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(S,S)-2,8-Diazabicyclo[4.3.0]nonane [Chemical Name]: (S,S)-2,8-Diazabicyclo[4,3,0]nonane [CAS No.]: 151213-42-2 [Structure Formula]: [Molecular For
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inquiryAbout Product Technical Details (S,S)-2,8-Diazabicyclo[4,3,0]nonane Chemical Properties Boiling point 198.5±8.0 °C(Predicted) density 0.950±0.06 g/cm3(Predicted)
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inquiry(S,S)-2,8-Diazabicyclo[4,3,0]nonane Basic information Product Name: (S,S)-2,8-Diazabicyclo[4,3,0]nonane Synonyms: [S,S]-2,8-Diazabicyclo[4.3.0]Nonane98%;(S,S)-2,8-Diazabicyclo[4,3,0]onoane;(S,S)-2,8-DIAZABICYCLO[4,3,0]NONANE [FOR MOXIFLOXACIN];(
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inquiryProduct name: 2,8-Diazabicyclo[4.3.0]nonane CAS No.: 151213-42-2, 151413-40-0 Molecular weight: 199.1213 Useing: Pharmaceutical intermediate Appearance: white powder Storage:Store in cool and dry
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inquiryMoxifloxacin intermediate:(S,S)-2,8-Diazabicyclo[4,3,0]nonane[CAS:151213-42-2] Name (1R,6R)-2,8-Diazabicyclo[4,3,0]nonane Molecular Structure Molecular Formula C7H14N2
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inquiry(S,S)-2,8-Diazabicyclo[4,3,0]nonane CAS: 151213-42-2 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high qu
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inquiryAppearance:white or light yellow crystalline powder Storage:Store in a cool,dry place and keep away from direct strong light Package:As customer request Application:Used for research and industrial manufacture. Transportation:By
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inquiry[R,R]-8-benzyl-2,8-diazabicyclo[4.3.0]nonane
[R,R]-2,8-diazabicyclo[4.3.0]nonane
Conditions | Yield |
---|---|
With hydrogen; 5%-palladium/activated carbon In methanol at 90℃; under 67506.8 Torr; for 5h; | 85% |
9.61 g (85%) | |
9.61 g (85%) | |
With palladium on activated charcoal; hydrogen In methanol |
(R,R)-6-(toluene-4-sulfonyl)-octahydro-pyrrolo[3,4-b]pyridine
[R,R]-2,8-diazabicyclo[4.3.0]nonane
Conditions | Yield |
---|---|
Stage #1: (R,R)-6-(toluene-4-sulfonyl)-octahydro-pyrrolo[3,4-b]pyridine With hydrogen bromide; propionic acid; phenol In water for 6 - 7h; Heating / reflux; Stage #2: With sodium hydroxide In water pH=11 - 12; | 80.1% |
[R,R]-2,8-diazabicyclo[4.3.0]nonane
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: D-tartaric acid / N,N-dimethyl-formamide; 2-methoxy-ethanol 2: palladium on activated charcoal; hydrogen / methanol View Scheme |
A
[R,R]-2,8-diazabicyclo[4.3.0]nonane
B
(1S,6S)-2,8-diazabicyclo[4.3.0]nonane
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 2 h / 25 - 35 °C 2.1: hydrogen; 5%-palladium/activated carbon / toluene / 24 h / 80 °C / 6000.6 Torr 2.2: Reflux View Scheme |
(S)-2-(6-methoxynaphthalen-2-yl)-1-(5H-pyrrolo[3,4-b]pyridin-6(7H)-yl)propan-1-one
A
[R,R]-2,8-diazabicyclo[4.3.0]nonane
B
(1S,6S)-2,8-diazabicyclo[4.3.0]nonane
Conditions | Yield |
---|---|
Stage #1: (S)-2-(6-methoxynaphthalen-2-yl)-1-(5H-pyrrolo[3,4-b]pyridin-6(7H)-yl)propan-1-one With 5%-palladium/activated carbon; hydrogen In toluene at 80℃; under 6000.6 Torr; for 24h; Stage #2: With hydrogen bromide; phenol In acetic acid; propionic acid Reflux; | A n/a B n/a |
6-(2,4-dimethoxybenzyl)-6,7-dihydro-5H-pyrrolo[3,4-b]pyridine
A
[R,R]-2,8-diazabicyclo[4.3.0]nonane
B
(1S,6S)-2,8-diazabicyclo[4.3.0]nonane
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: trifluoroacetic acid; triethylsilane / 4 h / 60 - 65 °C 1.2: 20 °C 2.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 2 h / 25 - 35 °C 3.1: hydrogen; 5%-palladium/activated carbon / toluene / 24 h / 80 °C / 6000.6 Torr 3.2: Reflux View Scheme |
[R,R]-2,8-diazabicyclo[4.3.0]nonane
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: sodium tetrahydroborate; boron trifluoride-tetrahydrofuran complex / tetrahydrofuran / -5 - 20 °C 2: palladium 10% on activated carbon; hydrogen / ethanol / 40 °C / 2250.23 - 3750.38 Torr 3: L-Tartaric acid / isopropyl alcohol; water / 20 - 80 °C View Scheme |
2,8-diazabicyclo-[4.3.0]-nonane
[R,R]-2,8-diazabicyclo[4.3.0]nonane
Conditions | Yield |
---|---|
With L-Tartaric acid In water; isopropyl alcohol at 20 - 80℃; | 3.8 g |
[R,R]-2,8-diazabicyclo[4.3.0]nonane
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: ethyl acetate / 70 °C 2: sodium tetrahydroborate; boron trifluoride-tetrahydrofuran complex / tetrahydrofuran / -5 - 20 °C 3: palladium 10% on activated carbon; hydrogen / ethanol / 40 °C / 2250.23 - 3750.38 Torr 4: L-Tartaric acid / isopropyl alcohol; water / 20 - 80 °C View Scheme |
[R,R]-2,8-diazabicyclo[4.3.0]nonane
1-cyclopropyl-6,7-difluoro-1,4-dihydro-8-methoxy-4-oxo-3-quinolinecarboxylic acid
Conditions | Yield |
---|---|
With nano iron oxide on ZrO2 coated sulfonic acid In water for 0.416667h; Reflux; | 96% |
at 150℃; Microwave irradiation; | 83% |
[R,R]-2,8-diazabicyclo[4.3.0]nonane
N-[2-amino-6-chloro-4-pyrimidinyl]-N-[3-fluoro-4-(1H-indazol-5-yloxy)phenyl]amine
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In 2-Ethylhexyl alcohol at 150℃; | 93% |
[R,R]-2,8-diazabicyclo[4.3.0]nonane
levofloxacin Q-acid
Conditions | Yield |
---|---|
With nano iron oxide on ZrO2 coated sulfonic acid In water for 0.45h; Reflux; | 93% |
at 150℃; Microwave irradiation; | 89% |
[R,R]-2,8-diazabicyclo[4.3.0]nonane
7-chloro-1-cyclopropyl-6-fluoro-1,4-dihydro-4-oxo-3-quinoline carboxylic acid
Conditions | Yield |
---|---|
With nano iron oxide on ZrO2 coated sulfonic acid In water for 0.3h; Reflux; | 91% |
at 150℃; Microwave irradiation; | 84% |
[R,R]-2,8-diazabicyclo[4.3.0]nonane
1-cyclopropyl-6,7-difluoro-1,4-dihydro-8-methoxy-4-oxo-3-quinoline carboxylic acid-O3,O4(bis(acyloxy-O)) borate
moxifloxacin hydrochloride
Conditions | Yield |
---|---|
Stage #1: [R,R]-2,8-diazabicyclo[4.3.0]nonane; 1-cyclopropyl-6,7-difluoro-1,4-dihydro-8-methoxy-4-oxo-3-quinoline carboxylic acid-O3,O4(bis(acyloxy-O)) borate With triethylamine In acetonitrile at 15 - 30℃; for 8h; Stage #2: With hydrogenchloride In methanol at 15 - 20℃; Temperature; | 71% |
[R,R]-2,8-diazabicyclo[4.3.0]nonane
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In 2-Ethylhexyl alcohol at 150℃; for 3h; | 14% |
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In ethanol at 60℃; for 2h; |
[R,R]-2,8-diazabicyclo[4.3.0]nonane
1-cyclopropyl-6,7-difluoro-8-methoxy-4-oxo-1,4-dihydro-3-quinoline carboxylic acid (O3,O4)bis(acyloxy-O)borate
Conditions | Yield |
---|---|
With triethylamine In acetonitrile for 1h; Heating / reflux; |
[R,R]-2,8-diazabicyclo[4.3.0]nonane
Conditions | Yield |
---|---|
With hydrogen bromide In ethanol |
[R,R]-2,8-diazabicyclo[4.3.0]nonane
2,4,8-trichloro-benzo[4,5]furo[3,2-d]pyrimidine
C17H16Cl2N4O
Conditions | Yield |
---|---|
In ethanol |
Conditions | Yield |
---|---|
With triethylamine In N,N-dimethyl-formamide at 20℃; for 3h; Cooling with ice; | |
With triethylamine In N,N-dimethyl-formamide at 20℃; for 3h; Cooling with ice; | |
With triethylamine In N,N-dimethyl-formamide at 20℃; for 3h; Cooling with ice; |
[R,R]-2,8-diazabicyclo[4.3.0]nonane
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: triethylamine / N,N-dimethyl-formamide / 3 h / 20 °C / Cooling with ice 2: N,N-dimethyl-formamide / 1 h / Inert atmosphere; Reflux 3: hydrogenchloride / methanol; water / 5 h / 20 °C 4: dicyclohexyl-carbodiimide View Scheme |
[R,R]-2,8-diazabicyclo[4.3.0]nonane
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: triethylamine / N,N-dimethyl-formamide / 3 h / 20 °C / Cooling with ice 2: N,N-dimethyl-formamide / 1 h / Inert atmosphere; Reflux 3: hydrogenchloride / methanol; water / 5 h / 20 °C 4: dicyclohexyl-carbodiimide; dmap / tetrahydrofuran / 20 °C View Scheme |
[R,R]-2,8-diazabicyclo[4.3.0]nonane
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: triethylamine / N,N-dimethyl-formamide / 3 h / 20 °C / Cooling with ice 2: N,N-dimethyl-formamide / 1 h / Inert atmosphere; Reflux View Scheme | |
Multi-step reaction with 2 steps 1: triethylamine / N,N-dimethyl-formamide / 3 h / 20 °C / Cooling with ice 2: N,N-dimethyl-formamide / 1 h / Reflux; Inert atmosphere View Scheme | |
Multi-step reaction with 2 steps 1: triethylamine / N,N-dimethyl-formamide / 3 h / 20 °C / Cooling with ice 2: N,N-dimethyl-formamide / 1 h / Inert atmosphere; Reflux View Scheme | |
Multi-step reaction with 2 steps 1: triethylamine / N,N-dimethyl-formamide / 3 h / 20 °C 2: N,N-dimethyl-formamide / 1 h / Inert atmosphere; Reflux View Scheme | |
Multi-step reaction with 2 steps 1: triethylamine / N,N-dimethyl-formamide / 3 h / 20 °C 2: N,N-dimethyl-formamide / 1 h / Reflux; Inert atmosphere View Scheme |
[R,R]-2,8-diazabicyclo[4.3.0]nonane
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: triethylamine / N,N-dimethyl-formamide / 3 h / 20 °C / Cooling with ice 2: N,N-dimethyl-formamide / 1 h / Inert atmosphere; Reflux 3: hydrogenchloride / methanol; water / 5 h / 20 °C View Scheme | |
Multi-step reaction with 3 steps 1: triethylamine / N,N-dimethyl-formamide / 3 h / 20 °C / Cooling with ice 2: N,N-dimethyl-formamide / 1 h / Reflux; Inert atmosphere 3: hydrogenchloride / methanol / 5 h / 20 °C View Scheme | |
Multi-step reaction with 3 steps 1: triethylamine / N,N-dimethyl-formamide / 3 h / 20 °C / Cooling with ice 2: N,N-dimethyl-formamide / 1 h / Inert atmosphere; Reflux 3: hydrogenchloride / water; methanol / 5 h / 20 °C View Scheme | |
Multi-step reaction with 3 steps 1: triethylamine / N,N-dimethyl-formamide / 3 h / 20 °C 2: N,N-dimethyl-formamide / 1 h / Inert atmosphere; Reflux 3: hydrogenchloride / methanol; water / 5 h / 20 °C View Scheme | |
Multi-step reaction with 3 steps 1: triethylamine / N,N-dimethyl-formamide / 3 h / 20 °C 2: N,N-dimethyl-formamide / 1 h / Reflux; Inert atmosphere 3: hydrogenchloride / methanol; water / 5 h / 20 °C View Scheme |
[R,R]-2,8-diazabicyclo[4.3.0]nonane
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: triethylamine / N,N-dimethyl-formamide / 3 h / 20 °C / Cooling with ice 2: N,N-dimethyl-formamide / 1 h / Inert atmosphere; Reflux 3: hydrogenchloride / methanol; water / 5 h / 20 °C 4: dicyclohexyl-carbodiimide; dmap / tetrahydrofuran / 20 °C View Scheme | |
Multi-step reaction with 4 steps 1: triethylamine / N,N-dimethyl-formamide / 3 h / 20 °C / Cooling with ice 2: N,N-dimethyl-formamide / 1 h / Reflux; Inert atmosphere 3: hydrogenchloride / methanol / 5 h / 20 °C 4: dmap; dicyclohexyl-carbodiimide / tetrahydrofuran / 20 °C View Scheme | |
Multi-step reaction with 4 steps 1: triethylamine / N,N-dimethyl-formamide / 3 h / 20 °C / Cooling with ice 2: N,N-dimethyl-formamide / 1 h / Inert atmosphere; Reflux 3: hydrogenchloride / methanol; water / 5 h / 20 °C 4: dmap; dicyclohexyl-carbodiimide / tetrahydrofuran / 20 °C View Scheme |
[R,R]-2,8-diazabicyclo[4.3.0]nonane
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: triethylamine / N,N-dimethyl-formamide / 3 h / 20 °C / Cooling with ice 2: N,N-dimethyl-formamide / 1 h / Inert atmosphere; Reflux View Scheme | |
Multi-step reaction with 2 steps 1: triethylamine / N,N-dimethyl-formamide / 3 h / 20 °C 2: N,N-dimethyl-formamide / 1 h / Inert atmosphere; Reflux View Scheme | |
Multi-step reaction with 2 steps 1: triethylamine / N,N-dimethyl-formamide / 3 h / 20 °C 2: N,N-dimethyl-formamide / 1 h / Reflux; Inert atmosphere View Scheme |
[R,R]-2,8-diazabicyclo[4.3.0]nonane
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: triethylamine / N,N-dimethyl-formamide / 3 h / 20 °C / Cooling with ice 2: N,N-dimethyl-formamide / 1 h / Inert atmosphere; Reflux 3: hydrogenchloride / methanol; water / 5 h / 20 °C View Scheme | |
Multi-step reaction with 3 steps 1: triethylamine / N,N-dimethyl-formamide / 3 h / 20 °C 2: N,N-dimethyl-formamide / 1 h / Inert atmosphere; Reflux 3: hydrogenchloride / methanol; water / 5 h / 20 °C View Scheme | |
Multi-step reaction with 3 steps 1: triethylamine / N,N-dimethyl-formamide / 3 h / 20 °C 2: N,N-dimethyl-formamide / 1 h / Reflux; Inert atmosphere 3: hydrogenchloride / methanol; water / 5 h / 20 °C View Scheme |
[R,R]-2,8-diazabicyclo[4.3.0]nonane
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: triethylamine / N,N-dimethyl-formamide / 3 h / 20 °C / Cooling with ice 2: N,N-dimethyl-formamide / 1 h / Inert atmosphere; Reflux 3: hydrogenchloride / methanol; water / 5 h / 20 °C 4: dicyclohexyl-carbodiimide; dmap / tetrahydrofuran / 20 °C View Scheme |
[R,R]-2,8-diazabicyclo[4.3.0]nonane
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: triethylamine / N,N-dimethyl-formamide / 3 h / 20 °C / Cooling with ice 2: dmap; dicyclohexyl-carbodiimide / tetrahydrofuran / 20 °C 3: hydrogenchloride / water; methanol / 5 h / 20 °C View Scheme |
[R,R]-2,8-diazabicyclo[4.3.0]nonane
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: triethylamine / N,N-dimethyl-formamide / 3 h / 20 °C / Cooling with ice 2: dmap; dicyclohexyl-carbodiimide / tetrahydrofuran / 20 °C 3: hydrogenchloride / water; methanol / 5 h / 20 °C 4: dmap; dicyclohexyl-carbodiimide / tetrahydrofuran / 20 °C View Scheme |
[R,R]-2,8-diazabicyclo[4.3.0]nonane
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: triethylamine / N,N-dimethyl-formamide / 3 h / 20 °C / Cooling with ice 2: dmap; dicyclohexyl-carbodiimide / tetrahydrofuran / 20 °C View Scheme |
[R,R]-2,8-diazabicyclo[4.3.0]nonane
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: triethylamine / N,N-dimethyl-formamide / 3 h / 20 °C / Cooling with ice 2: dmap; dicyclohexyl-carbodiimide / tetrahydrofuran / 20 °C 3: hydrogenchloride / water; methanol / 5 h / 20 °C View Scheme |
[R,R]-2,8-diazabicyclo[4.3.0]nonane
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: triethylamine / N,N-dimethyl-formamide / 3 h / 20 °C / Cooling with ice 2: dmap; dicyclohexyl-carbodiimide / tetrahydrofuran / 20 °C 3: hydrogenchloride / water; methanol / 5 h / 20 °C 4: dmap; dicyclohexyl-carbodiimide / tetrahydrofuran / 20 °C View Scheme |
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