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Cas:13954-38-6
Min.Order:1 Kilogram
FOB Price: $3.0
Type:Lab/Research institutions
inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
Cas:13954-38-6
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiryProduct Name: Tripiperidinophosphine Synonyms: Tri(piperidin-1-yl)phosphane;Tripiperidinophosphine;Tris(1-piperidinyl)phosphine CAS: 13954-38-6 MF: C15H30N3P MW: 283.39 EINECS: Product Categories: wq Mol File: 13954-38-6.mol Appearance:white
Lower price, sample is available,SDS test documents are available,large stock in warehouseAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:Fine chemical intermediates, used as the main raw material for the synthe
Shanghai Finebiotech Co.,Ltd.was established in 2020, which providing professional chemical services. As a customer-oriented company, we have distinguished ourself from others in providing worldwide customers with cost-effective and efficient service
TripiperidinophosphineAppearance:detailed see specifications Storage:Keep away of light, cool place Package:25kg/drum;200kg/drum Application:Used in Synthesis, Pharmaceuticals and other fields Transportation:Sea/air/courier
Tripiperidinophosphine cas 13954-38-6Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express
factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin
factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin
Price, service, company and transport advantage: 1. Best service, place of origin China, high quality, and reasonable price. 2. It's customers' right to choose the package (EMS, DHL, FEDEX, UPS). 3. It's customers' right
Cas:13954-38-6
Min.Order:0
Negotiable
Type:Trading Company
inquiry3-Methylpiperidine 3-Pipecoline,Hexahydro-3-picoline High Quality High Content cas626-56-2 Name3-MethylpiperidineSynonyms3-Pipecol…
Known for its best quality and competitve price, this chemicals we offered is widely appreciated by our customers. Package:According client's requirements Application:Pharmaceutical Intermediate Transportation:According client's requirements Port:SHA
Storage:Dark storage Package:1g,10g,50g 100g or kg Application:Pharmaceutical intermediates
piperidine
tripiperidino-phosphine
Conditions | Yield |
---|---|
With phosphorus trichloride In diethyl ether | 100% |
With triethylamine; phosphorus trichloride In diethyl ether at 20℃; for 1h; | 76% |
With phosphorus trichloride In diethyl ether at 0 - 20℃; | 76% |
Conditions | Yield |
---|---|
at 70℃; for 10h; | 95% |
C30H46N4O2P2
A
2,6-dipiperidino-1,3,5,7-tetraoxa-2,6-diphospha-4,8(1,3)-dinaphthalenacyclooctaphane
B
tripiperidino-phosphine
Conditions | Yield |
---|---|
A 41% B n/a |
Conditions | Yield |
---|---|
A 39% B n/a |
B
tripiperidino-phosphine
Conditions | Yield |
---|---|
A 28% B n/a |
Conditions | Yield |
---|---|
With triethylamine |
piperidine
diethyl ether
phosphorus trichloride
tripiperidino-phosphine
C16H25N2OP
A
1-Diphenoxyphosphinyl-piperidin
B
tripiperidino-phosphine
Conditions | Yield |
---|---|
In 1,4-dioxane at 20℃; for 936h; Title compound not separated from byproducts; | |
In 1,4-dioxane at 20℃; for 480h; Title compound not separated from byproducts.; |
Conditions | Yield |
---|---|
at 20℃; Title compound not separated from byproducts; |
Conditions | Yield |
---|---|
at 20℃; Title compound not separated from byproducts; |
Conditions | Yield |
---|---|
In acetonitrile at 20℃; for 1464h; Title compound not separated from byproducts.; |
Conditions | Yield |
---|---|
In acetonitrile at 20℃; for 2304h; Title compound not separated from byproducts.; |
Conditions | Yield |
---|---|
In acetonitrile at 20℃; for 960h; Title compound not separated from byproducts.; |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 52 percent / hexane / 0 - 20 °C 2: dioxane / 936 h / 20 °C View Scheme | |
Multi-step reaction with 2 steps 1: 81 percent / hexane / 0 - 20 °C 2: 20 °C View Scheme | |
Multi-step reaction with 2 steps 1: 85 percent / hexane / 0 - 20 °C 2: 20 °C View Scheme |
dichloro(1,5-cyclooctadiene)palladium(II)
tripiperidino-phosphine
dichloro{bis[1,1’,1’’-(phosphinetriyl)tripiperidine]}palladium(II)
Conditions | Yield |
---|---|
In toluene at 20℃; for 0.166667h; | 100% |
dichloro(1,5-cyclooctadiene)palladium(II)
tripiperidino-phosphine
dicloro(bis(1,1',1''-(phosphinetriyl)tripiperidine))palladium
Conditions | Yield |
---|---|
In toluene two equivalents of phosphine-compd. added to Pd-compd. in toluene under N2 at room temp.; | 99% |
tripiperidino-phosphine
t-butyl azide
Conditions | Yield |
---|---|
at 0 - 20℃; | 91% |
tripiperidino-phosphine
tetraphenylethylresorcin[4]arene
Conditions | Yield |
---|---|
In 1,4-dioxane at 20℃; for 168h; | 87% |
tripiperidino-phosphine
Conditions | Yield |
---|---|
In tetrahydrofuran at 20℃; for 0.333333h; | 78% |
tripiperidino-phosphine
1,8-diazidonaphthalene
Conditions | Yield |
---|---|
In tetrahydrofuran at 20℃; for 2h; Staudinger Azide Reduction; Inert atmosphere; Schlenk technique; | 77% |
tripiperidino-phosphine
trimethylsilylazide
Conditions | Yield |
---|---|
In toluene for 2h; Staudinger Azide Reduction; Reflux; Inert atmosphere; Schlenk technique; | 77% |
tripiperidino-phosphine
1,3-dihydroxynaphthalene
2,6-dipiperidino-1,3,5,7-tetraoxa-2,6-diphospha-4,8(1,3)-dinaphthalenacyclooctaphane
Conditions | Yield |
---|---|
In acetonitrile; benzene at 20℃; | 70% |
tripiperidino-phosphine
Conditions | Yield |
---|---|
With tetrafluoroboric acid In diethyl ether | 68% |
With tetrafluoroboric acid In diethyl ether |
tripiperidino-phosphine
Bromoacetaldehyde diethyl acetal
Conditions | Yield |
---|---|
at 80℃; for 4h; Inert atmosphere; | 63.5% |
Heating; |
Conditions | Yield |
---|---|
In 1,4-dioxane at 80 - 85℃; for 18h; Inert atmosphere; regioselective reaction; | 61% |
tripiperidino-phosphine
C64H64O8
Conditions | Yield |
---|---|
In 1,4-dioxane at 20℃; for 168h; | 60% |
tripiperidino-phosphine
ethene
nickel(II) acetylacetonate
C2H4Ni(P(NC5H10)3)2
Conditions | Yield |
---|---|
With (C2H5)2AlOC2H5 In not given prepn. at room temp.;; | 60% |
With (C2H5)2AlOC2H5 In not given prepn. at room temp.;; | 60% |
tripiperidino-phosphine
Ru(CO)(toluene)((9,9-dimethylxanthene-4,5-diyl)bis(dimethylsilyl))
Conditions | Yield |
---|---|
In tetrahydrofuran at 20℃; for 2h; | 60% |
tripiperidino-phosphine
C-methylcalix[4]resorcinarene
Conditions | Yield |
---|---|
In 1,4-dioxane at 20℃; for 168h; | 52% |
tripiperidino-phosphine
Conditions | Yield |
---|---|
Stage #1: tripiperidino-phosphine With trimethylsilylazide In toluene for 12h; Glovebox; Reflux; Schlenk technique; Inert atmosphere; Stage #2: With sulfuric acid In methanol for 24h; Inert atmosphere; Stage #3: With benzyl potassium In toluene for 3h; Inert atmosphere; | 52% |
Stage #1: tripiperidino-phosphine With trimethylsilylazide In toluene for 12h; Inert atmosphere; Reflux; Schlenk technique; Stage #2: With sulfuric acid In methanol for 24h; Inert atmosphere; Schlenk technique; Stage #3: With benzyl potassium In toluene for 3h; Glovebox; Inert atmosphere; | 52% |
Conditions | Yield |
---|---|
In 1,4-dioxane at 80 - 85℃; for 1h; Inert atmosphere; regioselective reaction; | 51% |
tripiperidino-phosphine
1,3-dihydroxynaphthalene
Conditions | Yield |
---|---|
In acetonitrile at 20℃; | 41% |
tripiperidino-phosphine
1,6-dihydroxynaphthalene
Conditions | Yield |
---|---|
In acetonitrile at 20℃; for 24h; | 41% |
Conditions | Yield |
---|---|
Stage #1: tripiperidino-phosphine In acetonitrile at 20℃; for 4h; Stage #2: 1,7-Dihydroxynaphthalene In acetonitrile at 20℃; for 4h; | A 39% B n/a |
In acetonitrile at 20℃; for 4h; | A 39% B n/a |
tripiperidino-phosphine
1,6-dihydroxynaphthalene
Conditions | Yield |
---|---|
In acetonitrile at 20℃; | 39% |
tripiperidino-phosphine
1,6-dihydroxynaphthalene
1,6-bis(dipiperidinothiophosphoryloxy)naphthalene
Conditions | Yield |
---|---|
Stage #1: tripiperidino-phosphine; 1,6-dihydroxynaphthalene In acetonitrile at 20℃; for 0.666667h; Stage #2: With sulfur In acetonitrile for 4h; | 39% |
tripiperidino-phosphine
1,7-Dihydroxynaphthalene
Conditions | Yield |
---|---|
Stage #1: tripiperidino-phosphine; 1,7-Dihydroxynaphthalene In acetonitrile at 20℃; for 4h; Stage #2: With sulfur In dichloromethane at 20℃; for 2.5h; | A 32% B 28% |
Stage #1: tripiperidino-phosphine In acetonitrile at 20℃; for 4h; Stage #2: 1,7-Dihydroxynaphthalene In acetonitrile at 20℃; for 4h; Stage #3: With sulfur In dichloromethane at 20℃; for 2.5h; |
tripiperidino-phosphine
p-xylylene glycol
Conditions | Yield |
---|---|
Stage #1: tripiperidino-phosphine; p-xylylene glycol In 1,4-dioxane at 20℃; for 48h; Stage #2: With sulfur In 1,4-dioxane at 20℃; for 72h; Further stages.; | 32% |
2,6-Dihydroxynaphthalene
tripiperidino-phosphine
Conditions | Yield |
---|---|
In acetonitrile at 20℃; | 28% |
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