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inquiryProduct Name: TRI-N-HEXYL ALUMINUM CAS: 1116-73-0 MF: C18H39Al MW: 282.48 EINECS: 214-241-6 Product Categories: Organometallics Mol File: 1116-73-0.mol TRI-N-HEXYL ALUMINUM Structure TRI-N-HEXYL ALUMINUM Chemical Properties Melt
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Known for its best quality and competitve price, this chemicals we offered is widely appreciated by our customers. Prompt reaction, good quality and best service make us reliable and outstanding in this industry.Appearance:yellow to white solid or po
lithium aluminium tetrahydride
1-hexene
di(n-hexyl)aluminum chloride
trihexylaluminium
Conditions | Yield |
---|---|
In n-heptane byproducts: LiCl; LiAlH4 loaded in a vertical-type ball mill under Ar or N2; heptane added; mixt. agitated for 15 min at 70°C; mixt. of (C6H13)2AlCl with hex-1-ene (LiAlH4:(C6H13)2AlCl:hex-1-ene=1.1:1.0:4.5) added; mixt. agitated for 1.5 h at 90°C; cooled; filtered under Ar; solvent and olefin removed (vac., 10 Torr) at60-70°C; elem. anal.; | 95% |
Conditions | Yield |
---|---|
With triisobutylaluminum In hexane (N2); heating (autoclave, 140°C, 1 h, 120°C, 8 h); distn.; elem. anal.; | 89.1% |
With NaAlEt4 In toluene under N2 or Ar; mixt. of AlH3, NaAlEt4, olefin (3.8 equiv.) and toluene heated at reflux; after 20 min temp. raised from 80 to 100°C and gradually decreased to 70-80°C; 2 h; cooled; filtered; ppt. washed with hexane; solvent and excess olefin removed in vac. at 60-80°C (7 Torr); elem. anal.; |
Conditions | Yield |
---|---|
Stage #1: 3-hexene; tri-n-propylaluminum at 70℃; under 760.051 Torr; Heating / reflux; Stage #2: cobalt(III) acetylacetonate In toluene for 2h; Stage #3: With hydrogenchloride | 6.1% |
Conditions | Yield |
---|---|
With aluminium hydride | |
With lithium aluminium tetrahydride |
Conditions | Yield |
---|---|
With aluminium trichloride In dichloromethane for 1h; Product distribution; Ambient temperature; other reaction time; other reagent: ZnCl2; other molecular proportion.; | 90% |
With aluminium trichloride In dichloromethane for 1h; Ambient temperature; | 90% |
Conditions | Yield |
---|---|
With iron(III) chloride In various solvent(s) at 40℃; for 15h; | A 86% B n/a |
Conditions | Yield |
---|---|
With aluminium trichloride In dichloromethane for 1h; Product distribution; Ambient temperature; other molecular proportion.; | 84% |
With aluminium trichloride In dichloromethane for 1h; Ambient temperature; | 84% |
Conditions | Yield |
---|---|
In toluene at -5 - 50℃; for 7h; Inert atmosphere; | 81.8% |
In toluene at -5 - 50℃; for 7h; Inert atmosphere; | 81.8% |
Conditions | Yield |
---|---|
With dilithium tetrachlorocuprate; triphenylphosphine In octane at 50℃; for 5h; | 78% |
Conditions | Yield |
---|---|
Stage #1: 1-hexene; trihexylaluminium With zirconocene dichloride In hexane at 0 - 20℃; Stage #2: butyraldehyde With copper(l) chloride In hexane at -15 - 20℃; | 78% |
Conditions | Yield |
---|---|
Stage #1: N,N'-ethylenediphthalimide; trihexylaluminium In toluene at -5 - 50℃; for 8h; Inert atmosphere; Stage #2: With water In toluene at 20℃; Inert atmosphere; | 78% |
Conditions | Yield |
---|---|
Stage #1: 1-hexene; trihexylaluminium With zirconocene dichloride In hexane at 0 - 20℃; Stage #2: isobutyraldehyde With copper(l) chloride In hexane at -15 - 20℃; | 76% |
Conditions | Yield |
---|---|
bis-triphenylphosphine-palladium(II) chloride In diethyl ether for 4h; Heating; | 75% |
trihexylaluminium
Conditions | Yield |
---|---|
Stage #1: N-benzyl-N-(3-oxobutyl)-(E)-3-phenylpropenamide With bis-acetylacetonatocobalt(II) dihydrate In tetrahydrofuran at 0 - 20℃; for 0.5h; Stage #2: trihexylaluminium In tetrahydrofuran; hexane at 0 - 20℃; for 15h; diastereoselective reaction; | 75% |
Conditions | Yield |
---|---|
In toluene at -5 - 80℃; for 2h; Inert atmosphere; | 75% |
In toluene at -5 - 80℃; for 2h; Inert atmosphere; | 75% |
Conditions | Yield |
---|---|
With aluminium trichloride In dichloromethane | 70% |
(1R,2R)-trans-N-phthaloyl-1,2-diaminocyclohexane
trihexylaluminium
Conditions | Yield |
---|---|
In hexane at -5 - 40℃; for 2h; Inert atmosphere; | 69.8% |
In hexane at -5 - 40℃; for 2h; Inert atmosphere; | 69.8% |
Conditions | Yield |
---|---|
In toluene at -5 - 90℃; for 2h; Inert atmosphere; | 69.1% |
In toluene at -5 - 90℃; for 2h; Inert atmosphere; | 69.1% |
In toluene at -5 - 90℃; for 2h; Inert atmosphere; | 69.1% |
Conditions | Yield |
---|---|
With iron(III) chloride In hexane at 25℃; | 67% |
trihexylaluminium
dimethyl 2-phenyl-cycloprop-2-ene-1,1-dicarboxylic ester
dimethyl (E)-2-(2-phenyloct-1-enyl)malonate
Conditions | Yield |
---|---|
With iron(III)-acetylacetonate In tetrahydrofuran; hexane at 0 - 20℃; for 16h; stereoselective reaction; | 66% |
chloro-trimethyl-silane
trihexylaluminium
A
trimethylhexylsilane
B
di-n-hexyldimethylsilane
Conditions | Yield |
---|---|
With potassium chloride at 150℃; for 6h; | A 65% B 35% |
Conditions | Yield |
---|---|
With aluminium trichloride In dichloromethane -10 deg C, then 20 deg C, 1 h; | 65% |
rac-3-acetoxycyclohexene
trihexylaluminium
Conditions | Yield |
---|---|
With copper(I) bromide In hexane at 25℃; | 63% |
Conditions | Yield |
---|---|
In dichloromethane | 62% |
acetic acid-(1,1-dimethyl-pent-4-en-2-ynyl ester)
trihexylaluminium
2-methyl-4-hexyl-2,3,5-hexatriene
Conditions | Yield |
---|---|
iron(III) chloride In diethyl ether at 20℃; for 2h; | 62% |
acetic acid-(1,1-dimethyl-pent-4-en-2-ynyl ester)
trihexylaluminium
A
2-methyl-4-hexyl-2,3,5-hexatriene
Conditions | Yield |
---|---|
With iron(III) chloride In diethyl ether at 20℃; for 2h; | A 62% B n/a |
N-benzyl-N-(3-oxobutyl)-(E)-3-(4-methoxyphenyl)propenamide
trihexylaluminium
Conditions | Yield |
---|---|
Stage #1: N-benzyl-N-(3-oxobutyl)-(E)-3-(4-methoxyphenyl)propenamide With bis-acetylacetonatocobalt(II) dihydrate In tetrahydrofuran at 0 - 20℃; for 18h; Stage #2: trihexylaluminium In tetrahydrofuran; hexane at 0 - 20℃; for 23h; diastereoselective reaction; | 61% |
trihexylaluminium
dimethylsilicon dichloride
A
dimethylhexylsilyl chloride
B
di-n-hexyldimethylsilane
C
dimethylhexylsilane
Conditions | Yield |
---|---|
With potassium chloride at 150℃; for 3h; | A 31% B 58% C 11% |
With potassium chloride at 150℃; for 3h; | A 56% B 34% C 10% |
2-butylcycloprop-2-ene-1,1-dicarboxylic acid dimethyl ester
trihexylaluminium
dimethyl (Z)-2-(2-butyloct-1-enyl)malonate
Conditions | Yield |
---|---|
With iron(III)-acetylacetonate In tetrahydrofuran; hexane at 0 - 20℃; for 16h; stereoselective reaction; | 52% |
trans-(Mo6Cl8)Cl4(tributylphosphine)2
trihexylaluminium
all-trans-(Mo6Cl8)Cl2(n-C6H13)2(tributylphosphine)2
Conditions | Yield |
---|---|
In toluene (N2); a soln. of Al(C6H13)3 added to a suspn. of Mo-compound at -15°C; stirred at -15°C for 20 h; evapd. in vacuo; ether added; ppte. washed with ether; dried in vacuo; dissolved in toluene at 60°C; filtered; concentrated; cooled to -20°C; elem. anal.; | 8% |
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