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inquiry4,6-Dichloro-2-(propylthio)pyrimidin-5-amine CAS No.:145783-15-9 Name 4,6-Dichloro-2-(propylthio)pyrimidin-5-amine Molecular Structure Molecular Formula C7H9Cl2N3S Molecular Weight 238.14
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inquiryhigh quality Appearance:White or off white powder Storage:Sealed, dry, microtherm , avoid light and smell Package:According to the demand of customer Application:Pharmaceutical intermediates Transportation:by air or by sea Port:shanghai
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inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
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inquiry1. made in GMP plant, commerially 2. Normal Stock: 500kgs 3. Audit accepted. Related documents are available to offer and audited by many clients, such as Lupin, MSN, Dr reddy etc 4. Chromatographic Purity (HPLC): not less than 99.0% Appearan
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inquiryCangzhou Enke Pharma Tech Co.,ltd. is located in Cangzhou City, Hebei province ,where is a famous petroleum chemical industry city in China. Enke Pharma a high-tech enterprise ,and we are dedicated to developing and manufacturing new ap
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inquiryProduct Description Product website: http://www.finerchem.com/pro01en/id/916.html Product Name 4,6-Dichloro-2-(propylthio)pyrimidin-5-amine CAS No. 36144
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inquiryLIDE PHARMACEUTICALS LIMITED is a professional chemicals and APIs leading manufacturer in China. Our core business line covers APIs, Intermediates, Herb extract, etc.
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inquiry4,6-dichloro-2-propylthiopyrimidine-5-amine Basic information Product Name: 4,6-dichloro-2-propylthiopyrimidine-5-amine Synonyms: 4,6-dichloro-2-propylthiopyrimidine-5-amine;4,6-dichloro
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inquiryProduct Name 4,6-Dichloro-2-(propylthio)pyrimidin-5-amine Synonyms 4,6-Dichloro-2-(propylthio)pyrimidin-5-amine CAS NO. 145783-1
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inquiryProduct Name: 4,6-dichloro-2-propylthiopyrimidine-5-amine CAS: 145783-15-9 MF: C7H9Cl2N3S MW: 238.14 EINECS: 808-051-8 Mol File: 145783-15-9.mol 4,6-dichloro-2-propylthiopyrimidine-5-amine Structure 4,6-dichloro-2-propylthiopyrimi
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inquiry4,6-dichloro-2-propylthiopyrimidine-5-amine CAS:145783-15-9 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in h
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
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inquiryAppearance: White or off white powder Storage:Store in a cool,dry place and keep away from direct strong light Package:As customer request Application:Used for research and industrial manufacture. Transportation:Common products:
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inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
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inquiry4,6-dichloro-5-nitro-2-(propylsulfanyl)pyrimidine
4,6-dichloro-2-(propylsulfanyl)-5-pyrimidinamine
Conditions | Yield |
---|---|
With ammonium molibdate; hydrogen; hypophosphorous acid; platinum on carbon In tert-butyl methyl ether at 20 - 65℃; under 7500.75 Torr; for 7h; Product distribution / selectivity; Inert atmosphere; | 100% |
Stage #1: 4,6-dichloro-5-nitro-2-(propylsulfanyl)pyrimidine With iron; acetic acid In methanol at 50℃; Stage #2: With sodium hydrogencarbonate In water; ethyl acetate Product distribution / selectivity; | 95% |
With iron; acetic acid for 4h; | 73% |
4,6-dihydroxy-5-amino-2-(propylmercapto)pyrimidine hydrochloride
4,6-dichloro-2-(propylsulfanyl)-5-pyrimidinamine
Conditions | Yield |
---|---|
With trichlorophosphate for 22.5h; Time; Concentration; Reflux; Sealed tube; | 96% |
With trichlorophosphate for 22.5h; Time; Sealed tube; Reflux; | 96% |
With pyridine; trichlorophosphate at 88 - 92℃; for 24h; | 84% |
4,6-dichloro-2-(propylsulfanyl)-5-pyrimidinamine
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine; trichlorophosphate at 75℃; for 4h; Reagent/catalyst; Temperature; | 93% |
With trichlorophosphate for 24h; Reflux; Large scale; | 90% |
4,6-dichloro-2-(propylsulfanyl)-5-pyrimidinamine
Conditions | Yield |
---|---|
With chlorine In chloroform at 30℃; for 6h; | 88% |
4,6-dichloro-2-(propylsulfanyl)-5-pyrimidinamine
Conditions | Yield |
---|---|
Stage #1: 4,6-dichloro-5-[(E)-2-(4-phenyl)diazenyl]-2-(propylsulfanyl)pyrimidine With ammonium formate; zinc In methanol; isopropyl alcohol for 0.166667h; Stage #2: With hydrogen; Raney Ni In methanol; isopropyl alcohol at 20℃; under 7500.75 Torr; for 11h; Product distribution / selectivity; | 78% |
4,6-dichloro-5-((E)-2-(4-methylphenyl)diazenyl)-2-(propylsulfanyl)pyrimidine
4,6-dichloro-2-(propylsulfanyl)-5-pyrimidinamine
Conditions | Yield |
---|---|
With hydrogen; 10 wt% platinum on carbon In ethyl acetate at 20 - 40℃; under 2250.23 Torr; for 0.5 - 2.5h; Product distribution / selectivity; | |
Multi-step reaction with 2 steps 1: ammonium formate; zinc / methanol; isopropyl alcohol / 0.33 h 2: hydrogen / 11 h / 20 °C View Scheme |
A
4,6-dichloro-2-(propylsulfanyl)-5-pyrimidinamine
Conditions | Yield |
---|---|
With hydrogen; platinum on carbon In methanol; isopropyl alcohol at 20℃; under 4500.45 Torr; for 32h; |
4,6-dihydroxy-2-(propylsulfanyl)pyrimidine
4,6-dichloro-2-(propylsulfanyl)-5-pyrimidinamine
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1.1: sodium acetate; sodium hydroxide / ethanol; water / 20 °C 1.2: 0.5 h / 0 °C 1.3: 0 - 5 °C 2.1: pyridine; trichlorophosphate / toluene / 4.75 h / 70 °C 3.1: ammonium formate; zinc / methanol; isopropyl alcohol / 0.33 h 4.1: hydrogen / 11 h / 20 °C View Scheme | |
Multi-step reaction with 3 steps 1: nitric acid; acetic acid / 55 °C 2: trichlorophosphate / N,N-dimethyl acetamide / Reflux 3: ammonia View Scheme | |
Multi-step reaction with 3 steps 1: nitric acid; acetic acid / 2 h / Cooling with ice 2: dmap; trichlorophosphate / 5 h / Reflux 3: iron; acetic acid / methanol / 2 h / Reflux View Scheme |
4,6-dihydroxy-5-((E)-2-(4-methylphenyl)diazenyl)-2-(propylsulfanyl)pyrimidine
4,6-dichloro-2-(propylsulfanyl)-5-pyrimidinamine
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: pyridine; trichlorophosphate / toluene / 4.75 h / 70 °C 2: ammonium formate; zinc / methanol; isopropyl alcohol / 0.33 h 3: hydrogen / 11 h / 20 °C View Scheme |
4,6-dichloro-2-(propylsulfanyl)-5-pyrimidinamine
Conditions | Yield |
---|---|
With hydrogen at 20℃; for 11h; |
4,6-dichloro-2-(propylsulfanyl)-5-pyrimidinamine
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine; trichlorophosphate at 90℃; for 5h; | 157 mg |
N-(4,6-dihydroxy-2-(propylthio)pyrimidin-5-yl)acetamide
4,6-dichloro-2-(propylsulfanyl)-5-pyrimidinamine
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: hydrogenchloride / methanol / 18 h / 50 °C 2: trichlorophosphate / 22.5 h / Sealed tube; Reflux View Scheme |
4,6-dichloro-2-(propylsulfanyl)-5-pyrimidinamine
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: ammonia / dichloromethane / 8 h / 30 °C 2: chlorine / chloroform / 6 h / 30 °C View Scheme |
4,6-dihydroxy-5-nitro-2-(propylthio)pyrimidine
4,6-dichloro-2-(propylsulfanyl)-5-pyrimidinamine
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: trichlorophosphate / N,N-dimethyl acetamide / Reflux 2: ammonia View Scheme | |
Multi-step reaction with 2 steps 1: dmap; trichlorophosphate / 5 h / Reflux 2: iron; acetic acid / methanol / 2 h / Reflux View Scheme | |
Multi-step reaction with 2 steps 1: trichlorophosphate / 2 h / Reflux 2: acetic acid; iron / methanol / 20 °C / Reflux View Scheme |
4,6-dichloro-2-(propylsulfanyl)-5-pyrimidinamine
trifluoroacetic anhydride
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 10 - 20℃; for 1h; | 96% |
4,6-dichloro-2-(propylsulfanyl)-5-pyrimidinamine
methylamine
Conditions | Yield |
---|---|
In methanol at 100℃; for 1h; Sealed tube; | 96% |
In methanol at 100℃; for 1h; Sealed tube; | 96% |
In methanol for 1h; Sealed tube; | 96% |
4,6-dichloro-2-(propylsulfanyl)-5-pyrimidinamine
cyclobutylamine
Conditions | Yield |
---|---|
In methanol at 100℃; for 1h; Sealed tube; | 96% |
In methanol at 100℃; for 1h; Sealed tube; | 96% |
4,6-dichloro-2-(propylsulfanyl)-5-pyrimidinamine
1-pentanamine
Conditions | Yield |
---|---|
In methanol at 100℃; for 0.5h; Sealed tube; | 96% |
In methanol at 100℃; for 0.5h; Sealed tube; | 96% |
4,6-dichloro-2-(propylsulfanyl)-5-pyrimidinamine
[3aR-(3aα,4α,6α,6aα)]-2-[[6-amino-2,2-dimethyl tetrahydro-4H-cyclopenta-1,3-dioxol-4-yl]oxy]ethanol
Conditions | Yield |
---|---|
Stage #1: 4,6-dichloro-2-(propylsulfanyl)-5-pyrimidinamine; [3aR-(3aα,4α,6α,6aα)]-2-[[6-amino-2,2-dimethyl tetrahydro-4H-cyclopenta-1,3-dioxol-4-yl]oxy]ethanol In water; N,N-dimethyl-formamide for 0.333333h; Stage #2: With triethylamine at 20℃; Reflux; | 95% |
With N-ethyl-N,N-diisopropylamine at 120 - 125℃; for 10h; Temperature; Inert atmosphere; | 93.5% |
With sodium hydrogencarbonate In water at 100℃; for 20h; Reagent/catalyst; Temperature; | 88.3% |
4,6-dichloro-2-(propylsulfanyl)-5-pyrimidinamine
Cyclopentamine
Conditions | Yield |
---|---|
In methanol at 100℃; for 2h; Sealed tube; | 95% |
In methanol at 100℃; for 2h; Sealed tube; | 95% |
In methanol Sealed tube; | 95% |
4,6-dichloro-2-(propylsulfanyl)-5-pyrimidinamine
isopropylamine
Conditions | Yield |
---|---|
In methanol at 100℃; for 1.5h; Sealed tube; | 95% |
In methanol at 100℃; for 1.5h; Sealed tube; | 95% |
4,6-dichloro-2-(propylsulfanyl)-5-pyrimidinamine
N-butylamine
Conditions | Yield |
---|---|
In methanol at 100℃; for 0.5h; Sealed tube; | 95% |
In methanol at 100℃; for 0.5h; Sealed tube; | 95% |
4,6-dichloro-2-(propylsulfanyl)-5-pyrimidinamine
Conditions | Yield |
---|---|
With sodium hydrogencarbonate In water at 85℃; Large scale; | 95% |
4,6-dichloro-2-(propylsulfanyl)-5-pyrimidinamine
2-[[(3aR,4S,6R,6aS)-6-aminotetrahydro-2,2-dimethyl-4H-cyclopenta-1,3-dioxol-4-yl]oxy]ethanol (2R,3R)-2,3-dihydroxybutanedioic acid
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In sulfolane at 107℃; for 3h; Large scale; | 94.75% |
With sodium hydroxide In ethyl acetate at 90℃; for 20h; Temperature; | 90.4% |
With sodium hydrogencarbonate In water at 87℃; Temperature; Large scale; | 90% |
4,6-dichloro-2-(propylsulfanyl)-5-pyrimidinamine
pentafluorophenyl trifloroacetate
Conditions | Yield |
---|---|
With pyridine In N,N-dimethyl-formamide at 10 - 20℃; for 5h; | 93% |
4,6-dichloro-2-(propylsulfanyl)-5-pyrimidinamine
Cyclopropylamine
Conditions | Yield |
---|---|
In methanol at 100℃; for 0.5h; Sealed tube; | 92% |
In methanol at 100℃; for 0.5h; Sealed tube; | 92% |
With triethylamine In ethanol at 120℃; for 30h; |
4,6-dichloro-2-(propylsulfanyl)-5-pyrimidinamine
1-amino-2-propene
Conditions | Yield |
---|---|
In methanol at 100℃; for 0.5h; Sealed tube; | 92% |
In methanol at 100℃; for 0.5h; Sealed tube; | 92% |
4,6-dichloro-2-(propylsulfanyl)-5-pyrimidinamine
(3aR,4S,6R,6aS)-6-amino-2,2-dimethyltetrahydro-3aH-cyclopenta[d][1,3]dioxol-4-ol
(3aR,4S,6R,6aS)-6-((5-amino-6-chloro-2-(propylthio)pyrimidin-4-yl)amino)-2,2-dimethyltetrahydro-3aH-cyclopenta[d][1,3]dioxol-4-ol
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In 1,4-dioxane at 100℃; for 16h; | 91% |
In methanol at 100℃; for 12h; Sealed tube; | 90% |
In methanol at 100℃; for 12h; Sealed tube; | 90% |
4,6-dichloro-2-(propylsulfanyl)-5-pyrimidinamine
benzylamine
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide | 91% |
With triethylamine In ethanol for 48h; Reflux; | |
With triethylamine In ethanol for 48h; Reflux; |
4,6-dichloro-2-(propylsulfanyl)-5-pyrimidinamine
(tert-butyl (1R,2S)-2-(3,4-difluorophenyl)cyclopropyl)carbamate
Conditions | Yield |
---|---|
With lithium hexamethyldisilazane In tetrahydrofuran at -85 - -75℃; for 2h; Inert atmosphere; | 91% |
propylamine
4,6-dichloro-2-(propylsulfanyl)-5-pyrimidinamine
Conditions | Yield |
---|---|
In methanol at 100℃; for 0.5h; Sealed tube; | 91% |
In methanol at 100℃; for 0.5h; Sealed tube; | 91% |
4,6-dichloro-2-(propylsulfanyl)-5-pyrimidinamine
cyclohexylamine
Conditions | Yield |
---|---|
In methanol at 100℃; for 1h; Sealed tube; | 91% |
In methanol at 100℃; for 1h; Sealed tube; | 91% |
With triethylamine In ethanol at 120℃; for 30h; | 90% |
4,6-dichloro-2-(propylsulfanyl)-5-pyrimidinamine
Conditions | Yield |
---|---|
With sodium hydrogencarbonate In water at 90℃; Large scale; | 89.4% |
4,6-dichloro-2-(propylsulfanyl)-5-pyrimidinamine
(3aS,4R,6S,6aR)-6-(2-(tert-butoxy)ethoxy)-2,2-dimethyltetrahydro-3aH-cyclopenta[d][1,3]dioxol-4-amine
Conditions | Yield |
---|---|
With triethylamine In ethanol at 100 - 130℃; Sealed tube; Inert atmosphere; | 89% |
Conditions | Yield |
---|---|
With triethylamine In isopropyl alcohol at 80℃; for 30h; Time; Industrial scale; | 89% |
4,6-dichloro-2-(propylsulfanyl)-5-pyrimidinamine
(1S,2S,3R,5S)-3-amino-5-(2-hydroxyethoxy)cyclopentane-1,2-diol
(1S 2S,3R,5S)-3-[(5-amino-6-chloro-2-(propylthio)pyrimidin-4-yl)amino]-5-(2-hydroxyethoxy)cyclopentane-1,2-diol
Conditions | Yield |
---|---|
With triethylamine at 75℃; for 48h; Concentration; Reagent/catalyst; Temperature; Time; | 88% |
With triethylamine at 75℃; for 48h; Reagent/catalyst; Time; Temperature; | 88% |
With triethylamine In methanol; water at 100℃; for 40h; | 14.5 g |
Conditions | Yield |
---|---|
With triethylamine In ethanol at 100 - 130℃; Sealed tube; Inert atmosphere; | 88% |
Conditions | Yield |
---|---|
With triethylamine In ethanol at 100 - 130℃; Sealed tube; Inert atmosphere; | 88% |
4,6-dichloro-2-(propylsulfanyl)-5-pyrimidinamine
tert-butylamine
Conditions | Yield |
---|---|
In methanol at 100℃; for 24h; Sealed tube; | 88% |
In methanol at 100℃; for 24h; Sealed tube; | 88% |
Conditions | Yield |
---|---|
With triethylamine In ethanol at 100 - 130℃; Sealed tube; Inert atmosphere; | 87% |
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