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Cas:142-81-4
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Ansciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali
1-Hexanamine,hydrochloride (1:1) Application:Organic Chemicals
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1-Hexanamine,hydrochloride (1:1) cas 142-81-4Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express
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hexan-1-amine,hydrochloride Storage:Store in dry and cool condition Package:25kg or according to cutomer's demand Application:Chemical research/Pharmaceutical intermediates Transportation:By Sea,by Air,By courier like DHL or Fedx. Port:Shanghai/Shenz
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Cas:142-81-4
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2-hexyl-2-azabicyclo[2.2.1]hept-5-ene
1-hexylamine hydrochloride
Conditions | Yield |
---|---|
copper(II) sulfate In ethanol at 70℃; for 5h; | 99% |
Conditions | Yield |
---|---|
Stage #1: 1-nitrohexane With iron(III)-acetylacetonate; hydrazine hydrate In methanol at 150℃; for 0.0333333h; Microwave irradiation; Stage #2: With hydrogenchloride In water; ethyl acetate chemoselective reaction; | 97% |
Stage #1: 1-nitrohexane With C36H56Cl3CrN2O; magnesium; 4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane In tetrahydrofuran at 60℃; for 24h; Inert atmosphere; Schlenk technique; Stage #2: With hydrogenchloride In tetrahydrofuran; water; ethyl acetate at 20℃; | 93% |
Conditions | Yield |
---|---|
Stage #1: hexanenitrile With ammonium hydroxide; hydrogen; nano-dicobalt phosphide on hydrotalcite In isopropyl alcohol at 130℃; under 30003 Torr; for 1h; Autoclave; Stage #2: With hydrogenchloride In 1,4-dioxane | 93% |
Stage #1: hexanenitrile With fac-[Mn(1,2-bis(di-n-propylphosphino)ethane)(CO)3(CH3)]; hydrogen In toluene at 100℃; under 37503.8 Torr; for 18h; Autoclave; Stage #2: With hydrogenchloride In diethyl ether Inert atmosphere; | 92% |
Multi-step reaction with 2 steps 1: potassium hydroxide / Raney nickel / Heating 2: hydrochloric acid / H2O View Scheme | |
Multi-step reaction with 2 steps 1: carbonylhydrido(tetrahydroborato)[bis(2-diphenylphosphinoethyl)amino]ruthenium(II); hydrogen / isopropyl alcohol / 3 h / 100 °C / 22502.3 Torr / Autoclave 2: hydrogenchloride / isopropyl alcohol; diethyl ether; methanol View Scheme | |
Multi-step reaction with 2 steps 1: hydrogen; ammonia / toluene / 16 h / 120 °C / 22502.3 Torr / Autoclave 2: hydrogenchloride / diethyl ether / 20 °C View Scheme |
Conditions | Yield |
---|---|
Stage #1: Caproamide With bis(cyclopentadienyl)dihydrozirconium; 4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane at 20℃; under 760.051 Torr; for 24h; Inert atmosphere; Stage #2: With hydrogenchloride In diethyl ether Inert atmosphere; | 78% |
Stage #1: Caproamide With bis(tetrahydrofuran)calcium di(bis(trimethylsilyl)amide); 4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane In toluene at 120℃; for 36h; Inert atmosphere; Schlenk technique; Stage #2: With hydrogenchloride In diethyl ether; toluene Inert atmosphere; Schlenk technique; | 75% |
Yield given. Multistep reaction; |
2-chloro-3-hexynylamine hydrochloride
1-hexylamine hydrochloride
Conditions | Yield |
---|---|
With hydrogen; palladium on activated charcoal In ethanol for 1h; | 29% |
Hexyl-phosphorimidic acid triethyl ester
1-hexylamine hydrochloride
Conditions | Yield |
---|---|
With hydrogenchloride In N,N-dimethyl-formamide; benzene for 2h; Ambient temperature; Yield given; |
A
1-hexylamine hydrochloride
Conditions | Yield |
---|---|
With water at 20℃; for 12h; Equilibrium constant; pH 11.6; pH 12.0; |
Conditions | Yield |
---|---|
With sodium hydroxide hydrolysis; |
hexyl-isopropyliden-amine
1-hexylamine hydrochloride
Conditions | Yield |
---|---|
With hydrogenchloride In water | |
With hydrogenchloride In water at 20℃; for 1h; |
N-(diphenylmethylene)hexan-1-amine
1-hexylamine hydrochloride
Conditions | Yield |
---|---|
With hydrogenchloride In diethyl ether for 6h; |
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: tetrahydrofuran; methanol / 1 h / 20 °C 1.2: 70 percent / sodium cyanoborohydride / tetrahydrofuran; methanol / 24 h 2.1: 2,3-dichloro-5,6-dicyanobenzoquinone; molecular sieves 4 Angstroem / benzene / 1 h / 60 °C 3.1: aq. HCl / diethyl ether / 6 h View Scheme |
N-diphenylmethyl-hexylamine
1-hexylamine hydrochloride
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 2,3-dichloro-5,6-dicyanobenzoquinone; molecular sieves 4 Angstroem / benzene / 1 h / 60 °C 2: aq. HCl / diethyl ether / 6 h View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: benzene; dimethylformamide / Ambient temperature 2: HCl / benzene; dimethylformamide / 2 h / Ambient temperature View Scheme |
Conditions | Yield |
---|---|
With hydrogenchloride In methanol; diethyl ether; isopropyl alcohol | |
With hydrogenchloride In methanol; diethyl ether at 20℃; Inert atmosphere; | |
With hydrogenchloride In diethyl ether at 20℃; |
hexane
A
1-hexylamine hydrochloride
B
hexan-3-amine hydrochloride
C
1-methyl-pentylamine hydrochloride
Conditions | Yield |
---|---|
Stage #1: hexane With cerium(III) chloride; 1,1,1-trichloroethanol; di-tert-butyl-diazodicarboxylate; tetrabutyl-ammonium chloride In acetonitrile at 20℃; for 12h; Irradiation; Inert atmosphere; Sealed tube; Stage #2: With trifluoroacetic acid In dichloromethane at 20℃; for 1h; Reagent/catalyst; Further stages; |
formaldehyd
1-hexylamine hydrochloride
cyclopenta-1,3-diene
2-hexyl-2-azabicyclo[2.2.1]hept-5-ene
Conditions | Yield |
---|---|
In water | 100% |
2-imino-2H-1-benzopyran-3-carboxamide
1-hexylamine hydrochloride
Conditions | Yield |
---|---|
In ethanol; isopropyl alcohol for 0.5h; Heating; | 97% |
Conditions | Yield |
---|---|
With potassium carbonate In water; ethyl acetate | 95% |
carbon disulfide
1-hexylamine hydrochloride
[1,4]naphthoquinone
A
4,9-dioxo-4.9-dihydronaphtho[2,3-d]-1,3-dithiole-2-thione
B
2-(hexylimino)naphtho[2,3-d][1,3]dithiole-4,9-dione
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 0℃; for 4h; | A 10% B 85.5% |
1-hexylamine hydrochloride
4-bromopyridine hydrochloride
4-(n-hexylamino)pyridine
Conditions | Yield |
---|---|
at 227℃; for 3.5h; | 75% |
2,3-Dichloro-1,4-naphthoquinone
carbon disulfide
1-hexylamine hydrochloride
2-(hexylimino)naphtho[2,3-d][1,3]dithiole-4,9-dione
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 0℃; for 2.5h; | 73.1% |
Conditions | Yield |
---|---|
With copper diacetate; air; palladium diacetate for 2h; Heating; | 73% |
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide under N2; alkylammonium salt dissolved in DMF at room temp., Pb salt added, soln. stirred for 1 h; soln. poured into acetone, ppt. filtered off; | 70% |
mixing stoich. amts. of components; DSC; |
Conditions | Yield |
---|---|
In butan-1-ol for 18h; Reflux; | 62% |
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide under N2; stoich. amts.; alkylammonium salts dissolved in DMF at 35°C, Pb salt added, soln. stirred for 1 h; soln. poured into acetone, ppt. sepd. by centrifugation; | 60% |
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide under N2; alkylammonium salts dissolved in DMF at 35°C, Pb salt added; ratio of C6H13NH3I:CH3NH3I:PbCl2 = 2:3:3; soln. poured into acetone, ppt. sepd. by centrifugation; | 60% |
1-hexylamine hydrochloride
Conditions | Yield |
---|---|
With N,N'-dicyclohexylcarbodiimide In acetonitrile byproducts: DCU, H2, (C4H9)4NCl; refluxed; | 57% |
1-hexylamine hydrochloride
Conditions | Yield |
---|---|
With triethylamine In ethanol at 80℃; for 1.5h; Microwave irradiation; | 53% |
Conditions | Yield |
---|---|
With N,N'-cyclohexylcarbodiimide In acetonitrile byproducts: N,N'-dicyclohexylurea; soln. of (Bu4N)4(α-Mo8O26), DCC and alkylamine hydrochloride in MeCN heated at 40°C for 120 h; soln. filtered, filtrate allowed to evap., residue recrystd. with acetone; elem. anal.; | 50% |
1,6-bis(N3-cyano-N1-guanidino)hexane
1-hexylamine hydrochloride
C22H48N10
Conditions | Yield |
---|---|
at 155℃; for 2h; | 50% |
Conditions | Yield |
---|---|
at 20 - 180℃; for 0.416667h; microwave irradiation; | 40% |
4,5-bis(3,5-di-tert-butylsalicylideneimine)benzo-18-crown-6
1-hexylamine hydrochloride
nickel(II) acetate tetrahydrate
nickel(II) 4,5-bis(3,5-di-tert-butylsalicylideneimine)benzo-18-crown-6*n-hexylammonium chloride
Conditions | Yield |
---|---|
In methanol; dichloromethane soln. of Ni-acetate in MeOH added to soln. of 4,5-bis(3,5-tBu-salicylideneimine)benzo-18-C-6 in the presence of hexylammonium chloride; crystd. from MeOH/acetone upon slow evapn. of acetone; | 40% |
Conditions | Yield |
---|---|
With N,N'-dicyclohexylcarbodiimide In acetonitrile byproducts: DCU, H2, (C4H9)4NCl; refluxed; | A n/a B n/a C 34% |
1-hexylamine hydrochloride
(R,R)-(+)-di-N,N'-hexyltartramide
Conditions | Yield |
---|---|
at 20 - 180℃; for 0.416667h; microwave irradiation; | 13% |
Conditions | Yield |
---|---|
In water at 20℃; for 24h; Chichibabin Pyridine Synthesis; Inert atmosphere; | 10% |
formaldehyd
hexamethylenetetramine
1-hexylamine hydrochloride
hexanal
Conditions | Yield |
---|---|
Eintragen des Reaktionsgemisches in wss.Essigsaeure und anschliessendes Durchleiten von Wasserdampf; |
1,1,2-triacetoxy-ethane
1-hexylamine hydrochloride
potassium cyanide
DL-N-Hexyl-serin
Conditions | Yield |
---|---|
(i) MeOH, (ii) aq. HCl; Multistep reaction; |
Conditions | Yield |
---|---|
In water for 2h; Ambient temperature; |
5'-deoxypyridoxal
1-hexylamine hydrochloride
4-[(E)-Hexyliminomethyl]-2,5-dimethyl-pyridin-3-ol
Conditions | Yield |
---|---|
With sodium hydroxide In water at 25℃; Rate constant; Equilibrium constant; |
Conditions | Yield |
---|---|
In methanol; water for 2h; Ambient temperature; |
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