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Cas:111-68-2
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inquiryHeptylaMine CAS: 111-68-2 Specification Product Name: 1-AMINOHEPTANE Synonyms: 1-Aminoheptan;1-Heptanamine;CH3(CH2)6NH2;n-Heptylamin;N-HEPTYLAMINE, 99+%;n-Heptylamine, 98+%;Heptylamin;Heptanamine CAS: 111-68-2
Cas:111-68-2
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inquirySuperior quality, moderate price & quick delivery. Appearance:white to off-white crystalline powder Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:1kg/bag, 1kg/drum or 25kg/drum or as per your request. Applic
1-Aminoheptane Heptan-1-amine; 1-Heptanamine; 1-Aminoheptane; Heptylamine; CAS: 111-68-2 Molecular formula: C7H17N Molecular weight: 115.21700 Exact quality: 115.13600 PSA: 26.02000 LogP: 2.61580 Physical and chemical properties Den
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1-AMINOHEPTANE CAS NO.111-68-2 Application:1-AMINOHEPTANE CAS NO.111-68-2
1-AMINOHEPTANE CAS NO.111-68-2Appearance:white powder Storage:Sealed,light and oxygen resistant Package:bag/drum Application:industrial grade Transportation:By express (Door to door) such as FEDEX, DHL, EMS for small amount. By air(airport to airport
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Storage:Keep container tightly closed in a dry, cool and well-ventilated place. Package:1Kg/package; 25Kg/package Application:Heptylamine,Used as a solvent, also used in organic synthesis Transportation:By Air, Sea, Courier Port:Shanghai; Qingdao;
1-azidoheptane
1-Heptylamine
Conditions | Yield |
---|---|
With magnesium In methanol for 0.25h; | 98% |
With chloro-trimethyl-silane; sodium iodide In acetonitrile for 0.333333h; Ambient temperature; | 92% |
With samarium diiodide In tetrahydrofuran for 1h; Ambient temperature; | 90% |
Conditions | Yield |
---|---|
With aminedehydrogenase; ammonia; ammonium chloride at 30℃; for 48h; pH=8.7; Enzymatic reaction; | 91% |
Multi-step reaction with 3 steps 1: sulfuric acid; sodium nitrite 2: hydrogen; nickel / 330 - 340 °C 3: nickel; hydrogen / 340 °C View Scheme | |
Multi-step reaction with 3 steps 1.1: pyridine / dichloromethane / 45 h / 0 - 20 °C / Inert atmosphere 2.1: sodium azide / N,N-dimethyl-formamide / 5 h / 80 °C / Inert atmosphere 3.1: triphenylphosphine / tetrahydrofuran / 22 h / 0 - 20 °C / Inert atmosphere 3.2: 2 h / 20 °C / Inert atmosphere View Scheme | |
With L-alanin; D-glucose; pyridoxal 5'-phosphate; alanine dehydrogenase from B. subtilis; catalase from M. lysodeikticus; glucose dehydrogenase from DSM; long-chain alcohol oxidase from Aspergillus fumigatus; w-transaminase from Chromobacterium violaceum; NAD; oxygen; ammonium chloride; flavin adenine dinucleotide In aq. phosphate buffer at 20℃; under 1500.15 Torr; for 24h; pH=10; Enzymatic reaction; | |
With formate dehydrogenase from Candida boidinii; alcohol dehydrogenase from Thermoanaerobacter ethanolicus I86A W110A variant; chimeric amine dehydrogenase generated through domain shuffling of Bb‐PhAmDH variant and L‐AmDH variant, the latter originated from the leucinedehydrogenase from Bacillus stearothermophilus; NADPH oxidase from Bacillus subtilis; nicotinamide adenine dinucleotide phosphate; nicotinamide adenine dinucleotide; catalase In aq. buffer at 30℃; for 12h; pH=8.5; Enzymatic reaction; |
heptylurea
1-Heptylamine
Conditions | Yield |
---|---|
With sodium hydroxide at 70 - 80℃; for 3h; | 90% |
(Z)-7-azidohepta-1,3-diene
1-Heptylamine
Conditions | Yield |
---|---|
With hydrogen; palladium on activated charcoal In ethanol | 90% |
Conditions | Yield |
---|---|
With poly(p-aminostyrene)-palladium(II); hydrogen In N,N-dimethyl-formamide at 70℃; under 760 Torr; for 6h; | 89% |
With iron; acetic acid |
(Z)-7-Azido-hept-3-ene
1-Heptylamine
Conditions | Yield |
---|---|
With hydrogen; palladium on activated charcoal In ethanol | 87% |
Conditions | Yield |
---|---|
With indium(III) chloride; sodium tetrahydroborate In tetrahydrofuran at 25℃; for 4h; Inert atmosphere; | 86% |
Stage #1: heptanenitrile With borane-2-methyltetrahydrofuran complex In 2-methyltetrahydrofuran at 0℃; for 4h; Heating / reflux; Stage #2: With methanol In 2-methyltetrahydrofuran at 0℃; Product distribution / selectivity; | 84.5% |
Stage #1: heptanenitrile With borane-THF In tetrahydrofuran at 0℃; for 4h; Heating / reflux; Stage #2: With methanol In tetrahydrofuran at 0℃; Product distribution / selectivity; | 80.7% |
Conditions | Yield |
---|---|
With 5-methyl-1,3,4-thiadiazol-2-amine; triethylamine In ethanol; water at 25℃; for 1h; | 85% |
With ethanol; ammonia at 100℃; |
N-allylheptan-1-amine
1-Heptylamine
Conditions | Yield |
---|---|
With tert.-butylhydroperoxide; chromia-pillared montmorillonite catalyst (Cr-PILC) In 2,2,4-trimethylpentane; dichloromethane for 22h; Ambient temperature; | 84% |
Conditions | Yield |
---|---|
With propylamine; lithium; tert-butyl alcohol In ethylenediamine at 20 - 53℃; for 1.75h; Reduction; | 55% |
With ethanol; platinum under 2206.5 Torr; Hydrogenation; | |
With ethanol; sodium |
Conditions | Yield |
---|---|
With tert.-butylhydroperoxide; chromium-pillared montmorillonite In 2,2,4-trimethylpentane; dichloromethane for 26h; Ambient temperature; | A 40% B 48% |
methyl N-heptylcarbamate
1-Heptylamine
Conditions | Yield |
---|---|
With sodium hydrogen telluride In N,N-dimethyl-formamide at 70 - 75℃; for 5h; | 45% |
With calcium hydroxide; water |
Conditions | Yield |
---|---|
With sodium hydroxide; sodium bromite In water at 80℃; for 0.5h; | 31% |
With 1,4-dioxane; sodium hypochlorite | |
With potassium hydroxide; bromine | |
Multi-step reaction with 2 steps 1: methanol; bromine 2: calcium hydroxide; water View Scheme |
1-n-heptylthymine
N-butylamine
A
1-Heptylamine
B
N-butylthymine
Conditions | Yield |
---|---|
With pH 9.5 at 35℃; for 60h; Irradiation; | A 16% B 17 % Turnov. |
In water Irradiation; |
Conditions | Yield |
---|---|
With methanol; ammonia; nickel at 150℃; under 110326 Torr; Hydrogenation; | |
With ethanol; ammonia; nickel at 90 - 130℃; under 44130.5 Torr; Hydrogenation; | |
With ethanol; ammonia; hydrogen; nickel | |
Multi-step reaction with 3 steps 1: KOH 2: 89 percent / KOH / 4 h / 160 °C 3: H2O / 20 °C View Scheme | |
With imine reductase from Streptomyces ipomoeae; ammonia; NADPH at 30℃; for 0.166667h; Catalytic behavior; Enzymatic reaction; |
Conditions | Yield |
---|---|
With ammonia; magnesium oxide at 310℃; |
Conditions | Yield |
---|---|
With methanol; ammonia at 25℃; | |
With methanol; ammonia |
Conditions | Yield |
---|---|
With diethyl ether; nickel kieselguhr at 100 - 125℃; under 73550.8 - 110326 Torr; Hydrogenation; | |
With ethanol; nickel kieselguhr at 100 - 125℃; under 73550.8 - 110326 Torr; Hydrogenation; | |
With ethanol; nickel at 15 - 18℃; Hydrogenation; | |
With nickel kieselguhr; methyl cyclohexane at 100 - 125℃; under 73550.8 - 110326 Torr; Hydrogenation; |
Conditions | Yield |
---|---|
With nickel kieselguhr; methyl cyclohexane at 100 - 125℃; under 73550.8 - 110326 Torr; Hydrogenation; | |
With diethyl ether; nickel kieselguhr at 100 - 125℃; under 73550.8 - 110326 Torr; Hydrogenation; | |
With ethanol; nickel kieselguhr at 100 - 125℃; under 73550.8 - 110326 Torr; Hydrogenation; | |
With nickel kieselguhr; 2-Methylcyclohexanone at 100 - 125℃; under 73550.8 - 110326 Torr; Hydrogenation; |
Conditions | Yield |
---|---|
With diethyl ether; nickel kieselguhr at 100 - 125℃; under 73550.8 - 110326 Torr; Hydrogenation; | |
With ethanol; nickel kieselguhr at 100 - 125℃; under 73550.8 - 110326 Torr; Hydrogenation; | |
With nickel kieselguhr; methyl cyclohexane at 100 - 125℃; under 73550.8 - 110326 Torr; Hydrogenation; |
Conditions | Yield |
---|---|
With sodium amalgam; ethanol; acetic acid | |
With ethanol; aluminium amalgam |
Conditions | Yield |
---|---|
at 175℃; Rate constant; |
Conditions | Yield |
---|---|
With ammonia; hydrogen; a fused iron catalyst at 280℃; Product distribution; percent of conversion; |
Conditions | Yield |
---|---|
With water Yield given; |
A
1-Heptylamine
B
alpha cyclodextrin
Conditions | Yield |
---|---|
With phosphate buffer In water-d2 at 25℃; Equilibrium constant; Thermodynamic data; standard molar enthalpy ΔrH0, standard molar Gibbs energy ΔrG0, standard molar entropy ΔrS0; | |
In alkaline aq. solution at 25℃; pH=11.60; Equilibrium constant; dissociation; |
(N-tert-Butyloxycarbonyl)heptylamine
1-Heptylamine
Conditions | Yield |
---|---|
With trifluoroacetic acid Deacylation; |
Conditions | Yield |
---|---|
at 175 - 250℃; under 73550.8 - 220652 Torr; Hydrogenation; |
Conditions | Yield |
---|---|
at 155℃; |
Conditions | Yield |
---|---|
at 155℃; |
1-Heptylamine
pantolactone
N-heptyl-2,4-dihydroxy-3,3-dimethylbutyramide
Conditions | Yield |
---|---|
In methanol at 20℃; for 20h; | 100% |
at 100 - 110℃; | |
at 100 - 110℃; |
Conditions | Yield |
---|---|
100% | |
With diethyl ether |
Conditions | Yield |
---|---|
With potassium carbonate In dichloromethane; water at 0 - 20℃; for 6.5h; | 100% |
In tetrahydrofuran; water | 99% |
In tetrahydrofuran; water | 99% |
In tetrahydrofuran; water | 99% |
With 1,2-dichloro-ethane at -10℃; |
1-Heptylamine
p-toluenesulfonyl chloride
N-heptyl-4-methylbenzenesulfonamide
Conditions | Yield |
---|---|
With dmap; triethylamine In dichloromethane at 0 - 20℃; for 12h; | 100% |
With ethanol | |
With triethylamine In dichloromethane at 0 - 20℃; | |
With triethylamine In dichloromethane at 0 - 25℃; |
1-Heptylamine
4-neopentylbenzoyl chloride
4-(2,2-Dimethyl-propyl)-N-heptyl-benzamide
Conditions | Yield |
---|---|
With triethylamine Ambient temperature; | 100% |
Conditions | Yield |
---|---|
With dmap; triethylamine In dichloromethane at 0 - 20℃; for 12h; | 100% |
With triethylamine In diethyl ether for 0.5h; Heating; | 83% |
In tetrahydrofuran |
Conditions | Yield |
---|---|
at 150℃; Paal-Knorr Pyrrole Synthesis; | 100% |
With Fe(3+)-montmorillonite K10 In dichloromethane at 20℃; for 2h; Paal-Knorr condensation; | 93% |
With [BMIm]I at 25℃; for 0.5h; Paal-Knorr condensation; | 95 % Chromat. |
With aminosulfonic acid at 18℃; for 0.5h; | 98 % Chromat. |
2,4-dichloro-7-methylthieno[3,2-d]pyrimidine
1-Heptylamine
2-chloro-4-heptylamino-7-methylthieno[3,2-d]pyrimidine
Conditions | Yield |
---|---|
In (2S)-N-methyl-1-phenylpropan-2-amine hydrate; N,N-dimethyl-formamide | 100% |
In water; N,N-dimethyl-formamide at 0 - 20℃; for 2h; | 100% |
1-Heptylamine
1-chloro-4-isothiocyanato-2,5-dimethoxybenzene
1-(4-chloro-2,5-dimethoxyphenyl)-3-heptylthiourea
Conditions | Yield |
---|---|
In chloroform at 20℃; | 100% |
Conditions | Yield |
---|---|
With C21H24N2; phenylsilane In tetrahydrofuran at 20℃; under 750.075 - 2250.23 Torr; for 22h; Reagent/catalyst; Solvent; Temperature; Time; Concentration; Inert atmosphere; Glovebox; | 100% |
With C21H39Cl2CoNP2; potassium tert-butylate; hydrogen; sodium triethylborohydride In toluene at 150℃; under 22502.3 Torr; for 36h; Autoclave; | 99% |
With C12H14N4*Ir(1+)*C8H12*I(1-)*C3H7NO; hydrogen In methanol at 100℃; under 45004.5 Torr; for 20h; Autoclave; | 97% |
1-Heptylamine
(7-(carboxymethyl)-1,3,6,8-tetraoxo-3,6,7,8-tetrahydro-1H-benzo[lmn][3,8]phenanthrolin-2-yl)-acetic acid
Conditions | Yield |
---|---|
In methanol at 20℃; | 100% |
Conditions | Yield |
---|---|
With potassium carbonate In dichloromethane at 20℃; for 2.16667h; Inert atmosphere; Reflux; | 100% |
With potassium carbonate In acetone Reflux; | 89% |
Conditions | Yield |
---|---|
Stage #1: bromoacetic acid With N-ethyl-N,N-diisopropylamine In dichloromethane at 20℃; for 1h; Stage #2: 1-Heptylamine In N,N-dimethyl-formamide at 20℃; for 0.666667h; Stage #3: bromoacetic acid Further stages; | 100% |
Conditions | Yield |
---|---|
In methanol for 3h; Ambient temperature; | 99.8% |
With Montmorillonite K10 clay Condensation; microwave irradiation; | |
With magnesium sulfate In dichloromethane at 20℃; | |
With alizarin red S-sensitized TiO2 In acetonitrile for 0.5h; |
Conditions | Yield |
---|---|
With palladium; oxygen; potassium iodide In 1,4-dioxane at 130℃; under 30003 Torr; for 24h; Autoclave; Green chemistry; | 99% |
Stage #1: 1-Heptylamine; carbon monoxide With sulfur at 80℃; under 760.051 Torr; for 4h; Stage #2: With oxygen at 20℃; under 760.051 Torr; for 1h; Further stages.; | 81% |
With iron(III) oxide; selenium; 3-trifluoromethylnitrobenzene In tetrahydrofuran at 64℃; under 760 Torr; for 2h; | 69% |
With oxygen; potassium iodide In neat (no solvent) at 122℃; for 6h; Green chemistry; | 58% |
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid In toluene for 3h; Heating; | 99% |
Conditions | Yield |
---|---|
With C22H22Cl2FeN2O8(2-)*2C16H36N(1+); oxygen In neat (no solvent) at 100℃; under 760.051 Torr; for 0.5h; Green chemistry; | 99% |
With tetrabutylammomium bromide; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione In acetonitrile at 20℃; for 0.0833333h; Inert atmosphere; Molecular sieve; | 89% |
With dichloro(1,5-cyclooctadiene)ruthenium(II); hexamethylenetetramine In toluene for 24h; Schlenk technique; Inert atmosphere; Reflux; | 80% |
With dichloro(benzene)ruthenium(II) dimer; hexamethylenetetramine In toluene for 24h; Schlenk technique; Inert atmosphere; Reflux; Green chemistry; | 72% |
With rhodium(III) chloride hydrate; C13H19N4(1+)*Br(1-) In toluene at 110℃; for 24h; Schlenk technique; Inert atmosphere; | 72% |
Conditions | Yield |
---|---|
With magnesium sulfate In dichloromethane at 20℃; | 99% |
1-Heptylamine
1-(3-chloroquinoxalin-2-yl)-3-phenylprop-2-yn-1-one
1-heptyl-2-phenylpyrido[2,3-b]quinoxalin-4(1H)-one
Conditions | Yield |
---|---|
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In N,N-dimethyl-formamide at 160℃; for 16h; Inert atmosphere; | 99% |
Conditions | Yield |
---|---|
With C24H21ClN2OPRu; potassium tert-butylate In toluene for 24h; Reflux; Inert atmosphere; | 99% |
With potassium tert-butylate; [Ru(PtBuNNHBn)H(CO)Cl] In diethyl ether at 50℃; under 760.051 Torr; for 22h; Reagent/catalyst; Inert atmosphere; | 85% |
Conditions | Yield |
---|---|
With immobilization of Candida cylindracea lipase In hexane at 55℃; for 14h; | 99% |
Conditions | Yield |
---|---|
In water; butan-1-ol at 20℃; for 3h; UV-irradiation; | 99% |
Conditions | Yield |
---|---|
With 4-methyl-morpholine; dmap; 2-chloro-4,6-dimethoxy-1 ,3,5-triazine In dichloromethane for 8h; Heating; | 98% |
Conditions | Yield |
---|---|
With Co2Rh2/C In toluene at 180℃; under 760.051 Torr; for 18h; Autoclave; Inert atmosphere; | 98% |
With hydrogen; nickel at 200℃; under 73550.8 Torr; | |
Multi-step reaction with 2 steps 1: 85 percent / triethylamine / tetrahydrofuran / 0.25 h / 2.5 - 20 °C 2: 84 percent / lithium aluminum hydride / diethyl ether / Heating View Scheme | |
Multi-step reaction with 2 steps 1: 97 percent / DMAP; Et3N / CH2Cl2 / 24 h / 20 °C 2: 99 percent / LiAlH4 / tetrahydrofuran / 24 h / Heating View Scheme |
Conditions | Yield |
---|---|
With pyridine In dichloromethane at 0 - 20℃; | 98% |
With pyridine In dichloromethane at 0 - 20℃; for 1.03333h; | 98% |
With pyridine In benzene |
1-Heptylamine
benzene-1,2-bis(sulphenyl chloride)
N-heptyl-1,3,2-benzodithiazole
Conditions | Yield |
---|---|
With triethylamine In diethyl ether 1.) -20 deg C, 1 h, 2.) RT, 16 h; | 98% |
Conditions | Yield |
---|---|
In benzene for 24h; Substitution; | 98% |
Conditions | Yield |
---|---|
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 20℃; | 98% |
1-Heptylamine
A
4,4-dimethyl-tetrahydro-pyran-2-one
B
N-heptyl-3,3-dimethyl-5-hydroxypentanamide
Conditions | Yield |
---|---|
In toluene | A 98% B n/a |
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