img _fcksavedurl="/UserAppearance:detailed see specifications Storage:Store in dry, dark and ventilated place. Package:according to the clients requirement Application:Used in Synthesis, Pharmaceuticals and other fields Transportation:by air or by
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Cas:110-42-9
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Cas:110-42-9
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Cas:110-42-9
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inquiryName Methyl decanoate Synonyms Methyl caprate CAS NO. 110-42-9 Molecular Formula C11H22O2 Molecular Weight 186.
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Cas:110-42-9
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Conditions | Yield |
---|---|
With tetrachloromethane at 20℃; for 12h; UV-irradiation; | 99% |
With Mesoscopically Assembled SulfatedZirconia Nanoparticles at 49.84℃; for 8h; Catalytic behavior; Reagent/catalyst; Temperature; | 97% |
With sulfuric acid; acetonitrile at 80 - 85℃; for 16 - 18h; | 97% |
Conditions | Yield |
---|---|
With hydrogenchloride; dihydrogen peroxide | 98% |
Dimethoxymethane
n-decanoyl chloride
A
Methyl decanoate
B
chloromethyl methyl ether
Conditions | Yield |
---|---|
sulfuric acid at 55 - 60℃; for 2h; exchange reaction; | A n/a B 97% |
Conditions | Yield |
---|---|
With sulfuric acid Reflux; regioselective reaction; | 97% |
Conditions | Yield |
---|---|
With hydrogenchloride; dihydrogen peroxide 1.) <20 deg C, 30 min; 2.) 40 deg C, 3 h; | 96% |
1-tert-Butylperoxy-1-methoxy-decane
Methyl decanoate
Conditions | Yield |
---|---|
In methanol at 60℃; | 94% |
Conditions | Yield |
---|---|
Stage #1: Decanoic acid, tert-butyldimethylsilyl ester; methanol; carbon tetrabromide at 20℃; for 0.5h; Irradiation; Stage #2: at 20℃; for 3h; | 92% |
Conditions | Yield |
---|---|
With [bis(acetoxy)iodo]benzene; iodine at 20℃; for 4h; | 91% |
With pyridine; tert-butylhypochlorite In dichloromethane for 1h; | 99 % Chromat. |
With (2-hydroxyethyl)(methyl)amine; bis[dichloro(pentamethylcyclopentadienyl)iridium(III)]; caesium carbonate In acetone at 25℃; for 24h; Inert atmosphere; | 82 %Chromat. |
Conditions | Yield |
---|---|
With hydrogenchloride; dihydrogen peroxide | 90% |
With potassium bromide for 1.8h; Ambient temperature; anode, platinum plate; cathode, carbon rod; | 85% |
With ammonium cerium (IV) nitrate; lithium bromide In neat liquid at 35 - 40℃; for 3.5h; | 74% |
Conditions | Yield |
---|---|
bis(trimethylsilyl)sulphate In dichloromethane; 1,2-dichloro-ethane for 8.5h; Heating; | A 89% B 82% |
Conditions | Yield |
---|---|
Stage #1: C19H40O2Si; methanol; carbon tetrabromide at 20℃; for 0.5h; Irradiation; Stage #2: at 20℃; for 8h; | 89% |
Conditions | Yield |
---|---|
With dipyridinium dichromate In N,N-dimethyl-formamide for 20h; Ambient temperature; | A n/a B 87% |
Conditions | Yield |
---|---|
With tetraethylammonium tosylate Ambient temperature; electrolysis; | 87% |
Conditions | Yield |
---|---|
With (N3/phenyl-/(diethylamino)methyl-triazolyl)-modified DMOF [DMOF= Zn2(2-amino-terephthalate)2(dabco)] at 130℃; for 20h; | 84% |
With di(n-butyl)tin oxide In methanol for 12h; Heating; | 80% |
With lanthanum complex grafted upon hydrotalcite for 8h; pH=10; Reflux; | 56% |
With nitrogen-functionalized metal-organic framework catalyst at 180℃; for 24h; Inert atmosphere; |
Conditions | Yield |
---|---|
With sodium periodate; ruthenium trichloride In tetrachloromethane; water; acetonitrile for 8h; Ambient temperature; | A 83% B n/a |
Conditions | Yield |
---|---|
Stage #1: C26H38O2Si; methanol; carbon tetrabromide at 20℃; for 0.5h; Irradiation; Stage #2: at 20℃; for 9h; | 81% |
Conditions | Yield |
---|---|
With tetraethylammonium tosylate Ambient temperature; electrolysis; | 77% |
Conditions | Yield |
---|---|
With tetraethylammonium tosylate Ambient temperature; electrolysis; | 76% |
Conditions | Yield |
---|---|
With methanol; tetrabutylammomium bromide; bromine In dichloromethane for 0.5h; Yields of byproduct given; | A 69% B n/a |
With methanol; tetrabutylammomium bromide; bromine In dichloromethane for 0.5h; Yield given; | A 69% B n/a |
C22H38O4
A
Methyl decanoate
B
dimethyl 1,18-octadecanedioate
C
(R)-6-hexyl-tetrahydro-2H-pyran-2-one
Conditions | Yield |
---|---|
Stage #1: C22H38O4 Stage #2: With hydrogen at 75℃; under 7500.75 Torr; for 14h; regioselective reaction; | A n/a B n/a C 66% |
Conditions | Yield |
---|---|
With C15H17ClIrNOP; potassium tert-butylate In neat (no solvent) at 60℃; for 12h; Schlenk technique; Inert atmosphere; Glovebox; | 59% |
Conditions | Yield |
---|---|
With lanthanum complex grafted upon hydrotalcite for 8h; pH=10; Catalytic behavior; Time; Reagent/catalyst; Concentration; pH-value; Reflux; | 55% |
methyl 9-decenoate
carbon monoxide
A
Methyl decanoate
B
methyl 11-oxoundecanoate
C
methyl 9-methyl-10-oxodecanoate
Conditions | Yield |
---|---|
With dicarbonylacetylacetonato rhodium (I); hydrogen; triphenylphosphine at 60℃; under 30003 Torr; for 12h; Temperature; Pressure; Reagent/catalyst; | A 6% B 55% C 28% D 11% |
methanol
caprinaldehyde
A
Methyl decanoate
B
methyl ester of α-bromodecanoic acid
Conditions | Yield |
---|---|
Stage #1: caprinaldehyde With ammonium cerium (IV) nitrate; lithium bromide In neat liquid Stage #2: methanol In neat liquid at 35 - 40℃; for 3.5h; | A 29 %Chromat. B 53% |
decanoylphenyldimethylsilane tosylhydrazone
A
n-decanenitrile
B
Methyl decanoate
Conditions | Yield |
---|---|
With tetrabutylammonium tetrafluoroborate In methanol; dichloromethane electrolysis; | A 45% B 11% |
methanol
capric anhydride
[hydroxy(tosyloxy)iodo]benzene
A
iodobenzene
B
Methyl decanoate
Conditions | Yield |
---|---|
Stage #1: capric anhydride; [hydroxy(tosyloxy)iodo]benzene at 100℃; for 0.333333h; Stage #2: methanol With toluene-4-sulfonic acid for 4h; Heating; | A n/a B n/a C 41% |
Conditions | Yield |
---|---|
With palladium 10% on activated carbon; W(OTf)6; hydrogen at 180℃; under 15001.5 Torr; for 8h; Autoclave; | A 2.7% B 15.3% |
Conditions | Yield |
---|---|
With methanol; sodium Electrolysis.an Platin-Elektroden; |
Conditions | Yield |
---|---|
for 0.5h; |
diazomethane
methyl 8-hydroxyoctadecanoate
A
Methyl decanoate
B
methyl undecanoate
C
dimethyl 1,7-heptanedioate
D
dimethyl subarate
Conditions | Yield |
---|---|
With potassium permanganate In acetic acid Product distribution; oxidative degradation and methylation; |
Conditions | Yield |
---|---|
With hydrogen In hexane at 200℃; under 15001.5 Torr; for 8h; Reagent/catalyst; | 99.8% |
Stage #1: Methyl decanoate With diethylzinc; lithium chloride In tetrahydrofuran; hexane at 20℃; for 6h; Inert atmosphere; Stage #2: With sodium hydroxide In tetrahydrofuran; hexane; water at 20℃; for 8h; Inert atmosphere; chemoselective reaction; | 98% |
With samarium diiodide; water; triethylamine In tetrahydrofuran at 20℃; for 15h; Inert atmosphere; | 95% |
Conditions | Yield |
---|---|
With sodium borohydrid In 5,5-dimethyl-1,3-cyclohexadiene | 99% |
Conditions | Yield |
---|---|
With C66H102N4OP2Ru; hydrogen In toluene at 105℃; under 22502.3 Torr; for 20h; Inert atmosphere; Glovebox; | A n/a B 99% |
With C30H37ClN4ORu; hydrogen; sodium t-butanolate In toluene at 105℃; under 22502.3 Torr; for 20h; Glovebox; Sealed tube; Overall yield = >99 %; |
Conditions | Yield |
---|---|
With sodium methylate In 5,5-dimethyl-1,3-cyclohexadiene for 1.25h; Claisen Condensation; Inert atmosphere; Reflux; Microwave irradiation; | 98.3% |
Conditions | Yield |
---|---|
With titanium(IV) isopropylate In diethyl ether at -78 - 0℃; for 0.5h; | 98% |
With titanium(IV) isopropylate In diethyl ether at 18 - 20℃; | 97% |
titanium(IV) isopropylate In diethyl ether at 18 - 20℃; | 95% |
Conditions | Yield |
---|---|
With sodium borohydrid In 5,5-dimethyl-1,3-cyclohexadiene | 98% |
Methyl decanoate
n-[1,1-2H2]decanol
Conditions | Yield |
---|---|
With lithium aluminium deuteride In tetrahydrofuran at -78℃; Reflux; | 98% |
Conditions | Yield |
---|---|
With sodium borohydrid In 5,5-dimethyl-1,3-cyclohexadiene | 97% |
Conditions | Yield |
---|---|
With 1,3-bis(3,5-bis(trifluoro-ethyl)phenyl)thiourea; 4-pyrrolidin-1-ylpyridine In n-heptane for 24h; Reflux; | 96% |
Methyl decanoate
phenyl trifluoromethylsulfide
1,1,1-trifluoro-2-undecanone
Conditions | Yield |
---|---|
With Triethylgermyl-natrium In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide at -60℃; for 1.5h; | 95% |
Conditions | Yield |
---|---|
With decacarbonyldirhenium(0) In toluene at 30℃; for 9h; Inert atmosphere; UV-irradiation; Schlenk technique; | 93% |
Methyl decanoate
[(1-methoxy-2-methyl-1-butenyl)oxy]trimethylsilane
Conditions | Yield |
---|---|
With sodium hydroxide In N,N-dimethyl-formamide at 20 - 25℃; for 1h; Claisen condensation; Inert atmosphere; | A 8% B 90% |
With sodium hydroxide In N,N-dimethyl-formamide at 15 - 20℃; for 1h; crossed Claisen condensation; |
Conditions | Yield |
---|---|
With sodium borohydrid In 5,5-dimethyl-1,3-cyclohexadiene | 90% |
Conditions | Yield |
---|---|
With n-butyllithium In tetrahydrofuran; hexane 1.) -95 deg C, 2 h, 2.) -78 deg C, 30 min; | 89% |
2-(tert-butyldimethylsilyloxy)-1-methoxy-1-trimethylsilyloxy-1-propene
Methyl decanoate
Conditions | Yield |
---|---|
Stage #1: 2-(tert-butyldimethylsilyloxy)-1-methoxy-1-trimethylsilyloxy-1-propene; Methyl decanoate With sodium hydroxide In 1-methyl-pyrrolidin-2-one at 20 - 25℃; for 3h; Claisen condensation; Inert atmosphere; Stage #2: With tetrabutyl ammonium fluoride In tetrahydrofuran at 0 - 5℃; for 1h; Inert atmosphere; | 89% |
Conditions | Yield |
---|---|
In tetrahydrofuran at -78℃; for 3h; | 88% |
tris(methylthio)methane
Methyl decanoate
A
tetrathioorthocarbonic acid tetramethyl ester
Conditions | Yield |
---|---|
With n-butyllithium In tetrahydrofuran; hexane 1.) -95 deg C, 2 h, 2.) -78 deg C, 30 min; | A n/a B 88% |
1-methyl-1H-benzo[d][1,2,3]triazole
Methyl decanoate
1-Benzotriazol-1-yl-undecan-2-one
Conditions | Yield |
---|---|
With n-butyllithium In tetrahydrofuran; hexane at -78 - 20℃; for 12h; | 88% |
Methyl decanoate
dimethyl 1-(1-diazo-2-oxopropyl)phosphonate
1-undecyne
Conditions | Yield |
---|---|
Stage #1: Methyl decanoate With diisobutylaluminium hydride In n-heptane; dichloromethane at -78℃; Stage #2: dimethyl 1-(1-diazo-2-oxopropyl)phosphonate With potassium carbonate In methanol; n-heptane; dichloromethane at 20℃; Further stages.; | 88% |
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