CAS No.19945-61-0,(3E)-4,8-dimethylnona-1,3,7-triene Suppliers

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(3E)-4,8-dimethylnona-1,3,7-triene CAS 19945-61-0

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(3E)-4,8-dimethylnona-1,3,7-triene CAS:19945-61-0

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(3E)-4,8-dimethylnona-1,3,7-triene

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(E)-4,8-dimethyl-1,3,7-nonatriene

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(3E)-4,8-DIMETHYLNONA-1,3,7-TRIENECASAppearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express

(3E)-4,8-DIMETHYLNONA-1,3,7-TRIENECAS

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(3E)-4,8-Dimethyl-1,3,7-nonatriene

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1,3,7-Nonatriene,4,8-dimethyl-, (3E)- CAS No.: 19945-61-0 Storage:as prescribe by the manufaurer Package:pack as requested

1,3,7-Nonatriene,4,8-dimethyl-, (3E)-

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Synthetic route

: 141-27-5
3,7-dimethyl-2,6-octadienal

: 1779-49-3
Methyltriphenylphosphonium bromide

: 19945-61-0
(E)-4,8-dimethylnona-1,3,7-triene

Conditions

Conditions	Yield
With sodium hexamethyldisilazane In tetrahydrofuran at 0 - 25℃;	92%
With potassium tert-butylate In dichloromethane Wittig reaction; Inert atmosphere;	84%
Stage #1: Methyltriphenylphosphonium bromide With sodium hexamethyldisilazane In tetrahydrofuran at 25℃; for 1h; Stage #2: 3,7-dimethyl-2,6-octadienal In tetrahydrofuran at 25℃; for 6h; Wittig reaction;	77%

: 78130-96-8
geranyl mesylate

: 47025-43-4, 19365-61-8
methylenetriphenylarsorane

: 19945-61-0
(E)-4,8-dimethylnona-1,3,7-triene

Conditions

Conditions	Yield
With n-butyllithium In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; hexane for 1h; Ambient temperature;	91%

: 141-27-5
3,7-dimethyl-2,6-octadienal

MePPh3Br: MePPh3Br

: 19945-61-0
(E)-4,8-dimethylnona-1,3,7-triene

Conditions

Conditions	Yield
With n-butyllithium In tetrahydrofuran Condensation;	90%

: 141-27-5
3,7-dimethyl-2,6-octadienal

: 18107-18-1
diazomethyl-trimethyl-silane

: 19945-61-0
(E)-4,8-dimethylnona-1,3,7-triene

Conditions

Conditions	Yield
With Wilkinson's catalyst; triphenylphosphine; isopropyl alcohol In tetrahydrofuran at 25℃; for 2h;	90%
With triphenylphosphine; isopropyl alcohol; RhCl(PPh3)3 In tetrahydrofuran at 25℃;	90%
With (IMes)CuCl; triphenylphosphine; isopropyl alcohol In 1,4-dioxane; diethyl ether at 60℃; for 16h;	74%

: 105865-47-2
dibromo-1,1 dimethyl-4,8 nonadiene-3 E, 7

A: 19945-61-0
(E)-4,8-dimethylnona-1,3,7-triene

B: 105865-53-0
2-Methyl-2-(4-methyl-pent-3-enyl)-bicyclo[1.1.0]butane

Conditions

Conditions	Yield
With n-butyllithium In diethyl ether at -30℃;	A 89% B 10%

: 78130-96-8
geranyl mesylate

: 2181-42-2
trimethylsulphonium iodide

: 19945-61-0
(E)-4,8-dimethylnona-1,3,7-triene

Conditions

Conditions	Yield
With n-butyllithium; lithium iodide In tetrahydrofuran; hexane from 0 degC to room temp.;	85%

: 141-27-5
3,7-dimethyl-2,6-octadienal

: 2065-66-9
methyl-triphenylphosphonium iodide

: 19945-61-0
(E)-4,8-dimethylnona-1,3,7-triene

Conditions

Conditions	Yield
Stage #1: methyl-triphenylphosphonium iodide With phenyllithium In tetrahydrofuran; diethyl ether; cyclohexane at 20℃; for 0.5h; Wittig Olefination; Inert atmosphere; Cooling with ice; Stage #2: 3,7-dimethyl-2,6-octadienal In tetrahydrofuran; diethyl ether; cyclohexane at 0 - 20℃; for 2h; Inert atmosphere;	80%
Stage #1: methyl-triphenylphosphonium iodide With phenyllithium In tetrahydrofuran; hexane at 0 - 20℃; Stage #2: 3,7-dimethyl-2,6-octadienal In tetrahydrofuran; hexane at 0 - 20℃;	60 g
With potassium tert-butylate In tetrahydrofuran Wittig Olefination;

: 106-24-1
Geraniol

: 18107-18-1
diazomethyl-trimethyl-silane

: 19945-61-0
(E)-4,8-dimethylnona-1,3,7-triene

Conditions

Conditions	Yield
Stage #1: Geraniol With 1,10-Phenanthroline; potassium tert-butylate; copper(l) chloride In fluorobenzene at 20℃; for 0.166667h; Inert atmosphere; Stage #2: With 1-methyl-1H-imidazole; di-tert-butyl-diazodicarboxylate; oxygen In fluorobenzene Reflux; Stage #3: diazomethyl-trimethyl-silane With triphenylphosphine; isopropyl alcohol In fluorobenzene; diethyl ether at 60℃; Inert atmosphere;	74%

: 81678-25-3
3,7-dimethyl-1-(N-methyl-2-imidazolylthio)-2,6-octadiene

A: 19945-61-0
(E)-4,8-dimethylnona-1,3,7-triene

B: 82895-46-3
1-Methyl-2-tributylstannanylmethylsulfanyl-1H-imidazole

C: 82895-45-2
2-((E)-3,7-Dimethyl-1-tributylstannanyl-octa-2,6-dienylsulfanyl)-1-methyl-1H-imidazole

Conditions

Conditions	Yield
With n-butyllithium; tri-n-butylstannylmethyl iodide Product distribution;	A 45% B 43% C 31%
With n-butyllithium; tri-n-butylstannylmethyl iodide Yield given. Multistep reaction;	A n/a B 43% C 31%

...Expand

: 593-60-2
Vinyl bromide

: 22842-10-0
2-methylhept-2-en-6-yne

: 75-24-1
trimethylaluminum

: 19945-61-0
(E)-4,8-dimethylnona-1,3,7-triene

Conditions

Conditions	Yield
(i) Zr catalyst, (ii) /BRN= 1361370/, Pd(PPh3)2Cl2, iBu2AlH, ZnCl2; Multistep reaction;

...Expand

: 75-11-6
diiodomethane

: 106-26-3
cis-3,7-dimethyl-2,6-octadienal

: 19945-61-0
(E)-4,8-dimethylnona-1,3,7-triene

Conditions

Conditions	Yield
With trimethylaluminum; zinc In tetrahydrofuran; hexane

: 69405-35-2
homogeranyl bromide

: 19945-61-0
(E)-4,8-dimethylnona-1,3,7-triene

Conditions

Conditions	Yield
With potassium hydroxide In methanol for 2h; Heating;

: 56691-80-6
geranyl phenyl sulfone

: 19945-61-0
(E)-4,8-dimethylnona-1,3,7-triene

Conditions

Conditions	Yield
With n-butyllithium; tri-n-butylstannylmethyl iodide 1.) THF, -78 deg C, 2.) -78 deg C, 1 h; Yield given. Multistep reaction;

: 82895-40-7
2-[(2E)-3,7-dimethyl-2,6-octadienyl]sulfanylpyridine

: 19945-61-0
(E)-4,8-dimethylnona-1,3,7-triene

Conditions

Conditions	Yield
With n-butyllithium; tri-n-butylstannylmethyl iodide 1.) THF, -78 deg C, 30 min, 2.) -78 deg C, 20 min and 0 deg C 1.5 h; Yield given. Multistep reaction;
With n-butyllithium; tri-n-butylstannylmethyl iodide 1) hexane, THF, -78 deg C, 30 min; 2) hexane, THF, -78 de C, 20 min; o deg C, 10 min; Yield given. Multistep reaction;

: 81678-25-3
3,7-dimethyl-1-(N-methyl-2-imidazolylthio)-2,6-octadiene

: 19945-61-0
(E)-4,8-dimethylnona-1,3,7-triene

Conditions

Conditions	Yield
Yield given. Multistep reaction;

: ((E)-2-Benzenesulfonyl-4,8-dimethyl-nona-3,7-dienyl)-trimethyl-silane

: 19945-61-0
(E)-4,8-dimethylnona-1,3,7-triene

Conditions

Conditions	Yield
With fluoride Yield given;

: 19493-09-5
Methylenetriphenylphosphorane

: 5392-40-5
(E/Z)-3,7-dimethyl-2,6-octadienal

A: 19945-61-0
(E)-4,8-dimethylnona-1,3,7-triene

B: 21214-62-0
(3Z)-4,8-dimethylnona-1,3,7-triene

Conditions

Conditions	Yield
Yield given. Yields of byproduct given;

...Expand

: C14H27(2)HSi

A: 19945-61-0
(E)-4,8-dimethylnona-1,3,7-triene

B: 21214-62-0
(3Z)-4,8-dimethylnona-1,3,7-triene

Conditions

Conditions	Yield
With P450 enzyme; Phaseolus lunatus Yield given. Yields of byproduct given;

: 141-27-5
3,7-dimethyl-2,6-octadienal

: 19493-09-5
Methylenetriphenylphosphorane

: 19945-61-0
(E)-4,8-dimethylnona-1,3,7-triene

Conditions

Conditions	Yield
In tetrahydrofuran Substitution;
Wittig Olefination;

: 56691-80-6
geranyl phenyl sulfone

(tributylstannyl)methyl iodide: (tributylstannyl)methyl iodide

: 19945-61-0
(E)-4,8-dimethylnona-1,3,7-triene

Conditions

Conditions	Yield
With n-butyllithium; ammonium chloride 1) hexane, THF, -78 deg C, 95 min; Yield given. Multistep reaction;

: 92531-85-6
2-((phenylsulfonyl)methyl)prop-2-enylphenylsulfone

(tributylstannyl)methyl iodide: (tributylstannyl)methyl iodide

A: 19945-61-0
(E)-4,8-dimethylnona-1,3,7-triene

B: 82895-44-1
2,6-dimethyl-8-(2-pyridylthio)-2,6-dodecadiene

Conditions

Conditions	Yield
With n-butyllithium; ammonium chloride 1) hexane, THF, -78 deg C, 60 min; RT, 1 h; Yield given. Multistep reaction;

...Expand

: 106-24-1
Geraniol

: 19945-61-0
(E)-4,8-dimethylnona-1,3,7-triene

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: 7 percent / SO3*pyridine; DMSO; Et3N / CH2Cl2 / -10 °C 2: 92 percent / NaHMDS / tetrahydrofuran / 0 - 25 °C View Scheme
Multi-step reaction with 2 steps 1: (COCl)2; DMSO / CH2Cl2 2: tetrahydrofuran View Scheme
Multi-step reaction with 2 steps 1: 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene / acetonitrile / 3 h / 0 °C / pH 7 / Inert atmosphere 2: potassium tert-butylate / tetrahydrofuran / 0.5 h / 20 °C / Inert atmosphere View Scheme

: 106-24-1
Geraniol

sodium ammonium: sodium ammonium

: 19945-61-0
(E)-4,8-dimethylnona-1,3,7-triene

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: 79 percent / MnO2 / CH2Cl2 2: 90 percent / n-BuLi / tetrahydrofuran View Scheme

: 5389-87-7
1-chloro-3,7-dimethylocta-2,6-diene

: 19945-61-0
(E)-4,8-dimethylnona-1,3,7-triene

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: 80 percent / tetrabutylammonium bromide / tetrahydrofuran / 17 h / Ambient temperature 2: 1) butyllithium; 2) aq. NH4Cl / 1) hexane, THF, -78 deg C, 95 min View Scheme
Multi-step reaction with 2 steps 1: butan-2-one View Scheme
Multi-step reaction with 2 steps 2: 1.) n-butyllithium(in hexane), 2.) tri-n-butylstannylmethyl iodide / 1.) THF, -78 deg C, 30 min, 2.) -78 deg C, 20 min and 0 deg C 1.5 h View Scheme
Multi-step reaction with 2 steps 1: tetrabutylammonium bromide 2: 1.) n-butyllithium(in hexane), 2.) tri-n-butylstannylmethyl iodide / 1.) THF, -78 deg C, 2.) -78 deg C, 1 h View Scheme

: 2270-59-9
1-bromo-4-methylpent-3-ene

: 19945-61-0
(E)-4,8-dimethylnona-1,3,7-triene

Conditions

Conditions	Yield
Multi-step reaction with 3 steps 1: (i) Mg, Et2O, (ii) /BRN= 1633817/ 2: aq. HBr / 0.5 h / 10 - 15 °C 3: KOH / methanol / 2 h / Heating View Scheme

: 65017-88-1
2-cyclopropyl-6-methyl-hept-5-en-2-ol

: 19945-61-0
(E)-4,8-dimethylnona-1,3,7-triene

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: aq. HBr / 0.5 h / 10 - 15 °C 2: KOH / methanol / 2 h / Heating View Scheme

: 1313-13-9
manganese dioxide

: 106-24-1
Geraniol

: 19945-61-0
(E)-4,8-dimethylnona-1,3,7-triene

Conditions

Conditions	Yield
In dichloromethane

: 1193-10-8
3-methyl-2,5-dihydrothiophen-1,1-dioxide

: 1192-16-1
2,3-dihydrothiophene-1,1-dioxide

: 19945-61-0
(E)-4,8-dimethylnona-1,3,7-triene

Conditions

Conditions	Yield
With sodium hydroxide In diethyl ether; water

: 50-00-0
formaldehyd

: triethylgeranylphosphonium bromide

: 19945-61-0
(E)-4,8-dimethylnona-1,3,7-triene

Conditions

Conditions	Yield
With potassium carbonate In water at 100℃; for 0.0833333h; Wittig reaction; Microwave irradiation;

: 13038-21-6
non-8-en-1-ol

: 19945-61-0
(E)-4,8-dimethylnona-1,3,7-triene

: (8Z,10E)-11,15-dimethylhexadeca-8,10,14-trien-1-ol

Conditions

Conditions	Yield
With C35H47N3O4Ru In neat (no solvent) at 50℃; for 24h; Cross Metathesis; Inert atmosphere; chemoselective reaction;	95%

: 19945-61-0
(E)-4,8-dimethylnona-1,3,7-triene

: 459-88-1
(E)-4,8-dimethylnona-3,7-dien-1-ol

Conditions

Conditions	Yield
Stage #1: (E)-4,8-dimethylnona-1,3,7-triene With disiamylborane In tetrahydrofuran at 0 - 20℃; for 16h; Inert atmosphere; Stage #2: With dihydrogen peroxide; sodium hydroxide In tetrahydrofuran; ethanol at 0 - 20℃; for 3h; Inert atmosphere; stereoselective reaction;	91%
With sodium hydroxide; 9-borabicyclo[3.3.1]nonane dimer; dihydrogen peroxide In tetrahydrofuran at 0℃;	75%
With sodium hydroxide; (Si1)2BH; dihydrogen peroxide In tetrahydrofuran Addition;
Stage #1: (E)-4,8-dimethylnona-1,3,7-triene With 9-bora-bicyclo[3.3.1]nonane In tetrahydrofuran Stage #2: With dihydrogen peroxide

: 74-90-8
hydrogen cyanide

: 19945-61-0
(E)-4,8-dimethylnona-1,3,7-triene

: 2,6-dimethyl-2-propenyl-hept-5-enenitrile

Conditions

Conditions	Yield
rac-1,2-trans-bis-(diphenylphosphinooxy)cyclohexane; bis(1,5-cyclooctadiene)nickel (0) In toluene at 50℃; for 24h;	83%

: 19945-61-0
(E)-4,8-dimethylnona-1,3,7-triene

: 318967-93-0
(E)-2-bromo-6-methylocta-2,6-diene-1,8-diol

: 64218-02-6
plaunotol

Conditions

Conditions	Yield
Stage #1: (E)-4,8-dimethylnona-1,3,7-triene With 9-borabicyclo[3.3.1]nonane dimer In tetrahydrofuran at 20℃; for 4h; Reduction; Stage #2: (E)-2-bromo-6-methylocta-2,6-diene-1,8-diol With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; triphenyl-arsane; caesium carbonate In N,N-dimethyl-formamide at 50℃; for 2.5h; Suzuki coupling;	77%

: 19945-61-0
(E)-4,8-dimethylnona-1,3,7-triene

: 168113-15-3
(E)-2,2-dimethyl-3-(3-methylhexa-3,5-dienyl) oxirane

Conditions

Conditions	Yield
With 3-chloro-benzenecarboperoxoic acid In dichloromethane at 0℃;	75%

: 19945-61-0
(E)-4,8-dimethylnona-1,3,7-triene

: 117582-50-0
(Z)-β-bromocrotyl alcohol 2-tetrahydropyranyl ether

: 280-64-8
9-bora-bicyclo[3.3.1]nonane

: 110990-63-1
(2Z,6E)-3,7,11-trimethyl-2,6,10-dodecatrien-1-ol 2-tetrahydropyranyl ether

Conditions

Conditions	Yield
With sodium hydroxide; cis-dichloro-1,1'-bis(diphenylphosphino)ferrocene palladium(II) In tetrahydrofuran; N,N-dimethyl-formamide To a soln. of triene is added a soln. of 9-BBN at 0°C over 10 min, mixt. stirred for 1 h at 0°C, then for 4 h at room temp., addn. of soln. of bromocrotyl ether, catalyst and NaOH, after heating at 50°C for 8 h poured into water.; Extracted with benzene, washed with water, dried (MgSO4), chromy. over silica gel with benzene-acetate, final product is identified by (1)H NMR, IR, elem. anal.;	67%

Yield

With sodium hydroxide; cis-dichloro-1,1'-bis(diphenylphosphino)ferrocene palladium(II) In tetrahydrofuran; N,N-dimethyl-formamide To a soln. of triene is added a soln. of 9-BBN at 0°C over 10 min, mixt. stirred for 1 h at 0°C, then for 4 h at room temp., addn. of soln. of bromocrotyl ether, catalyst and NaOH, after heating at 50°C for 8 h poured into water.; Extracted with benzene, washed with water, dried (MgSO4), chromy. over silica gel with benzene-acetate, final product is identified by (1)H NMR, IR, elem. anal.;

67%

...Expand

: 19945-61-0
(E)-4,8-dimethylnona-1,3,7-triene

: 126554-35-6
methyl 2-diazobut-3-enoate

: 4-methyl-4-(4-methyl-pent-3-enyl)-cyclohepta-1,5-dienecarboxylic acid methyl ester

Conditions

Conditions	Yield
With Rh2(S-PTAD)4 In hexane; toluene at 20℃; Reflux;	67%

Conditions

Conditions	Yield
With dibenzyl diselenide In tetrahydrofuran; acetonitrile at 20℃; for 18h; regioselective reaction;	66%

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