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inquirydichloroformoxine CAS:1794-86-1 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic intermed
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Min.Order:10 Gram
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Min.Order:1 Gram
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Carbonimidicdichloride, hydroxy- (9CI)Appearance:Off white to slight yellow solid Storage:Store in dry and cool condition Package:25kg or according to cutomer's demand Application:Chemical research/Pharmaceutical intermediates Transportation:By Sea,b
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Chloronitroacetyl chloride
dichloroformoxime
Conditions | Yield |
---|---|
With urea In diethyl ether for 0.5h; Heating; further reagents (C6H11NH)2CO, (MeNH)2CO, thiourea, (PhNH)2CO; | 75% |
A
3,4-dichloro-1,2,5-oxadiazole-N-oxide
B
dichloroformoxime
Conditions | Yield |
---|---|
With chlorine In water under cooling with ice-water Cl2 is led into the suspension; dichlorofuroxane isolated as oil; dichlorofuroxim extracted with ether; | A n/a B 40% |
With Cl2 In water under cooling with ice-water Cl2 is led into the suspension; dichlorofuroxane isolated as oil; dichlorofuroxim extracted with ether; | A n/a B 40% |
With chlorine In hydrogenchloride | |
With Cl2 In hydrogenchloride |
Conditions | Yield |
---|---|
With tin In acetonitrile | 16.8% |
Conditions | Yield |
---|---|
With hydrogenchloride; diethyl ether; tin(ll) chloride | |
With ethanol; sulfur dioxide; water | |
With ethanol; hydrogen sulfide | |
With methanol; hydrogen sulfide | |
With methanol; aluminium amalgam |
bromodichloronitrosomethane
dichloroformoxime
Conditions | Yield |
---|---|
With methanol; hydrogen sulfide |
Conditions | Yield |
---|---|
With sulfuric acid durch elektrolytische Reduktion an einer Zinnkathode; | |
With hydrogenchloride; tin; diethyl ether at 0 - 5℃; | |
(reduction); |
chloropicrin
A
dichloroformoxime
B
N-Methylhydroxylamine
C
trichloronitrosomethane
D
methylamine
Conditions | Yield |
---|---|
Bei der elektrolytischen Reduktion entstehen je nach den Bedingungen wechselnde Menge; |
Conditions | Yield |
---|---|
With hydrogenchloride; tin; diethyl ether at 0 - 5℃; |
mercury fulminate
dichloroformoxime
Conditions | Yield |
---|---|
With water; chlorine | |
With hydrogenchloride; chlorine | |
With chloroethane; chlorine | |
With sodium hypochlorite |
sodium cyanate
dichloroformoxime
Conditions | Yield |
---|---|
With sulfuric acid; water; chlorine at 0℃; |
Conditions | Yield |
---|---|
With chlorine |
Conditions | Yield |
---|---|
With N-chloro-succinimide In 1,2-dimethoxyethane for 0.166667h; Heating; | |
With N-chloro-succinimide In 1,2-dimethoxyethane Heating; | |
With N-chloro-succinimide In 1,2-dimethoxyethane at 55 - 110℃; |
Conditions | Yield |
---|---|
With hydroxylamine hydrochloride; chlorine; sodium hydrogencarbonate 1.) water, 18 h; Multistep reaction; |
glyoxylic acid aldoxime
dichloroformoxime
Conditions | Yield |
---|---|
With N-chloro-succinimide In 1,2-dimethoxyethane Heating; |
pyruvohydroximoyl chloride
water
chlorine
A
dichloroformoxime
B
chloropicrin
Conditions | Yield |
---|---|
at 10 - 20℃; |
dichloroformoxime
Conditions | Yield |
---|---|
With water; chlorine at 10 - 20℃; |
methanol
trichloronitrosomethane
hydrogen sulfide
dichloroformoxime
ethanol
trichloronitrosomethane
hydrogen sulfide
dichloroformoxime
Conditions | Yield |
---|---|
at 0 - 5℃; |
fulminic acid
dichloroformoxime
Conditions | Yield |
---|---|
With chlorine In water | |
With chlorine In diethyl ether -80°C; | |
With chlorine In further solvent(s) in ethyl chloride; |
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide at 45℃; for 0.616667h; | 97% |
dichloroformoxime
copper(I) 4-methoxyphenylacetylenide
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide at 45℃; for 0.783333h; | 95% |
dichloroformoxime
1-copper(I) (4-chlorophenyl)ethyne
3-chloro-5-(4-chlorophenyl)isoxazole
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide at 45℃; for 0.783333h; | 95% |
Conditions | Yield |
---|---|
With iodine; sodium hydrogencarbonate In N,N-dimethyl-formamide at 20℃; for 6.16667h; | 94% |
copper(I) phenylacetylenide
dichloroformoxime
Conditions | Yield |
---|---|
With iodine; sodium hydrogencarbonate In N,N-dimethyl-formamide at 20℃; for 6.16667h; Concentration; Temperature; | 94% |
dichloroformoxime
copper(I) cyclohexylethynylide
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide at 45℃; for 0.5h; | 93% |
dichloroformoxime
1-copper(I) (3-methylphenyl)ethyne
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide at 45℃; for 0.683333h; | 93% |
dichloroformoxime
1-copper(I) (4-chlorophenyl)ethyne
Conditions | Yield |
---|---|
With iodine; sodium hydrogencarbonate In N,N-dimethyl-formamide at 20℃; for 6.16667h; | 93% |
Conditions | Yield |
---|---|
With iodine; sodium hydrogencarbonate In N,N-dimethyl-formamide at 20℃; for 6.16667h; | 93% |
copper(I) phenylacetylenide
dichloroformoxime
3-chloro-5-phenylisoxazole
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide at 45℃; for 1h; | 92% |
dichloroformoxime
Conditions | Yield |
---|---|
With iodine; sodium hydrogencarbonate In N,N-dimethyl-formamide at 20℃; for 6.16667h; | 92% |
dichloroformoxime
1-copper(I) (4-bromophenyl)ethyne
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide at 45℃; for 0.583333h; | 91% |
dichloroformoxime
Conditions | Yield |
---|---|
With iodine; sodium hydrogencarbonate In N,N-dimethyl-formamide at 20℃; for 6.16667h; | 91% |
dichloroformoxime
1-copper(I) (4-bromophenyl)ethyne
Conditions | Yield |
---|---|
With iodine; sodium hydrogencarbonate In N,N-dimethyl-formamide at 20℃; for 6.16667h; | 91% |
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide at 45℃; for 0.9h; | 90% |
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide at 45℃; for 1.5h; | 90% |
dichloroformoxime
Conditions | Yield |
---|---|
With iodine; sodium hydrogencarbonate In N,N-dimethyl-formamide at 20℃; for 6.16667h; | 90% |
dichloroformoxime
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide at 45℃; for 0.5h; | 89% |
dichloroformoxime
N-allylacetamide
5-<(acetylamino)methyl>-3-chloro-2-isoxazoline
Conditions | Yield |
---|---|
With potassium hydrogencarbonate In water; ethyl acetate for 20h; | 88% |
Conditions | Yield |
---|---|
With iodine; sodium hydrogencarbonate In N,N-dimethyl-formamide at 20℃; for 6.16667h; | 87% |
dichloroformoxime
(p-tolylethynyl)copper
3-chloro-5-(4-methylphenyl)isoxazole
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide at 45℃; for 0.5h; | 85% |
Conditions | Yield |
---|---|
With iodine; sodium hydrogencarbonate In N,N-dimethyl-formamide at 20℃; for 6.16667h; | 84% |
dichloroformoxime
1-copper(I) (4-nitrophenyl)ethyne
3-chloro-5-(4-nitrophenyl)isoxazole
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide at 45℃; for 0.55h; | 83% |
dichloroformoxime
1-copper(I) (4-nitrophenyl)ethyne
Conditions | Yield |
---|---|
With iodine; sodium hydrogencarbonate In N,N-dimethyl-formamide at 20℃; for 6.16667h; | 83% |
styrene
dichloroformoxime
butyl 3-(trichlorovinyl)-4,5-dihydroisoxazole-5-carboxylate
Conditions | Yield |
---|---|
With potassium hydrogencarbonate In 1,2-dimethoxyethane; water at 25℃; for 12h; | 82% |
With silver nitrate In tetrahydrofuran at 60 - 65℃; for 0.333333h; | 73% |
With silver nitrate In tetrahydrofuran at 60 - 65℃; for 0.333333h; Product distribution; Var. alkene; | 73% |
With sodium carbonate In diethyl ether; water for 26h; | 32.02% |
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide at 45℃; for 1.33333h; | 82% |
dichloroformoxime
1-copper(I) (3-methylphenyl)ethyne
Conditions | Yield |
---|---|
With iodine; sodium hydrogencarbonate In N,N-dimethyl-formamide at 20℃; for 6.16667h; | 82% |
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide at 45℃; for 0.2h; | 81% |
Conditions | Yield |
---|---|
With iodine; sodium hydrogencarbonate In N,N-dimethyl-formamide at 20℃; for 6.16667h; | 81% |
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide at 45℃; for 0.5h; | 80% |
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