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Cas:183905-31-9
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inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
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inquiry1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s
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inquiryDayangChem exported this product to many countries and regions at best price. If you are looking for the material's manufacturer or supplier in China, DayangChem is your best choice. Pls contact with us freely for getting detailed product spe
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inquiryName:Acetamide CAS NO:183905-31-9 Grade:Medical scientific research and export Molecular formula: C7H12NCl Molecular weight:193.5 Product Quality 12 years of chemical raw materials Mature operation of the industry System stability Data s
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inquiryProduct Description Product website: http://www.finerchem.com/pro01en/id/1486.html Product Name (S)-1-[(Acetylamino)methyl]-2-ch
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inquiryOur company engages in Sodium Tripolyphosphate (STPP) and Sodium Hexametabphosphate (SHMP) production; development of noble metal catalysts, synthesis of electronic chemical materials and general chemicals Imp&Exp trading business. The company
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inquiryOur advantages: 1. All inquiries will be replied within 12 hours. 2. Dedication to quality, supply & service. 3. Strictly on selecting raw materials. 4. Reasonable & competitive price, fast lead time. 5. Sample is available for your eva
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inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
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inquiryName: (S)-N-[2-(Acetyloxy)-3-chloropropyl]acetamide Synonyms: Acetamide, N-[(2S)-2-(acetyloxy)-3-chloropropyl]-; N-[(2S)-2-(acetyloxy)-3-chloropropyl]-acetamide; Intermediate of Linezolid 1; (S)-1-[(Acetylamino)methyl]-2-chloroethyl acetate CAS: 18
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inquiryAdvantages: Hubei XinRunde Chemical Co., Ltd is a renowned pharmaceutical manufacturer. We can offer high quality products at competitive price in quick delivery with 100% custom pass guaranteed. Never stop striving to offer our best service is
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inquiry1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized
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inquiryOur company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At prese
Cas:183905-31-9
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inquiryAcetaMide, N-[(2S)-2-(acetyloxy)-3-chloropropyl]- CAS:183905-31-9 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializin
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inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
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Cas:183905-31-9
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Cas:183905-31-9
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Cas:183905-31-9
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inquiryCompany Introduction 1. Established in 2005, with two independent business divisions: Fine chemicals division; Pharmaceutical division. 2. Main product: Optical brightener Textile auxiliary Dye stuff Pigments
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inquiryA substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc
Cas:183905-31-9
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inquiryWhy Choose Us: 1. Factory direct sales, so we can provide the competitive price and high quality product base on 8 years of production and R&D experience. 2. It is available in stock for quick shipment.Products could be packaged according to cu
Cas:183905-31-9
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inquirylow price high quality high purity good sevice stock Appearance:off-White Storage:Preserve In Well-Closed, Light-Resistant and Tight Containers. Store In Cool & Dry Place Package:1g,5g,10g...1kg,5kg...more Application:Pharmaceutical int
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inquiryMassive Chemical is certified with ISO9001 and ISO14001 manufacturer for this product. We will offer all documents as requirement for the materials which includes, Certificate of Analysis, Material Safety Data Sheet, and Method of Analysis and
Cas:183905-31-9
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Cas:183905-31-9
Min.Order:10 Gram
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inquiryWe are one of a few suppliers that can offer custom synthesis service of this product We are specialized in custom synthesis, chemical/pharmaceutical/ pesticides outsourcing and contract research. We are committed to prov
Cas:183905-31-9
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inquirySuperior quality, moderate price & quick delivery. Appearance:white crystalline powder Storage:stored in a cool, dry and ventilated place to provent sun and rain Package:25kg/drum, or as per your request. Application:Used as Pharmaceutical
Cas:183905-31-9
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inquiryEstablished in May 2015, TaiChem Ltd. is initially invested by a British research and development company and started by PhDs back from aboard. The company is registered in China Medical City (CMC), Taizhou, Jiangsu Province, and the production site
Cas:183905-31-9
Min.Order:10 Gram
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inquiryProduct name: (S)-N-[2-(Acetyloxy)-3-Chloropropyl]acetamide CAS No.: 183905-31-9 Molecule Formula:C7H12ClNO3 Molecule Weight:No Purity: 99.0% Package: 25kg/drum Description:White powder Manufacture Standards:Enterprise Standard
Cas:183905-31-9
Min.Order:1 Kilogram
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Type:Trading Company
inquiryacetic anhydride
(S)-1-amino-3-chloropropan-2-ol
N-[(2S)-2-acetoxy-3-chloropropyl]acetamide
Conditions | Yield |
---|---|
With triethylamine at 0 - 20℃; for 4h; | 98% |
With pyridine In tetrahydrofuran at 35 - 45℃; for 12h; |
acetic anhydride
N-[(2S)-2-acetoxy-3-chloropropyl]acetamide
Conditions | Yield |
---|---|
With pyridine In dichloromethane at 30℃; for 20h; | 90.6% |
acetic anhydride
N-[(2S)-2-acetoxy-3-chloropropyl]acetamide
Conditions | Yield |
---|---|
With pyridine In dichloromethane at 20 - 40℃; for 22h; | 89% |
With pyridine In dichloromethane at 18 - 40℃; for 5h; | 75% |
With pyridine at 20℃; | 47.98% |
acetyl chloride
N-[(2S)-2-acetoxy-3-chloropropyl]acetamide
Conditions | Yield |
---|---|
With pyridine In dichloromethane at 0 - 20℃; for 10h; | 86.1% |
acetic anhydride
C
N-[(2S)-2-acetoxy-3-chloropropyl]acetamide
Conditions | Yield |
---|---|
With pyridine In dichloromethane for 19h; Time; Temperature; | A n/a B 0.27% C 82.9% |
(S)-N-[[3-[3-fluoro-4-[4-morpholinyl]phenyl]-2-oxo-5-oxazolidinyl]methyl]amine
N-[(2S)-2-acetoxy-3-chloropropyl]acetamide
Conditions | Yield |
---|---|
With sodium hydride In N,N-dimethyl-formamide; mineral oil at 0 - 20℃; for 2h; | 97.9% |
[4-(3-oxo-morpholin-4-yl)phenyl]carbamic acid benzyl ester
N-[(2S)-2-acetoxy-3-chloropropyl]acetamide
(S)-N-[{3-(4-(3-oxomorpholin-4-yl)phenyl)-2-oxo-1,3-oxazolidin-5-yl}methyl]acetamide
Conditions | Yield |
---|---|
With lithium tert-butoxide In dichloromethane; N,N-dimethyl-formamide for 10h; Reagent/catalyst; Reflux; | 93% |
N-ethoxycarbonyl-3-fluoro-4-morpholinyl aniline
N-[(2S)-2-acetoxy-3-chloropropyl]acetamide
linezolid
Conditions | Yield |
---|---|
With lithium; tert-butyl alcohol In tetrahydrofuran; N,N-dimethyl acetamide; isopropyl alcohol at 0 - 20℃; Reagent/catalyst; Solvent; Concentration; | 90.3% |
N-[(2S)-2-acetoxy-3-chloropropyl]acetamide
N-[(2S)oxiranylmethyl]acetamide
Conditions | Yield |
---|---|
With potassium carbonate In methanol for 2h; Ambient temperature; | 89% |
(1-fluoro-5-oxo-6,7,8,9-tetrahydro-5H-benzocyclohepten-2-yl)-carbamic acid ethyl ester
N-[(2S)-2-acetoxy-3-chloropropyl]acetamide
(S)-N-[3-(1-fluoro-5-oxo-6,7,8,9-tetrahydro-5H-benzocyclohepten-2-yl)-2-oxo-oxazolidin-5-ylmethyl]-acetamide
Conditions | Yield |
---|---|
Stage #1: (1-fluoro-5-oxo-6,7,8,9-tetrahydro-5H-benzocyclohepten-2-yl)-carbamic acid ethyl ester With methanol; lithium tert-butoxide In DMF (N,N-dimethyl-formamide); hexane at 20℃; for 3.5h; Stage #2: N-[(2S)-2-acetoxy-3-chloropropyl]acetamide In DMF (N,N-dimethyl-formamide); hexane at 20℃; for 18.5h; | 88% |
With lithium tert-butoxide In hexane; N,N-dimethyl-formamide |
benzyl-carbamic acid benzyl ester
N-[(2S)-2-acetoxy-3-chloropropyl]acetamide
Conditions | Yield |
---|---|
Stage #1: benzyl-carbamic acid benzyl ester With lithium tert-butoxide In tetrahydrofuran at 20℃; for 0.5h; Stage #2: N-[(2S)-2-acetoxy-3-chloropropyl]acetamide In tetrahydrofuran; methanol at 10 - 25℃; for 15.5h; | 82.7% |
(4-bromo-3-fluoro-phenyl)-carbamic acid methyl ester
N-[(2S)-2-acetoxy-3-chloropropyl]acetamide
(5S)-N-[[3-(3-fluoro-4-bromophenyl)-2-oxo-oxazolidin-5-yl]methyl]acetamide
Conditions | Yield |
---|---|
Stage #1: (4-bromo-3-fluoro-phenyl)-carbamic acid methyl ester With lithium tert-butoxide In methanol; N,N-dimethyl-formamide at 5℃; for 1.5h; Inert atmosphere; Stage #2: N-[(2S)-2-acetoxy-3-chloropropyl]acetamide In methanol; N,N-dimethyl-formamide at 25℃; for 20h; Inert atmosphere; | 82.5% |
With lithium tert-butoxide In methanol; N,N-dimethyl-formamide at 20℃; for 20h; |
[4-(3,6-dihydro-2H-pyridin-1-yl)-3-fluoro-phenyl]-carbamic acid benzyl ester
N-[(2S)-2-acetoxy-3-chloropropyl]acetamide
N-{3-[4-(3,6-dihydro-2H-pyridin-1-yl)-3-fluoro-phenyl]-2-oxo-oxazolidin-5-ylmethyl}-acetamide
Conditions | Yield |
---|---|
Stage #1: [4-(3,6-dihydro-2H-pyridin-1-yl)-3-fluoro-phenyl]-carbamic acid benzyl ester With lithium tert-butoxide In tetrahydrofuran; methanol; DMF (N,N-dimethyl-formamide) at 0 - 20℃; Stage #2: N-[(2S)-2-acetoxy-3-chloropropyl]acetamide In tetrahydrofuran; methanol; DMF (N,N-dimethyl-formamide) at 0 - 20℃; | 82% |
N-benzyloxycarbonyl-3-fluoro-4-(4-(pyridin-2-yl)-1H-pyrazol-1-yl)aniline
N-[(2S)-2-acetoxy-3-chloropropyl]acetamide
(S)-N-((3-(3-fluoro-4-(4-(pyridin-2-yl)-1H-pyrazol-1-yl)-phenyl)-2-oxooxazolidin-5-yl)methyl)acetamide
Conditions | Yield |
---|---|
Stage #1: N-benzyloxycarbonyl-3-fluoro-4-(4-(pyridin-2-yl)-1H-pyrazol-1-yl)aniline; N-[(2S)-2-acetoxy-3-chloropropyl]acetamide With methanol In tetrahydrofuran at -5℃; for 0.166667h; Inert atmosphere; Stage #2: With lithium tert-butoxide In tetrahydrofuran at -5 - 17℃; for 16h; Inert atmosphere; Stage #3: With acetic acid In tetrahydrofuran at 10℃; for 0.5h; Inert atmosphere; | 82% |
With lithium tert-butoxide In tetrahydrofuran; methanol at -5 - 20℃; Concentration; Inert atmosphere; Large scale; | 82% |
Stage #1: N-benzyloxycarbonyl-3-fluoro-4-(4-(pyridin-2-yl)-1H-pyrazol-1-yl)aniline With lithium tert-butoxide In tetrahydrofuran for 0.0833333h; Inert atmosphere; Cooling with ice; Stage #2: N-[(2S)-2-acetoxy-3-chloropropyl]acetamide In tetrahydrofuran at 20℃; for 36h; Cooling with ice; | 38.2% |
Stage #1: N-benzyloxycarbonyl-3-fluoro-4-(4-(pyridin-2-yl)-1H-pyrazol-1-yl)aniline With lithium tert-butoxide In tetrahydrofuran for 0.0833333h; Inert atmosphere; Cooling with ice; Stage #2: N-[(2S)-2-acetoxy-3-chloropropyl]acetamide In tetrahydrofuran at 20℃; for 36h; | 38.2% |
benzyl 3-fluoro-4-(4-morpholinyl)phenylcarbamate
N-[(2S)-2-acetoxy-3-chloropropyl]acetamide
linezolid
Conditions | Yield |
---|---|
Stage #1: benzyl 3-fluoro-4-(4-morpholinyl)phenylcarbamate With lithium tert-butoxide In tetrahydrofuran; methanol; N,N-dimethyl-formamide Stage #2: N-[(2S)-2-acetoxy-3-chloropropyl]acetamide at 21℃; for 21h; Solvent; | 80.6% |
Stage #1: benzyl 3-fluoro-4-(4-morpholinyl)phenylcarbamate With lithium tert-butoxide In tetrahydrofuran; methanol at 10 - 25℃; Large scale; Stage #2: N-[(2S)-2-acetoxy-3-chloropropyl]acetamide at 8℃; Temperature; Large scale; | |
With lithium tert-butoxide In tetrahydrofuran; methanol at 20℃; for 16h; | 83 g |
Stage #1: benzyl 3-fluoro-4-(4-morpholinyl)phenylcarbamate With lithium tert-butoxide In tetrahydrofuran; methanol; N,N-dimethyl-formamide at 0 - 5℃; for 4h; Inert atmosphere; Stage #2: N-[(2S)-2-acetoxy-3-chloropropyl]acetamide In tetrahydrofuran; methanol; N,N-dimethyl-formamide at 0 - 20℃; for 46h; Temperature; Inert atmosphere; |
isobutyl 4-(1,1-dioxidothiomorpholin-4-yl)-3,5-difluorophenylcarbamate
N-[(2S)-2-acetoxy-3-chloropropyl]acetamide
Conditions | Yield |
---|---|
Stage #1: isobutyl 4-(1,1-dioxidothiomorpholin-4-yl)-3,5-difluorophenylcarbamate; N-[(2S)-2-acetoxy-3-chloropropyl]acetamide With methanol In acetonitrile at 0 - 5℃; Large scale; Stage #2: With lithium tert-butoxide In tetrahydrofuran; acetonitrile at 16℃; Temperature; Time; Solvent; Large scale; | 80.3% |
With lithium tert-butoxide In tetrahydrofuran; methanol; acetonitrile at 4 - 16℃; for 15.5h; Solvent; Time; Temperature; | 77.6% |
N-[(2S)-2-acetoxy-3-chloropropyl]acetamide
(S)-N-[3-(3-fluoro-4-iodophenyl)-2-oxo-1,3-oxazolidine-5-ylmethyl]acetamide
Conditions | Yield |
---|---|
Stage #1: (3-fluoro-4-iodophenyl)carbamic acid methyl ester With lithium tert-butoxide In methanol; N,N-dimethyl-formamide at 45℃; for 1.5h; Inert atmosphere; Stage #2: N-[(2S)-2-acetoxy-3-chloropropyl]acetamide In methanol; N,N-dimethyl-formamide at 20℃; for 30h; Inert atmosphere; | 79.5% |
Stage #1: (3-fluoro-4-iodophenyl)carbamic acid methyl ester With lithium tert-butoxide In N,N-dimethyl-formamide at 30 - 35℃; for 1h; Inert atmosphere; Stage #2: With methanol In N,N-dimethyl-formamide at 5 - 10℃; for 1.5h; Inert atmosphere; Stage #3: N-[(2S)-2-acetoxy-3-chloropropyl]acetamide In N,N-dimethyl-formamide at 20℃; for 24h; Inert atmosphere; | 79.5% |
Stage #1: (3-fluoro-4-iodophenyl)carbamic acid methyl ester With lithium tert-butoxide In N,N-dimethyl-formamide at 30 - 35℃; for 1h; Inert atmosphere; Stage #2: With methanol In N,N-dimethyl-formamide at 5 - 10℃; for 1.5h; Inert atmosphere; Stage #3: N-[(2S)-2-acetoxy-3-chloropropyl]acetamide In N,N-dimethyl-formamide at 10 - 20℃; for 24h; Inert atmosphere; | 79.5% |
In methanol at 25℃; for 24h; |
N-[(2S)-2-acetoxy-3-chloropropyl]acetamide
(S)-N-[3-(3-fluoro-4-iodophenyl)-2-oxo-1,3-oxazolidine-5-ylmethyl]acetamide
Conditions | Yield |
---|---|
Stage #1: methyl N-(3-iodo-4-fluorophenyl)carbamate With methanol; potassium tert-butylate In N,N-dimethyl-formamide at 0 - 5℃; for 1.5h; Inert atmosphere; Stage #2: N-[(2S)-2-acetoxy-3-chloropropyl]acetamide In N,N-dimethyl-formamide at 25℃; for 24h; Inert atmosphere; | 79.5% |
N-[(2S)-2-acetoxy-3-chloropropyl]acetamide
benzyl benzyl(4-(((benzyloxy)carbonyl)amino)-2-fluorophenyl)carbamate
benzyl 4-{(5S)-5-[(acetylamino)methyl]-2-oxo-1,3-oxazolidin-3-yl}-2-fluorophenyl(benzyl)carbamate
Conditions | Yield |
---|---|
Stage #1: benzyl benzyl(4-{[(benzyloxy)carbonyl]amino}-2-fluorophenyl)carbamate With lithium tert-butoxide In tetrahydrofuran at -5℃; for 0.25h; Inert atmosphere; Stage #2: N-[(2S)-2-acetoxy-3-chloropropyl]acetamide With acetic acid In tetrahydrofuran; methanol at 0 - 5℃; for 17h; | 79% |
Stage #1: benzyl benzyl(4-{[(benzyloxy)carbonyl]amino}-2-fluorophenyl)carbamate With lithium tert-butoxide In tetrahydrofuran for 0.25h; Inert atmosphere; Cooling with ice; Stage #2: N-[(2S)-2-acetoxy-3-chloropropyl]acetamide In tetrahydrofuran at 20℃; | 51.1% |
Stage #1: benzyl benzyl(4-{[(benzyloxy)carbonyl]amino}-2-fluorophenyl)carbamate With lithium tert-butoxide In tetrahydrofuran for 0.25h; Inert atmosphere; Cooling with ice; Stage #2: N-[(2S)-2-acetoxy-3-chloropropyl]acetamide In tetrahydrofuran; methanol at 20℃; | 51.1% |
(3-fluoro-4-iodophenyl)carbamic acid benzyl ester
N-[(2S)-2-acetoxy-3-chloropropyl]acetamide
(S)-N-[3-(3-fluoro-4-iodophenyl)-2-oxo-1,3-oxazolidine-5-ylmethyl]acetamide
Conditions | Yield |
---|---|
Stage #1: (3-fluoro-4-iodophenyl)carbamic acid benzyl ester With lithium tert-butoxide In methanol; N,N-dimethyl-formamide at 45℃; for 1.5h; Inert atmosphere; Stage #2: N-[(2S)-2-acetoxy-3-chloropropyl]acetamide In methanol; N,N-dimethyl-formamide at 20℃; for 30h; Inert atmosphere; | 78.5% |
[3,5-difluoro-4-(4-hydroxy-4-methoxymethyl-piperidin-1-yl)-phenyl]-carbamic acid benzyl ester
N-[(2S)-2-acetoxy-3-chloropropyl]acetamide
(5S)-N-{3-[3,5-difluoro-4-(4-hydroxy-4-methoxymethyl-piperidin-1-yl)phenyl]-2-oxo-oxazolidin-5-ylmethyl}-acetamide
Conditions | Yield |
---|---|
Stage #1: [3,5-difluoro-4-(4-hydroxy-4-methoxymethyl-piperidin-1-yl)-phenyl]-carbamic acid benzyl ester With lithium 2-methylpropan-2-olate In tetrahydrofuran at 20℃; for 3h; Stage #2: N-[(2S)-2-acetoxy-3-chloropropyl]acetamide In tetrahydrofuran; methanol at 10 - 20℃; for 21h; | 77% |
N-[(2S)-2-acetoxy-3-chloropropyl]acetamide
2-methylpropyl [3-fluoro-4-(tetrahydro-2H-thiopyran-4-yl)phenyl]carbamate
Conditions | Yield |
---|---|
With 2-methylbutan-2-ol (lithium salt) In methanol; N,N-dimethyl-formamide at 2 - 23℃; | 73.9% |
{4-[(1α,5α,6α)-6-(tert-butyldimethylsilanyloxy)-3-azabicyclo[3.1.0]hex-3-yl]-3,5-difluorophenyl}carbamic acid benzyl ester
N-[(2S)-2-acetoxy-3-chloropropyl]acetamide
Conditions | Yield |
---|---|
With lithium tert-butoxide In tetrahydrofuran; methanol; N,N-dimethyl-formamide at 20℃; for 20h; | 73% |
With methanol; lithium butoxide In tetrahydrofuran; DMF (N,N-dimethyl-formamide) at 0 - 20℃; for 20h; | 73% |
(1α,5α,6α)-3-(4-benzyloxycarbonylamino-2,6-difluorophenyl)-3-azabicyclo[3.1.0]hexane-6-carboxylic acid tert-butyl ester
N-[(2S)-2-acetoxy-3-chloropropyl]acetamide
(S)-(1α,5α,6α)-3-{4-[5-(acetylaminomethyl)-2-oxooxazolidin-3-yl]-2,6-difluorophenyl}-3-azabicyclo[3.1.0]hexane-6-carboxylic acid tert-butyl ester
Conditions | Yield |
---|---|
With lithium tert-butoxide In tetrahydrofuran; methanol; N,N-dimethyl-formamide at 20℃; for 20h; | 72% |
With methanol; lithium butoxide In tetrahydrofuran; DMF (N,N-dimethyl-formamide) at 0 - 20℃; for 20h; | 72% |
[9-(tetrahydro-pyran-2-yloxy)-6,7,8,9-tetrahydro-5H-cyclohepta[b]pyridin-3-yl]-carbamic acid ethyl ester
N-[(2S)-2-acetoxy-3-chloropropyl]acetamide
N-{2-oxo-3-[9-(tetrahydro-pyran-2-yloxy)-6,7.8.9-tetrahydro-5H-cyclohepta[b]pyridin-3-yl]-oxazolidin-5(S)-ylmethyl}-acetamide
Conditions | Yield |
---|---|
With lithium tert-butoxide In methanol; N,N-dimethyl-formamide | 71% |
Stage #1: [9-(tetrahydro-pyran-2-yloxy)-6,7,8,9-tetrahydro-5H-cyclohepta[b]pyridin-3-yl]-carbamic acid ethyl ester With methanol; lithium tert-butoxide In DMF (N,N-dimethyl-formamide); hexane at 20℃; for 1h; Stage #2: N-[(2S)-2-acetoxy-3-chloropropyl]acetamide In DMF (N,N-dimethyl-formamide); hexane at 0 - 20℃; |
N-[(2S)-2-acetoxy-3-chloropropyl]acetamide
Conditions | Yield |
---|---|
With lithium tert-butoxide In methanol; DMF (N,N-dimethyl-formamide) at 0 - 20℃; for 20h; | 71% |
[4-(3-azabicyclo[3.1.0]hex-3-yl)-3,5-difluorophenyl]carbamic acid benzyl ester
N-[(2S)-2-acetoxy-3-chloropropyl]acetamide
Conditions | Yield |
---|---|
With lithium tert-butoxide In tetrahydrofuran; methanol; N,N-dimethyl-formamide at 20℃; for 20h; | 70% |
With methanol; lithium butoxide In tetrahydrofuran; DMF (N,N-dimethyl-formamide) at 0 - 20℃; for 20h; | 70% |
[(1α,5α,6α)-3-(4-benzyloxycarbonylamino-2,6-difluorophenyl)-3-azabicyclo[3.1.0]hex-6-yl]carbamic acid tert-butyl ester
N-[(2S)-2-acetoxy-3-chloropropyl]acetamide
(S)-((1α,5α,6α)-3-{4-[5-(acetylaminomethyl)-2-oxooxazolidin-3-yl]-2,6-difluorophenyl}-3-azabicyclo[3.1.0]hex-6-yl)carbamic acid tert-butyl ester
Conditions | Yield |
---|---|
With lithium tert-butoxide In tetrahydrofuran; methanol; N,N-dimethyl-formamide at 20℃; for 20h; | 70% |
With methanol; lithium butoxide In tetrahydrofuran; DMF (N,N-dimethyl-formamide) at 0 - 20℃; for 20h; | 70% |
N-[(2S)-2-acetoxy-3-chloropropyl]acetamide
Conditions | Yield |
---|---|
With lithium tert-butoxide In methanol; DMF (N,N-dimethyl-formamide) at 0 - 20℃; for 20h; | 70% |
benzyl 3-fluoro-4-[(1α,5α,6β)-3-thiabicyclo[3.1.0]hex-6-yl]phenylcarbamate
N-[(2S)-2-acetoxy-3-chloropropyl]acetamide
Conditions | Yield |
---|---|
With lithium tert-butoxide In tetrahydrofuran; methanol; N,N-dimethyl-formamide at 0 - 20℃; for 20h; | 68% |
With methanol; lithium tert-butoxide In N,N-dimethyl-formamide |
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