Hebei yanxi chemical co., LTD is a professional research, development and production 2-phenylacetamide enterprise backbone members by local well-known entrepreneurs and professional senior engineers in the party's "low carbon environ
Cas:1024598-06-8
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inquiryThe company has a professional R & D team, mature technology, very competitive prices and stable high quality products for customers to order high quality and low price product efforts! Appearance:White or off-white Solid Storage:Sealed, dr
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inquiry1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s
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inquiryDayangchem’s R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. Near 20 years DayangChem has provided dif
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inquiryProduct Description Product website: http://www.finerchem.com/pro01en/id/299.html Product Name 11,12-Dihydro-11-phenylindolo[2,3-a]carbazole CAS
Cas:1024598-06-8
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inquiryAbout Product Details CAS: 1
Cas:1024598-06-8
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inquiryWith our good experience, we offer detailed technical support and advice to assist customers. We communicate closely with customers to establish their quality requirements. Consistent Quality Our plant has strict quality control in each manufacturin
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inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
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inquiryOur Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We
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inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by email in time prod
Cas:1024598-06-8
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inquiryProduct Name 11,12-Dihydro-11-phenylindolo[2,3-a]carbazole Structural formula CAS No. 1024598-06-8 appearance:off-white solid assay:98% Appearance:White powder Storage:Store in cool and dry place,
Cas:1024598-06-8
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inquiry11,12-Dihydro-11-phenylindolo[2,3-a]carbazole CAS:1024598-06-8 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing i
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Min.Order:1 Gram
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inquiry1.high quality: quality is life. quality is the most important element for all goods. we have a lab doing research in wuhan china. hplc and nmr is available if needed. 2.reasonable price: we provide high quality products wi
Cas:1024598-06-8
Min.Order:10 Gram
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inquiry1,we produce and sell good chemicals around the world. 2,our success rate is about 95%. this means, if customer order is accepted, the probability that the customer will obtain the ordered substances, is 95%. 3,our staff consists
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inquiryA substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc
Cas:1024598-06-8
Min.Order:4 Kilogram
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inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
Cas:1024598-06-8
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inquirySupply lowest price 1024598-06-8 High quality 11,12-Dihydro-11-phenylindolo[2,3-a]carbazole Molecular Formula C24H16N2 Molar Mass 332.4 Density 1.26 Boling Point 598.8±32.0 °C(Predicted)
Cas:1024598-06-8
Min.Order:1 Gram
Negotiable
Type:Other
inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:1024598-06-8
Min.Order:10 Gram
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inquiryWe are one of a few suppliers that can offer custom synthesis service of this product We are specialized in custom synthesis, chemical/pharmaceutical/ pesticides outsourcing and contract research. We are committed to prov
Cas:1024598-06-8
Min.Order:100 Gram
FOB Price: $100.0 / 2000.0
Type:Lab/Research institutions
inquiryProduct name: 11-Phenyl-11,12-Dihydroindolo[2,3-a]Carbazole CAS No.:1024598-06-8 Molecule Formula:C24H16N2 Molecule Weight:332.40 Purity: 97.0% Package: 25kg/drum Description:White to off-white solid Manufacture Standards:Enterprise Standard
Cas:1024598-06-8
Min.Order:1 Kilogram
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inquiryWe are leading fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so on.Our main business covers the fields below: 1.Noble Metal Catalysts (Pt.Pd...)
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inquiryWe're in good position to supply OLED intermediates . In the past 25 years, we have won technical support from several well-known universities and institutes. We have developed many chemicals together. It makes us capable of developing Cust
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inquiryGMP standard, high purity, competitive price, in stock 1. Quick Response: within 6 hours after receiving your email. 2. Quality Guarantee: All products are strictly tested by our QC, confirmed by QA, and approved by a third-party lab in China, USA,
Cas:1024598-06-8
Min.Order:1 Milligram
Negotiable
Type:Trading Company
inquiryProduct Name: 11,12-Dihydro-11-phenylindolo[2,3-a]carbazole Synonyms: 11,12-Dihydro-11-phenylindolo[2,3-a]carbazole;11-phenyl-11,12-dihydroindolo[2,3-a]carbazole;Indolo[2,3-a]carbazole, 11,12-dihydro-11-phenyl-;11-phenylindolo[2,3-a]carbazole;1
Cas:1024598-06-8
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryfactory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B
Cas:1024598-06-8
Min.Order:1 Kilogram
FOB Price: $18.0 / 20.0
Type:Trading Company
inquiryZhenyu biotech exported this product to many countries and regions at best price. if you are looking for the material's manufacturer or supplier in china, zhenyu biotech is your best choice. pls contact with us freely for getting detailed
Cas:1024598-06-8
Min.Order:1 Kilogram
FOB Price: $2.0
Type:Lab/Research institutions
inquiryShandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W
Cas:1024598-06-8
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryOur company advantages: 1 The highest quality with the competitive price. 2、 Professional human services. 3、 The fastest and safest delivery service. 4、Our old customers all around the world. 5、 The high purity products. 6、We have a suf
Cas:1024598-06-8
Min.Order:10 Gram
Negotiable
Type:Trading Company
inquiry1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer
Cas:1024598-06-8
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inquiryProduct Name 11-Phenyl-11,12-dihydroindolo[2,3-a]carbazole CAS No. 1024598-06-8 Appearance White powder Puri
Cas:1024598-06-8
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquirybromobenzene
11,12-dihydroindolo[2,3-a]carbazole
11,12-dihydro-11-phenylindolo[2,3-a]carbazole
Conditions | Yield |
---|---|
With tris-(dibenzylideneacetone)dipalladium(0); tri-tert-butyl phosphine; sodium t-butanolate In o-xylene at 160℃; for 48h; | 83% |
With tris-(dibenzylideneacetone)dipalladium(0); tri-tert-butyl phosphine; sodium t-butanolate In 5,5-dimethyl-1,3-cyclohexadiene; toluene for 24h; Inert atmosphere; Reflux; | 75% |
With bis(tri-t-butylphosphine)palladium(0); sodium t-butanolate In 5,5-dimethyl-1,3-cyclohexadiene for 17h; Inert atmosphere; | 73% |
9-phenyl-9H-carbazol-1-amine
(2-bromophenyl)boronic acid
11,12-dihydro-11-phenylindolo[2,3-a]carbazole
Conditions | Yield |
---|---|
Stage #1: 9-phenyl-9H-carbazol-1-amine With hydrogen bromide; dihydrogen peroxide In water; acetonitrile at -20℃; Stage #2: (2-bromophenyl)boronic acid With palladium diacetate; caesium carbonate; (RP,RP)-1,2-bis[(o-anisyl)(phenyl)phosphino]ethane In 1-methyl-pyrrolidin-2-one at 20℃; Inert atmosphere; Reflux; | 78.4% |
2-(2-nitrophenyl)-9-phenyl-9H-carbazole
11,12-dihydro-11-phenylindolo[2,3-a]carbazole
Conditions | Yield |
---|---|
With triphenylphosphine In 1,2-dichloro-benzene at 180℃; for 12h; Inert atmosphere; | 71.5% |
With triphenylphosphine In 1,2-dichloro-benzene at 180℃; for 24h; Inert atmosphere; | 55% |
iodobenzene
11,12-dihydroindolo[2,3-a]carbazole
11,12-dihydro-11-phenylindolo[2,3-a]carbazole
Conditions | Yield |
---|---|
With tris-(dibenzylideneacetone)dipalladium(0); tri-tert-butyl phosphine; sodium t-butanolate In toluene for 3h; Inert atmosphere; Reflux; | 65% |
With 18-crown-6 ether; copper; potassium carbonate In 1,2-dichloro-benzene for 12h; Reflux; Inert atmosphere; | 64% |
With 18-crown-6 ether; copper In 1,2-dichloro-benzene for 12h; Reflux; Inert atmosphere; | 64% |
bromobenzene
tri-tert-butyl phosphine
11,12-dihydroindolo[2,3-a]carbazole
11,12-dihydro-11-phenylindolo[2,3-a]carbazole
Conditions | Yield |
---|---|
With tris-(dibenzylideneacetone)dipalladium(0) In water; toluene | 55% |
iodobenzene
indolo[2,3-a]carbazole
11,12-dihydro-11-phenylindolo[2,3-a]carbazole
Conditions | Yield |
---|---|
With potassium phosphate; copper(l) iodide; trans-1,2-cyclohexanediamine In 1,4-dioxane for 24h; Inert atmosphere; Reflux; | 51% |
phenylhydrazine hydrochloride
11,12-dihydro-11-phenylindolo[2,3-a]carbazole
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: sulfuric acid / ethanol / 4.08 h / 20 - 65 °C / Inert atmosphere 1.2: 15 h / 100 °C 2.1: potassium carbonate; copper(l) iodide; quinoline / 72 h / 190 °C / Inert atmosphere View Scheme | |
Multi-step reaction with 2 steps 1.1: sulfuric acid / ethanol / 4 h / 60 °C / Inert atmosphere 1.2: 12 h / 100 °C 2.1: copper; 18-crown-6 ether / 1,2-dichloro-benzene / 12 h / Reflux; Inert atmosphere View Scheme | |
Multi-step reaction with 2 steps 1.1: sulfuric acid / ethanol / 4 h / 60 °C 1.2: 100 °C 2.1: copper; potassium carbonate; 18-crown-6 ether / 1,2-dichloro-benzene / Reflux View Scheme | |
Multi-step reaction with 2 steps 1.1: sulfuric acid / ethanol / 4 h / 60 °C / Inert atmosphere 1.2: 12 h / 100 °C 2.1: potassium carbonate; copper; 18-crown-6 ether / 1,2-dichloro-benzene / 12 h / Reflux; Inert atmosphere View Scheme | |
Multi-step reaction with 2 steps 1.1: ethanol / 0.5 h 1.2: 10 h / 65 °C 2.1: copper; 18-crown-6 ether; potassium carbonate / 1,2-dichloro-benzene / 48 h / 180 °C View Scheme |
cyclohexane-1,2-dione
11,12-dihydro-11-phenylindolo[2,3-a]carbazole
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: sulfuric acid / ethanol / 4.08 h / 20 - 65 °C / Inert atmosphere 1.2: 15 h / 100 °C 2.1: potassium carbonate; copper(l) iodide; quinoline / 72 h / 190 °C / Inert atmosphere View Scheme |
11,12-dihydro-11-phenylindolo[2,3-a]carbazole
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: sulfuric acid / ethanol / 4 h / 60 °C / Inert atmosphere 1.2: 12 h / 100 °C / Inert atmosphere 2.1: potassium carbonate; copper; 18-crown-6 ether / 1,2-dichloro-benzene / 12 h / Reflux; Inert atmosphere View Scheme |
(9‐phenyl‐9H‐carbazol‐2‐yl)boronic acid
11,12-dihydro-11-phenylindolo[2,3-a]carbazole
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: tetrakis(triphenylphosphine) palladium(0); potassium carbonate / toluene; water; ethanol / 24 h / 120 °C / Inert atmosphere 2: triphenylphosphine / 1,2-dichloro-benzene / 12 h / 180 °C / Inert atmosphere View Scheme | |
Multi-step reaction with 2 steps 1: potassium carbonate; tetrakis(triphenylphosphine) palladium(0) / toluene; ethanol; water / 12 h / 100 °C / Inert atmosphere 2: triphenylphosphine / 1,2-dichloro-benzene / 24 h / 180 °C / Inert atmosphere View Scheme | |
Multi-step reaction with 2 steps 1: potassium carbonate; tetrakis(triphenylphosphine) palladium(0) / toluene; ethanol; water / 12 h / 100 °C / Inert atmosphere 2: triphenylphosphine / 1,2-dichloro-benzene / 24 h / 180 °C / Inert atmosphere View Scheme |
2-nitrophenyl bromide
11,12-dihydro-11-phenylindolo[2,3-a]carbazole
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: tetrakis(triphenylphosphine) palladium(0); potassium carbonate / toluene; water; ethanol / 24 h / 120 °C / Inert atmosphere 2: triphenylphosphine / 1,2-dichloro-benzene / 12 h / 180 °C / Inert atmosphere View Scheme | |
Multi-step reaction with 2 steps 1: potassium carbonate; tetrakis(triphenylphosphine) palladium(0) / toluene; ethanol; water / 12 h / 100 °C / Inert atmosphere 2: triphenylphosphine / 1,2-dichloro-benzene / 24 h / 180 °C / Inert atmosphere View Scheme | |
Multi-step reaction with 2 steps 1: potassium carbonate; tetrakis(triphenylphosphine) palladium(0) / toluene; ethanol; water / 12 h / 100 °C / Inert atmosphere 2: triphenylphosphine / 1,2-dichloro-benzene / 24 h / 180 °C / Inert atmosphere View Scheme | |
Multi-step reaction with 3 steps 1: tetrakis(triphenylphosphine) palladium(0); calcium carbonate / 1,4-dioxane / 12 h / Reflux 2: triphenylphosphine / 1,2-dichloro-benzene / 8 h / 180 °C / Inert atmosphere 3: caesium carbonate; palladium diacetate; tri-tert-butyl phosphine / toluene / 20 °C / Inert atmosphere; Reflux View Scheme |
2-(2-nitrophenyl)-9-phenyl-9H-carbazole
A
11,12-dihydro-11-phenylindolo[2,3-a]carbazole
B
5-phenyl-5,11-dihydro-indolo[3,2-b]carbazole
Conditions | Yield |
---|---|
With triphenylphosphine In 1,2-dichloro-benzene at 180℃; for 24h; Inert atmosphere; Overall yield = 63 %; |
benzene-1,4-diboronic acid bispinacol ester
11,12-dihydro-11-phenylindolo[2,3-a]carbazole
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: tetrakis(triphenylphosphine) palladium(0); calcium carbonate / 1,4-dioxane / 12 h / Reflux 2: triphenylphosphine / 1,2-dichloro-benzene / 8 h / 180 °C / Inert atmosphere 3: caesium carbonate; palladium diacetate; tri-tert-butyl phosphine / toluene / 20 °C / Inert atmosphere; Reflux View Scheme |
2,2''-dinitro-p-terphenyl
11,12-dihydro-11-phenylindolo[2,3-a]carbazole
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: triphenylphosphine / 1,2-dichloro-benzene / 8 h / 180 °C / Inert atmosphere 2: caesium carbonate; palladium diacetate; tri-tert-butyl phosphine / toluene / 20 °C / Inert atmosphere; Reflux View Scheme |
11,12-dihydro-11-phenylindolo[2,3-a]carbazole
Conditions | Yield |
---|---|
With sodium hydride In N,N-dimethyl-formamide; mineral oil for 6h; Inert atmosphere; | 90% |
With sodium hydride In N,N-dimethyl-formamide at 20℃; for 12h; | 81% |
11,12-dihydro-11-phenylindolo[2,3-a]carbazole
2-chloro-4-(4-chlorophenyl)-6-phenyl-1,3,5-triazine
Conditions | Yield |
---|---|
With bis(tri-t-butylphosphine)palladium(0); sodium t-butanolate In toluene for 3h; Reflux; | 88% |
iodobenzene
11,12-dihydro-11-phenylindolo[2,3-a]carbazole
Conditions | Yield |
---|---|
With 3,5-ditertbutyl salicylic acid; copper; potassium carbonate for 48h; Reflux; Inert atmosphere; | 87% |
11,12-dihydro-11-phenylindolo[2,3-a]carbazole
2-bromo-5-phenyl-1,3-oxazole
Conditions | Yield |
---|---|
With tris-(dibenzylideneacetone)dipalladium(0); tri-tert-butyl phosphine; sodium t-butanolate In o-xylene at 160℃; for 48h; | 86% |
11,12-dihydro-11-phenylindolo[2,3-a]carbazole
2-bromobenzo[d]benzo[4,5]imidazo[2,1-b]thiazole
Conditions | Yield |
---|---|
With tris-(dibenzylideneacetone)dipalladium(0); 4,5-bis(diphenylphos4,5-bis(diphenylphosphino)-9,9-dimethylxanthenephino)-9,9-dimethylxanthene; sodium t-butanolate In toluene for 12h; Inert atmosphere; Reflux; | 85% |
Conditions | Yield |
---|---|
With tri-tert-butyl phosphine; bis(dibenzylideneacetone)-palladium(0); sodium t-butanolate In toluene for 3h; Reflux; Inert atmosphere; | 85% |
With copper(l) iodide; potassium carbonate; rac-diaminocyclohexane In 5,5-dimethyl-1,3-cyclohexadiene Reflux; |
Conditions | Yield |
---|---|
With tris-(dibenzylideneacetone)dipalladium(0); tri-tert-butyl phosphine; sodium t-butanolate In toluene at 105℃; for 24h; Inert atmosphere; | 84.7% |
11,12-dihydro-11-phenylindolo[2,3-a]carbazole
Conditions | Yield |
---|---|
With tris-(dibenzylideneacetone)dipalladium(0); tri-tert-butyl phosphine; sodium t-butanolate In toluene at 105℃; for 24h; Inert atmosphere; | 84.7% |
11,12-dihydro-11-phenylindolo[2,3-a]carbazole
Conditions | Yield |
---|---|
With tris-(dibenzylideneacetone)dipalladium(0); tri-tert-butyl phosphine; sodium t-butanolate In toluene at 105℃; for 24h; Inert atmosphere; | 84.7% |
11,12-dihydro-11-phenylindolo[2,3-a]carbazole
Conditions | Yield |
---|---|
With caesium carbonate In N,N-dimethyl-formamide at 120℃; | 84% |
Conditions | Yield |
---|---|
With palladium diacetate; potassium carbonate In tetrahydrofuran at 80℃; for 12h; Inert atmosphere; | 82.1% |
11,12-dihydro-11-phenylindolo[2,3-a]carbazole
3-bromo-5-chloro-1,1’-biphenyl
Conditions | Yield |
---|---|
With bis(tri-t-butylphosphine)palladium(0); sodium t-butanolate In toluene for 6h; Reflux; | 81% |
Conditions | Yield |
---|---|
With tris-(dibenzylideneacetone)dipalladium(0); sodium t-butanolate In toluene at 130℃; for 3h; | 80% |
Conditions | Yield |
---|---|
With potassium phosphate; copper(l) iodide; trans-1,2-cyclohexanediamine In 1,4-dioxane for 24h; Reflux; | 80% |
11,12-dihydro-11-phenylindolo[2,3-a]carbazole
Conditions | Yield |
---|---|
With tris-(dibenzylideneacetone)dipalladium(0); 4,5-bis(diphenylphos4,5-bis(diphenylphosphino)-9,9-dimethylxanthenephino)-9,9-dimethylxanthene; sodium t-butanolate In toluene for 12h; Inert atmosphere; Reflux; | 80% |
11,12-dihydro-11-phenylindolo[2,3-a]carbazole
3-bromobenzo[4’,5’]imidazo[2’,1’:2,3]thiazolo[5,4-b]pyridine
Conditions | Yield |
---|---|
With tris-(dibenzylideneacetone)dipalladium(0); 4,5-bis(diphenylphos4,5-bis(diphenylphosphino)-9,9-dimethylxanthenephino)-9,9-dimethylxanthene; sodium t-butanolate In toluene for 12h; Inert atmosphere; Reflux; | 80% |
11,12-dihydro-11-phenylindolo[2,3-a]carbazole
2-(4-bromobenzenyl)-4,6-diphenyl-1,3,5-triazine
Conditions | Yield |
---|---|
With tri-tert-butyl phosphine; palladium diacetate; sodium t-butanolate In toluene at 80℃; for 24h; Inert atmosphere; | 80% |
With palladium diacetate; sodium t-butanolate; tri tert-butylphosphoniumtetrafluoroborate In toluene at 110℃; for 5h; Buchwald-Hartwig Coupling; Inert atmosphere; | 50% |
Conditions | Yield |
---|---|
With 1-dodecylbenzene; 3,5-ditertbutyl salicylic acid; copper; potassium carbonate for 18h; Inert atmosphere; Reflux; | 80% |
Conditions | Yield |
---|---|
With bis(tri-t-butylphosphine)palladium(0); sodium t-butanolate In 5,5-dimethyl-1,3-cyclohexadiene for 6h; Reflux; | 80% |
5-bromo-2-phenyl-1,3-thiazole
11,12-dihydro-11-phenylindolo[2,3-a]carbazole
Conditions | Yield |
---|---|
With tris-(dibenzylideneacetone)dipalladium(0); tri-tert-butyl phosphine; sodium t-butanolate In o-xylene at 160℃; for 48h; | 79% |
11,12-dihydro-11-phenylindolo[2,3-a]carbazole
2-chloro-4,6-diphenyl-1,3,5-triazine
11-(4,6-diphenyl-1,3,5-triazin-2-yl)-12-phenyl-11,12-dihydroindolo[2,3-a]carbazole
Conditions | Yield |
---|---|
Stage #1: 11-phenyl-11,12-dihydroindolo[2,3-a]carbazole With sodium hydride In N,N-dimethyl-formamide at 0 - 20℃; for 0.5h; Inert atmosphere; Stage #2: 2-chloro-4,6-diphenyl-1,3,5-triazine In N,N-dimethyl-formamide at 60℃; for 12h; | 78% |
Stage #1: 11-phenyl-11,12-dihydroindolo[2,3-a]carbazole With sodium hydride In N,N-dimethyl-formamide at 0 - 20℃; for 0.5h; Inert atmosphere; Stage #2: 2-chloro-4,6-diphenyl-1,3,5-triazine In N,N-dimethyl-formamide at 60℃; for 12h; | 78% |
Stage #1: 11-phenyl-11,12-dihydroindolo[2,3-a]carbazole With sodium hydride In N,N-dimethyl-formamide for 1.16667h; Stage #2: 2-chloro-4,6-diphenyl-1,3,5-triazine In N,N-dimethyl-formamide for 4h; | 54.6% |
Stage #1: 11-phenyl-11,12-dihydroindolo[2,3-a]carbazole With sodium hydride In N,N-dimethyl-formamide; paraffin oil at 20℃; for 0.5h; Stage #2: 2-chloro-4,6-diphenyl-1,3,5-triazine In N,N-dimethyl-formamide; paraffin oil at 20℃; for 7h; |
11,12-dihydro-11-phenylindolo[2,3-a]carbazole
4'-(4-bromo-phenyl)-[2,2';6',2'']terpyridine
Conditions | Yield |
---|---|
With copper(l) iodide; 18-crown-6 ether; potassium carbonate at 175℃; for 36h; Inert atmosphere; | 78% |
Conditions | Yield |
---|---|
With 1,10-Phenanthroline; potassium carbonate; copper(I) bromide In toluene at 110 - 120℃; for 7h; Inert atmosphere; | 76.2% |
11,12-dihydro-11-phenylindolo[2,3-a]carbazole
Conditions | Yield |
---|---|
With tris-(dibenzylideneacetone)dipalladium(0); tri-tert-butyl phosphine; sodium t-butanolate In o-xylene at 160℃; for 48h; | 76% |
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