As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem's R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis ch
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inquiry1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s
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inquiryShanghai Seasonsgreen Chemical is a high-tech research and development, production, sale and custom synthesis set in one high-tech chemical products enterprises. Our sales and marketing division is located in Shanghai, serving international pharmaceu
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inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
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inquiryOur Advantage Rich Experience Our products are sold all over Europe,North&South America, Sino-East, Asia and pacific area as well as Africa,we establish long term. Quality service Company cooperates with research institutes. We strictly con
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inquiryOur Adwantage: 1.We have stock so we can delivery quickly at the very day when receive the payment. 2.Best price, first class service, high successful delivery rate. A discount would be given when you make a large order. 3.High quality gua
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inquiry1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized
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inquiryWuhan hanweishi Pharmchem Co., Ltd(Hanways chempharm) is a specialized company concentrating on the R&D, production, marketing and technical service of APIs and pharmaceutical intermediates. The leading products range are APIs, Hormones, Peptides
Cas:136236-51-6
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inquiryOur company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At present
Cas:136236-51-6
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inquiryRasagiline CAS:136236-51-6 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic intermediates
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inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
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inquirySuperior quality, moderate price & quick delivery. Appearance:NA Storage:Sealed in a cool ,dry and microtherm place , avoid light . Package:1kg/bag, 1kg/drum or 25kg/drum or as per your request. Application:It is an important raw material and
Our Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We
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inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
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inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:136236-51-6
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inquiryEstablished in May 2015, TaiChem Ltd. is initially invested by a British research and development company and started by PhDs back from aboard. The company is registered in China Medical City (CMC), Taizhou, Jiangsu Province, and the production site
The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providing h
1H-Inden-1-amine,2,3-dihydro-N-2-propyn-1-yl-, (1R)- (R)-2,3-DIHYDRO-N-2-PROPYNYL-1H-INDEN-1-AMINE;Rasagiline -13C3;Rasagiline;(R)-N-2-Propynyl-1-indanamine;1H-Inden-1-amine, 2,3-dihydro-N-2-propynyl-, (1R);1-Indanamine, N-2-propynyl-, (R)-;Unii-
factory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B
Cas:136236-51-6
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inquiryHunan chemfish Pharmaceutical co.,Ltd.located in Lugu High-tech industral park ,Hunan province . with its own R&D center and more than 10000㎡manufacture plant . Chemfish owns 40 reactors from 1000L to 8000L. With complete auxiliary equipment as
Cas:136236-51-6
Min.Order:0 Metric Ton
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Type:Manufacturers
inquiryZhenyu biotech exported this product to many countries and regions at best price. if you are looking for the material's manufacturer or supplier in china, zhenyu biotech is your best choice. pls contact with us freely for getting detailed
Cas:136236-51-6
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inquiryProduct Name: Rasagiline Synonyms: (R)-2,3-DIHYDRO-N-2-PROPYNYL-1H-INDEN-1-AMINE;Rasagiline -13C3;Rasagiline;(R)-N-2-Propynyl-1-indanamine;1H-Inden-1-amine, 2,3-dihydro-N-2-propynyl-, (1R);1-Indanamine, N-2-propynyl-, (R)-;Unii-003N66ts6t;(R)-N
Shandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W
1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer
Cas:136236-51-6
Min.Order:1 Metric Ton
FOB Price: $1.5
Type:Trading Company
inquiryGOLDEN PHARMA CO.,LIMITED.is a professional pharmaceutical company,our team have more than 20years expereince in pharmaceutical production and sales. we are a professional technical enterprise specializing in the R & D, production,QA regulation
Stock products, own laboratory Package:Grams, Kilograms Application:For R&D Transportation:According to customer request Port:Shanghai
Cas:136236-51-6
Min.Order:0
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Type:Lab/Research institutions
inquiryWe are a Union of chemistry in China, consists of chemists,engineers, laboratories,factories in China. We organize surplus capacity of R&D and production as well as custom synthesis for chemical products and chemical business project. We are supp
Cas:136236-51-6
Min.Order:1 Metric Ton
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Type:Trading Company
inquiryISO Factory/Good qualityAppearance:off white Storage:dry and cool place Package:10G/BAG; 1KG/BAG ;25KG/DRUM Application:Active pharaceutical ingredients Transportation:BY SEA,AIR,EXPRESS Port:SHANGHAI;BEIJING
rasagiline
Conditions | Yield |
---|---|
With sodium hydroxide In water; toluene at 45℃; for 0.25h; pH=13 - 14; | 96% |
With sodium hydroxide In water; toluene at 45℃; for 0.25h; Product distribution / selectivity; | 92% |
With sodium hydroxide In water pH=11.98; Product distribution / selectivity; | n/a |
(R)-tert-butyl 2,3-dihydro-1H-inden-1-yl(prop-2-ynyl)carbamate
rasagiline
Conditions | Yield |
---|---|
Stage #1: (R)-tert-butyl 2,3-dihydro-1H-inden-1-yl(prop-2-ynyl)carbamate With hydrogenchloride; water In 1,4-dioxane at 20℃; for 0.5h; Inert atmosphere; Stage #2: With sodium hydrogencarbonate In 1,4-dioxane; water Inert atmosphere; | 95% |
rasagiline mesylate
rasagiline
Conditions | Yield |
---|---|
With sodium hydroxide In water at 3 - 5℃; for 1h; pH=7.5 - 11; Product distribution / selectivity; | 91.6% |
With sodium hydroxide In water at 3 - 5℃; pH=11; | 91.6% |
With sodium hydroxide In water; toluene pH=~ 14; | |
With sodium hydroxide In water; toluene pH=14; |
R-(+)-N-propargyl-1-aminoindane L-(+)-mandelate
rasagiline
Conditions | Yield |
---|---|
With sodium hydroxide | 90% |
(R)-N-(2-chloroallyl)-2,3-dihydro-1H-inden-1-amine
rasagiline
Conditions | Yield |
---|---|
With sodium t-butanolate In ISOPROPYLAMIDE at 0 - 5℃; for 2.16667h; Product distribution / selectivity; Inert atmosphere; | 82% |
Conditions | Yield |
---|---|
With potassium carbonate In acetonitrile at 60℃; for 16h; | 79% |
With potassium carbonate In acetonitrile at 60℃; for 16h; |
Conditions | Yield |
---|---|
With sodium hydroxide In water; toluene at 30 - 50℃; Product distribution / selectivity; | 74.56% |
propargyl benzenesulfonate
rasagiline
Conditions | Yield |
---|---|
With sodium hydroxide In toluene at 30℃; for 29h; | 65.8% |
With sodium hydroxide In toluene at 30℃; for 29h; | 65.8% |
Stage #1: (R)-2,3-dihydro-1H-inden-1-amine hydrochloride With tetrabutylammomium bromide; sodium hydroxide In water at 15 - 20℃; for 0.25h; Stage #2: propargyl benzenesulfonate In water at 15 - 20℃; for 2.75h; | |
Stage #1: (R)-2,3-dihydro-1H-inden-1-amine hydrochloride With tetrabutylammomium bromide; sodium hydroxide In water at 15 - 20℃; for 0.25h; Stage #2: propargyl benzenesulfonate In water at 15 - 20℃; for 2.75h; | 81.0 g |
(R)-N-indan-1-yl-4-nitro-N-prop-2-ynyl-benzenesulfonamide
rasagiline
Conditions | Yield |
---|---|
With 1,8-diazabicyclo[5.4.0]undec-7-ene; 2-hydroxyethanethiol | 64% |
Conditions | Yield |
---|---|
With potassium carbonate In acetonitrile at 30℃; for 12h; Reflux; | 59.7% |
With N-ethyl-N,N-diisopropylamine In acetonitrile at 80℃; for 0.166667h; Flow reactor; | 58% |
With triethylamine In tetrahydrofuran at 50℃; |
INDANE
rasagiline
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: Rh2[(S)-(adamantan-1-yl)(tetrachlorophthalimido)CHCOO]4; PhI(OAc)2 / various solvent(s) / 3 h / 23 °C 2: 75 percent / K2CO3 3: 64 percent / DBU; HSC2H4OH View Scheme |
(R)-N-indan-1-yl-4-nitrobenzenesulfonamide
rasagiline
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 75 percent / K2CO3 2: 64 percent / DBU; HSC2H4OH View Scheme |
Conditions | Yield |
---|---|
In dichloromethane at -29 - 20℃; | A n/a B n/a |
rasagiline
Conditions | Yield |
---|---|
With sodium hydroxide In water; toluene | |
With sodium hydroxide In water at 20℃; |
Conditions | Yield |
---|---|
With sodium hydroxide In water; toluene at 40 - 50℃; pH=14; Product distribution / selectivity; |
R-(-)-N-(2,3 dibromopropyl)-1-aminoindan
rasagiline
Conditions | Yield |
---|---|
With potassium hydroxide In denaturated industrial spirit; water at 80 - 90℃; for 5h; |
Conditions | Yield |
---|---|
Stage #1: (R)-1-Aminoindane With 1,8-diazabicyclo[5.4.0]undec-7-ene In tetrahydrofuran at 0 - 5℃; Stage #2: propargyl p-toluenesulfonate In tetrahydrofuran at 0 - 25℃; Stage #3: With sodium hydroxide In water for 0.25h; | |
Stage #1: (R)-1-Aminoindane With 1,8-diazabicyclo[5.4.0]undec-7-ene In tetrahydrofuran at 0 - 5℃; Stage #2: propargyl p-toluenesulfonate In tetrahydrofuran at 15 - 20℃; |
2,3-dihydro-1H-inden-1-amine
rasagiline
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: sodium hydroxide / toluene; water / 4.95 h / 20 - 47 °C / Inert atmosphere; Industry scale 2: isopropyl alcohol; water / 25 °C / Reflux; Inert atmosphere; Industry scale; Resolution of racemate 3: sodium hydroxide / toluene; water / 40 - 47 °C / Industry scale; Inert atmosphere View Scheme | |
Multi-step reaction with 3 steps 1: potassium carbonate; N,N-dimethyl-formamide; sodium hydroxide / 7 h / 40 - 70 °C 2: 0.75 h / 25 - 65 °C 3: sodium hydroxide / water / 20 °C View Scheme | |
Multi-step reaction with 3 steps 1: Candida antarctica lipase B; Pd/AlO(OH); potassium carbonate / toluene / 12 h / 50 °C / Resolution of racemate; Inert atmosphere; Schlenk technique; Enzymatic reaction 2: triethanolamine; sodium hydroxide / water / 6.25 h / 80 °C / Reflux 3: potassium carbonate / acetonitrile / 12 h / 30 °C / Reflux View Scheme | |
Multi-step reaction with 5 steps 1: ethanol; tert-butyl methyl ether / 20 °C 2: ethanol / 2.32 h / 79 °C 3: sodium hydroxide / ethyl acetate / 0.5 h / 20 °C 4: hydrogenchloride / isopropyl alcohol / 0.5 h / 5 - 20 °C / Inert atmosphere 5: sodium hydroxide / toluene / 29 h / 30 °C View Scheme |
rasagiline
Conditions | Yield |
---|---|
With sodium hydroxide In water; toluene at 40 - 47℃; Industry scale; Inert atmosphere; |
inden-1-one
rasagiline
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1.1: toluene-4-sulfonic acid / tert-butyl methyl ether / 8 h 1.2: 1 h / -70 - -30 °C 2.1: diisobutylaluminium hydride / toluene; hexane / 1 h / -70 - -30 °C 2.2: 1 h / 20 °C 3.1: tert-butyl methyl ether / 21 h / 10 °C / Heating 4.1: sodium hydroxide View Scheme | |
Multi-step reaction with 5 steps 1: hydroxylamine hydrochloride; sodium hydroxide / water; methanol / 70 - 75 °C 2: hydrogen; ammonia / Raney nickel / methanol / 10 - 42 °C / Autoclave 3: potassium carbonate; N,N-dimethyl-formamide; sodium hydroxide / 7 h / 40 - 70 °C 4: 0.75 h / 25 - 65 °C 5: sodium hydroxide / water / 20 °C View Scheme | |
Multi-step reaction with 5 steps 1: hydroxylamine hydrochloride / ethanol; water / 0.75 h / Reflux 2: palladium 10% on activated carbon; hydrogen / ethanol / 4 h / 70 °C 3: Candida antarctica lipase B; Pd/AlO(OH); potassium carbonate / toluene / 12 h / 50 °C / Resolution of racemate; Inert atmosphere; Schlenk technique; Enzymatic reaction 4: triethanolamine; sodium hydroxide / water / 6.25 h / 80 °C / Reflux 5: potassium carbonate / acetonitrile / 12 h / 30 °C / Reflux View Scheme |
N-(2,3-dihydroinden-1-ylidene)prop-2-yn-1-amine
rasagiline
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: diisobutylaluminium hydride / toluene; hexane / 1 h / -70 - -30 °C 1.2: 1 h / 20 °C 2.1: tert-butyl methyl ether / 21 h / 10 °C / Heating 3.1: sodium hydroxide View Scheme |
N-trifluoroacetyl-(R)-1-aminoindan
rasagiline
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: caesium carbonate / acetonitrile / 0.17 h / 30 - 35 °C 1.2: 4 h / 30 - 35 °C 2.1: potassium hydroxide / water; methanol / 30 - 35 °C View Scheme | |
Multi-step reaction with 2 steps 1: caesium carbonate / acetonitrile; toluene / 30 - 35 °C 2: potassium hydroxide; water / methanol / 0.5 h / 30 - 35 °C View Scheme |
rasagiline
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: pyridine / dichloromethane / 0.58 h / 20 °C / Ice bath 2.1: caesium carbonate / acetonitrile / 0.17 h / 30 - 35 °C 2.2: 4 h / 30 - 35 °C 3.1: potassium hydroxide / water; methanol / 30 - 35 °C View Scheme |
C14H12F3NO
rasagiline
Conditions | Yield |
---|---|
With potassium hydroxide In methanol; water at 30 - 35℃; | |
With water; potassium hydroxide In methanol at 30 - 35℃; for 0.5h; | 14.3 g |
N-propargyl-1-aminoindan
rasagiline
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 0.75 h / 25 - 65 °C 2: sodium hydroxide / water / 20 °C View Scheme |
indan-1-one oxime
rasagiline
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: hydrogen; ammonia / Raney nickel / methanol / 10 - 42 °C / Autoclave 2: potassium carbonate; N,N-dimethyl-formamide; sodium hydroxide / 7 h / 40 - 70 °C 3: 0.75 h / 25 - 65 °C 4: sodium hydroxide / water / 20 °C View Scheme | |
Multi-step reaction with 4 steps 1: palladium 10% on activated carbon; hydrogen / ethanol / 4 h / 70 °C 2: Candida antarctica lipase B; Pd/AlO(OH); potassium carbonate / toluene / 12 h / 50 °C / Resolution of racemate; Inert atmosphere; Schlenk technique; Enzymatic reaction 3: triethanolamine; sodium hydroxide / water / 6.25 h / 80 °C / Reflux 4: potassium carbonate / acetonitrile / 12 h / 30 °C / Reflux View Scheme | |
Multi-step reaction with 6 steps 1: ammonia; hydrogen / methanol / 20 h / 42 °C / 2625.26 Torr 2: ethanol; tert-butyl methyl ether / 20 °C 3: ethanol / 2.32 h / 79 °C 4: sodium hydroxide / ethyl acetate / 0.5 h / 20 °C 5: hydrogenchloride / isopropyl alcohol / 0.5 h / 5 - 20 °C / Inert atmosphere 6: sodium hydroxide / toluene / 29 h / 30 °C View Scheme |
Conditions | Yield |
---|---|
Stage #1: (R)-2,3-dihydro-1H-inden-1-amine hydrochloride With potassium carbonate In acetonitrile at 60 - 62℃; for 1h; Stage #2: propargyl bromide In acetonitrile for 28h; Concentration; Time; | 22 g |
Conditions | Yield |
---|---|
With Chiralcel-OJ-H (4-methylbenzoate cellulose coated on silica) column In ethanol; hexane; diethylamine; isopropyl alcohol at 27℃; Temperature; Solvent; Resolution of racemate; |
Conditions | Yield |
---|---|
In ethanol; water for 2h; Product distribution / selectivity; | 100% |
In water; isopropyl alcohol at 40℃; for 1h; |
Conditions | Yield |
---|---|
In acetone for 2h; | 100% |
Conditions | Yield |
---|---|
In di-isopropyl ether for 1.5h; | 100% |
Conditions | Yield |
---|---|
In di-isopropyl ether for 1.5h; | 100% |
Conditions | Yield |
---|---|
In acetone for 2h; | 100% |
Conditions | Yield |
---|---|
Stage #1: sodium docusate With hydrogenchloride In dichloromethane; water Stage #2: rasagiline In acetone for 2h; Product distribution / selectivity; | 100% |
Conditions | Yield |
---|---|
In acetone | 100% |
In isopropyl alcohol at 20℃; Cooling with ice; | 63% |
sodium 4-dodecylbenzenesulfonate
rasagiline
rasagiline 4-dodecylbenzenesulfonate
Conditions | Yield |
---|---|
With acetic acid In water; acetone for 2h; | 100% |
benzenesulfonic acid
rasagiline
R-(+)-N-propargyl-1-aminoindan besylate
Conditions | Yield |
---|---|
In toluene at 20℃; Product distribution / selectivity; | 99.5% |
In ethyl acetate at 10 - 25℃; for 3h; Product distribution / selectivity; |
rasagiline
[14C]-Rasagiline hydrochloride
Conditions | Yield |
---|---|
With hydrogenchloride In tert-butyl methyl ether at 10 - 15℃; for 0.5h; Product distribution / selectivity; | 99% |
With hydrogenchloride In diethyl ether Product distribution / selectivity; Cooling with ice; | |
With hydrogenchloride In water; isopropyl alcohol at 40℃; for 2h; Product distribution / selectivity; |
Conditions | Yield |
---|---|
In di-isopropyl ether for 1.5h; Inert atmosphere; | 99% |
Conditions | Yield |
---|---|
In di-isopropyl ether for 1.5h; Product distribution / selectivity; Inert atmosphere; | 99% |
Conditions | Yield |
---|---|
In tert-butyl methyl ether at 5 - 10℃; for 0.5h; Solvent; Acidic conditions; | 99% |
Conditions | Yield |
---|---|
In isopropyl alcohol for 1h; Reflux; | 98% |
In toluene; acetonitrile at 40 - 80℃; Product distribution / selectivity; | 86.2% |
In isopropyl alcohol at 5 - 10℃; for 0.5h; | 83% |
Conditions | Yield |
---|---|
In di-isopropyl ether for 1.5h; Inert atmosphere; | 96% |
Conditions | Yield |
---|---|
In di-isopropyl ether for 1.5h; Product distribution / selectivity; Inert atmosphere; | 94% |
Conditions | Yield |
---|---|
In isopropyl alcohol | 93.1% |
rasagiline
(1R)-2,3-dihydro-N-2-propynyl-1H-indane-1-amine hydrobromide
Conditions | Yield |
---|---|
With hydrogen bromide In isopropyl alcohol at 5 - 10℃; for 0.5h; | 90% |
With hydrogen bromide at 25 - 65℃; for 0.5h; Product distribution / selectivity; |
hydrogen bromide
rasagiline
(1R)-2,3-dihydro-N-2-propynyl-1H-indane-1-amine hydrobromide
Conditions | Yield |
---|---|
In isopropyl alcohol at 5 - 10℃; for 0.5h; | 90% |
L-Tartaric acid
rasagiline
Conditions | Yield |
---|---|
In isopropyl alcohol at 40℃; for 2.16667h; | 88% |
In methanol; butanone for 1.16667h; Solvent; Time; Temperature; Reflux; | 72% |
In isopropyl alcohol at 40℃; for 2h; Product distribution / selectivity; |
naphthalene-1,5-disulfonate
rasagiline
Conditions | Yield |
---|---|
In isopropyl alcohol at 20℃; Cooling with ice; | 86% |
(S)-Mandelic acid
rasagiline
R-(+)-N-propargyl-1-aminoindane L-(+)-mandelate
Conditions | Yield |
---|---|
In isopropyl alcohol at 20℃; Heating; Cooling with ice; | 85% |
In n-heptane; isopropyl alcohol | |
In ethyl acetate; isopropyl alcohol at 20℃; for 24h; Heating; |
1-hexadecylcarboxylic acid
rasagiline
(1R)-2,3-dihydro-N-2-propynyl-1H-indane-1-amine palmitate
Conditions | Yield |
---|---|
In isopropyl alcohol at 5 - 10℃; for 0.5h; | 85% |
In isopropyl alcohol at 5 - 10℃; for 0.5h; | 85% |
Conditions | Yield |
---|---|
In isopropyl alcohol Heating; Cooling with ice; | 84% |
(1S)-10-camphorsulfonic acid
rasagiline
rasagiline (1S)-(+)-10-camphorsulfonate
Conditions | Yield |
---|---|
In methanol at 20℃; for 1h; | 79% |
In n-heptane; isopropyl alcohol |
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