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Conditions | Yield |
---|---|
With [((Me)NN2)NiCl] In tetrahydrofuran; ISOPROPYLAMIDE at -35 - 20℃; Inert atmosphere; | 98% |
Conditions | Yield |
---|---|
With triethylsilane; Naftion-H (perfluororesinsulfonic acid) In dichloromethane for 2h; Heating; | 95.3% |
Conditions | Yield |
---|---|
With potassium hydroxide at 20℃; for 14h; Methylation; | 95% |
With mercury(II) oxide In toluene at 20℃; for 12h; | 93% |
tetra(n-butyl)ammonium hydrogensulfate at 40 - 45℃; |
Conditions | Yield |
---|---|
With 3-chloro-benzenecarboperoxoic acid at 20℃; | 87% |
Conditions | Yield |
---|---|
In methanol at 25℃; for 42h; Temperature; | 81.1% |
Conditions | Yield |
---|---|
In methanol at 20℃; for 3h; | 73% |
1-bromo dodecane
potassium methanolate
A
1-methoxydecane
B
1-Decene
Conditions | Yield |
---|---|
In methanol at 25℃; for 48h; | A 46% B 35% |
In methanol; dimethyl sulfoxide at 20℃; Rate constant; estimation H--function; | A n/a B 18.6% |
benzene-1,3-dicarbonitrile
C12H23O3(1-)*Na(1+)
phenanthrene
A
1-methoxydecane
B
3-(10-methoxydecyl)-1-cyanobenzene
C
4-(10-methoxydecyl)-1,3-dicyanobenzene
D
9-(9,10-dihydro)phenanthrenecarbonitrile
Conditions | Yield |
---|---|
In water; acetonitrile at 20℃; for 6h; Inert atmosphere; Irradiation; | A 26% B 4% C 11% D 1% |
terephthalonitrile
C12H23O3(1-)*Na(1+)
phenanthrene
A
1-methoxydecane
B
4-(10-methoxydecyl)-1-cyanobenzene
C
9-(9,10-dihydro)phenanthrenecarbonitrile
Conditions | Yield |
---|---|
In water; acetonitrile at 20℃; for 6h; Inert atmosphere; Irradiation; | A 8% B 25% C 1% |
C12H23O3(1-)*Na(1+)
phenanthrene
phthalonitrile
A
1-methoxydecane
B
2-(10-methoxydecyl)-1-cyanobenzene
C
4-(10-methoxydecyl)-1,2-dicyanobenzene
D
9-(9,10-dihydro)phenanthrenecarbonitrile
Conditions | Yield |
---|---|
In water; acetonitrile at 20℃; for 6h; Inert atmosphere; Irradiation; | A 20% B 24% C 5% D 1% |
1-Decanol
1-methyl pyridinium iodide
A
decyl ether
B
1-methoxydecane
C
1-Decene
Conditions | Yield |
---|---|
at 220℃; | |
at 200℃; |
Conditions | Yield |
---|---|
(i) HgO, aq. HClO4, (ii) /BRN= 1735227/; Multistep reaction; |
Conditions | Yield |
---|---|
In methanol; dimethyl sulfoxide at 20℃; Rate constant; effect of 18-crown-6; | |
In methanol; dimethyl sulfoxide at 20℃; Rate constant; estimation H--function; |
Conditions | Yield |
---|---|
aluminum oxide In cyclohexane for 2h; Heating; Yield given; |
Conditions | Yield |
---|---|
silica gel Ambient temperature; | 99 % Chromat. |
Conditions | Yield |
---|---|
With benzene |
(decylselenonyl)benzene
1-methoxydecane
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 62 percent / PI3 / CHCl3 / 0.5 h / 0 °C 2: 87 percent / m-CPBA / 20 °C View Scheme |
methanol
1-bromo dodecane
N,N-dimethyldecylamine
A
1-Decanol
B
1-methoxydecane
C
1-Decene
D
N,N-didecyl-N,N-dimethylammonium bromide
Conditions | Yield |
---|---|
at 65 - 142℃; Product distribution / selectivity; | |
With sodium hydroxide at 65 - 142℃; Product distribution / selectivity; |
Conditions | Yield |
---|---|
With fixed bed acidic PURALOX NWa-155 γ-alumina at 219℃; under 760.051 Torr; Automated supercritical flow reactor; | 90 %Chromat. |
Conditions | Yield |
---|---|
With sodium periodate; ruthenium trichloride In tetrachloromethane; water; acetonitrile for 8h; Ambient temperature; | A 83% B n/a |
Conditions | Yield |
---|---|
With chloro-trimethyl-silane; acetic acid; sodium iodide; zinc In acetonitrile Product distribution; 1.) 70 - 75 deg C, 1.5 h; 2.) 75 - 85 deg C, 4.5 h; various ethers; | 82% |
Conditions | Yield |
---|---|
With [RhCl2(p-cymene)]2 In neat (no solvent) at 135℃; under 1125.11 Torr; for 24h; | A n/a B 74 %Spectr. |
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