Dayangchem's R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantities
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inquiryOur main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
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inquiryOur company was built in 2009 with an ISO certificate.In the past 5 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so on.O
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inquiryOur advantages: 1. All inquiries will be replied within 12 hours. 2. Dedication to quality, supply & service. 3. Strictly on selecting raw materials. 4. Reasonable & competitive price, fast lead time. 5. Sample is available for your eva
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inquiry2-(4-OCTYLPHENYL)ETHANOL CAS:162358-05-6 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic
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inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
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inquiryA substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc
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inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
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Min.Order:10 Gram
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inquirySuperior quality, moderate price & quick delivery. Appearance:light yellow liquid Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:10g/bag,or as your request Application:For medicine , pesticide intermediates T
Product name: 2-(4-Ocytlphenyl)Ethanol CAS No.:162358-05-6 Molecule Formula:C16H26O Molecule Weight:234.37 Purity: 98.0% Package: 25kg/drum Description:White crystalline powder Manufacture Standards:Enterprise Standard TESTING IT
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inquiry1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer
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inquiryhigh purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:Foil bag; Drum; Plastic bottle Application:Pharma;Industry;Agricultural Transportation:by sea or air Port:Beijing or Guangzhou
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inquiryAnsciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali
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inquiryWe are committed to providing our customers with the best products and services at the most competitive prices.Appearance:white powder Storage:Room temperature with sealed well Package:according to the clients requirement Application:Use as primary a
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2-(4-Octylphenyl)ethanolAppearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express
factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin
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inquiryGood Quality Package:1kg/bag Application:Medical or chemical Transportation:Air/Train/Sea Port:Shenzhen
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inquiryKnown for its best quality and competitve price, this chemicals we offered is widely appreciated by our customers.Appearance:White powder Storage:keep sealed and keep from direct light Package:According client's requirements Application:pharmaceutica
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inquiryfactory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin
Our mission is to provide high-quality and innovative products to our customers. By offering a broad range of products, custom synthesis and personalized services, Bide can help scientists speeding up their research in the chemical and pharmaceutical
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inquiry2-(4-Octylphenyl)ethyl alcohol
Conditions | Yield |
---|---|
With palladium 10% on activated carbon; hydrogen In ethyl acetate at 20℃; for 17h; | 98% |
acetic acid 2-(4-octylphenyl)ethyl ester
2-(4-Octylphenyl)ethyl alcohol
Conditions | Yield |
---|---|
With sodium methylate In methanol at 20℃; for 8h; | 93% |
With sodium methylate In methanol for 6h; Reflux; | 92% |
With sodium methylate In methanol for 6h; Reflux; | 92% |
Conditions | Yield |
---|---|
Stage #1: 1-bromo-octane With iodine; magnesium In tetrahydrofuran for 1h; Inert atmosphere; Reflux; Stage #2: C28H25BrO With pyridine; dmap; sodium hydroxide Heating; Stage #3: With palladium 10% on activated carbon; hydrogen In tetrahydrofuran at 120℃; for 4h; | 80% |
1-bromo-octane
4-(2-hydroxyethyl)benzyl bromide
2-(4-Octylphenyl)ethyl alcohol
Conditions | Yield |
---|---|
Stage #1: 1-bromo-octane With iodine; magnesium In diethyl ether for 1h; Inert atmosphere; Reflux; Stage #2: 4-(2-hydroxyethyl)benzyl bromide With sodium hydroxide In tetrahydrofuran at 110℃; for 4h; Temperature; | 75% |
octylmagnesium bromide
acetic acid 2-[4-(trifluoromethanesulfonyloxy)phenyl]ethyl ester
A
2-(4-Octylphenyl)ethyl alcohol
B
acetic acid 2-(4-octylphenyl)ethyl ester
Conditions | Yield |
---|---|
With 1-methyl-pyrrolidin-2-one; iron(III)-acetylacetonate In tetrahydrofuran for 1h; | A 20% B 64% |
1-Chlorooctane
4-(2-hydroxyethyl)benzyl bromide
2-(4-Octylphenyl)ethyl alcohol
Conditions | Yield |
---|---|
Stage #1: n-chlorooctane With iodine; magnesium In tetrahydrofuran for 1h; Inert atmosphere; Reflux; Stage #2: 4-(2-hydroxyethyl)benzyl bromide With sodium hydroxide In tetrahydrofuran at 120℃; for 4h; | 20% |
p-hydroxyphenethyl alcohol
2-(4-Octylphenyl)ethyl alcohol
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 98 percent / NaHSO4 on silica / hexane / 26 h / Heating 2: 94 percent / pyridine / CH2Cl2 / 1 h / 20 °C 3: 20 percent / Fe(acac)3; NMP / tetrahydrofuran / 1 h View Scheme |
2-(4-hydroxyphenyl)ethyl acetate
2-(4-Octylphenyl)ethyl alcohol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 94 percent / pyridine / CH2Cl2 / 1 h / 20 °C 2: 20 percent / Fe(acac)3; NMP / tetrahydrofuran / 1 h View Scheme |
n-octanoic acid chloride
2-(4-Octylphenyl)ethyl alcohol
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 43 percent / AlCl3 / 1,2-dichloro-ethane / 3 h / 20 °C 2: triethylsilane; TFA / 1,2-dichloro-ethane / 3 h / 20 °C 3: 3.40 g / NaOMe; MeOH / 2 h / Heating View Scheme | |
Multi-step reaction with 3 steps 1.1: aluminum (III) chloride / 1,2-dichloro-ethane / 1 h / 20 °C 1.2: 12 h / 20 °C 2.1: trifluoroacetic acid; triethylsilane / 3 h / 20 °C 3.1: sodium methylate / methanol / 6 h / Reflux View Scheme | |
Multi-step reaction with 3 steps 1.1: aluminum (III) chloride / 1,2-dichloro-ethane / 1 h / 20 °C 1.2: 12 h / 20 °C 2.1: trifluoroacetic acid; triethylsilane / 3 h / 20 °C 3.1: sodium methylate / methanol / 6 h / Reflux View Scheme | |
Multi-step reaction with 3 steps 1: aluminum (III) chloride / 1,2-dichloro-ethane / 0 - 20 °C 2: triethylsilane; trifluoroacetic acid / 20 °C 3: sodium methylate / methanol / 3 h / 20 °C View Scheme | |
Multi-step reaction with 4 steps 1.1: aluminum (III) chloride / 0.01 h / 0.25 - 0.3 °C 1.2: 0 h / 0.2 - 0.5 °C 2.1: sodium hydroxide / water; methanol / 1.5 h / 0.1 - 0.3 °C 3.1: palladium 10% on activated carbon; hydrogen / 0 h / 0.4 °C / Autoclave 4.1: sodium hydroxide / water; methanol / 0.2 - 0.3 °C View Scheme |
acetic acid phenethyl ester
2-(4-Octylphenyl)ethyl alcohol
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 43 percent / AlCl3 / 1,2-dichloro-ethane / 3 h / 20 °C 2: triethylsilane; TFA / 1,2-dichloro-ethane / 3 h / 20 °C 3: 3.40 g / NaOMe; MeOH / 2 h / Heating View Scheme | |
Multi-step reaction with 3 steps 1.1: aluminum (III) chloride / 1,2-dichloro-ethane / 1 h / 20 °C 1.2: 12 h / 20 °C 2.1: trifluoroacetic acid; triethylsilane / 3 h / 20 °C 3.1: sodium methylate / methanol / 6 h / Reflux View Scheme | |
Multi-step reaction with 3 steps 1.1: aluminum (III) chloride / 1,2-dichloro-ethane / 1 h / 20 °C 1.2: 12 h / 20 °C 2.1: trifluoroacetic acid; triethylsilane / 3 h / 20 °C 3.1: sodium methylate / methanol / 6 h / Reflux View Scheme | |
Multi-step reaction with 4 steps 1.1: aluminum (III) chloride / 0.01 h / 0.25 - 0.3 °C 1.2: 0 h / 0.2 - 0.5 °C 2.1: sodium hydroxide / water; methanol / 1.5 h / 0.1 - 0.3 °C 3.1: palladium 10% on activated carbon; hydrogen / 0 h / 0.4 °C / Autoclave 4.1: sodium hydroxide / water; methanol / 0.2 - 0.3 °C View Scheme |
2-(4-octanoylphenyl)ethyl acetate
2-(4-Octylphenyl)ethyl alcohol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: triethylsilane; TFA / 1,2-dichloro-ethane / 3 h / 20 °C 2: 3.40 g / NaOMe; MeOH / 2 h / Heating View Scheme | |
Multi-step reaction with 2 steps 1: trifluoroacetic acid; triethylsilane / 3 h / 20 °C 2: sodium methylate / methanol / 6 h / Reflux View Scheme | |
Multi-step reaction with 2 steps 1: trifluoroacetic acid; triethylsilane / 3 h / 20 °C 2: sodium methylate / methanol / 6 h / Reflux View Scheme | |
Multi-step reaction with 2 steps 1: triethylsilane; trifluoroacetic acid / 20 °C 2: sodium methylate / methanol / 3 h / 20 °C View Scheme | |
Multi-step reaction with 3 steps 1: sodium hydroxide / water; methanol / 1.5 h / 0.1 - 0.3 °C 2: palladium 10% on activated carbon; hydrogen / 0 h / 0.4 °C / Autoclave 3: sodium hydroxide / water; methanol / 0.2 - 0.3 °C View Scheme |
4-iodophenethyl alcohol
2-(4-Octylphenyl)ethyl alcohol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: tetrakis(triphenylphosphine) palladium(0); copper(l) iodide; triethylamine / 17 h / 20 °C / Inert atmosphere 2: palladium 10% on activated carbon; hydrogen / ethyl acetate / 17 h / 20 °C View Scheme |
n-octyne
2-(4-Octylphenyl)ethyl alcohol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: tetrakis(triphenylphosphine) palladium(0); copper(l) iodide; triethylamine / 17 h / 20 °C / Inert atmosphere 2: palladium 10% on activated carbon; hydrogen / ethyl acetate / 17 h / 20 °C View Scheme |
methanesulfonyl chloride
2-(4-Octylphenyl)ethyl alcohol
4-octylphenethyl methanesulfonate
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 20℃; for 5h; | 95% |
With triethylamine In dichloromethane at 20℃; for 5h; | 95% |
With triethylamine In dichloromethane for 1h; |
2-(4-Octylphenyl)ethyl alcohol
diethyl 2-acetamido-2-[2-(4-octylphenyl)ethyl]malonate
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: Et3N / CH2Cl2 / 1 h 2.1: 5.37 g / LiI / tetrahydrofuran / 4 h / 20 °C 3.1: NaH / dimethylformamide / 30 h 3.2: 82 percent / dimethylformamide / 1 h / 50 - 60 °C View Scheme | |
Multi-step reaction with 3 steps 1.1: Et3N / CH2Cl2 / 1 h / 20 °C 2.1: 16.0 g / NaI / butan-2-one / 2 h / Heating 3.1: sodium ethoxide / ethanol / 0.5 h / 20 °C 3.2: 61 percent / ethanol / 3 h / 65 °C View Scheme | |
Multi-step reaction with 3 steps 1.1: triethylamine / dichloromethane / 0.5 h 1.2: 3 h / 0 - 20 °C 2.1: sodium iodide / tetrahydrofuran / 20 °C 3.1: caesium carbonate / dimethyl sulfoxide / 3 h / 60 °C / Inert atmosphere 3.2: 60 - 80 °C View Scheme | |
Multi-step reaction with 2 steps 1.1: sodium iodide / butanone / 0.67 h / 0.8 - 0.85 °C 2.1: sodium hydride / N,N-dimethyl-formamide / 0.5 h / 0.45 - 0.5 °C / Inert atmosphere 2.2: 0.4 - 0.45 °C / Inert atmosphere View Scheme | |
Multi-step reaction with 3 steps 1: triethylamine / dichloromethane / 0 - 30 °C / Inert atmosphere 2: tetra-(n-butyl)ammonium iodide; sodium iodide / 3 h / Inert atmosphere 3: tetra-(n-butyl)ammonium iodide; caesium carbonate / dimethyl sulfoxide / 25 - 85 °C / Inert atmosphere View Scheme |
2-(4-Octylphenyl)ethyl alcohol
1-(2-iodoethyl)-4-octylbenzene
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: Et3N / CH2Cl2 / 1 h 2: 5.37 g / LiI / tetrahydrofuran / 4 h / 20 °C View Scheme | |
Multi-step reaction with 2 steps 1: Et3N / CH2Cl2 / 1 h / 20 °C 2: 16.0 g / NaI / butan-2-one / 2 h / Heating View Scheme | |
Multi-step reaction with 2 steps 1.1: triethylamine / dichloromethane / 0.5 h 1.2: 3 h / 0 - 20 °C 2.1: sodium iodide / tetrahydrofuran / 20 °C View Scheme |
2-(4-Octylphenyl)ethyl alcohol
fingolimod
Conditions | Yield |
---|---|
Multi-step reaction with 6 steps 1.1: Et3N / CH2Cl2 / 1 h / 20 °C 2.1: 16.0 g / NaI / butan-2-one / 2 h / Heating 3.1: sodium ethoxide / ethanol / 0.5 h / 20 °C 3.2: 61 percent / ethanol / 3 h / 65 °C 4.1: LiAlH4 / tetrahydrofuran / 2 h / 20 °C 5.1: 8.25 g / pyridine / 16 h / 20 °C 6.1: 2 N aq. LiOH / methanol / 2 h / Heating View Scheme | |
Multi-step reaction with 4 steps 1.1: sodium iodide / butanone / 0.67 h / 0.8 - 0.85 °C 2.1: sodium hydride / N,N-dimethyl-formamide / 0.5 h / 0.45 - 0.5 °C / Inert atmosphere 2.2: 0.4 - 0.45 °C / Inert atmosphere 3.1: calcium chloride / water; isopropyl alcohol / 0 h / 0.2 - 0.3 °C 3.2: 0.01 h / 0 - 0.5 °C 3.3: 0 h / 0.15 - 0.5 °C 4.1: sodium hydroxide / water; methanol / 2 h / Reflux View Scheme |
2-(4-Octylphenyl)ethyl alcohol
2-amino-2-hydroxymethyl-4-(4-octyl-phenyl)-butyric acid
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1.1: Et3N / CH2Cl2 / 1 h / 20 °C 2.1: 16.0 g / NaI / butan-2-one / 2 h / Heating 3.1: sodium ethoxide / ethanol / 0.5 h / 20 °C 3.2: 75 percent / ethanol / 3 h / 65 °C 4.1: 54 percent / LiBH4 / tetrahydrofuran / 6 h / Heating 5.1: 66 percent / aq. HCl; AcOH / 7 h / Heating View Scheme |
2-(4-Octylphenyl)ethyl alcohol
Conditions | Yield |
---|---|
Multi-step reaction with 8 steps 1.1: Et3N / CH2Cl2 / 1 h / 20 °C 2.1: 16.0 g / NaI / butan-2-one / 2 h / Heating 3.1: NaH / dimethylformamide / 0.5 h 3.2: dimethylformamide / 3 h 4.1: 1 N aq. HCl / methanol / 5 h 5.1: 0.25 N aq. NaOH / acetone / 1.5 h / 20 °C 6.1: Et3N / tetrahydrofuran / 0.25 h / -5 °C 7.1: aq. NaN3 / tetrahydrofuran / 1 h / 0 °C 8.1: benzene / 1 h / Heating View Scheme |
2-(4-Octylphenyl)ethyl alcohol
Conditions | Yield |
---|---|
Multi-step reaction with 13 steps 1.1: Et3N / CH2Cl2 / 1 h / 20 °C 2.1: 16.0 g / NaI / butan-2-one / 2 h / Heating 3.1: NaH / dimethylformamide / 0.5 h 3.2: dimethylformamide / 3 h 4.1: 1 N aq. HCl / methanol / 5 h 5.1: 0.25 N aq. NaOH / acetone / 1.5 h / 20 °C 6.1: Et3N / tetrahydrofuran / 0.25 h / -5 °C 7.1: aq. NaN3 / tetrahydrofuran / 1 h / 0 °C 8.1: benzene / 1 h / Heating 9.1: benzene / 7 h / Heating 10.1: LiBH4 / tetrahydrofuran / 0.5 h / Heating 11.1: pyridine / 13 h / 20 °C 12.1: Me3SiI / CH2Cl2 / 7 h 12.2: pyridine / 13 h 13.1: 2 M aq. LiOH / tetrahydrofuran; methanol / 2 h / Heating View Scheme |
2-(4-Octylphenyl)ethyl alcohol
N-[1-cyano-1-hydroxymethyl-3-(4-octylphenyl)propyl]acetamide
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1.1: Et3N / CH2Cl2 / 1 h / 20 °C 2.1: 16.0 g / NaI / butan-2-one / 2 h / Heating 3.1: sodium ethoxide / ethanol / 0.5 h / 20 °C 3.2: 75 percent / ethanol / 3 h / 65 °C 4.1: 54 percent / LiBH4 / tetrahydrofuran / 6 h / Heating View Scheme |
2-(4-Octylphenyl)ethyl alcohol
3-[2-(4-octyl-phenyl)-ethyl]-2-oxo-tetrahydro-furan-3-carboxylic acid
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1.1: Et3N / CH2Cl2 / 1 h / 20 °C 2.1: 16.0 g / NaI / butan-2-one / 2 h / Heating 3.1: NaH / dimethylformamide / 0.5 h 3.2: dimethylformamide / 3 h 4.1: 1 N aq. HCl / methanol / 5 h 5.1: 0.25 N aq. NaOH / acetone / 1.5 h / 20 °C View Scheme |
2-(4-Octylphenyl)ethyl alcohol
Conditions | Yield |
---|---|
Multi-step reaction with 11 steps 1.1: Et3N / CH2Cl2 / 1 h / 20 °C 2.1: 16.0 g / NaI / butan-2-one / 2 h / Heating 3.1: NaH / dimethylformamide / 0.5 h 3.2: 76 percent / dimethylformamide / 3 h 4.1: KOH / ethanol / 6 h / 50 °C 5.1: Et3N / tetrahydrofuran / 0.25 h / -5 °C 6.1: aq. NaN3 / tetrahydrofuran / 1 h / 0 °C 7.1: benzene / 1 h / Heating 8.1: benzene / 7 h / Heating 9.1: LiBH4 / tetrahydrofuran / 3 h / Heating 10.1: 5 N aq. KOH / tetrahydrofuran; methanol / 13 h / Heating 11.1: HCl; MeOH / diethyl ether / 0.5 h View Scheme |
2-(4-Octylphenyl)ethyl alcohol
N-(1-hydroxy-2-(hydroxymethyl)-4-(4-octylphenyl) butan-2-yl) acetamide
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1.1: Et3N / CH2Cl2 / 1 h / 20 °C 2.1: 16.0 g / NaI / butan-2-one / 2 h / Heating 3.1: sodium ethoxide / ethanol / 0.5 h / 20 °C 3.2: 61 percent / ethanol / 3 h / 65 °C 4.1: LiAlH4 / tetrahydrofuran / 2 h / 20 °C View Scheme | |
Multi-step reaction with 4 steps 1.1: triethylamine / dichloromethane / 0.5 h 1.2: 3 h / 0 - 20 °C 2.1: sodium iodide / tetrahydrofuran / 20 °C 3.1: caesium carbonate / dimethyl sulfoxide / 3 h / 60 °C / Inert atmosphere 3.2: 60 - 80 °C 4.1: sodium tetrahydroborate / methanol / 20 °C View Scheme |
2-(4-Octylphenyl)ethyl alcohol
3-[2-(4-octyl-phenyl)-ethyl]-2-oxo-tetrahydro-furan-3-carboxylic acid ethyl ester
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1.1: Et3N / CH2Cl2 / 1 h / 20 °C 2.1: 16.0 g / NaI / butan-2-one / 2 h / Heating 3.1: NaH / dimethylformamide / 0.5 h 3.2: dimethylformamide / 3 h 4.1: 1 N aq. HCl / methanol / 5 h View Scheme |
2-(4-Octylphenyl)ethyl alcohol
Conditions | Yield |
---|---|
Multi-step reaction with 7 steps 1.1: Et3N / CH2Cl2 / 1 h / 20 °C 2.1: 16.0 g / NaI / butan-2-one / 2 h / Heating 3.1: NaH / dimethylformamide / 0.5 h 3.2: dimethylformamide / 3 h 4.1: 1 N aq. HCl / methanol / 5 h 5.1: 0.25 N aq. NaOH / acetone / 1.5 h / 20 °C 6.1: Et3N / tetrahydrofuran / 0.25 h / -5 °C 7.1: aq. NaN3 / tetrahydrofuran / 1 h / 0 °C View Scheme |
2-(4-Octylphenyl)ethyl alcohol
ethyl 2-acetamido-2-cyano-4-(4-octylphenyl)butyrate
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: Et3N / CH2Cl2 / 1 h / 20 °C 2.1: 16.0 g / NaI / butan-2-one / 2 h / Heating 3.1: sodium ethoxide / ethanol / 0.5 h / 20 °C 3.2: 75 percent / ethanol / 3 h / 65 °C View Scheme |
2-(4-Octylphenyl)ethyl alcohol
2-Methoxycarbonylamino-2-[2-(4-octylphenyl)ethyl]-γ-butyrolactone
Conditions | Yield |
---|---|
Multi-step reaction with 9 steps 1.1: Et3N / CH2Cl2 / 1 h / 20 °C 2.1: 16.0 g / NaI / butan-2-one / 2 h / Heating 3.1: NaH / dimethylformamide / 0.5 h 3.2: dimethylformamide / 3 h 4.1: 1 N aq. HCl / methanol / 5 h 5.1: 0.25 N aq. NaOH / acetone / 1.5 h / 20 °C 6.1: Et3N / tetrahydrofuran / 0.25 h / -5 °C 7.1: aq. NaN3 / tetrahydrofuran / 1 h / 0 °C 8.1: benzene / 1 h / Heating 9.1: benzene / 7 h / Heating View Scheme |
2-(4-Octylphenyl)ethyl alcohol
2-Methoxycarbonylamino-2-[2-(4-octylphenyl)ethyl]butane 1,4-diol
Conditions | Yield |
---|---|
Multi-step reaction with 10 steps 1.1: Et3N / CH2Cl2 / 1 h / 20 °C 2.1: 16.0 g / NaI / butan-2-one / 2 h / Heating 3.1: NaH / dimethylformamide / 0.5 h 3.2: dimethylformamide / 3 h 4.1: 1 N aq. HCl / methanol / 5 h 5.1: 0.25 N aq. NaOH / acetone / 1.5 h / 20 °C 6.1: Et3N / tetrahydrofuran / 0.25 h / -5 °C 7.1: aq. NaN3 / tetrahydrofuran / 1 h / 0 °C 8.1: benzene / 1 h / Heating 9.1: benzene / 7 h / Heating 10.1: LiBH4 / tetrahydrofuran / 0.5 h / Heating View Scheme |
2-(4-Octylphenyl)ethyl alcohol
2-acetamido-2-[2-(4-octylphenyl)ethyl]propane-1,3-diol diacetate
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1.1: Et3N / CH2Cl2 / 1 h / 20 °C 2.1: 16.0 g / NaI / butan-2-one / 2 h / Heating 3.1: sodium ethoxide / ethanol / 0.5 h / 20 °C 3.2: 61 percent / ethanol / 3 h / 65 °C 4.1: LiAlH4 / tetrahydrofuran / 2 h / 20 °C 5.1: 8.25 g / pyridine / 16 h / 20 °C View Scheme | |
Multi-step reaction with 3 steps 1.1: sodium iodide / butanone / 0.67 h / 0.8 - 0.85 °C 2.1: sodium hydride / N,N-dimethyl-formamide / 0.5 h / 0.45 - 0.5 °C / Inert atmosphere 2.2: 0.4 - 0.45 °C / Inert atmosphere 3.1: calcium chloride / water; isopropyl alcohol / 0 h / 0.2 - 0.3 °C 3.2: 0.01 h / 0 - 0.5 °C 3.3: 0 h / 0.15 - 0.5 °C View Scheme |
2-(4-Octylphenyl)ethyl alcohol
Conditions | Yield |
---|---|
Multi-step reaction with 6 steps 1.1: Et3N / CH2Cl2 / 1 h / 20 °C 2.1: 16.0 g / NaI / butan-2-one / 2 h / Heating 3.1: NaH / dimethylformamide / 0.5 h 3.2: dimethylformamide / 3 h 4.1: 1 N aq. HCl / methanol / 5 h 5.1: 0.25 N aq. NaOH / acetone / 1.5 h / 20 °C 6.1: Et3N / tetrahydrofuran / 0.25 h / -5 °C View Scheme |
2-(4-Octylphenyl)ethyl alcohol
3-Acetamido-3-acetoxymethyl-5-(4-octylphenyl)pentyl acetate
Conditions | Yield |
---|---|
Multi-step reaction with 12 steps 1.1: Et3N / CH2Cl2 / 1 h / 20 °C 2.1: 16.0 g / NaI / butan-2-one / 2 h / Heating 3.1: NaH / dimethylformamide / 0.5 h 3.2: dimethylformamide / 3 h 4.1: 1 N aq. HCl / methanol / 5 h 5.1: 0.25 N aq. NaOH / acetone / 1.5 h / 20 °C 6.1: Et3N / tetrahydrofuran / 0.25 h / -5 °C 7.1: aq. NaN3 / tetrahydrofuran / 1 h / 0 °C 8.1: benzene / 1 h / Heating 9.1: benzene / 7 h / Heating 10.1: LiBH4 / tetrahydrofuran / 0.5 h / Heating 11.1: pyridine / 13 h / 20 °C 12.1: Me3SiI / CH2Cl2 / 7 h 12.2: pyridine / 13 h View Scheme |
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