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Cas:111969-64-3
Min.Order:1 Kilogram
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inquiryProduct informations Product Name L-Menthyl glyoxylate hydrate CAS No. 111969-64-3
Cas:111969-64-3
Min.Order:1 Gram
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inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
Cas:111969-64-3
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inquiryWe are very compeitive on Lamivudine .Our mfr is Chinese GMP certified for this item with DMF/CEP document. It has a great function of potassium-sparing diuretics. our advantage of Lamivudine USP/EP/CEP Stable supply. Because the mfr is eq
Cas:111969-64-3
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inquiryAs a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem’s R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis
Cas:111969-64-3
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inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
Cas:111969-64-3
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inquiryAppearance:White to Almost white powder to crystal Storage:R T Package:25kg/Barrel Application:Chemicals Transportation:Express/Sea/Air Port:Any port in China
Cas:111969-64-3
Min.Order:1 Kilogram
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inquiryOur advantages: 1. All inquiries will be replied within 12 hours. 2. Dedication to quality, supply & service. 3. Strictly on selecting raw materials. 4. Reasonable & competitive price, fast lead time. 5. Sample is available for your eva
Cas:111969-64-3
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inquiry1,In No Less five years exporting experience. 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Appearance:White powder Storage:storage in a dr
Cas:111969-64-3
Min.Order:1 Gram
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inquiryOur company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At prese
Cas:111969-64-3
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inquiry(1R,2S,5R)-5-Methyl-2-(1-methylethyl)cyclohexyl dihydroxy-acetate CAS:111969-64-3 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermedia
Cas:111969-64-3
Min.Order:1 Gram
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
Best quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia
Company Introduction 1. Established in 2005, with two independent business divisions: Fine chemicals division; Pharmaceutical division. 2. Main product: Optical brightener Textile auxiliary Dye stuff Pigments
Cas:111969-64-3
Min.Order:1 Gram
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inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
Cas:111969-64-3
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inquiryA substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc
Cas:111969-64-3
Min.Order:4 Kilogram
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Type:Lab/Research institutions
inquiryour strengths: 1: Fast and guaranteed shipment (TNT;EMS;FEDEX;DHL;UPS;EUB, special line) 2: Various payment items accepted (Btc; MoneyGram; WU) 3: Valued package (Paraffin coating; Double aluminum foil bag; Vacuum packaging) 4: Efficient delivery
Cas:111969-64-3
Min.Order:1 Gram
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Type:Other
inquiryProduct name: L-Menthyl Glyoxylate Hydrate CAS No.: 111969-64-3 Molecule Formula:C12H22O4 Molecule Weight:230.30 Purity: 99.0% Package: 25kg/drum Description:White powder Manufacture Standards:Enterprise Standard T
Cas:111969-64-3
Min.Order:1 Kilogram
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Type:Trading Company
inquiryL-Mengchi glyoxylate properties Melting point 76-78 ° C Boiling point 320 ° C The density is 1.09 A flash point of 113 ° C Sensitivity BRN 4905777 CAS Database 111969-64-3 (CAS DataBase Reference) L-Menthyl 2,2-Dihyd
Cas:111969-64-3
Min.Order:100 Gram
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inquiryGMP standard, high purity, competitive price, in stock 1. Quick Response: within 6 hours after receiving your email. 2. Quality Guarantee: All products are strictly tested by our QC, confirmed by QA, and approved by a third-party lab in China, USA,
Cas:111969-64-3
Min.Order:1 Milligram
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inquiryHunan Kaimir Biotechnology Co., Ltd. is a professional technology company specializing in the research and production of raw materials and intermediates. In 2017, it was recognized as a high-tech enterprise and a small technological innovation giant
Product Name: (1R,2S,5R)-5-Methyl-2-(1-methylethyl)cyclohexyl dihydroxy-acetate Synonyms: (1S)-(+)-MENTHYL GLYOXYLATE HYDRATE;Glyoxylic acid (1S)-menthyl ester hydrate;L)-Menthyl glyoxylate monohydrate;(S)-(+)-MENTHYL GLYOXYLATE HYDRATE;(1R,2S,5R
Cas:111969-64-3
Min.Order:100 Gram
Negotiable
Type:Trading Company
inquiry1,we produce and sell good chemicals around the world. 2,our success rate is about 95%. this means, if customer order is accepted, the probability that the customer will obtain the ordered substances, is 95%. 3,our staff consists
Cas:111969-64-3
Min.Order:1 Kilogram
FOB Price: $100.0
Type:Trading Company
inquiryProductName:L-Menthyl glyoxylate hydrate CAS:111969-64-3 Molecular Formula:C12H22O4 Molecular Weight:230.30100 Description:off white to pale yellow crystalline off white Solubility:soluble in methanol Identification:the retention time o
Cas:111969-64-3
Min.Order:10 Gram
Negotiable
Type:Lab/Research institutions
inquiryAppearance:95%+ Package:R&D,Pilot run Transportation:per client require Port:Express ,Air, Sea
Jinlan Pharm-Drugs Technology Co.,Limited (with its export company Hangzhou Royall Import & Export Co.,Ltd.)is located in Hangzhou, Zhejiang Province. Neighboring Ningbo port, Shanghai port, Hangzhou Xiaoshan Int’l Airport and Shanghai Pudong Int’l A
Cas:111969-64-3
Min.Order:0
Negotiable
Type:Other
inquirySuperior quality, moderate price & quick delivery. Appearance:White crystalline powder Storage:stored in a cool, dry and ventilated place to provent sun and rain Package:25kg/drum, or as per your request. Application:For medicine , pesticid
Cas:111969-64-3
Min.Order:1 Kilogram
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Type:Trading Company
inquiryStock products, own laboratory Package:Grams, Kilograms Application:For R&D Transportation:According to customer request Port:Shanghai
Cas:111969-64-3
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiryWe are a Union of chemistry in China, consists of chemists,engineers, laboratories,factories in China. We organize surplus capacity of R&D and production as well as custom synthesis for chemical products and chemical business project. We are supp
Cas:111969-64-3
Min.Order:0
Negotiable
Type:Trading Company
inquiryLower price, sample is available,SDS test documents are available,large stock in warehouseAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:Fine chemical intermediates, used as the main raw material for the synthe
Cas:111969-64-3
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiryL-menthol glyoxylate monohydrate
Conditions | Yield |
---|---|
With formaldehyd; water In cyclohexane at 25℃; for 4h; pH=6.7 - 7.7; | 86% |
B
L-menthol glyoxylate monohydrate
Conditions | Yield |
---|---|
With formaldehyd; water In cyclohexane at 20℃; for 16h; pH=6.7 - 7.7; | A 10% B 70% |
(1R,2S,5R)-2-isopropyl-5-methylcyclohexyl 2-chloro-2-oxoacetate
A
L-menthyl glyoxylate
B
L-menthol glyoxylate monohydrate
Conditions | Yield |
---|---|
With tri-n-butyl-tin hydride; tetrakis(triphenylphosphine) palladium(0) 1.) PhH, r.t., 2 h, 2.) PhH, CH2Cl2, reflux, 1 h; Title compound not separated from byproducts; |
(1R,2S,5R)-2-isopropyl-5-methylcyclohexyl 2-chloro-2-oxoacetate
L-menthol glyoxylate monohydrate
Conditions | Yield |
---|---|
With water; tri-n-butyl-tin hydride; tetrakis(triphenylphosphine) palladium(0) 1.) PhH, r.t., 2 h; PhH, CH2Cl2, reflux, 1 h; Multistep reaction; |
(-)-menthol
L-menthol glyoxylate monohydrate
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: CHCl3 / 2 h / Ambient temperature 2: Bu3SnH / Pd(Ph3P)4 / 1.) PhH, r.t., 2 h, 2.) PhH, CH2Cl2, reflux, 1 h View Scheme | |
Multi-step reaction with 2 steps 1: CHCl3 / 2 h / Ambient temperature 2: 1.) Bu3SnH, 2.) H2O / 1.) Pd(Ph3P)4 / 1.) PhH, r.t., 2 h; PhH, CH2Cl2, reflux, 1 h View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: sulfuric acid / cyclohexane / 5 h / Reflux 2: sodium hydrogensulfite / cyclohexane; water / 8 h / 25 - 30 °C / pH 4.5 - 5.5 3: formaldehyd; water / cyclohexane / 16 h / 20 °C / pH 6.7 - 7.7 View Scheme |
(-)-menthol
L-menthol glyoxylate monohydrate
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: sulfuric acid / cyclohexane / 5 h / Reflux 2: sodium hydrogensulfite / cyclohexane; water / 8 h / 25 - 30 °C / pH 4.5 - 5.5 3: formaldehyd; water / cyclohexane / 4 h / 25 °C / pH 6.7 - 7.7 View Scheme | |
Multi-step reaction with 3 steps 1: sulfuric acid / cyclohexane / 4 h / 79 - 80 °C 2: sodium hydrogensulfite; sodium carbonate / water / 1.5 h / 50 °C / pH 4.7 - 5.4 3: water; formaldehyd; sodium carbonate / 0.5 h / 20 °C View Scheme | |
Multi-step reaction with 3 steps 1: sulfuric acid / cyclohexane / Reflux 2: sodium carbonate / -75 - 80 °C / pH 4 - 5 3: acetaldehyde / cyclohexane / 2.5 h / 0 - 40 °C View Scheme |
L-menthyl glyoxylate
L-menthol glyoxylate monohydrate
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: sodium hydrogensulfite / cyclohexane; water / 8 h / 25 - 30 °C / pH 4.5 - 5.5 2: formaldehyd; water / cyclohexane / 4 h / 25 °C / pH 6.7 - 7.7 View Scheme |
L-menthol glyoxylate monohydrate
Conditions | Yield |
---|---|
With formaldehyd; water; sodium carbonate at 20℃; for 0.5h; |
A
L-menthol glyoxylate monohydrate
B
potassium 1-hydroxyethane-1-sulfonate
Conditions | Yield |
---|---|
With acetaldehyde In cyclohexane at 0 - 40℃; for 2.5h; |
B
L-menthol glyoxylate monohydrate
(-)-menthol
Glyoxilic acid
A
bis[(1R,2S,5R)-2-isopropyl-5-methylcyclohexyl]oxalate
B
L-menthol glyoxylate monohydrate
Conditions | Yield |
---|---|
With Amberlyst-15 In acetonitrile at 120℃; under 7500.75 Torr; Reagent/catalyst; Microwave irradiation; |
1,4-dithiane-2,5-diol
L-menthol glyoxylate monohydrate
(1R,2S,5R)-2-isopropyl-5-methylcyclohexyl 5-hydroxy-1,3-oxathiolane-2-carboxylate
Conditions | Yield |
---|---|
Stage #1: L-menthyl glyoxylate monohydrate With acetic acid In toluene at 110 - 115℃; Stage #2: 1,4-dithiane-2,5-diol In toluene Heating; | 100% |
Stage #1: 1,4-dithiane-2,5-diol With acetic acid In acetonitrile at 40 - 45℃; for 0.166667h; Stage #2: L-menthyl glyoxylate monohydrate In acetonitrile at 90℃; for 0.166667h; | 88% |
Stage #1: L-menthyl glyoxylate monohydrate With acetic acid In toluene at 110 - 111℃; for 3h; Stage #2: 1,4-dithiane-2,5-diol In toluene at 85 - 90℃; for 2h; Stage #3: With triethylamine In n-heptane at 0 - 5℃; for 6h; | 80% |
Stage #1: L-menthyl glyoxylate monohydrate With acetic acid In toluene at 120℃; for 2h; Dean-Stark; Stage #2: 1,4-dithiane-2,5-diol In toluene for 4h; Reflux; Stage #3: With triethylamine In hexane; toluene at 0℃; for 16h; |
1,4-dithiane-2,5-diol
L-menthol glyoxylate monohydrate
(2R,5R)-5-hydroxy-1,3-oxathiolane-2-carboxylic acid (1R,2S,5R)-5-methyl-2-isopropylcyclohexyl ester
Conditions | Yield |
---|---|
With acetic acid In acetone at 50 - 125℃; Temperature; Solvent; | 88% |
Stage #1: 1,4-dithiane-2,5-diol; L-menthyl glyoxylate monohydrate In toluene Stage #2: With triethylamine In hexane; toluene | 80% |
With acetic acid In toluene at 50 - 115℃; | 100 g |
trimethylsilyl cyanide
L-menthol glyoxylate monohydrate
Conditions | Yield |
---|---|
With ytterbium(III) triflate In dichloromethane for 2h; Ambient temperature; | 82% |
L-menthol glyoxylate monohydrate
N-benzyl hydroxylalmine
C19H27NO3
Conditions | Yield |
---|---|
In benzene for 1.5h; Heating; | 80.7% |
L-menthol glyoxylate monohydrate
allyl-trimethyl-silane
Conditions | Yield |
---|---|
With methanesulfonic acid In dichloromethane at 25℃; for 15h; Hosomi-Sakurai reaction; | 72% |
p,p'-dimethoxybenzhydrylamine
L-menthol glyoxylate monohydrate
[(E)-Bis-(4-methoxy-phenyl)-methylimino]-acetic acid (1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl ester
Conditions | Yield |
---|---|
In toluene Heating; |
L-menthol glyoxylate monohydrate
L-menthyl glyoxylate
Conditions | Yield |
---|---|
With pyridinium p-toluenesulfonate In benzene for 4h; Heating; |
L-menthol glyoxylate monohydrate
(1R,2S,5R)-2-isopropyl-5-methylcyclohexyl (2R,5S)-5-(4-amino-2-oxo-1,2-dihydro-1-pyrimidinyl)-1,3-oxathialane-2-carbaxylate
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: toluene 1.2: 80 percent / Et3N / toluene; hexane 2.1: SOCl2 / dimethylformamide; CH2Cl2 View Scheme | |
Multi-step reaction with 4 steps 1.1: acetic acid / acetonitrile / 0.17 h / 40 - 45 °C 1.2: 0.17 h / 90 °C 2.1: pyridine / acetonitrile / 20 °C 2.2: 0.08 h / 20 °C 3.1: triethylamine / hexane / 36 h / -20 °C 4.1: pyridinium triflate / acetonitrile / 0.14 h / 80 °C / 517.16 Torr / Flow reactor View Scheme | |
Multi-step reaction with 3 steps 1.1: acetic acid / acetone / 50 - 125 °C 2.1: pyridine / acetone; dichloromethane / 20 °C 2.2: 24 h / -10 °C 3.1: acetonitrile / 0.17 h 3.2: 2 h / 80 °C View Scheme |
L-menthol glyoxylate monohydrate
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: toluene 1.2: 80 percent / Et3N / toluene; hexane 2.1: SOCl2 / dimethylformamide; CH2Cl2 View Scheme |
L-menthol glyoxylate monohydrate
5S-chloro-[1,3]oxathiolane-2R-carboxilic acid 2-(1'R,2'S,5'R)-isopropyl-5-methyl-cyclohexyl ester
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: toluene 1.2: 80 percent / Et3N / toluene; hexane 2.1: SOCl2 / dimethylformamide; CH2Cl2 View Scheme |
L-menthol glyoxylate monohydrate
(3S,4R)-3-<(R)-1'-hydroxyethyl>-4-(-)menthyloxycarbonyl-1-dimethyl-t-butylsilylazetidin-2-one
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1: 80.7 percent / benzene / 1.5 h / Heating 2: benzene / 5 h / Heating 3: H2 / platinum oxide / methanol / 50 h / Ambient temperature 4: DCC / acetonitrile / 3 h / 60 °C 5: 23 percent / triethylamine / dimethylformamide / 24 h / Ambient temperature View Scheme |
L-menthol glyoxylate monohydrate
Conditions | Yield |
---|---|
Multi-step reaction with 6 steps 1: 80.7 percent / benzene / 1.5 h / Heating 2: benzene / 5 h / Heating 3: H2 / platinum oxide / methanol / 50 h / Ambient temperature 4: DCC / acetonitrile / 3 h / 60 °C 5: 56 percent / triethylamine / dimethylformamide / 24 h / Ambient temperature 6: 48 percent / aqueous sodium hydroxide / tetrahydrofuran; methanol / 8 h / Ambient temperature View Scheme |
L-menthol glyoxylate monohydrate
(3S,4S)-3-<(R)-1'-hydroxyethyl>-4-(-)-menthyloxycarbonylazetidin-2-one
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: 80.7 percent / benzene / 1.5 h / Heating 2: 30 percent / benzene / 5 h / Heating 3: H2 / platinum oxide / methanol / 20 h / Ambient temperature 4: DCC / acetonitrile / 3 h / 60 °C View Scheme |
L-menthol glyoxylate monohydrate
(3S,4R)-3-<(R)-1'-hydroxyethyl>-4-(-)-menthyloxycarbonylazetidin-2-one
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: 80.7 percent / benzene / 1.5 h / Heating 2: benzene / 5 h / Heating 3: H2 / platinum oxide / methanol / 50 h / Ambient temperature 4: DCC / acetonitrile / 3 h / 60 °C View Scheme |
L-menthol glyoxylate monohydrate
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 80.7 percent / benzene / 1.5 h / Heating 2: 30 percent / benzene / 5 h / Heating 3: H2 / platinum oxide / methanol / 20 h / Ambient temperature View Scheme |
L-menthol glyoxylate monohydrate
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 80.7 percent / benzene / 1.5 h / Heating 2: benzene / 5 h / Heating 3: H2 / platinum oxide / methanol / 50 h / Ambient temperature View Scheme |
L-menthol glyoxylate monohydrate
(3S,4S)-4-(-)-menthyloxycarbonyl-1-dimethyl-t-butylsilyl-3-<(R)-1-(dimethyl-t-butylsilyloxy)ethyl>azetidin-2-one
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1: 80.7 percent / benzene / 1.5 h / Heating 2: 30 percent / benzene / 5 h / Heating 3: H2 / platinum oxide / methanol / 20 h / Ambient temperature 4: DCC / acetonitrile / 3 h / 60 °C 5: 80 percent / triethylamine / dimethylformamide / 16 h / Ambient temperature View Scheme |
L-menthol glyoxylate monohydrate
(3S,4R)-3-<(R)-1'-(dimethyl-t-butylsilyloxy)ethyl>-4-(-)-menthyloxycarbonyl-1-dimethyl-t-butylsilylazetidin-2-one
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1: 80.7 percent / benzene / 1.5 h / Heating 2: benzene / 5 h / Heating 3: H2 / platinum oxide / methanol / 50 h / Ambient temperature 4: DCC / acetonitrile / 3 h / 60 °C 5: 56 percent / triethylamine / dimethylformamide / 24 h / Ambient temperature View Scheme |
L-menthol glyoxylate monohydrate
(3R,4S,5R)-2-benzyl-4-benzyloxycarbonyl-3-(-)-menthyloxycarbonyl-5-methylisoxazolidine
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 80.7 percent / benzene / 1.5 h / Heating 2: benzene / 5 h / Heating View Scheme |
L-menthol glyoxylate monohydrate
(3S,4S,5R)-2-benzyl-4-benzyloxycarbonyl-3-(-)-menthyloxycarbonyl-5-methylisoxazolidine
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 80.7 percent / benzene / 1.5 h / Heating 2: 30 percent / benzene / 5 h / Heating View Scheme |
L-menthol glyoxylate monohydrate
(3S,4R,5S)-2-benzyl-4-benzyloxycarbonyl-3-(-)-menthyloxycarbonyl-5-methylisoxazolidine
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 80.7 percent / benzene / 1.5 h / Heating 2: benzene / 5 h / Heating View Scheme |
L-menthol glyoxylate monohydrate
(2S,3S)-1-[Bis-(4-methoxy-phenyl)-methyl]-4-oxo-3-vinyl-azetidine-2-carboxylic acid (1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl ester
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: toluene / Heating View Scheme |
L-menthol glyoxylate monohydrate
(2R,3R)-1-[Bis-(4-methoxy-phenyl)-methyl]-4-oxo-3-vinyl-azetidine-2-carboxylic acid (1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl ester
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: toluene / Heating View Scheme |
L-menthol glyoxylate monohydrate
L-menthyl 5-cytosin-1-yl-1,3-oxathiolane-2-carboxylate
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: acetic acid / toluene / 110 - 115 °C 1.2: Heating 2.1: thionyl chloride / N,N-dimethyl-formamide / dichloromethane / 5 - 30 °C 3.1: chloro-trimethyl-silane; 1,1,1,3,3,3-hexamethyl-disilazane / dichloromethane / 110 - 120 °C 3.2: 30 - 35 °C View Scheme |
L-menthol glyoxylate monohydrate
C14H23ClO3S
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: acetic acid / toluene / 110 - 115 °C 1.2: Heating 2.1: thionyl chloride / N,N-dimethyl-formamide / dichloromethane / 5 - 30 °C View Scheme |
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