly con
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inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by email in time prod
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inquiryProduct Name: Glibenclamide MF: C23H28ClN3O5S MW: 494.00 CAS NO. 10238-21-8 Appearance: White crystalline powder Appearance:Wh
Appearance:Off-white powder Storage:R.T Package:25kg/drum Application:Oral sulfonylurea hypoglycemic drug Transportation:Express/Sea/Air Port:Any port in China
Cas:10238-21-8
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inquiry1. Guaranteed purity; 2. Large quantity in stock; 3. Largest manufacturer; 4. Best service after shipment with email; 5. High quality & competitive price; Appearance:white crystalline powder Storage:Store in sealed containers
Cas:10238-21-8
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Cas:10238-21-8
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Cas:10238-21-8
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Min.Order:100 Gram
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inquiryAppearance:white powder Storage:Store in a cool,dry place and keep away from direct strong light Package:packaged in foil bags or tins Application:Use only for laboratory research Transportation:Sea,Air,DHL/TNT/FEdex/UPS/EMS Por
Cas:10238-21-8
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inquiryOur Services 1. New Molecules R&D 2. Own test center HPLC NMR GC LC-MS 3. API and Intermediates from China reputed manufacturers 4. Documents support COA MOA MSDS DMF open part Our advantages 1. Government awarded company. Top 100 enter
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inquiry5-chloro-2-methoxy-N-(4-sulfamoylphenethyl)benzamide
Cyclohexyl isocyanate
Glibenclamid
Conditions | Yield |
---|---|
With copper(l) chloride In nitromethane at 20℃; for 2h; Reagent/catalyst; Solvent; Concentration; Milling; | 100 %Spectr. |
With potassium carbonate In N,N-dimethyl-formamide at 80℃; for 0.166667h; Sealed tube; | 81 mg |
With 18-crown-6 ether; potassium tert-butylate In N,N-dimethyl-formamide at 0 - 5℃; for 6h; Reflux; | 4.49 g |
Conditions | Yield |
---|---|
With palladium diacetate In acetonitrile at 20℃; under 15 Torr; Schlenk technique; Sealed tube; | 99% |
Glibenclamid
Conditions | Yield |
---|---|
In toluene at 110℃; Industrial scale; |
5-chloro-2-methoxybenzoic acid
Glibenclamid
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: oxalyl dichloride / dichloromethane / 12 h / 20 °C / Schlenk technique 2: triethylamine / dichloromethane / 6 h / 20 °C / Schlenk technique 3: palladium diacetate / acetonitrile / 20 °C / 15 Torr / Schlenk technique; Sealed tube View Scheme | |
Multi-step reaction with 5 steps 1: oxalyl dichloride / dichloromethane / 12 h / 20 °C / Schlenk technique 2: triethylamine / dichloromethane / 6 h / 20 °C / Schlenk technique 3: chlorosulfonic acid / 1,2-dichloro-ethane / 50 °C / Schlenk technique 4: sodium azide / acetonitrile / 50 °C / Schlenk technique 5: palladium diacetate / acetonitrile / 20 °C / 15 Torr / Schlenk technique; Sealed tube View Scheme | |
Multi-step reaction with 4 steps 1: phosphorus trichloride / tetrahydrofuran / 0.08 h / 150 °C / Sealed tube 2: chlorosulfonic acid / chloroform / 0.17 h / 60 °C / Sealed tube 3: ammonium hydroxide / 1,4-dioxane / 0.17 h / 120 °C / Sealed tube; Cooling with ice 4: potassium carbonate / N,N-dimethyl-formamide / 0.17 h / 80 °C / Sealed tube View Scheme |
DK13
Glibenclamid
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: chlorosulfonic acid / 1,2-dichloro-ethane / 50 °C / Schlenk technique 2: sodium azide / acetonitrile / 50 °C / Schlenk technique 3: palladium diacetate / acetonitrile / 20 °C / 15 Torr / Schlenk technique; Sealed tube View Scheme | |
Multi-step reaction with 3 steps 1: chlorosulfonic acid / chloroform / 0.17 h / 60 °C / Sealed tube 2: ammonium hydroxide / 1,4-dioxane / 0.17 h / 120 °C / Sealed tube; Cooling with ice 3: potassium carbonate / N,N-dimethyl-formamide / 0.17 h / 80 °C / Sealed tube View Scheme |
phenethylamine
Glibenclamid
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: phosphorus trichloride / tetrahydrofuran / 0.08 h / 150 °C / Sealed tube 2: chlorosulfonic acid / chloroform / 0.17 h / 60 °C / Sealed tube 3: ammonium hydroxide / 1,4-dioxane / 0.17 h / 120 °C / Sealed tube; Cooling with ice 4: potassium carbonate / N,N-dimethyl-formamide / 0.17 h / 80 °C / Sealed tube View Scheme | |
Multi-step reaction with 5 steps 1.1: pyridine / tetrahydrofuran / 4 h / 20 °C / Cooling with ice 2.1: chlorosulfonic acid / 2 h / 20 °C / Cooling with ice 3.1: ammonium hydroxide / acetone / 20 °C 4.1: 1,1'-carbonyldiimidazole / tetrahydrofuran / 4 h / 20 °C / Inert atmosphere 4.2: 16 h / 20 °C 5.1: potassium tert-butylate; 18-crown-6 ether / N,N-dimethyl-formamide / 6 h / 0 - 5 °C / Reflux View Scheme |
2-methoxy-5-chlorobenzoyl chloride
Glibenclamid
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: triethylamine / dichloromethane / 6 h / 20 °C / Schlenk technique 2: palladium diacetate / acetonitrile / 20 °C / 15 Torr / Schlenk technique; Sealed tube View Scheme | |
Multi-step reaction with 4 steps 1: triethylamine / dichloromethane / 6 h / 20 °C / Schlenk technique 2: chlorosulfonic acid / 1,2-dichloro-ethane / 50 °C / Schlenk technique 3: sodium azide / acetonitrile / 50 °C / Schlenk technique 4: palladium diacetate / acetonitrile / 20 °C / 15 Torr / Schlenk technique; Sealed tube View Scheme |
4-(2-[(5-chloro-2-methoxyphenyl)formamido]ethyl)benzene-1-sulfonyl chloride
Glibenclamid
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: sodium azide / acetonitrile / 50 °C / Schlenk technique 2: palladium diacetate / acetonitrile / 20 °C / 15 Torr / Schlenk technique; Sealed tube View Scheme |
5-chloro-2-methoxy-N-(4-sulfamoylphenethyl)benzamide
Glibenclamid
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: ammonium hydroxide / acetone / Industrial scale 2.1: pyrographite / acetone / 1.17 h / Reflux; Industrial scale 2.2: 0.5 h / 58 °C / Industrial scale 3.1: toluene / 110 °C / Industrial scale View Scheme |
2,2,2-trifluoro-N-(2-phenylethyl)acetamide
Glibenclamid
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1.1: chlorosulfonic acid / 2 h / 20 °C / Cooling with ice 2.1: ammonium hydroxide / acetone / 20 °C 3.1: 1,1'-carbonyldiimidazole / tetrahydrofuran / 4 h / 20 °C / Inert atmosphere 3.2: 16 h / 20 °C 4.1: potassium tert-butylate; 18-crown-6 ether / N,N-dimethyl-formamide / 6 h / 0 - 5 °C / Reflux View Scheme |
4-[2-(2,2,2-trifluoroacetamido)ethyl]benzenesulfonyl chloride
Glibenclamid
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: ammonium hydroxide / acetone / 20 °C 2.1: 1,1'-carbonyldiimidazole / tetrahydrofuran / 4 h / 20 °C / Inert atmosphere 2.2: 16 h / 20 °C 3.1: potassium tert-butylate; 18-crown-6 ether / N,N-dimethyl-formamide / 6 h / 0 - 5 °C / Reflux View Scheme |
Conditions | Yield |
---|---|
at 25℃; pH=7; aq. phosphate buffer; |
Glibenclamid
tetra(n-butyl)ammonium hydroxide
Conditions | Yield |
---|---|
In methanol | 100% |
Glibenclamid
Conditions | Yield |
---|---|
With [(1,5-cyclooctadiene)Ir(1,3-bis(2,4,6-trimethylphenyl)imidazol-2-ylidene)(PPh3)]PF6; deuterium In dichloromethane at 20℃; for 2h; Sealed tube; | 100% |
With deuterium at 100℃; Sealed tube; |
Glibenclamid
Conditions | Yield |
---|---|
With Kerr's catalyst; deuterium In chlorobenzene at 120℃; for 1h; Reagent/catalyst; Temperature; | 90% |
Glibenclamid
acetic anhydride
Conditions | Yield |
---|---|
With pyridine for 0.25h; | 84% |
diethylenetriaminepentaacetic dianhydride
Glibenclamid
DTPA-glyburide
Conditions | Yield |
---|---|
Stage #1: Glibenclamid With sodium amide In dimethyl sulfoxide at 20℃; for 0.166667h; Stage #2: diethylenetriaminepentaacetic dianhydride With sodium amide In dimethyl sulfoxide for 22h; | 80% |
Conditions | Yield |
---|---|
With C17H24N5Ru(1+)*F6P(1-); Potassium benzoate; potassium carbonate In 1-methyl-pyrrolidin-2-one at 50℃; for 72h; Inert atmosphere; | 78% |
With C17H24N5Ru(1+)*F6P(1-); Potassium benzoate; potassium carbonate In 1-methyl-pyrrolidin-2-one at 50℃; for 72h; Inert atmosphere; Glovebox; | 78% |
Conditions | Yield |
---|---|
In ethanol; water addn. of hot soln. (60°C) of CuCl2*2H2O in EtOH-H2O mixt. (1:1) to hot soln. (60°C) of MeOC6H3(Cl)CONHCH2CH2C6H4SO2NHCONHC6H11 in the same solvent; stirring under reflux for 1 h; pptn., filtration, washing several times with 1:1 EtOH:H2O mixt. and then with Et2O; elem. anal.; | 76% |
Conditions | Yield |
---|---|
Reflux; | 76% |
Conditions | Yield |
---|---|
In ethanol; water addn. of hot soln. (60°C) of NiCl2*6H2O in EtOH-H2O mixt. (1:1) to hot soln. (60°C) of MeOC6H3(Cl)CONHCH2CH2C6H4SO2NHCONHC6H11 in the same solvent; stirring under reflux for 1 h; pptn., filtration, washing several times with 1:1 EtOH:H2O mixt. and then with Et2O; elem. anal.; | 74% |
Conditions | Yield |
---|---|
In ethanol; water addn. of hot soln. (60°C) of MnCl2 in EtOH-H2O mixt. (1:1) to hotsoln. (60°C) of MeOC6H3(Cl)CONHCH2CH2C6H4SO2NHCONHC6H11 in the s ame solvent; stirring under reflux for 1 h; pptn., filtration, washing several times with 1:1 EtOH:H2O mixt. and then with Et2O; elem. anal.; | 73% |
Conditions | Yield |
---|---|
With potassium phosphate monohydrate; palladium diacetate; N2Phos In water at 60℃; for 24h; Reagent/catalyst; Suzuki-Miyaura Coupling; | 73% |
Conditions | Yield |
---|---|
In ethanol; water addn. of hot soln. (60°C) of CrCl3*6H2O in EtOH-H2O mixt. (1:1) to hot soln. (60°C) of MeOC6H3(Cl)CONHCH2CH2C6H4SO2NHCONHC6H11 in the same solvent; stirring under reflux for 1 h; pptn., filtration, washing several times with 1:1 EtOH:H2O mixt. and with Et2O; elem. anal.; | 70% |
Conditions | Yield |
---|---|
In ethanol; water addn. of hot soln. (60°C) of FeCl3*6H2O in EtOH-H2O mixt. (1:1) to hot soln. (60°C) of MeOC6H3(Cl)CONHCH2CH2C6H4SO2NHCONHC6H11 in the same solvent; stirring under reflux for 1 h; pptn., filtration, washing several times with 1:1 EtOH:H2O mixt. and then with Et2O; elem. anal.; | 68% |
Conditions | Yield |
---|---|
In ethanol; water addn. of hot soln. (60°C) of ZnCl2 in EtOH-H2O mixt. (1:1) to hotsoln. (60°C) of MeOC6H3(Cl)CONHCH2CH2C6H4SO2NHCONHC6H11 in the s ame solvent; stirring under reflux for 1 h; pptn., filtration, washing several times with 1:1 EtOH:H2O mixt. and then with Et2O; elem. anal.; | 65% |
Conditions | Yield |
---|---|
In ethanol; water addn. of hot soln. (60°C) of CoCl2 in EtOH-H2O mixt. (1:1) to hotsoln. (60°C) of MeOC6H3(Cl)CONHCH2CH2C6H4SO2NHCONHC6H11 in the s ame solvent; stirring under reflux for 1 h; pptn., filtration, washing several times with 1:1 EtOH:H2O mixt. and then with Et2O; elem. anal.; | 65% |
Conditions | Yield |
---|---|
With 2,6-di(t-butyl)-4-phenylphenol; caesium carbonate In dimethyl sulfoxide at 20℃; for 20h; Irradiation; Inert atmosphere; | 61% |
Glibenclamid
N-[2-(4-[N-(cyclohexylcarbamoyl)-sulfamoyl]-phenyl)-ethyl]-5-hydroxy-2-methoxybenzamide
Conditions | Yield |
---|---|
With sodium hydroxide In ethanol at 20℃; for 24h; | 60% |
Conditions | Yield |
---|---|
With O4P(3-)*3K(1+)*5H2O; tris(1-adamantyl)phosphine; C28H26N2O8Pd2S2 In tetrahydrofuran at 100℃; for 5h; Suzuki-Miyaura Coupling; Inert atmosphere; Schlenk technique; | 37% |
With 1,2,3-trimethoxybenzene; O4P(3-)*3K(1+)*5H2O; tris(1-adamantyl)phosphine; {2-[((acetyl-κO)amino)phenyl-κC](tri-1-adamantylphosphine)palladium}(p-toluenesulfonate) In tetrahydrofuran at 100℃; for 5h; Suzuki-Miyaura Coupling; Inert atmosphere; | 37% |
phthalic anhydride
Glibenclamid
A
N-cyclohexylphthalimide
B
5-chloro-2-methoxy-N-(4-sulfamoylphenethyl)benzamide
Conditions | Yield |
---|---|
With pyridine; dmap for 4h; Heating; | A 34% B 29% |
Glibenclamid
A
N-cyclohexylphthalimide
B
5-chloro-2-methoxy-N-(4-sulfamoylphenethyl)benzamide
Conditions | Yield |
---|---|
With pyridine; dmap; phthalic anhydride for 4h; Heating; | A 34% B 29% |
Glibenclamid
Conditions | Yield |
---|---|
Stage #1: Glibenclamid With sulfuric acid; nitric acid In 1,4-dioxane at 0 - 20℃; for 1.5h; Cooling with ice; Stage #2: Sonication; | 11% |
With sulfuric acid; nitric acid In 1,4-dioxane at 0 - 20℃; for 1.5h; | 11% |
Glibenclamid
Conditions | Yield |
---|---|
With tritium; [Ir(1,5-COD)(P(C6H5)3)2]BF4 In dichloromethane for 16h; Ambient temperature; |
Glibenclamid
N-{4-[β-(2-hydroxy-5-chlorobenzene carboxamido)ethyl]benzene-sulfonyl}-N'-cyclohexylurea
Conditions | Yield |
---|---|
With boron tribromide |
Glibenclamid
2-amino-2-hydroxymethyl-1,3-propanediol
C4H11NO3*C23H28ClN3O5S
Conditions | Yield |
---|---|
In methanol at 5℃; |
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