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Cas:13750-62-4
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inquiryHigh quality 1-Benzyl-2-methyl-1H-imidazole CAS 13750-62-4 with factory price Company profile Wuhan Fortuna Chemical Co.,Ltd established in 2006, is a big integrative chemical enterprise being engaged in Pharmaceutical & its intermediates, F
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inquiry1-Benzyl-2-methyl-1H-imidazole Basic information Product Name: 1-Benzyl-2-methyl-1H-imidazole Synonyms: N-BENZYL-2-METHYLIMIDAZOLE;2-methyl-1-(phenylmethyl)-1h-imidazol;2-methyl-1-(pheny
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inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
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inquiryProduct name :1-Benzyl-2-methylimidazole CAS NO : 13750-62-4 Brown Liquid Assay(GC)≥98.0% Water≤0.5% Product name :1-Benzyl-2-methylimidazole CAS NO : 13750-62-4 Brown Liquid Assay(GC)≥98.0
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inquiryAbout Product Details Items Specifications Test Results Appearance White to white crystalline powde
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inquiry1-Benzyl-2-methyl-1H-imidazole CAS:13750-62-4 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality or
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inquiryProduct name: 1-Benzyl-2-Methylimidazole CAS No.:13750-62-4 Molecule Formula:C11H12N2 Molecule Weight:172.23 Purity: 99.0% Package: 25kg/drum Description:Brown liquid Manufacture Standards:Enterprise Standard TESTI
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inquiryConditions | Yield |
---|---|
Stage #1: 2-methylimidazole With sodium hydride at -0.16℃; Schlenk technique; Inert atmosphere; Stage #2: benzyl bromide In tetrahydrofuran Inert atmosphere; Schlenk technique; Reflux; | 99% |
With sodium hydroxide In water at 20℃; for 0.333333h; Temperature; Micellar solution; | 93% |
With N,N,N',N'',N'''-pentamethyldiethylenetriamine; potassium tert-butylate; copper(I) bromide In toluene at 20℃; for 9.5h; Inert atmosphere; | 90% |
With potassium carbonate In acetonitrile at 70℃; |
2-methylimidazole
N-benzyl-2-methylimidazole
Conditions | Yield |
---|---|
With ammonium formate; palladium on activated charcoal In methanol for 1h; Heating; | 97% |
Conditions | Yield |
---|---|
With N,N,N',N'',N'''-pentamethyldiethylenetriamine; potassium tert-butylate; copper(I) bromide In toluene at 20℃; for 9.5h; Inert atmosphere; | 89% |
With potassium carbonate In acetonitrile Reflux; | 80% |
With potassium carbonate In chloroform for 6h; Reflux; | 75.56% |
1-benzyl-2-(hydroxymethyl)imidazole hydrochloride
N-benzyl-2-methylimidazole
Conditions | Yield |
---|---|
With phosphorus; hydrogen iodide at 160℃; |
Conditions | Yield |
---|---|
With n-butyllithium 1.) Et2O, -78 deg C, 2.5 h; 20 deg C, 1 h, 2.) -78 deg C -> room temperature; room temperature, 15 min; Yield given. Multistep reaction; |
1-benzylimidazole
methyl iodide
A
N-benzyl-2-methylimidazole
B
2-methyl-1-(1-phenylethyl)-1H-imidazole
Conditions | Yield |
---|---|
With n-butyllithium Product distribution; multistep reaction: 1.) Et2O, -78 deg C, 0.5 h; other temperatures, times; reactions of lithiated N-protected imidazoles with various electrophiles; | A 46 % Spectr. B 25 % Spectr. |
With n-butyllithium 1) dimethoxyethane, -60 deg C, 10 min, 2) -60 deg C, 1.5 h, warm to r.t.; Yield given. Multistep reaction. Yields of byproduct given; |
2-methylimidazole
benzyl bromide
A
N-benzyl-2-methylimidazole
B
2-Methyl-4-phenylmethyl-1H-imidazole
Conditions | Yield |
---|---|
With sodium hydroxide 1) EtOH, reflux, 1 h; 2) reflux, 24 h; Yield given. Multistep reaction; |
N-benzyl-2-methylimidazole
2-methylimidazole
Conditions | Yield |
---|---|
With triethylsilane; palladium 10% on activated carbon In tetrahydrofuran at 20℃; for 24h; Inert atmosphere; | 97% |
With potassium tert-butylate; oxygen; dimethyl sulfoxide at 0℃; for 0.25h; | 85% |
With ammonia; sodium |
Conditions | Yield |
---|---|
With dodecacarbonyl-triangulo-triruthenium In toluene at 160℃; under 15201 Torr; for 20h; Carbonylation; | 96% |
N-benzyl-2-methylimidazole
methyl iodide
1,2-Dimethyl-3-benzyl-imidazoliumiodid
Conditions | Yield |
---|---|
at 60℃; | 95% |
N-benzyl-2-methylimidazole
Pd(SCN)2(1-benzyl-2-methylimidazole)2
Conditions | Yield |
---|---|
In acetonitrile for 2h; Reflux; | 92% |
N-benzyl-2-methylimidazole
chloroacetone
trans dichlorobispyridine palladium (II)
Conditions | Yield |
---|---|
In tetrahydrofuran for 48h; Inert atmosphere; Schlenk technique; Reflux; | A n/a B 90% |
N-benzyl-2-methylimidazole
PdCl2(1-benzyl-2-methylimidazole)2
Conditions | Yield |
---|---|
In acetonitrile for 2h; Reflux; | 88% |
3-Methylindole
N-benzyl-2-methylimidazole
1-benzyl-2-methyl-3-(3-methyl-1H-indol-2-yl)imidazolium bromide
Conditions | Yield |
---|---|
With N-Bromosuccinimide In 1,4-dioxane at 12 - 15℃; for 0.5h; | 88% |
Conditions | Yield |
---|---|
With potassium carbonate; triphenylphosphine; palladium diacetate In N,N-dimethyl-formamide at 140℃; for 24h; Phenylation; | 85% |
N-benzyl-2-methylimidazole
Conditions | Yield |
---|---|
In methanol at 25℃; | 85% |
In methanol at 25℃; for 24h; | 85% |
N-benzyl-2-methylimidazole
Conditions | Yield |
---|---|
In dichloromethane at 20℃; for 1h; | 85% |
N-benzyl-2-methylimidazole
Conditions | Yield |
---|---|
In dichloromethane at 20℃; for 1h; | 82% |
Conditions | Yield |
---|---|
In methanol at 25℃; | 81% |
N-benzyl-2-methylimidazole
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide at 90 - 110℃; for 24h; Inert atmosphere; Schlenk technique; | 81% |
N-benzyl-2-methylimidazole
(4Z)-5-(bromo-methyl)-2,2,6,6-tetramethylhept-4-en-3-one
1-benzyl-3-[(2Z)-2-tert-butyl-5,5-dimethyl-4-oxohex-2-en-1-yl]-2-methyl-1H-imidazol-3-ium bromide
Conditions | Yield |
---|---|
In benzene at 20℃; | 79% |
N-benzyl-2-methylimidazole
(2Z)-4-bromo-1,3-diphenylbut-2-en-1-one
Br(1-)*C27H25N2O(1+)
Conditions | Yield |
---|---|
In benzene at 20℃; | 78% |
Conditions | Yield |
---|---|
In tetrahydrofuran at 5 - 20℃; for 12h; Inert atmosphere; Cooling with ice; | 78% |
N-benzyl-2-methylimidazole
5-(bromomethyl)-4,5-dihydro-3,3-diphenyl-2(3H)-furanone
Conditions | Yield |
---|---|
In diethyl ether at 100℃; for 16h; | 75% |
N-benzyl-2-methylimidazole
4-(2-bromoethyl)phenol
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide at 90 - 110℃; for 24h; Inert atmosphere; Schlenk technique; | 75% |
N-benzyl-2-methylimidazole
acrylic acid n-butyl ester
Conditions | Yield |
---|---|
With copper diacetate; palladium diacetate In 1,4-dioxane at 100℃; for 15h; Reagent/catalyst; regioselective reaction; | A 74% B 12 %Spectr. |
N-benzyl-2-methylimidazole
tert-Butyl acrylate
Conditions | Yield |
---|---|
With copper diacetate; palladium diacetate In 1,4-dioxane at 100℃; for 15h; regioselective reaction; | 74% |
2-(but-3-en-1-yl)-2-methyl-1,3-dioxolane
N-benzyl-2-methylimidazole
carbon monoxide
Conditions | Yield |
---|---|
With dodecacarbonyl-triangulo-triruthenium In toluene at 160℃; under 15200 Torr; for 20h; | 72% |
N-benzyl-2-methylimidazole
4-Vinylbenzyl chloride
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide at 90 - 110℃; for 24h; Inert atmosphere; Schlenk technique; | 72% |
N-benzyl-2-methylimidazole
N-(bromomethyl)phtalimide
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide at 90 - 110℃; for 24h; Inert atmosphere; Schlenk technique; | 71% |
N-benzyl-2-methylimidazole
Conditions | Yield |
---|---|
In methanol; water | 70% |
N-benzyl-2-methylimidazole
sodium dicyanamide
Conditions | Yield |
---|---|
In methanol for 0.25h; | 70% |
N-benzyl-2-methylimidazole
ethyl acrylate
Conditions | Yield |
---|---|
With copper diacetate; palladium diacetate In 1,4-dioxane at 100℃; for 15h; regioselective reaction; | 70% |
N-benzyl-2-methylimidazole
2-bromoethanol
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide at 90 - 110℃; for 24h; Inert atmosphere; Schlenk technique; | 68% |
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