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Simagchem Corporation

Welcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our

High quality N-Cyanoethyl Aniline supplier in China

Cas:1075-76-9

Min.Order:1 Metric Ton

Negotiable

Type:Manufacturers

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Ality Chemical Corporation

The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi

Factory Supply 3-anilinopropionitrile

Cas:1075-76-9

Min.Order:1

Negotiable

Type:Other

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Xi'an Xszo Chem Co., Ltd.

1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s

High Quality 99% 3-Anilinopropionitrile 1075-76-9 GMP Manufacturer

Cas:1075-76-9

Min.Order:1 Gram

FOB Price: $0.1

Type:Manufacturers

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Dayang Chem (Hangzhou) Co.,Ltd.

DayangChem exported this product to many countries and regions at best price in China. If you are looking for the product’s supplier in China, DayangChem is your best choice. Pls contact with us freely for getting detailed product specifica

3-Anilinopropionitrile

Cas:1075-76-9

Min.Order:1 Kilogram

FOB Price: $2.0

Type:Lab/Research institutions

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Chemwill Asia Co., Ltd.

Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block

N-(2-Cyanoethyl)-aniline

Cas:1075-76-9

Min.Order:5 Kiloliter

FOB Price: $1.2 / 5.0

Type:Manufacturers

inquiry

Hebei Nengqian Chemical Import and Export Co., LTD

Our advantages: 1. All inquiries will be replied within 12 hours. 2. Dedication to quality, supply & service. 3. Strictly on selecting raw materials. 4. Reasonable & competitive price, fast lead time. 5. Sample is available for your eva

3-Anilinopropionitrile

Cas:1075-76-9

Min.Order:1 Kilogram

FOB Price: $9.0 / 99.0

Type:Trading Company

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Henan Tianfu Chemical Co., Ltd.

Our company was built in 2009 with an ISO certificate.In the past 5 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so on.O

1075-76-9

Cas:1075-76-9

Min.Order:1 Pound

FOB Price: $1.0

Type:Lab/Research institutions

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Zhuozhou Wenxi import and Export Co., Ltd

WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et

Pharmaceutical Grade CAS 1075-76-9 with competitive price

Cas:1075-76-9

Min.Order:1 Kilogram

FOB Price: $139.0 / 210.0

Type:Trading Company

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Hangzhou Sartort Biopharma Co., Ltd

Appearance:White to Orange to Green powder Storage:room temperature Package:25kg/drum Application:chemicals Transportation:Express/Sea/Air Port:any port in china

3-Anilinopropionitrile factory price

Cas:1075-76-9

Min.Order:1 Kilogram

FOB Price: $1.0

Type:Lab/Research institutions

inquiry

Shanghai Upbio Tech Co.,Ltd

1.In No Less 10 years exporting experience. you can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specializ

Propanenitrile,3-(phenylamino)-

Cas:1075-76-9

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

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Lonwin Chemical Group Limited

3-Anilinopropionitrile CAS: 1075-76-9 Specificatio Category Pharmaceutical Raw Materials, Fine Chemicals, Bulk drug Standard Medical standard Shelf life 2 years Storage should be stored in a we

Factory supply 3-Anilinopropionitrile

Cas:1075-76-9

Min.Order:1 Kilogram

FOB Price: $100.0 / 150.0

Type:Other

inquiry

Xiamen Hisunny Chemical Co.,Ltd

Best quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia

N-Cyanoethyl Aniline

Cas:1075-76-9

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Hangzhou J&H Chemical Co., Ltd.

J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

3-Anilinopropionitrile

Cas:1075-76-9

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Henan Wentao Chemical Product Co., Ltd.

We are leading fine chemicals supplier in China with ISO certificate, Our main business covers the fields below: 1.Noble Metal Catalysts (Pt.Pd...) 2.Organic Phosphine Ligands (Tert-butyl-phosphine.Cyclohexyl-phosphine...) 3.OLED

3-AnilinopropionitrileCAS NO.: 1075-76-9

Cas:1075-76-9

Min.Order:1 Kilogram

FOB Price: $4.0

Type:Lab/Research institutions

inquiry

TAIZHOU ZHENYU BIOTECHNOLOGY CO., LTD

Zhenyu biotech exported this product to many countries and regions at best price. if you are looking for the material's manufacturer or supplier in china, zhenyu biotech is your best choice. pls contact with us freely for getting detailed

3-Anilinopropionitrile

Cas:1075-76-9

Min.Order:1 Kilogram

FOB Price: $2.0

Type:Lab/Research institutions

inquiry

Hunan chemfish Pharmaceutical co.,Ltd

Appearance:95%+ Package:R&D,Pilot run Transportation:per client require Port:Express ,Air, Sea

3-Anilinopropionitrile

Cas:1075-76-9

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Kono Chem Co.,Ltd

high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou

3-Anilinopropionitrile

Cas:1075-76-9

Min.Order:0

Negotiable

Type:Other

inquiry

GIHI CHEMICALS CO.,LIMITED

high purity,in stock Package:25kg/drum,or as per customers'demand Application:API,Pharmaceutical intermediates Transportation:air,sea,courier

3-Anilinopropionitrile

Cas:1075-76-9

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Hefei TNJ chemical industry co.,ltd

Name: 3-Anilinopropionitrile CAS: 1075-76-9 Molecular Formula: C9H11N2 Molecular Weight: 147.197 Application:Fine chemical

3-Anilinopropionitrile CAS 1075-76-9

Cas:1075-76-9

Min.Order:0 Metric Ton

Negotiable

Type:Trading Company

inquiry

Wuhan Fortuna Chemical Co.,Ltd

Best service,high quality and cheap price. Storage:Keep away from heat,sparks and flames. Package:25kg/50kg/200kg drum or Customer demand Application:Used as pharmaceutical intermediates Transportation:BY sea/air or by courier

3-Anilinopropionitrile

Cas:1075-76-9

Min.Order:0

Negotiable

Type:Trading Company

inquiry

DB BIOTECH CO., LTD

Q1: Are you a manufacturer Answer: Yes, we are factory founded on 2012.Q2: How to contact with us Click "contact supplier" And then send us message the product you interest in, you will get reply within 12 hours.Q3:Which kind of payment terms do you

3-Anilinopropionitrile

Cas:1075-76-9

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Henan Allgreen Chemical Co.,Ltd

high quality Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea

3-Anilinopropionitrile

Cas:1075-76-9

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Aecochem Corp.

Our clients, like BASF,CHEMO,Brenntag,ASR,Evonik,Merck and etc.Appearance:COA Storage:in stock Application:MSDS/TDS

N-Cyanoethyl Aniline

Cas:1075-76-9

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Hubei Taiho Chemical Co.,LTD

TAIHO Unique Advantages:1.We're factory2.Free samples available3.Commodity inspection can be done4.ISO9001,Kosher certifications5.10 years experiences Storage:Store in cool &dry place Package:aluminium foil bag/fiber can/plastic drum Application:comp

3-Anilinopropionitrile

Cas:1075-76-9

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Antimex Chemical Limied

Ansciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali

3-Anilinopropionitrile

Cas:1075-76-9

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

BOC Sciences

We are committed to providing our customers with the best products and services at the most competitive prices.Appearance:Powder Storage:Room temperature with sealed well Package:according to the clients requirement Application:Use as primary and sec

3-Anilinopropionitrile

Cas:1075-76-9

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Hangzhou Fandachem Co.,Ltd

3-Anilinopropionitrile cas 1075-76-9Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express

3-Anilinopropionitrile cas 1075-76-9

Cas:1075-76-9

Min.Order:0

Negotiable

Type:Other

inquiry

Henan Kanbei Chemical Co.,LTD

factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin

3-Anilinopropionitrile

Cas:1075-76-9

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Hubei Jiutian Bio-medical Technology Co., Ltd

Trimeric sodium phosphate detergent auxiliary agent is a kind of excellent properties, is one of the biggest component of detergent consumption during the production, it has four aspects: 1, chelation of heavy metal ions, heavy metal ions in the wate

3-Anilinopropionitrile

Cas:1075-76-9

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Shanghai Yuanye Bio-Technology Co., Ltd.

good quality, competitive price, thoughtful after sale serviceAppearance:white powder Storage:Keep it in dry,shady and cool place Package:5g Application:Pharma;Industry;Agricultural;chemical reaserch Transportation:by express or by sea Port:Any port

3-Anilinopropionitrile

Cas:1075-76-9

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Synthetic route

acrylonitrile
107-13-1

acrylonitrile

aniline
62-53-3

aniline

N-cyanoethylaniline
1075-76-9

N-cyanoethylaniline

Conditions
ConditionsYield
With bis{(1R)-1-[(S)-2-(diphenylphosphino)ferrocenyl]ethyl}cyclohexylphosphine; nickel(II) perchlorate hexahydrate In tetrahydrofuran at 20℃; for 24h; Inert atmosphere;99%
With nickel(II) ferrite In water at 100℃; Michael Addition; Green chemistry;99%
With aluminum oxide at 20℃; for 8h; aza-Michael addition; Neat (no solvent);98%
2-cyanoethylamine
151-18-8

2-cyanoethylamine

cyclohexanone
108-94-1

cyclohexanone

N-cyanoethylaniline
1075-76-9

N-cyanoethylaniline

Conditions
ConditionsYield
With styrene; 10 wt% Pd(OH)2 on carbon In toluene at 140℃; under 3750.38 Torr; for 13h; Flow reactor;96%
2-cyanoethylamine
151-18-8

2-cyanoethylamine

phenol
108-95-2

phenol

N-cyanoethylaniline
1075-76-9

N-cyanoethylaniline

Conditions
ConditionsYield
With styrene; 5%-palladium/activated carbon; 10 wt% Pd(OH)2 on carbon; hydrogen In cyclohexanone; toluene at 140℃; under 1500.15 - 3750.38 Torr; for 13h;96%
3-Chloropropionitrile
542-76-7

3-Chloropropionitrile

aniline
62-53-3

aniline

N-cyanoethylaniline
1075-76-9

N-cyanoethylaniline

Conditions
ConditionsYield
With potassium iodide In acetonitrile at 170℃; under 4875.39 Torr; for 0.166667h; microwave irradiation;83%
N-phenyl-2-oxazolidinone
703-56-0

N-phenyl-2-oxazolidinone

N-cyanoethylaniline
1075-76-9

N-cyanoethylaniline

Conditions
ConditionsYield
With potassium cyanide; 18-crown-6 ether at 100℃; for 10h; Neat (no solvent);82%
acrylonitrile
107-13-1

acrylonitrile

aniline
62-53-3

aniline

A

N,N-bis(2-cyanoethyl)aniline
1555-66-4

N,N-bis(2-cyanoethyl)aniline

B

N-cyanoethylaniline
1075-76-9

N-cyanoethylaniline

Conditions
ConditionsYield
With OMS-MIL-100(Fe) In toluene at 50℃; for 24h; Michael Addition; Sealed tube; Schlenk technique; Green chemistry;A 9%
B 71%
N-(2-cyanoethyl)-N-methylaniline
94-34-8

N-(2-cyanoethyl)-N-methylaniline

A

3-(methylphenylamino)-2-propenenitrile
107591-19-5

3-(methylphenylamino)-2-propenenitrile

B

N-cyanoethylaniline
1075-76-9

N-cyanoethylaniline

Conditions
ConditionsYield
With oxygen In N,N-dimethyl acetamide; water at 110℃; under 760.051 Torr; for 12h;A 13 %Chromat.
B 19%
3-diethylaminopropionitrile
5351-04-2

3-diethylaminopropionitrile

aniline hydrochloride
142-04-1

aniline hydrochloride

N-cyanoethylaniline
1075-76-9

N-cyanoethylaniline

3-diethylaminopropionitrile
5351-04-2

3-diethylaminopropionitrile

aniline benzenesulfonate
4484-20-2

aniline benzenesulfonate

N-cyanoethylaniline
1075-76-9

N-cyanoethylaniline

acetic acid
64-19-7

acetic acid

acrylonitrile
107-13-1

acrylonitrile

aniline
62-53-3

aniline

A

N,N-bis(2-cyanoethyl)aniline
1555-66-4

N,N-bis(2-cyanoethyl)aniline

B

N-cyanoethylaniline
1075-76-9

N-cyanoethylaniline

Conditions
ConditionsYield
at 150℃;
aniline hydrochloride
142-04-1

aniline hydrochloride

acrylonitrile
107-13-1

acrylonitrile

N-cyanoethylaniline
1075-76-9

N-cyanoethylaniline

Conditions
ConditionsYield
With diethylamine at 180℃;
aniline hydrochloride
142-04-1

aniline hydrochloride

acrylonitrile
107-13-1

acrylonitrile

aniline
62-53-3

aniline

N-cyanoethylaniline
1075-76-9

N-cyanoethylaniline

Conditions
ConditionsYield
at 140℃;
2--buttersaeure
100133-37-7

2--buttersaeure

aniline
62-53-3

aniline

N-cyanoethylaniline
1075-76-9

N-cyanoethylaniline

Conditions
ConditionsYield
With water
diethyl-(2-cyano-ethyl)-methyl-ammonium; iodide
93115-66-3

diethyl-(2-cyano-ethyl)-methyl-ammonium; iodide

aniline
62-53-3

aniline

N-cyanoethylaniline
1075-76-9

N-cyanoethylaniline

bromopropionitrile
2417-90-5

bromopropionitrile

aniline
62-53-3

aniline

N-cyanoethylaniline
1075-76-9

N-cyanoethylaniline

Conditions
ConditionsYield
With potassium carbonate In acetone
In water Heating;
N-<2-Cyan-aethyl>-norleucin
51078-50-3

N-<2-Cyan-aethyl>-norleucin

aniline
62-53-3

aniline

N-cyanoethylaniline
1075-76-9

N-cyanoethylaniline

Conditions
ConditionsYield
With water
acrylonitrile
107-13-1

acrylonitrile

aniline
62-53-3

aniline

aniline acetate

aniline acetate

N-cyanoethylaniline
1075-76-9

N-cyanoethylaniline

Conditions
ConditionsYield
at 140℃;
acrylonitrile
107-13-1

acrylonitrile

aniline
62-53-3

aniline

aniline phosphate

aniline phosphate

N-cyanoethylaniline
1075-76-9

N-cyanoethylaniline

Conditions
ConditionsYield
at 140℃;
3-Chloropropionitrile
542-76-7

3-Chloropropionitrile

water
7732-18-5

water

aniline
62-53-3

aniline

N-cyanoethylaniline
1075-76-9

N-cyanoethylaniline

naphthalene-2-boronic acid
32316-92-0

naphthalene-2-boronic acid

3-chloro-1-phenyl-2-pyrazoline
58469-32-2

3-chloro-1-phenyl-2-pyrazoline

A

3-naphthalen-2-yl-1-phenyl-4,5-dihydro-1H-pyrazole
3314-37-2

3-naphthalen-2-yl-1-phenyl-4,5-dihydro-1H-pyrazole

B

N-cyanoethylaniline
1075-76-9

N-cyanoethylaniline

Conditions
ConditionsYield
With sodium carbonate; tetrakis(triphenylphosphine) palladium(0) In acetonitrile at 140℃; for 0.0833333h; Product distribution; Further Variations:; Catalysts; Temperatures; Suzuki cross-coupling reaction; microwave irradiation;A 90 % Spectr.
B 9 % Spectr.
(1,3-bis(2,6-diisopropylphenyl)imidazol-2-ylidene)Cu{N(Ph)(CH2CH2CN)}

(1,3-bis(2,6-diisopropylphenyl)imidazol-2-ylidene)Cu{N(Ph)(CH2CH2CN)}

N-cyanoethylaniline
1075-76-9

N-cyanoethylaniline

Conditions
ConditionsYield
With hydrogenchloride In benzene-d6100 % Spectr.
trans-hydrido-2-{3-(phenylamino)propionitrilo}bis(triethylphosphine)platinum(II)

trans-hydrido-2-{3-(phenylamino)propionitrilo}bis(triethylphosphine)platinum(II)

N-cyanoethylaniline
1075-76-9

N-cyanoethylaniline

Conditions
ConditionsYield
In not given (N2); when heating at 70°C overnight C-H reductive elimination occurs; not isolated; detected by (1)H-NMR;
[(η6-toluene)RuCl(κ2-(P,N)-(1,3,5-triaza-7-phosphaadamantan-6-yl)CH(p-C6H4OCH3)NHPh)]Cl

[(η6-toluene)RuCl(κ2-(P,N)-(1,3,5-triaza-7-phosphaadamantan-6-yl)CH(p-C6H4OCH3)NHPh)]Cl

acrylonitrile
107-13-1

acrylonitrile

A

N-cyanoethylaniline
1075-76-9

N-cyanoethylaniline

B

2-propenamide
79-06-1

2-propenamide

Conditions
ConditionsYield
With water at 100℃; for 7h; Overall yield = 57 %Chromat.;
phenol
108-95-2

phenol

N-cyanoethylaniline
1075-76-9

N-cyanoethylaniline

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: hydrogen; palladium on activated charcoal / toluene / 140 °C / 1500.15 Torr / Flow reactor
2: styrene; 10 wt% Pd(OH)2 on carbon / toluene / 13 h / 140 °C / 3750.38 Torr / Flow reactor
View Scheme
acrylonitrile
107-13-1

acrylonitrile

aniline
62-53-3

aniline

A

2-anilinopropionitrile
2182-39-0

2-anilinopropionitrile

B

N-cyanoethylaniline
1075-76-9

N-cyanoethylaniline

Conditions
ConditionsYield
With C25H23Cl5N2Ru; potassium carbonate In toluene at 100℃; for 20h; Catalytic behavior; Reagent/catalyst; Solvent; Inert atmosphere; Autoclave;
N-cyanoethylaniline
1075-76-9

N-cyanoethylaniline

5-(p-tolyl)-2,3-dihydro-2,3-furandione
55991-68-9

5-(p-tolyl)-2,3-dihydro-2,3-furandione

N-(2-Cyano-ethyl)-2,4-dioxo-N-phenyl-4-p-tolyl-butyramide
113308-08-0

N-(2-Cyano-ethyl)-2,4-dioxo-N-phenyl-4-p-tolyl-butyramide

Conditions
ConditionsYield
In 1,4-dioxane for 0.166667h;99%
p-tolyl isoselenocyanate
14223-45-1

p-tolyl isoselenocyanate

N-cyanoethylaniline
1075-76-9

N-cyanoethylaniline

1-(2-cyanoethyl)-1-phenyl-3-(4-tolyl)selenourea
1332566-41-2

1-(2-cyanoethyl)-1-phenyl-3-(4-tolyl)selenourea

Conditions
ConditionsYield
With pyridine In toluene at 20℃; for 24h; Inert atmosphere;99%
benzyl chloride
100-44-7

benzyl chloride

N-cyanoethylaniline
1075-76-9

N-cyanoethylaniline

N-(β-cyanoethyl)-N-benzylaniline
26322-20-3

N-(β-cyanoethyl)-N-benzylaniline

Conditions
ConditionsYield
With ammonium hydroxide; tetramethlyammonium chloride at 50 - 100℃; for 4h; pH=5 - 7; Reagent/catalyst; Temperature; Large scale;97.8%
With sodium carbonate In water
N-cyanoethylaniline
1075-76-9

N-cyanoethylaniline

5-phenylfuran-2,3-dione
55991-67-8

5-phenylfuran-2,3-dione

N-(2-Cyano-ethyl)-2,4-dioxo-4,N-diphenyl-butyramide
113308-07-9

N-(2-Cyano-ethyl)-2,4-dioxo-4,N-diphenyl-butyramide

Conditions
ConditionsYield
In 1,4-dioxane for 0.166667h;97%
3-methyl-5H-1,4,2-dioxazol-5-one

3-methyl-5H-1,4,2-dioxazol-5-one

N-cyanoethylaniline
1075-76-9

N-cyanoethylaniline

C11H13N3O

C11H13N3O

Conditions
ConditionsYield
With bis[dichloro(pentamethylcyclopentadienyl)iridium(III)] In chloroform at 25℃; for 12h; Inert atmosphere; Sealed tube;95%
N-cyanoethylaniline
1075-76-9

N-cyanoethylaniline

tetramethylammonium trifluoromethanethiolate

tetramethylammonium trifluoromethanethiolate

3-(phenyl(trifluoromethyl)amino)propanenitrile

3-(phenyl(trifluoromethyl)amino)propanenitrile

Conditions
ConditionsYield
Stage #1: N-cyanoethylaniline; tetramethylammonium trifluoromethanethiolate In dichloromethane at 20℃;
Stage #2: With silver fluoride In dichloromethane at 20℃; for 1h; Sonication;
94%
1-isoquinolinecarbonitrile
1198-30-7

1-isoquinolinecarbonitrile

N-cyanoethylaniline
1075-76-9

N-cyanoethylaniline

3-(isoquinolin-1-yl(phenyl)amino)propanenitrile

3-(isoquinolin-1-yl(phenyl)amino)propanenitrile

Conditions
ConditionsYield
With 1,4-diaza-bicyclo[2.2.2]octane; 1,3-dicyano-5-fluoro-2,4,6-tris(diphenylamino)benzene In acetonitrile at 20℃; for 12h; Inert atmosphere; Irradiation;94%
N-cyanoethylaniline
1075-76-9

N-cyanoethylaniline

acetonitrile
75-05-8

acetonitrile

N-(2-cyanoethyl)-N-methylaniline
94-34-8

N-(2-cyanoethyl)-N-methylaniline

Conditions
ConditionsYield
With 18-crown-6 ether; carbon dioxide at 80℃; under 750.075 Torr; for 24h; Inert atmosphere; Schlenk technique; Glovebox;93%
methyl β-hydroxy-β-(3,4,5-triethoxyphenyl)ethyl sulfone
39666-75-6

methyl β-hydroxy-β-(3,4,5-triethoxyphenyl)ethyl sulfone

N-cyanoethylaniline
1075-76-9

N-cyanoethylaniline

β-anilino-β-(3,4,5-triethoxybenzyl)acrylonitrile
105639-94-9

β-anilino-β-(3,4,5-triethoxybenzyl)acrylonitrile

Conditions
ConditionsYield
With potassium tert-butylate In dimethyl sulfoxide; tert-butyl alcohol at 45℃; for 3.5h;92%
N-cyanoethylaniline
1075-76-9

N-cyanoethylaniline

N-phenylpropane-1,3-diamine hydrochloride (N-phenyl-1,3-propanediamine hydrochloride)

N-phenylpropane-1,3-diamine hydrochloride (N-phenyl-1,3-propanediamine hydrochloride)

Conditions
ConditionsYield
Stage #1: N-cyanoethylaniline With ammonia; hydrogen In water; isopropyl alcohol at 80℃; under 15001.5 Torr; for 24h; Autoclave;
Stage #2: With hydrogenchloride In d(4)-methanol; ethyl acetate Cooling with ice;
91%
N-cyanoethylaniline
1075-76-9

N-cyanoethylaniline

N'-hydroxy-3-(phenylamino)propanimidamide
16387-47-6

N'-hydroxy-3-(phenylamino)propanimidamide

Conditions
ConditionsYield
With hydroxylamine In etahol; water for 24h; Heating / reflux;90.1%
formic acid
64-18-6

formic acid

N-cyanoethylaniline
1075-76-9

N-cyanoethylaniline

N-(2-cyanoethyl)-N-methylaniline
94-34-8

N-(2-cyanoethyl)-N-methylaniline

Conditions
ConditionsYield
With tris(pentafluorophenyl)borate In dibutyl ether at 100℃; Schlenk technique; Inert atmosphere;87%
With dipotassium hydrogenphosphate; 18-crown-6 ether In tetrahydrofuran at 80℃; for 12h; Molecular sieve;85%
With platinum on carbon; phenylsilane In toluene at 80℃; for 15h;55%
With platinum on activated charcoal; phenylsilane In toluene at 80℃; for 15h; Schlenk technique; Inert atmosphere;55%
With platinum(0)-1,3-divinyl-1,1,3,3-tetramethyldisiloxane complex; 1,3-bis-(diphenylphosphino)propane; phenylsilane In dibutyl ether at 60℃; for 18h; Schlenk technique; Inert atmosphere;70 %Chromat.
N-cyanoethylaniline
1075-76-9

N-cyanoethylaniline

chloroacetyl chloride
79-04-9

chloroacetyl chloride

3-propionitril
16231-77-9

3-propionitril

Conditions
ConditionsYield
With potassium carbonate In 1,4-dioxane at 60℃; for 2h;83%
With potassium carbonate In 1,4-dioxane
N-cyanoethylaniline
1075-76-9

N-cyanoethylaniline

4,5-Dichlor-2-dicyanmethylen-cyclopent-4-en-1,3-dion
84557-23-3

4,5-Dichlor-2-dicyanmethylen-cyclopent-4-en-1,3-dion

4-Chlor-5-(N-2-cyanoethyl-N-phenyl-amino)-2-dicyanmethylen-cyclopent-4-en-1,3-dion
84557-34-6

4-Chlor-5-(N-2-cyanoethyl-N-phenyl-amino)-2-dicyanmethylen-cyclopent-4-en-1,3-dion

Conditions
ConditionsYield
In ethanol for 0.0833333h; Heating;83%
N-cyanoethylaniline
1075-76-9

N-cyanoethylaniline

N-(2-cyanoethyl)-N-phenylnitrosamine
55919-60-3

N-(2-cyanoethyl)-N-phenylnitrosamine

Conditions
ConditionsYield
With hydrogenchloride; sodium nitrite In water at 10℃;83%
N-cyanoethylaniline
1075-76-9

N-cyanoethylaniline

2,4-dinitro-N-<2-cyanoethyl>aniline
15942-22-0

2,4-dinitro-N-<2-cyanoethyl>aniline

Conditions
ConditionsYield
With bismuth (III) nitrate pentahydrate; palladium diacetate In 2,2,2-trifluoroethanol; trifluoroacetic acid at 20 - 90℃; for 24h; Inert atmosphere;78%
N-cyanoethylaniline
1075-76-9

N-cyanoethylaniline

N-phenyl-β-alanine
5652-38-0

N-phenyl-β-alanine

Conditions
ConditionsYield
Stage #1: N-cyanoethylaniline With sodium hydroxide; water for 1h; Heating / reflux;
Stage #2: With water; acetic acid
77.7%
With sodium hydroxide for 6h; Heating;
Stage #1: N-cyanoethylaniline With sodium hydroxide; water at 20℃; Heating / reflux;
Stage #2: With hydrogenchloride In water pH=~ 3;
N-cyanoethylaniline
1075-76-9

N-cyanoethylaniline

5-(2-hydroxyethyl)-4-methylthiophene-3-carbaldehyde
334687-35-3

5-(2-hydroxyethyl)-4-methylthiophene-3-carbaldehyde

3-(2-Cyano-3-phenylaminoprop-2-en-1-yl)-5-(2-hydroxyethyl)-4-methylthiophene

3-(2-Cyano-3-phenylaminoprop-2-en-1-yl)-5-(2-hydroxyethyl)-4-methylthiophene

Conditions
ConditionsYield
With potassium tert-butylate In dimethyl sulfoxide; tert-butyl alcohol at 55℃;77%
5-(2-hydroxyethyl)furan-3-carbaldehyde

5-(2-hydroxyethyl)furan-3-carbaldehyde

N-cyanoethylaniline
1075-76-9

N-cyanoethylaniline

3-(5-(2-hydroxyethyl)furan-3-yl)-2-(phenylaminomethyl)acrylonitrile

3-(5-(2-hydroxyethyl)furan-3-yl)-2-(phenylaminomethyl)acrylonitrile

Conditions
ConditionsYield
With sodium methylate In methanol; dimethyl sulfoxide at 45℃; for 3h; Inert atmosphere;76%
carbon dioxide
124-38-9

carbon dioxide

N-cyanoethylaniline
1075-76-9

N-cyanoethylaniline

N-(2-cyanoethyl)-N-methylaniline
94-34-8

N-(2-cyanoethyl)-N-methylaniline

Conditions
ConditionsYield
With dimanganese decacarbonyl; phenylsilane; C29H33N2P In acetonitrile at 100℃; under 750.075 Torr; for 15h;75%
With diphenylsilane; caesium carbonate In acetonitrile at 80℃;56%
terephthalonitrile
623-26-7

terephthalonitrile

N-cyanoethylaniline
1075-76-9

N-cyanoethylaniline

4-(2-cyano-1-(phenylamino)ethyl)benzonitrile
1149665-95-1

4-(2-cyano-1-(phenylamino)ethyl)benzonitrile

Conditions
ConditionsYield
With Quinuclidine; (4,4'-di-tert-butyl-2,2'-dipyridyl)-bis-(2-phenylpyridine(-1H))-iridium(III) hexafluorophosphate In acetonitrile for 24h; Sealed tube; Inert atmosphere; Irradiation;75%
N-cyanoethylaniline
1075-76-9

N-cyanoethylaniline

α-bromoacetophenone
70-11-1

α-bromoacetophenone

3-[(2-Oxo-2-phenyl-ethyl)-phenyl-amino]-propionitrile
138652-96-7

3-[(2-Oxo-2-phenyl-ethyl)-phenyl-amino]-propionitrile

Conditions
ConditionsYield
In ethanol for 4h; Heating;74%
benzaldehyde
100-52-7

benzaldehyde

N-cyanoethylaniline
1075-76-9

N-cyanoethylaniline

2-Benzyl-3-(phenylamino)acrylonitrile

2-Benzyl-3-(phenylamino)acrylonitrile

Conditions
ConditionsYield
With potassium tert-butylate In dimethyl sulfoxide; tert-butyl alcohol at 55℃; for 1.5h;74%
N-cyanoethylaniline
1075-76-9

N-cyanoethylaniline

ortho-anisaldehyde
135-02-4

ortho-anisaldehyde

(E)-3-(2-Methoxy-phenyl)-2-phenylaminomethyl-acrylonitrile

(E)-3-(2-Methoxy-phenyl)-2-phenylaminomethyl-acrylonitrile

Conditions
ConditionsYield
With sodium methylate In dimethyl sulfoxide at 125 - 130℃; for 2h;72%
2-amino-4,5-dimethylthiophene-3-carbonitrile
4651-94-9

2-amino-4,5-dimethylthiophene-3-carbonitrile

N-cyanoethylaniline
1075-76-9

N-cyanoethylaniline

4-amino-2-(2-anilino)ethyl-5,6-dimethylthieno[2,3-d]pyrimidine

4-amino-2-(2-anilino)ethyl-5,6-dimethylthieno[2,3-d]pyrimidine

Conditions
ConditionsYield
With hydrogenchloride In 1,4-dioxane for 6h;72%

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