As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem's R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis ch
Cas:1889-71-0
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inquiryOur main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
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inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
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inquiryProduct Name: 4'-Chloro-2-phenylacetophenone Synonyms: -Chloro-2-phenylacetophenone;JR-8345, 4'-Chloro-2-phenylacetophenone, 97%;BENZYL 4-CHLOROPHENYL KETONE;DEOXY-4-CHLOROBENZOIN;CHLORODEOXYBENZOIN;4-CHLORODEOXYBENZOIN;4'-CHLORO-2-
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inquiry1.In No Less 10 years exporting experience. you can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specializ
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inquiryOur Advantage Rich Experience Our products are sold all over Europe,North&South America, Sino-East, Asia and pacific area as well as Africa,we establish long term. Quality service Company cooperates with research institutes. We strictly con
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
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inquiry1. Timely and efficient service to ensure communication with customers 2. Produce products of different specifications and sizes according to your requirements. 3. Quality procedures and standards recognized by SGS. Advanced plant equipment ensures
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inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
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inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
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inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providing h
Our company was built in 2009 with an ISO certificate.In the past 6 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so on.O
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inquiryZhenyu biotech exported this product to many countries and regions at best price. if you are looking for the material's manufacturer or supplier in china, zhenyu biotech is your best choice. pls contact with us freely for getting detailed
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inquiryAppearance:95%+ Package:R&D,Pilot run Transportation:per client require Port:Express ,Air, Sea
High quality,stable supply chain.Appearance:white/off-white or light yellow Storage:Store in cool and dry place, keep away from strong light and heat. Package:aluminum bottle,glass bottle,PTFE bottle,cardboard drum Application:This product can be use
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inquiryR & D enterprises have their own stock in stockAppearance:To be subject to the object Package:Customized Application:pharmaceutical intermediates Transportation:Air Port:Shanghai;Guangzhou
high purity,in stock Package:25kg/drum,or as per customers'demand Application:API,or Intermediates,fine chemicals Transportation:air,sea,courier
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inquiryhigh quality Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea
high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:Foil bag; Drum; Plastic bottle Application:Pharma;Industry;Agricultural Transportation:by sea or air Port:Beijing or Guangzhou
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inquirybulk productiongoods in stockswe have the best competitive price in the marketmeantime,we are committed to service to our every customer Chemsigma International Co.,Ltd. is a chemical manufacturer, specialize in custom synthesis and organic chemical
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inquiryBoiling point 393.8 °C at 760 mmHg Melting point 67 °C Density 1.094 g/cm3 Storage
factory?direct?sale Application:healing drugs
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inquiryFactory supply high purity low priceAppearance:solid or liquid Storage:sealed in cool and dry place Package:As customer's requested Application:Pharma Intermediate Transportation:by courier/air/sea Port:Any port in China
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inquiryWe are committed to providing our customers with the best products and services at the most competitive prices.Appearance:crystalline powder Storage:Room temperature with sealed well Package:according to the clients requirement Application:Use as pri
4'-Chloro-2-phenylacetophenone cas 1889-71-0Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express
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inquiryfactory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin
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inquiryHangzhou ZeErRui Chemical Co., Ltd. is focused on customization, research and development and production of APIs and advanced intermediates, which can effectively compensate for the deficiencies of traditional CRO and CMO. Priority of high-tech barri
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inquiry1889-71-0 Application:intermediate
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Type:Lab/Research institutions
inquiryConditions | Yield |
---|---|
With tetra-n-butylammonium cyanide In tetrahydrofuran for 1.5h; Ambient temperature; | A 12% B 100% |
N-[1-(4-Chloro-phenyl)-1-cyano-2-phenyl-ethyl]-N-phenyl-benzamide
4'-chloro-2-phenylacetophenone
Conditions | Yield |
---|---|
With potassium hydroxide In ethanol; water Heating; | 99% |
S-phenyl 4-chlorobenzothioate
benzyl(bromo)zinc
4'-chloro-2-phenylacetophenone
Conditions | Yield |
---|---|
With (phenyl)(bis-triphenylphosphine)palladium(II) chloride In tetrahydrofuran; toluene at 20℃; for 1h; Fukuyama Coupling; Inert atmosphere; | 98% |
4-chlorobenzenesulfinic acid
phenylacetonitrile
4'-chloro-2-phenylacetophenone
Conditions | Yield |
---|---|
With [2,2]bipyridinyl; sulfuric acid; water; palladium diacetate In 2-methyl-propan-1-ol at 100℃; for 6h; Inert atmosphere; | 95% |
2-(4-chlorophenyl)-2-oxo-1-phenylethyl benzoate
4'-chloro-2-phenylacetophenone
Conditions | Yield |
---|---|
With palladium(II) trifluoroacetate; hydrogen; [(4S)-4-[5-bis(3,5-di-tert-butyl-4-methoxyphenyl)phosphanyl-1,3-benzodioxol-4-yl]-4,5,6,7-tetrahydro-1,3-benzodioxol-5-yl]-bis(3,5-di-tert-butyl-4-methoxyphenyl)phosphane In acetone at 60℃; under 45004.5 Torr; for 24h; Glovebox; Autoclave; chemoselective reaction; | 94% |
2-(4-chlorophenyl)-2-oxo-1-phenylethyl acetate
4'-chloro-2-phenylacetophenone
Conditions | Yield |
---|---|
With tris(bipyridine)ruthenium(II) dichloride hexahydrate; diethyl 2,6-dimethyl-1,4-dihydropyridine-3,5-dicarboxylate; triethylamine In acetonitrile at 20℃; for 1h; Inert atmosphere; UV-irradiation; | 92% |
Conditions | Yield |
---|---|
With bis-triphenylphosphine-palladium(II) chloride; zinc In 1,2-dimethoxyethane for 0.333333h; Ambient temperature; | 90% |
With bis-triphenylphosphine-palladium(II) chloride; zinc In 1,2-dimethoxyethane at 20℃; for 0.5h; Inert atmosphere; Schlenk technique; |
Conditions | Yield |
---|---|
With iron(II) chloride In tetrahydrofuran at 25℃; for 0.5h; Reagent/catalyst; Solvent; Inert atmosphere; Schlenk technique; | 90% |
4'-chloro-2-phenylacetophenone
Conditions | Yield |
---|---|
With ethylenediamine In tetrahydrofuran for 4h; Heating; | 88% |
Conditions | Yield |
---|---|
With zinc(II) oxide at 20℃; for 0.0833333h; Friedel-Crafts acylation; | 85% |
With aluminum (III) chloride In dichloromethane at 0 - 20℃; | 79% |
With aluminium trichloride at 20℃; | 74% |
4-chloro-benzoyl chloride
benzyltetrabutyl stiborane
4'-chloro-2-phenylacetophenone
Conditions | Yield |
---|---|
In tetrahydrofuran for 1h; Ambient temperature; | 85% |
phenyl 1H-imidazole-1-sulfonate
para-chloroacetophenone
4'-chloro-2-phenylacetophenone
Conditions | Yield |
---|---|
With palladium diacetate; caesium carbonate; 4,5-bis(diphenylphos4,5-bis(diphenylphosphino)-9,9-dimethylxanthenephino)-9,9-dimethylxanthene In 1,4-dioxane at 110℃; for 24h; Inert atmosphere; chemoselective reaction; | 84% |
Conditions | Yield |
---|---|
With 1,4-diaza-bicyclo[2.2.2]octane; 3,7-bis(dimethylamine)phenothiazonium In acetonitrile at 25℃; Irradiation; Green chemistry; | 83% |
4'-chloro-2-phenylacetophenone
Conditions | Yield |
---|---|
With ammonium cerium(IV) nitrate In water; acetonitrile at 50 - 55℃; for 0.166667h; | 81% |
4-Chlorophenylboronic acid
phenylacetonitrile
4'-chloro-2-phenylacetophenone
Conditions | Yield |
---|---|
With [2,2]bipyridinyl; potassium fluoride; acetic acid; palladium diacetate In tetrahydrofuran at 80℃; for 48h; | 80% |
phenylacetic acid
Methyl 4-chlorobenzoate
4'-chloro-2-phenylacetophenone
Conditions | Yield |
---|---|
With lithium hexamethyldisilazane In tetrahydrofuran; N,N-dimethyl-formamide at -4℃; Claisen Condensation; Inert atmosphere; | 80% |
With sodium hexamethyldisilazane In N,N-dimethyl-formamide at -10℃; for 3.5h; |
Conditions | Yield |
---|---|
With methanol In water at -5℃; for 0.5h; Irradiation; Green chemistry; | 77% |
1-(2-(4-chlorophenyl)-2-oxoethyl)tetrahydro-1H-thiophen-1-ium tetraphenylborate
4'-chloro-2-phenylacetophenone
Conditions | Yield |
---|---|
In toluene at 120℃; Inert atmosphere; | 76% |
1-(4-chloro-benzoyl)-1H-imidazole
diethyl 2,6-dimethyl-4-benzyl-1,4-dihydropyridine-3,5-dicarboxylate
4'-chloro-2-phenylacetophenone
Conditions | Yield |
---|---|
With [4,4’-bis(1,1-dimethylethyl)-2,2’-bipyridine-N1,N1‘]bis [3,5-difluoro-2-[5-(trifluoromethyl)-2-pyridinyl-N]phenyl-C]iridium(III) hexafluorophosphate; caesium carbonate; 1,4-dimethyl-1,2,4-triazolium iodide In acetonitrile at 20℃; Inert atmosphere; Irradiation; Sealed tube; | 76% |
benzyl chloride
4-chloro-benzoyl chloride
4'-chloro-2-phenylacetophenone
Conditions | Yield |
---|---|
With nickel In 1,2-dimethoxyethane at 85℃; for 0.25h; | 72% |
tris(4-chlorophenyl)bismuthane
phenylacetyl chloride
A
4,4'-dichlorobiphenyl
B
4'-chloro-2-phenylacetophenone
Conditions | Yield |
---|---|
With bis-triphenylphosphine-palladium(II) chloride; triethylamine In tetrahydrofuran at 80℃; for 3h; Schlenk tube; Inert atmosphere; | A n/a B 71% |
4-vinylbenzyl chloride
benzenediazonium tetrafluoroborate
4'-chloro-2-phenylacetophenone
Conditions | Yield |
---|---|
With ascorbic acid In N,N-dimethyl-formamide at 20℃; for 20h; Cooling with ice; | 71% |
N-Benzyl-N-(benzylsulfanyl-phenyl-methyl)-4-chloro-benzamide
A
N-benzylidene benzylamine
B
4'-chloro-2-phenylacetophenone
Conditions | Yield |
---|---|
With lithium diisopropyl amide In tetrahydrofuran for 4h; Ambient temperature; addition, -70 deg C; | A n/a B 70% C n/a |
1-(4-Chloro-phenyl)-2-phenyl-1-quinazolin-4-yl-ethanol
4'-chloro-2-phenylacetophenone
Conditions | Yield |
---|---|
With potassium cyanide In N,N-dimethyl-formamide at 80℃; for 1h; | 68% |
1-(4-Chloro-phenyl)-2-phenyl-1-quinazolin-4-yl-ethanol
A
quinazoline-4-carbonitrile
B
quinazoline-4-carbonamide
C
4-benzyl-quinazoline
D
4'-chloro-2-phenylacetophenone
Conditions | Yield |
---|---|
With potassium cyanide In N,N-dimethyl-formamide at 80℃; for 1h; | A 9% B 10% C 9% D 68% |
sodium p-chlorobenzenesulphinate
phenylacetonitrile
4'-chloro-2-phenylacetophenone
Conditions | Yield |
---|---|
With palladium(II) trifluoroacetate; trifluoroacetic acid; 6-methyl-2,2'-bipyridine In tetrahydrofuran; water at 100℃; for 1h; Microwave irradiation; | 66% |
Conditions | Yield |
---|---|
With copper(l) cyanide; lithium chloride In tetrahydrofuran at 0℃; for 2h; Inert atmosphere; | 60% |
Conditions | Yield |
---|---|
With dipotassium hydrogenphosphate; nickel(II) chloride hexahydrate; 4-acetoxybenzophenone; 4,4'-di-tert-butyl-2,2'-bipyridine at 35℃; for 48h; Inert atmosphere; Sealed tube; Irradiation; Schlenk technique; | 60% |
4'-chloro-2-phenylacetophenone
Conditions | Yield |
---|---|
With potassium hydroxide In ethanol Heating; | 58% |
benzyl (N-benzyl-p-chlorobenzamido)methylsulfide
4'-chloro-2-phenylacetophenone
Conditions | Yield |
---|---|
With sodium hydride In tetrahydrofuran for 13h; Heating; | 55% |
With sodium hydride In tetrahydrofuran for 13h; Heating; | 55% |
Conditions | Yield |
---|---|
With bromine In diethyl ether for 0.5h; | 100% |
With copper(II) nitrate trihydrate; hydrogen bromide; oxygen In acetic acid at 60℃; for 4.5h; Green chemistry; | 91% |
With bromine In chloroform; acetic acid at 20℃; for 24h; | 86% |
4'-chloro-2-phenylacetophenone
4-chlorobenzil
Conditions | Yield |
---|---|
With 1,4-diaza-bicyclo[2.2.2]octane In N,N-dimethyl-formamide at 90℃; for 24h; | 100% |
With potassium hydrogencarbonate; dimethyl sulfoxide at 80℃; | 91% |
With oxygen; copper(II) acetate monohydrate; potassium carbonate In N,N-dimethyl-formamide at 50℃; under 760.051 Torr; for 0.5h; | 87% |
N,N-dimethyl-formamide dimethyl acetal
4'-chloro-2-phenylacetophenone
C17H16ClNO
Conditions | Yield |
---|---|
In toluene at 20 - 50℃; for 156h; | 100% |
3-Iodotoluene
4'-chloro-2-phenylacetophenone
1-(4-chlorophenyl)-2-phenyl-2-m-tolylethanone
Conditions | Yield |
---|---|
With copper(l) iodide; 1,10-Phenanthroline; caesium carbonate In 1,4-dioxane at 110℃; for 24h; Inert atmosphere; | 99% |
3,5-dimethylphenyl iodide
4'-chloro-2-phenylacetophenone
1-(4-chlorophenyl)-2-(3,5-dimethylphenyl)-2-phenylethanone
Conditions | Yield |
---|---|
With copper(l) iodide; 1,10-Phenanthroline; caesium carbonate In 1,4-dioxane at 110℃; for 24h; Inert atmosphere; | 99% |
With copper(l) iodide; caesium carbonate; 1,7-phenanthroline In 1,4-dioxane at 110℃; for 24h; Inert atmosphere; | 95% |
4-fluoro-1-iodobenzene
4'-chloro-2-phenylacetophenone
2-(4-fluorophenyl)-2-(4-chlorophenyl)-1-phenylethanone
Conditions | Yield |
---|---|
With copper(l) iodide; 2-acetylcyclohexanone; caesium carbonate In tert-butyl alcohol at 70℃; for 24h; Inert atmosphere; | 99% |
4'-chloro-2-phenylacetophenone
(1S)-(-)-1-(4'-chlorophenyl)-2-phenylethanol
Conditions | Yield |
---|---|
With (S)-methyl oxazaboralidine; borane In tetrahydrofuran at 30℃; for 1h; | 98% |
With D-glucose In ethanol; hexane; water; allyl alcohol at 50℃; for 168h; optical yield given as %ee; enantioselective reaction; |
4'-chloro-2-phenylacetophenone
(R)-1-(4'-chlorophenyl)-2-phenylethanol
Conditions | Yield |
---|---|
With borane-THF In tetrahydrofuran at 30℃; for 16h; Inert atmosphere; optical yield given as %ee; enantioselective reaction; | 98% |
Multi-step reaction with 2 steps 1: sodium tetrahydroborate / methanol; dichloromethane / 24 h / 20 °C 2: Pseudomonas cepacia lipase / tert-butyl methyl ether / 168 h / 20 °C / Resolution of racemate View Scheme | |
Multi-step reaction with 2 steps 1: sodium tetrahydroborate / methanol; dichloromethane / 24 h / 20 °C 2: Porcine pancreas lipase type II / tert-butyl methyl ether / 264 h / 40 °C / Resolution of racemate View Scheme |
5,5-dimethyl-2-(2-methylallyl)-1,3,2-dioxaborinane
4'-chloro-2-phenylacetophenone
(R)-2-(4-chlorophenyl)-4-methyl-1-phenylpent-4-en-2-ol
Conditions | Yield |
---|---|
With (S)-3,3'-difluoro-1,1'-binaphthyl-2,2'-diol In tert-Amyl alcohol at 40℃; for 2h; Inert atmosphere; enantioselective reaction; | 97% |
Conditions | Yield |
---|---|
With tetrabutylammonium tricarbonylnitrosylferrate In acetonitrile at 100℃; for 30h; Michael Addition; Inert atmosphere; Schlenk technique; | 97% |
4'-chloro-2-phenylacetophenone
1-(4-chlorophenyl)-2-phenylethanol
Conditions | Yield |
---|---|
With sodium tetrahydroborate In ethanol | 96% |
With sodium tetrahydroborate In methanol; dichloromethane at 20℃; for 24h; | 94% |
With C19H29N4Ru(1+)*C24H20B(1-); potassium hydroxide In isopropyl alcohol at 80℃; for 2h; Inert atmosphere; Schlenk technique; | 92% |
1,2-diamino-benzene
4'-chloro-2-phenylacetophenone
2-(4-chlorophenyl)-3-phenylquinoxaline
Conditions | Yield |
---|---|
With 1,4-diaza-bicyclo[2.2.2]octane In N,N-dimethyl-formamide at 90℃; for 3h; | 96% |
With [Cu(II)[5,11,17,23-tetrakis(trimethylammonium)-25,26,27,28-tetrahydroxycalix[4]arene](H2O)]I2; oxygen; potassium carbonate In water for 15h; Reflux; Green chemistry; | 88% |
2-azido-1,3-dimethyl-4,5-dihydro-1H-imidazol-3-ium hexafluorophosphate (V)
4'-chloro-2-phenylacetophenone
C19H20ClN3O
Conditions | Yield |
---|---|
With triethylamine In tetrahydrofuran; acetonitrile at 0℃; for 0.5h; | 96% |
methanol
4'-chloro-2-phenylacetophenone
1-(4-chlorophenyl)-2-phenyl-1-propanone
Conditions | Yield |
---|---|
With C34H27IrN2P(1+)*C32H12BF24(1-); caesium carbonate at 65℃; for 24h; Inert atmosphere; | 96% |
With sodium hydroxide at 100℃; for 15h; Sealed tube; Autoclave; Inert atmosphere; | 85% |
bromoacetic acid methyl ester
4'-chloro-2-phenylacetophenone
β-p-Chlorbenzoyl-β-phenyl-propionsaeure-methylester
Conditions | Yield |
---|---|
With sodium hydride In dimethyl sulfoxide at 20℃; for 1h; | 95% |
benzaldehyde
toluene-4-sulfonamide
4'-chloro-2-phenylacetophenone
(2S,3S)-1-(4-chlorophenyl)-2,3-diphenyl-3-(tosylamino)propan-1-one
Conditions | Yield |
---|---|
With C35H32F6N4OS In toluene at 0℃; for 35h; Mannich Aminomethylation; Molecular sieve; enantioselective reaction; | 95% |
Conditions | Yield |
---|---|
With 1,8-diazabicyclo[5.4.0]undec-7-ene In dimethyl sulfoxide at 25℃; for 0.82h; regioselective reaction; | 95% |
2-Amino-5-chlorobenzophenone
4'-chloro-2-phenylacetophenone
2-(4-chlorophenyl)-3,4-diphenyl-6-chloroquinoline
Conditions | Yield |
---|---|
With 2,4,6-tripropyl-1,3,5,2,4,6-trioxatriphosphinane-2,4,6-trioxide In ethyl acetate at 60℃; Friedlaender synthesis; | 94% |
Conditions | Yield |
---|---|
With C34H27MnNO3P2(1+)*Br(1-); potassium tert-butylate In tert-Amyl alcohol at 135℃; for 24h; | 94% |
4'-chloro-2-phenylacetophenone
1,4-bis(4-chlorophenyl)-2,3-diphenylbutane-1,4-dione
Conditions | Yield |
---|---|
With silver fluoride In 5,5-dimethyl-1,3-cyclohexadiene at 140℃; for 4.5h; | 93% |
With copper(II) acetate monohydrate In 5,5-dimethyl-1,3-cyclohexadiene at 140℃; for 2h; | 81% |
In benzene Irradiation; |
Conditions | Yield |
---|---|
With 1,8-diazabicyclo[5.4.0]undec-7-ene In dimethyl sulfoxide at 25℃; for 0.5h; regioselective reaction; | 93% |
2-aminopyridine
4'-chloro-2-phenylacetophenone
2-(4-chlorophenyl)-3-phenylimidazo[1,2-a]pyridine
Conditions | Yield |
---|---|
With potassium hydrogencarbonate In acetonitrile at 80℃; for 4h; | 91% |
thiourea
4'-chloro-2-phenylacetophenone
Conditions | Yield |
---|---|
With cesium bicarbonate; Bromotrichloromethane In acetonitrile at 80℃; for 2h; | 91% |
Conditions | Yield |
---|---|
With tetra(n-butyl)ammonium hydrogensulfate; potassium hydroxide In water at 100℃; for 24h; Inert atmosphere; regioselective reaction; | 91% |
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