As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem’s R&D center offer custom synthesis according to the contract research and development services for t
Cas:116-02-9
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inquiryWelcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our
Cas:116-02-9
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inquiryhigh quality Appearance:White or off-white Solid Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea Port:shanghai
Cas:116-02-9
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inquiry1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s
Cas:116-02-9
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inquiryOur main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
Cas:116-02-9
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inquirychengdu and import and export trade co., LTD., who registered capital of 10 million yuan, nearly to $2 million, we have a pharmaceutical raw materials factory production of pharmaceutical raw materials, and a reagent r&d center, and we do res
Cas:116-02-9
Min.Order:100 Kilogram
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Type:Trading Company
inquiryOur Advantage Rich Experience Our products are sold all over Europe,North&South America, Sino-East, Asia and pacific area as well as Africa,we establish long term. Quality service Company cooperates with research institutes. We strictly con
Cas:116-02-9
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inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
Cas:116-02-9
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inquiry1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized
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inquiry3,3,5-Trimethylcyclohexanol CAS:116-02-9 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic
Cas:116-02-9
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inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
Cas:116-02-9
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
Cas:116-02-9
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inquiryTriumph has the complete production of G- KG - MT service chain,we can make the new technology into productivity quickly in the research and development of new products. Main Service 1.Own made fine chemical products 2.Out sourcing and qualit
Cas:116-02-9
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inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
Cas:116-02-9
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inquiryadvantage: 1. The best price, satisfactory quality; 2. customers have the right to choose the delivery of parcels (EMS, DHL, FedEx, UPS); 3. customers have the right to choose from the recent effective packaging methods of their products packaging
Cas:116-02-9
Min.Order:1 Gram
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inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:116-02-9
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inquirySuperior quality, moderate price & quick delivery. Appearance:WHITE CRYSTALLINE MASS Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:25kg/drum;200kg/drum as per your request Application:Is synthesis of mandeli
Cas:116-02-9
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inquiryProduct Name: 3,3,5-Trimethylcyclohexanol Synonyms: 1-methyl-3-dimethylcyclohexanol-5;3,3,5-trimethyl;3,3,5-trimethyl-cyclohexano;3,3,5-Trimethylcyclohexanol (c,t);3,3,5-Trimethylcyclohexanol,c&t;3,3,5-trimethylcyclohexanol,mixture
Cas:116-02-9
Min.Order:1 Metric Ton
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inquiryProduct name: 3,3,5-Trimethylcyclohexanol CAS No.:116-02-9 Molecule Formula:C9H18O Molecule Weight:142.24 Purity: 98.0% Package: 25kg/drum Description:White crystalline powder Manufacture Standards:Enterprise Standard
Cas:116-02-9
Min.Order:1 Kilogram
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inquiryGMP standard, high purity, competitive price, in stock 1. Quick Response: within 6 hours after receiving your email. 2. Quality Guarantee: All products are strictly tested by our QC, confirmed by QA, and approved by a third-party lab in China, USA,
Cas:116-02-9
Min.Order:1 Milligram
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inquiryAppearance:95%+ Package:R&D,Pilot run Transportation:per client require Port:Express ,Air, Sea
We are a Union of chemistry in China, consists of chemists,engineers, laboratories,factories in China. We organize surplus capacity of R&D and production as well as custom synthesis for chemical products and chemical business project. We are supp
high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou
high purity,in stock Package:25kg/drum,or as per customers'demand Application:API,Pharmaceutical intermediates Transportation:air,sea,courier
Cas:116-02-9
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inquiryJinhua huayi chemical co., ltd. is dedicated to the development, production and marketing of chemicals. On the basis of equality and mutual benefit, and under the principle of customer first, credit first, quality first, we are ready to join hands
Cas:116-02-9
Min.Order:100 Gram
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inquiryOur clients, like BASF,CHEMO,Brenntag,ASR,Evonik,Merck and etc.Appearance:COA Storage:in stock Application:MSDS/TDS
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Cas:116-02-9
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inquiryAnsciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali
Cas:116-02-9
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inquiryConditions | Yield |
---|---|
With zinc hydride In tetrahydrofuran for 24h; Ambient temperature; | 100% |
Stage #1: dihydroisophorone In diethyl ether for 12h; Stage #2: With sodium tetrahydroborate In diethyl ether; ethanol for 6h; Reagent/catalyst; Reflux; | 97% |
With magnesium; mercury dichloride In ethanol at 20℃; for 12h; | 92% |
3,5,5-Trimethylcyclohex-2-en-1-one
A
3,3,5-trimethylcyclohexanol
B
dihydroisophorone
Conditions | Yield |
---|---|
With NiCRASi In tetrahydrofuran at 45℃; for 0.75h; | A n/a B 88% |
With hydrogen In tetrahydrofuran at 24.84℃; under 15001.5 Torr; for 2h; Reagent/catalyst; Solvent; Time; | A 26.5% B 72.5% |
With potassium bis(trimethylsilyl)amide In tetrahydrofuran at 25℃; for 5h; | A 8.5 % Chromat. B 83.0 % Chromat. |
With bis[1-butyl-2-(diphenylphosphanyl)-3-methylimidazolium]tetrachloridoruthenium(III) hexafluorophosphate; potassium tert-butylate; isopropyl alcohol at 100℃; for 2h; Inert atmosphere; Autoclave; | |
With hydrogen In hexane at 25℃; under 7500.75 Torr; for 16h; Reagent/catalyst; Autoclave; |
3,5,5-Trimethylcyclohex-2-en-1-one
A
3,3,5-trimethylcyclohexanol
B
(R)-3,3,5-trimethylcyclohexanone
Conditions | Yield |
---|---|
With (R)-((4,4’-bi-1,3-benzodioxole)-5,5’-diyl)bis(bis(3,5-di-t-butyl-4-methoxyphenyl))phosphine; bis(triphenylphosphane)copper(I) nitrate; hydrogen; sodium t-butanolate In isopropyl alcohol at 30℃; under 37503.8 Torr; for 18h; optical yield given as %ee; enantioselective reaction; | A n/a B 51% |
Conditions | Yield |
---|---|
With isopropyl alcohol; Ni(0) nanoparticles In tetrahydrofuran at 76℃; for 1h; | 39% |
With ethanol; sodium of Knoevenagel as 'trans-form' designated substance; | |
With diethyl ether; sodium of Knoevenagel as 'trans-form' designated substance; | |
With hydrogen In hexane at 25℃; under 7500.75 Torr; for 16h; Autoclave; | n/a |
With 5%-palladium/activated carbon; water; aluminium at 50℃; for 1h; Temperature; | 100 %Chromat. |
4,6-dimethylbicyclo<4.1.0>heptan-2-one
A
3,3,5-trimethylcyclohexanol
B
dihydroisophorone
Conditions | Yield |
---|---|
With triethylamine In acetonitrile Irradiation; | A 15% B 10% |
With triethylamine In acetonitrile for 5h; Mechanism; effect of lithium perchlorate; |
Conditions | Yield |
---|---|
With potassium hydroxide for 4h; Ambient temperature; | 8% |
Mechanism; Product distribution; Irradiation; |
3,5,5-Trimethylcyclohex-2-en-1-one
A
3,3,5-trimethylcyclohexanol
B
1.1'-Dioxy-3.3.5.3'.3'.5'-hexamethyl-dicyclohexyl-(1.1')
Conditions | Yield |
---|---|
With diethyl ether; sodium |
3,5,5-Trimethylcyclohex-2-en-1-one
A
isophorol
B
3,3,5-trimethylcyclohexanol
Conditions | Yield |
---|---|
With potassium tri-sec-butyl-borohydride In tetrahydrofuran at 0℃; for 1h; | A 84.6 % Chromat. B 5.8 % Chromat. |
With potassium bis(trimethylsilyl)amide In tetrahydrofuran at -78℃; for 10h; | A 53.9 % Chromat. B 19.7 % Chromat. |
With zinc-modified cyanobrohydride In diethyl ether for 6h; Ambient temperature; Yield given; |
3,5,5-Trimethylcyclohex-2-en-1-one
A
isophorol
B
3,3,5-trimethylcyclohexanol
C
dihydroisophorone
Conditions | Yield |
---|---|
With Li(1+)*C12H28AlO3(1-) In tetrahydrofuran; hexane at -78℃; for 3h; Yield given. Yields of byproduct given; | |
With lithium aluminium tetrahydride; cryptand 211 In tetrahydrofuran for 2h; Ambient temperature; Yield given. Yields of byproduct given; | |
With sodium hydroxide; sodium tetrahydroborate In 1,4-dioxane; water at 24.9℃; Rate constant; regioselectivity of reduction investigated; |
Conditions | Yield |
---|---|
under 760 Torr; |
diethyl ether
carbon dioxide
dihydroisophorone
A
3,3,5-trimethylcyclohexanol
B
2,4,4-trimethyl-6-oxo-cyclohexanecarboxylic acid
Conditions | Yield |
---|---|
Behandeln mit Wasser; |
3,5,5-Trimethylcyclohex-2-en-1-one
A
3,3,5-trimethylcyclohexanol
B
dihydroisophorone
Conditions | Yield |
---|---|
at 180℃; under 70 - 75 Torr; beim Leiten ueber Nickel; |
3,3,5-trimethylcyclohexanol
Conditions | Yield |
---|---|
With hydrogen iodide; acetic acid; zinc of Knoevenagel as 'cis-form' designated substance; |
carbon dioxide
dihydroisophorone
A
3,3,5-trimethylcyclohexanol
B
2,4,4-trimethyl-6-oxo-cyclohexanecarboxylic acid
Conditions | Yield |
---|---|
With diethyl ether; sodium |
3,5,5-Trimethylcyclohex-2-en-1-one
A
isophorol
B
3,3,5-trimethylcyclohexanol
C
(R)-3,3,5-trimethylcyclohexanone
Conditions | Yield |
---|---|
With bis(triphenylphosphane)copper(I) nitrate; hydrogen; (2S,4S)-2,4-bis(diphenylphosphino)pentane; sodium t-butanolate In isopropyl alcohol at 30℃; under 37503.8 Torr; for 18h; enantioselective reaction; | |
With hydrogen; (2S,4S)-2,4-bis(diphenylphosphino)pentane; sodium t-butanolate; (R)-segphos In isopropyl alcohol at 30℃; under 37503.8 Torr; for 18h; enantioselective reaction; |
3,5,5-Trimethylcyclohex-2-en-1-one
A
3,3,5-trimethylcyclohexanol
B
dihydroisophorone
C
1,1,3-trimethylcyclohexane
Conditions | Yield |
---|---|
With carbon dioxide; hydrogen at 350℃; under 90009 Torr; Supercritical conditions; Flow reactor; | A 21 %Chromat. B 50 %Chromat. C 28 %Chromat. |
3,5,5-Trimethylcyclohex-2-en-1-one
A
(+)-3,3,5(S)-trimethylcyclohexanone
B
3,3,5-trimethylcyclohexanol
Conditions | Yield |
---|---|
With dicarbonylacetylacetonato rhodium (I); (1S,1′S)-(-)-(2,7-di-tert-butyl-9,9-dimethyl-9H-xanthene-4,5-diyl)bis((2-ethoxy-phenyl)(phenyl)phosphine); hydrogen In toluene at 40℃; under 7500.75 - 37503.8 Torr; for 8h; Reagent/catalyst; Solvent; Autoclave; | A n/a B n/a |
3,5,5-Trimethylcyclohex-2-en-1-one
A
(+)-3,3,5(S)-trimethylcyclohexanone
B
3,3,5-trimethylcyclohexanol
C
(R)-3,3,5-trimethylcyclohexanone
Conditions | Yield |
---|---|
With (acetylacetonato)dicarbonylrhodium (l); (1S,1′S)-(+)-(9,9-dimethyl-9H-xanthene-4,5-diyl)bis((2-methoxyphenyl)(phenyl)phosphine); hydrogen In toluene at 40℃; under 37503.8 Torr; for 8h; Solvent; Reagent/catalyst; Autoclave; enantioselective reaction; | A n/a B n/a C n/a |
With acetylacetonato(1,5-cyclooctadiene)rhodium(I); (1S,1′S)-(+)-(9,9-dimethyl-9H-xanthene-4,5-diyl)bis((2-methoxyphenyl)(phenyl)phosphine); hydrogen In toluene at 40℃; under 37503.8 Torr; for 8h; Reagent/catalyst; Solvent; Autoclave; enantioselective reaction; | A n/a B n/a C n/a |
3,3,5-trimethylcyclohexanol
MANDELIC ACID
cyclandelate
Conditions | Yield |
---|---|
With C12H22O3Zr*2C8F17O3S(1-) In acetonitrile at 10℃; for 4h; | 95% |
3,3,5-trimethylcyclohexanol
Benzoylformic acid
3,3,5-trimethylcyclohexyl 2-oxo-2-phenylacetate
Conditions | Yield |
---|---|
With dmap; dicyclohexyl-carbodiimide In dichloromethane at 0℃; for 0.333333h; | 92% |
Conditions | Yield |
---|---|
Stage #1: 3,3,5-trimethylcyclohexanol With ammonium tungstate In water at 20℃; for 0.25h; Green chemistry; Stage #2: With dihydrogen peroxide In water at 70℃; for 11h; Green chemistry; | 90% |
With imidazolium dichromate In N,N-dimethyl-formamide for 24h; Ambient temperature; | 87% |
With sodium dichromate; sulfuric acid at 55℃; | |
With potassium dichromate; sulfuric acid at 55℃; |
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