DayangChem exported this product to many countries and regions at best price in China. If you are looking for the product’s supplier in China, DayangChem is your best choice. Pls contact with us freely for getting detailed product specifica
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inquiryOur Advantages: Geographical advantages: the processing base is located in Jiangsu Coastal Chemical Industrial Park with convenient transportation, good human, economic and social environment, and huge potential for market development; Technol
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inquiryWelcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our
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inquiryhigh quality Appearance:white powder Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea Port:shanghai
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inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
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inquiryOur main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
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inquiryCAS No.121-17-5 Our company was built in 2009 with an ISO certificate.In the past 5 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scie
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inquiryProduct Name 4-Chloro-3-nitrobenzotrifluoride Synonyms TIMTEC-BB SBB009923;1-chloro-2-nitro-4-(trifluoromethyl)-benzen;2-Chloro-5-(trifluoromethyl)nitrobenzene;3-Nitro-4-(chloro)trifluoromethylbenzene;3-N
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inquiryMinimum Order Qty. 10 Gram Supply Ability 500 Kilograms/Month Storage store in cool, dry, ventilated place 20℃ Delivery Time 3 business days after payment Payment Term TT,western union,Paypal,MoneyGram Package 10g,20g,50g,100g,500g,1KGS,
Cas:121-17-5
Min.Order:10 Gram
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inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
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inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
Cas:121-17-5
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inquiryMassive Chemical is certified with ISO9001 and ISO14001 manufacturer for this product. We will offer all documents as requirement for the materials which includes, Certificate of Analysis, Material Safety Data Sheet, and Method of Analysis and
Cas:121-17-5
Min.Order:1 Gram
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inquiry4-Chloro-3-nitrobenzotrifluorideAppearance:Pls see the Details Storage:Keep away of light, hot, water, Store in dry, dark and ventilated place Package:according to customers' requirements Application:Steroids, Cosmetics Ingredients, APIs, Intermediat
Product Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
Cas:121-17-5
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inquiry1)quick response within 12 hours; 2)quality guarantee: all products are strictly tested by our qc, confirmed by qa and approved by third party lab in china, usa, canada, germany, uk, italy, france etc. 3) oem/odm available; 4) rea
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inquiryAppearance:95%+ Package:R&D,Pilot run Transportation:per client require Port:Express ,Air, Sea
Superior quality, moderate price & quick delivery. Appearance:light yellow liquid Storage:stored in a cool, dry and ventilated place to provent sun and rain Package:25kg/drum, or as per your request. Application:Used as Pharmaceutical Inter
Cas:121-17-5
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inquiryOur company is engaged in customizing the benzene ring and pyridine derivative organic intermediates, and the quantity is flexible according to customer's needs. It mainly provides high-quality intermediates for domestic and foreign pharmaceutical an
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inquiryhigh purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou
high purity,in stock Package:25kg/drum,or as per customers'demand Application:API,Pharmaceutical intermediates Transportation:air,sea,courier
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inquiryJinhua huayi chemical co., ltd. is dedicated to the development, production and marketing of chemicals. On the basis of equality and mutual benefit, and under the principle of customer first, credit first, quality first, we are ready to join hands
Cas:121-17-5
Min.Order:100 Gram
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inquiryOur clients, like BASF,CHEMO,Brenntag,ASR,Evonik,Merck and etc.Appearance:COA Storage:in stock Application:MSDS/TDS
Cangzhou Enke Pharma Tech Co.,ltd. is located in Cangzhou City, Hebei province ,where is a famous petroleum chemical industry city?in China. Enke Pharma a high-tech enterprise ,and we are dedicated to developing and manufacturing new api,?intermediat
Ansciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali
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inquiryProduct Description Description & Specification Category Pharmaceutical Raw Materials, Fine Chemicals, Bulk drug Standard Medical standard
Cas:121-17-5
Min.Order:1 Kilogram
FOB Price: $112.0
Type:Trading Company
inquiryAmoychem is committed to providing the top-quality chemical products and services Internationally. We offer our customers with friendly, professional service and reliable, high performance products that have been manufactured according to the accredi
TIANFUCHEM--High purity 121-17-5 4-Chloro-3-nitrobenzotrifluoride Application:TIANFUCHEM--High purity 121-17-5 4-Chloro-3-nitrobenzotrifluoride
Cas:121-17-5
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inquiryreagent grade ex stockAppearance:white or off-white crystalline powder Storage:Keep away of light,cool place Package:1L 5L 10L 25L bottle Application:pharma intermediate Transportation:by Fedex, ship or plane
Cas:121-17-5
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inquiryHangzhou ZeErRui Chemical Co., Ltd. located in Lingang industrial areas, our plant covers an area of 6000 square meters.ZeErRui dedicated to the development, production and marketing of chemicals. We have earned ourselves a good reputation at home an
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inquiryTIANFUCHEM--High purity 121-17-5 4-Chloro-3-nitrobenzotrifluorideAppearance:powder Storage:room tempurature Package:As required Application:medical Transportation:By express (Door to door) such as FEDEX, DHL, EMS for small amount. By air(airport to
Cas:121-17-5
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inquiryConditions | Yield |
---|---|
With ammonium nitrate; 3-(N,N-dimethyldodecylammonium)propanesulfonic acid hydrogen sulphate at 70℃; for 9h; Temperature; | 85% |
With sulfuric acid; nitric acid | 73.2% |
With sulfuric acid; nitric acid |
Conditions | Yield |
---|---|
Stage #1: 4-Chloro-3-nitroaniline With hydrogenchloride In water at 0℃; for 0.0833333h; Inert atmosphere; Schlenk technique; Stage #2: With tert.-butylnitrite at 0℃; for 0.25h; Inert atmosphere; Schlenk technique; Stage #3: trifluoromethylsilver at -78 - 20℃; for 4h; Inert atmosphere; Schlenk technique; | 81% |
Stage #1: 4-Chloro-3-nitroaniline With hydrogenchloride In water at 0℃; for 0.0833333h; Sandmeyer Reaction; Schlenk technique; Stage #2: With tert.-butylnitrite In water at -196 - 20℃; Sandmeyer Reaction; Schlenk technique; Inert atmosphere; Stage #3: trifluoromethylsilver In water at -78 - 20℃; for 5h; Sandmeyer Reaction; Schlenk technique; Inert atmosphere; | 81% |
Conditions | Yield |
---|---|
With copper(l) iodide; oxygen; copper(l) chloride In dimethyl sulfoxide at 160℃; under 760.051 Torr; for 30h; Schlenk technique; Sealed tube; | 44% |
With 2.9-dimethyl-1,10-phenanthroline; oxygen; copper (I) acetate; silver sulfate; sodium chloride In dimethyl sulfoxide at 160℃; for 24h; Schlenk technique; | 20% |
With 2.9-dimethyl-1,10-phenanthroline; oxygen; copper diacetate; silver sulfate; sodium chloride In dimethyl sulfoxide at 160℃; under 760.051 Torr; for 20h; Schlenk technique; | 16% |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: hydrogen fluoride / 110 °C / 7355.08 - 10297.1 Torr 2: Nitrierung View Scheme |
piperazine
2-chloro-3-nitro-5-trifluoromethylbenzene
1,4-Bis(1'-nitro-3'-(trifluoromethyl)-6'-phenyl)piperazine
Conditions | Yield |
---|---|
With triethylamine In tetrahydrofuran at 100℃; under 6000480 Torr; for 120h; | 100% |
piperidine
2-chloro-3-nitro-5-trifluoromethylbenzene
1-(2-nitro-4-(trifluoromethyl)phenyl)piperidine
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide at 0℃; for 0.666667h; Product distribution / selectivity; | 100% |
With N,N,N',N'-tetramethyl-1,8-diaminonaphthalene In various solvent(s) at 26.84℃; Kinetics; Further Variations:; Reagents; | |
In acetonitrile at 25℃; Kinetics; Further Variations:; amine concentration; |
2-chloro-3-nitro-5-trifluoromethylbenzene
Conditions | Yield |
---|---|
With potassium cyanocarbonimidodithioate In N,N-dimethyl-formamide at 80 - 90℃; for 24h; | 99% |
With selenium; sodium thiosulfate In dimethyl sulfoxide | 50% |
With sodium disulfide In ethanol |
2-chloro-3-nitro-5-trifluoromethylbenzene
N-<2-chloro-5-(trifluoromethyl)phenyl>hydroxylamine
Conditions | Yield |
---|---|
With 5% rhodium-on-charcoal; hydrazine hydrate In tetrahydrofuran at 0℃; for 1.5h; Inert atmosphere; | 99% |
With 5% rhodium-on-charcoal; hydrazine hydrate In tetrahydrofuran at 0℃; Inert atmosphere; | 99% |
With ammonium chloride; zinc In ethanol; water for 0.5h; Heating; | 90% |
With sodium hypophosphite; palladium on activated charcoal In tetrahydrofuran | |
With 5% rhodium-on-charcoal; hydrazine hydrate In tetrahydrofuran at 0 - 20℃; Inert atmosphere; |
2-chloro-3-nitro-5-trifluoromethylbenzene
phenylboronic acid
2-nitro-4-(trifluoromethyl)-1,1'-biphenyl
Conditions | Yield |
---|---|
With bis(η3-allyl-μ-chloropalladium(II)); N,N,N',N'-tetra(diphenylphosphinomethyl)benzene-1,3-diamine; potassium carbonate In N,N-dimethyl acetamide at 130℃; for 20h; Time; Concentration; Suzuki-Miyaura Coupling; Inert atmosphere; Schlenk technique; | 99% |
With potassium carbonate; bis(η3-allyl-μ-chloropalladium(II)); Tedicyp In xylene at 130℃; for 20h; Suzuki reaction; | 95% |
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In water; toluene for 4h; Suzuki-Miyaura cross coupling; Heating; | 91% |
With potassium phosphate; tetraphosphine N,N,N′,N′-tetra(diphenylphosphinomethyl)-pyridine-2,6-diamine; palladium dichloride In toluene at 120℃; for 72h; Reagent/catalyst; Solvent; Temperature; Suzuki-Miyaura Coupling; Inert atmosphere; Schlenk technique; | 91% |
isobutylamine
2-chloro-3-nitro-5-trifluoromethylbenzene
N-isobutyl-2-nitro-4-(trifluoromethyl)aniline
Conditions | Yield |
---|---|
With triethylamine In tetrahydrofuran for 20h; Heating; | 99% |
2-chloro-3-nitro-5-trifluoromethylbenzene
Conditions | Yield |
---|---|
With 1,3-dibromo-5,5-dimethylimidazolidine-2,4-dione; sulfuric acid at 15℃; for 18h; | 99% |
ethanolamine
2-chloro-3-nitro-5-trifluoromethylbenzene
2-((2-nitro-4-(trifluoromethyl)phenyl)amino)ethanol
Conditions | Yield |
---|---|
With potassium carbonate In ethanol for 5h; Reflux; | 98% |
With potassium carbonate In butan-1-ol for 4.5h; Reflux; | 97% |
Heating; | 95% |
dibromodifluoromethane
2-chloro-3-nitro-5-trifluoromethylbenzene
1,4-Bis(trifluoromethyl)-2-nitro-benzene
Conditions | Yield |
---|---|
With copper In N,N-dimethyl acetamide at 100℃; for 4h; Product distribution; with or without charcoal; | 98% |
With copper; pyrographite In N,N-dimethyl acetamide at 100℃; for 2h; | 98 % Turnov. |
2-chloro-3-nitro-5-trifluoromethylbenzene
N-butylamine
N-butyl-2-nitro-4-(trifluoromethyl)aniline
Conditions | Yield |
---|---|
With potassium carbonate In butan-1-ol at 145℃; for 15h; | 98% |
In N,N-dimethyl-formamide at 80℃; for 4h; | 90.5% |
With sodium hydroxide; tetrabutylammomium bromide In water; benzene at 31℃; Product distribution; Rate constant; various amines under different reaction conditions; | |
for 3.5h; Heating; | |
In acetonitrile at 25℃; Kinetics; Further Variations:; amine concentration; |
2-chloro-3-nitro-5-trifluoromethylbenzene
phenol
2-nitro-1-phenoxy-4-(trifluoromethyl)benzene
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 100℃; Inert atmosphere; | 98% |
With 18-crown-6 ether; Methyl trichloroacetate; potassium carbonate at 150℃; for 2h; | 72% |
With potassium hydroxide In ethanol at 45℃; for 2h; |
Conditions | Yield |
---|---|
at 90℃; for 1h; | 98% |
at 90℃; |
2-chloro-3-nitro-5-trifluoromethylbenzene
diethyl malonate
diethyl 2-(2-nitro-4-(trifluoromethyl)phenyl)malonate
Conditions | Yield |
---|---|
With potassium carbonate; sodium hydroxide In N,N-dimethyl-formamide at 45℃; for 1h; | 98% |
Conditions | Yield |
---|---|
With potassium hydroxide In N,N-dimethyl-formamide at 30℃; for 1h; | 98% |
Conditions | Yield |
---|---|
Stage #1: nitromethane With sodium hydroxide In 1-methyl-pyrrolidin-2-one at 5℃; for 0.5h; Stage #2: 2-chloro-3-nitro-5-trifluoromethylbenzene In 1-methyl-pyrrolidin-2-one at 5℃; for 2h; | 98% |
2-hydroxybromobenzene
2-chloro-3-nitro-5-trifluoromethylbenzene
1-(2-bromophenoxy)-2-nitro-4-(trifluoromethyl)benzene
Conditions | Yield |
---|---|
With potassium carbonate In dimethyl sulfoxide at 100℃; Inert atmosphere; | 97% |
With sodium methylate In ethanol at 195℃; | |
With potassium hydroxide |
2-chloro-3-nitro-5-trifluoromethylbenzene
ethyl 2-cyanoacetate
Ethyl 2-cyano-2-(2-nitro-4-(trifluoromethyl)phenyl)acetate
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 50℃; for 1h; | 97% |
With N,N,N',N'-tetramethylguanidine In dichloromethane at 50℃; under 3878.71 Torr; Reagent/catalyst; Solvent; Temperature; Flow reactor; | 96% |
With potassium carbonate In N,N-dimethyl-formamide at 100℃; | 74% |
With potassium carbonate In N,N-dimethyl-formamide | |
With sodium ethanolate 1.) EtOH, 2.) EtOH, reflux, 8 h; Multistep reaction; |
dibromodifluoromethane
2-chloro-3-nitro-5-trifluoromethylbenzene
A
1,4-Bis(trifluoromethyl)-2-nitro-benzene
B
4-Pentafluoroethyl-3-nitro-benzotrifluoride
Conditions | Yield |
---|---|
With ISOPROPYLAMIDE; copper at 100℃; for 8h; | A 97% B 3% |
2-chloro-3-nitro-5-trifluoromethylbenzene
1-(indolyl-2-carbonyl)-4-<2-nitro-4-(trifluoromethyl)phenyl>piperazine
Conditions | Yield |
---|---|
With potassium carbonate In acetonitrile for 4h; Ambient temperature; | 97% |
thiophenol
2-chloro-3-nitro-5-trifluoromethylbenzene
(2-nitro-4-(trifluoromethyl)phenyl)phenylthioether
Conditions | Yield |
---|---|
With ethylenediamine; copper(l) chloride In water at 120℃; for 36h; Inert atmosphere; | 97% |
With sodium In methanol at 20℃; | 85% |
With sodium hydroxide In ethanol; water | |
With potassium hydroxide; copper In ethanol; water |
benzyl 2-cyanoacetate
2-chloro-3-nitro-5-trifluoromethylbenzene
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 70℃; for 24h; | 97% |
copper(I) cyanide
2-chloro-3-nitro-5-trifluoromethylbenzene
2-nitro-4-trifluoromethyl-benzonitrile
Conditions | Yield |
---|---|
lithium bromide In tetrahydrofuran at 130℃; for 6h; Product distribution / selectivity; | 97% |
In acetonitrile at 110℃; for 6h; Product distribution / selectivity; | 93% |
lithium bromide In acetonitrile at 110℃; for 6h; Product distribution / selectivity; | 91% |
decylthiol
2-chloro-3-nitro-5-trifluoromethylbenzene
4-decylthio-3-nitrobenzotrifluoride
Conditions | Yield |
---|---|
With sodium methylate In methanol | 96.9% |
2-chloro-3-nitro-5-trifluoromethylbenzene
6-trifluoromethyl-1-hydroxybenzotriazole
Conditions | Yield |
---|---|
With hydrazine hydrate In ethanol for 24h; Heating; | 96% |
With hydrazine hydrate In ethanol; sodium carbonate | |
With hydrazine hydrate In ethanol for 24h; Reflux; | |
With hydrazine hydrate In ethanol for 24h; Reflux; |
2-chloro-3-nitro-5-trifluoromethylbenzene
2,5-dimethoxyaniline
2,5-Dimethoxy-2'-nitro-4'-trifluoromethyldiphenylamine
Conditions | Yield |
---|---|
With 1-methyl-pyrrolidin-2-one; potassium carbonate at 140℃; | 96% |
Conditions | Yield |
---|---|
With potassium phosphate; bis(η3-allyl-μ-chloropalladium(II)); tetraphosphine N,N,N′,N′-tetra(diphenylphosphinomethyl)-pyridine-2,6-diamine In N,N-dimethyl acetamide; water at 100℃; for 20h; Catalytic behavior; Time; Sonogashira Cross-Coupling; Schlenk technique; Inert atmosphere; | 96% |
With potassium carbonate; bis(η3-allyl-μ-chloropalladium(II)); (1RS,2RS,3SR,4SR)-1,2,3,4-tetrakis((diphenylphosphanyl)methyl)cyclopentane In N,N-dimethyl-formamide at 100℃; for 20h; Sonogashira cross-coupling; | 91% |
2-chloro-3-nitro-5-trifluoromethylbenzene
5-trifluoromethylbenzofuroxan
Conditions | Yield |
---|---|
With sodium azide; N-ethyl-N-methylpyrrolidinium tetrafluoroborate; tetrabutylammomium bromide In water at 60℃; for 4h; | 96% |
1,2,3-Benzotriazole
2-chloro-3-nitro-5-trifluoromethylbenzene
1-[2-nitro-4-(trifluoromethyl)phenyl]-1H-1,2,3-benzotriazole
Conditions | Yield |
---|---|
With copper(l) iodide; N-[phenyl(acetylamino)methyl]acetamide; sodium methylate In dimethyl sulfoxide at 130℃; for 12h; | 95% |
With copper 2-phenylcyclopropanecarboxylate; cetyltrimethylammonim bromide; potassium carbonate In xylene for 8h; Arylation; Heating; | 89% |
With copper(l) iodide; (E)-3-(dimethylamino)-1-(2-hydroxyphenyl)prop-2-en-1-one; caesium carbonate In acetonitrile at 82℃; for 12h; Ullmann type coupling; Inert atmosphere; | 89% |
With triethylamine In N,N-dimethyl-formamide at 100℃; for 17h; | 87% |
2-Mercaptobenzothiazole
2-chloro-3-nitro-5-trifluoromethylbenzene
2-((2-nitro-4-(trifluoromethyl)phenyl)thio)benzo[d]thiazole
Conditions | Yield |
---|---|
With triethylamine In N,N-dimethyl-formamide at 70℃; for 1.5h; | 95% |
Conditions | Yield |
---|---|
at 20℃; for 3h; Irradiation; | 95% |
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