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inquiryName: Manganese(IV) oxide Synonyms: Manganese dioxide CAS:1313-13-9 MF: MnO2 Appearance:black powder Storage:Store in cool and dry place, away from sun light. Package: 25kgs/drum Application: It is used for the preparation of manganese salt, ox
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inquirymanganese(IV) oxide
Conditions | Yield |
---|---|
at 430℃; for 4h; | 95.5% |
In neat (no solvent) Kinetics; byproducts: nitrous gases; investigation of thermal decompn. at 163-196 °C;; | |
With chlorine In water Irradiation (UV/VIS); |
manganese(II) nitrate
manganese(IV) oxide
Conditions | Yield |
---|---|
at 430℃; for 4h; | 95.5% |
Conditions | Yield |
---|---|
In neat (no solvent, solid phase) byproducts: Cl2, O2; thermal decompn., 190-240°C; | A 95% B 5% |
manganese(IV) oxide
Conditions | Yield |
---|---|
With fluorine In nitric acid oxidn. of weakly H2SO4-acidic ice-cooled Mn(II)-salt-soln. with F2;; | 91.5% |
With hypochloric acid In not given | |
With bromine In ammonia oxidn. of ammoniacal Mn(II)-salt-soln. at 50 °C with Br2;; |
A
manganese(IV) oxide
Conditions | Yield |
---|---|
With O2 In pyridine 1 atm O2, refluxing for 10 h (pptn.); collection (filtration); second crop and MnO2 on evapn. of filtrate; elem. anal.; | A 7% B 90% |
Mn(N,N'-bis(salicylaldehyde)-1,1,2,2-tetramethylethylenediimine)
A
manganese(IV) oxide
Conditions | Yield |
---|---|
With O2 In pyridine 1 atm O2, refluxing for 10 h (pptn.); collection (filtration); second crop and MnO2 on evapn. of filtrate; elem. anal.; | A 10% B 90% |
A
manganese(IV) oxide
Conditions | Yield |
---|---|
With O2 In pyridine 1 atm O2, refluxing for 10 h (pptn.); collection (filtration); second crop and MnO2 on evapn. of filtrate; elem. anal.; | A 9% B 90% |
A
manganese(IV) oxide
Conditions | Yield |
---|---|
With O2 In pyridine 1 atm O2, refluxing for 10 h (pptn.); collection (filtration); second crop and MnO2 on evapn. of filtrate; elem. anal.; | A 9% B 89% |
Mn(N,N'-bis(salicylaldehyde)-1,3-propanediimine) * H2O
A
manganese(IV) oxide
Conditions | Yield |
---|---|
With O2 In pyridine 1 atm O2, refluxing for 10 h (pptn.); collection (filtration); second crop and MnO2 on evapn. of filtrate; elem. anal.; | A 9% B 88% |
A
manganese(IV) oxide
Conditions | Yield |
---|---|
With O2 In pyridine 1 atm O2, refluxing for 10 h (pptn.); collection (filtration); second crop and MnO2 on evapn. of filtrate; elem. anal.; | A 10% B 87% |
Mn(N,N'-bis(salicylaldehyde)o-phenylenediimine) * H2O
A
manganese(IV) oxide
Conditions | Yield |
---|---|
With O2 In pyridine 1 atm O2, refluxing for 10 h (pptn.); collection (filtration); second crop and MnO2 on evapn. of filtrate; elem. anal.; | A 14% B 83% |
Conditions | Yield |
---|---|
In further solvent(s) Electrolysis; in K2CO3 soln., current density 11.4-18.2 A/dm2 at 19°C; | A 3.9% B 81% |
In further solvent(s) Electrolysis; in K2CO3 soln., current density 11.4-18.2 A/dm2 at 25-32°C; | A 11% B 67.6% |
In further solvent(s) Electrolysis; in K2CO3 soln., current density 11.4-18.2 A/dm2 at 37°C; | A 15.1% B 58.5% |
manganese(IV) oxide
Conditions | Yield |
---|---|
In sulfuric acid aq. H2SO4; Electrolysis; electrolytic deposition from soln. of MnSO4 in aq. H2SO4 at 30 °C (graphite-anode coated with PbO2, c.d. 5 A/dm*dm);; product contains PbO2 (88% MnO2);; | 75% |
With potassium permanganate In water at 80℃; for 16h; | |
With sodium hydroxide; potassium permanganate In water at 70℃; for 13.5h; |
Conditions | Yield |
---|---|
potassium hydroxide; sodium hydroxide In water oxidn. of Mn(2+) in alkaline soln. with oxygen;; | 70% |
iron(III) oxide; lead(II) oxide; tin(IV) oxide In water oxidn. of Mn(2+) in alkaline soln. with oxygen;; | |
calcium oxide In water oxidn. of Mn(2+) in alkaline soln. with oxygen;; | |
cobalt(II) chloride; copper dichloride In water oxidn. of Mn(2+) in alkaline soln. with oxygen;; |
A
manganese(IV) oxide
Conditions | Yield |
---|---|
With O2; pyridine In pyridine dissoln. of Mn-complex (N2-atmosphere), exposing to 1 atm O2; manometricfollowing of O2 uptake (-15°C, 1 week); filtration (under O2), crystn. (-15°C, 1 week); O2(1-) and OH(1-)complexes by chromy. of filtrate (Al2O3); elem. anal.; | A n/a B 15% C 40% D 15% |
A
manganese(IV) oxide
Conditions | Yield |
---|---|
With O2; pyridine In pyridine dissoln. of Mn-complex (N2-atmosphere), exposing to 1 atm O2; manometricfollowing of O2 uptake (-15°C, 10 h); filtration (under O2), crystn. (-15°C, 1 week); elem. anal.; | A n/a B 38% |
A
manganese(IV) oxide
Conditions | Yield |
---|---|
With O2; pyridine In pyridine dissoln. of Mn-complex (N2-atmosphere), exposing to 1 atm O2; manometricfollowing of O2 uptake (-15°C, 10 h); filtration (under O2), crystn. (-15°C, 1 week); elem. anal.; | A n/a B 37% |
A
manganese(IV) oxide
Conditions | Yield |
---|---|
With O2; pyridine In pyridine dissoln. of Mn-complex (N2-atmosphere), exposing to 1 atm O2; manometricfollowing of O2 uptake (-15°C, 10 h); filtration (under O2), crystn. (-15°C, 1 week); elem. anal.; | A n/a B 36% |
A
manganese(IV) oxide
Conditions | Yield |
---|---|
With O2; pyridine In pyridine dissoln. of Mn-complex (N2-atmosphere), exposing to 1 atm O2; manometricfollowing of O2 uptake (-15°C, 10 h); filtration (under O2), crystn. (-15°C, 1 week); elem. anal.; | A n/a B 36% |
A
manganese(IV) oxide
Conditions | Yield |
---|---|
With O2; pyridine In pyridine dissoln. of Mn-complex (N2-atmosphere), exposing to 1 atm O2; manometricfollowing of O2 uptake (-15°C, 10 h); filtration (under O2), crystn. (-15°C, 1 week); elem. anal.; | A n/a B 35% |
A
manganese(IV) oxide
Conditions | Yield |
---|---|
With O2; pyridine In pyridine dissoln. of Mn-complex (N2-atmosphere), exposing to 1 atm O2; manometricfollowing of O2 uptake (-15°C, 1 week); filtration (under O2), crystn. (-15°C, 1 week); O2(1-) and OH(1-)complexes by chromy. of filtrate (Al2O3); elem. anal.; | A n/a B 35% C 14% D 12% |
A
manganese(IV) oxide
Conditions | Yield |
---|---|
With O2; pyridine In pyridine dissoln. of Mn-complex (N2-atmosphere), exposing to 1 atm O2; manometricfollowing of O2 uptake (-15°C, 10 h); filtration (under O2), crystn. (-15°C, 1 week); elem. anal.; | A n/a B 34% |
A
manganese(IV) oxide
Conditions | Yield |
---|---|
With O2; pyridine In pyridine dissoln. of Mn-complex (N2-atmosphere), exposing to 1 atm O2; manometricfollowing of O2 uptake (-15°C, 10 h); filtration (under O2), crystn. (-15°C, 1 week); elem. anal.; | A n/a B 32% |
A
manganese(IV) oxide
Conditions | Yield |
---|---|
With O2; pyridine In pyridine dissoln. of Mn-complex (N2-atmosphere), exposing to 1 atm O2; manometricfollowing of O2 uptake (-15°C, 10 h); filtration (under O2), crystn. (-15°C, 1 week); elem. anal.; | A n/a B 30% |
A
manganese(IV) oxide
Conditions | Yield |
---|---|
With O2; pyridine In pyridine dissoln. of Mn-complex (N2-atmosphere), exposing to 1 atm O2; manometricfollowing of O2 uptake (-15°C, 10 h); filtration (under O2), crystn. (-15°C, 1 week); elem. anal.; | A n/a B 30% |
A
manganese(IV) oxide
Conditions | Yield |
---|---|
With Na2S2O8; NaCl In water mixing MnCl2*4H2O in aq. NaCl, As compd. at 65°C, mixing for 30 min, addn. of Na2S2O8, heating to 80°C for 2 h; hot filtration, storage at room temp. in air, filtration, washing with 1 M NaCl and EtOH, air drying; | A n/a B 30% |
A
manganese(IV) oxide
Conditions | Yield |
---|---|
With O2; pyridine In pyridine dissoln. of Mn-complex (N2-atmosphere), exposing to 1 atm O2; manometricfollowing of O2 uptake (-15°C, 10 h); filtration (under O2), crystn. (-15°C, 1 week); elem. anal.; | A n/a B 28% |
manganese(IV) oxide
Conditions | Yield |
---|---|
With air; (CH2N(i-Pr)CH2C9H6N)2; H2O2 In methanol mixt. of ligand and Mn salt (1 equiv.) in MeOH was stirred for 2 d in air at room temp.; filtered; H2O2 added to filtrate; | 27% |
manganese(IV) oxide
Conditions | Yield |
---|---|
Stage #1: 4C48H44O16(4-)*9Mn(2+)*22H2O*4C3H7NO*2CHO2(1-) at 212℃; Stage #2: at 302℃; | 15.1% |
manganese(IV) oxide
Conditions | Yield |
---|---|
With potassium permanganate In water at 30 - 70℃; for 16h; | |
With sodium hydroxide; potassium permanganate In water at 70℃; for 13h; | |
With chlorine In water Irradiation (UV/VIS); |
Conditions | Yield |
---|---|
In dichloromethane | 100% |
Conditions | Yield |
---|---|
copper(II) sulfate In not given 80-90°C, 20 min; not isolated; UV/VIS spectrometry; | 98.5% |
cobalt(II) nitrate In not given 80-90°C, 20 min; not isolated; | 73% |
silver nitrate In not given 80-90°C, 20 min; not isolated; | 72% |
iron(III) sulfate In not given 80-90°C, 20 min; not isolated; | 65% |
Conditions | Yield |
---|---|
Stage #1: manganese(IV) oxide; copper(II) oxide In water at 110℃; Green chemistry; Stage #2: at 180℃; for 3h; Green chemistry; Stage #3: at 900℃; for 20h; Calcination; Green chemistry; | 98% |
manganese(IV) oxide
Conditions | Yield |
---|---|
In dichloromethane 23°C, 5-30 min; IR, (1)H- and (13)C-NMR spectroscopy, DEPT, MS; | 96% |
manganese(IV) oxide
pentafluorobenzenesulfinamide
2,3,4,5,6-pentafluorobenzenesulfonamide
Conditions | Yield |
---|---|
In benzene oxidn., in anhydr. C6H6 at 70°C, 16 h; | 96% |
In benzene oxidn., in anhydr. C6H6 at 70°C, 16 h; | 96% |
In benzene in dry benzene 70°C; | |
In benzene in dry benzene 70°C; |
Conditions | Yield |
---|---|
In melt mixing of LiOH*H2O, LiNO3 and MnO2 by grinding in a mortar, heating at 280°C for 12 h in air, cooling to room temp.; washing with distd. water, centrifuging, drying at 80°C under vac.; | 95% |
Conditions | Yield |
---|---|
In water High Pressure; MnO2 (5 mmol), B compd. (10 mmol), and H3PO3 (45 mmol) in H2O, mixt. sealed, heated at 200°C for 4 d; washed hot water (80°C), elem. anal.; | 95% |
manganese(IV) oxide
dicarbonyl[1-4-η-5-(2-hydroxyethyl)cyclohepta-1,3-diene](triphenyl phosphite)iron
Fe(CO)2(P(OC6H5)3)(C7H8(CH2CH2O))
Conditions | Yield |
---|---|
In benzene refluxing MnO2 (overnight, water separator), cooling, addn. Fe-compd., refluxing (20 min); cooling, filtration (Celite), removal solvent; | 90% |
Conditions | Yield |
---|---|
In neat (no solvent) byproducts: Fe2O3; on heating at 800°C for 0.5hours;; | 89% |
In neat (no solvent) byproducts: Fe2O3; on heating at 800°C for 0.5hours;; | 89% |
In neat (no solvent) temp. should not be higher then 700 up to 800°C (thermal decompn. of MnSO4);; | |
In neat (no solvent) temp. should not be higher then 700 up to 800°C (thermal decompn. of MnSO4);; |
Conditions | Yield |
---|---|
In neat (no solvent) MnO2:pyrite=1:1, 7h, 500°C;; MnSO4 as crust on MnO2;; | 88% |
In neat (no solvent) MnO2:pyrite=1:1, 7h, 500°C;; MnSO4 as crust on MnO2;; | 88% |
In neat (no solvent) best react. conditions: 500°C, 1h;; |
manganese(IV) oxide
Conditions | Yield |
---|---|
In dichloromethane (Ar); addn. of MnO2 to CH2Cl2 soln. of ferrocenophane deriv., stirring at room temp. for 12 h; filtration through celite, evapn., elem. anal.; | 88% |
manganese(IV) oxide
[Cu(bis[2-(diphenylphosphino)phenyl]ether)2]tetrafluoroborate
[Cu(κ2-P,P'-bis(2-(diphenylphosphino)phenyl) ether)(κ2-P,O-Ph2PC6H4OC6H4P(O)Ph2)][BF4]
Conditions | Yield |
---|---|
In dichloromethane under N2; mixt. of Cu complex and MnO2 in CH2Cl2 stirred at room temp. for 2 h; filtered; concd.; Et2O added; crystals collected; elem. anal.; | 87% |
manganese(IV) oxide
2,2-bis(3,5-bis(2-isopropoxyphenyl)-1H-pyrazol-1-yl)acetic acid
potassium tert-butylate
bis(2,2-bis(3,5-bis(2-isopropoxyphenyl)-1H-pyrazol-1-yl)acetate)manganese(II)
Conditions | Yield |
---|---|
Stage #1: 2,2-bis(3,5-bis(2-isopropoxyphenyl)-1H-pyrazol-1-yl)acetic acid; potassium tert-butylate In tetrahydrofuran at 20℃; for 0.5h; Schlenk technique; Stage #2: manganese(IV) oxide In tetrahydrofuran for 1h; Reflux; Stage #3: In tetrahydrofuran at 20℃; for 24h; Schlenk technique; | 87% |
Conditions | Yield |
---|---|
at 150℃; for 65h; | 85% |
manganese(IV) oxide
pentafluorophenylmercaptoamine
2,3,4,5,6-pentafluorobenzenesulfonamide
Conditions | Yield |
---|---|
In benzene oxidn., in anhydr. C6H6 at 70°C, 16 h; | 83% |
In benzene oxidn., in anhydr. C6H6 at 70°C, 16 h; | 83% |
70°C, 16 h; | |
70°C, 16 h; |
manganese(IV) oxide
trans-1,2-Cyclohexanediaminetetraacetic acid
Conditions | Yield |
---|---|
molar ratio of C14H22N2O8:Mn(NO3)2=2:1, 0°C, 0.5-1 h; filtrn. of excess MnO2, addn. of an equal vol. of cold ethanol, then standing for several hours at 0°C, washing with abs. ethanol, drying in vac. at room temp.; | 80% |
molar ratio of C14H22N2O8:Mn(NO3)2=2:1, 0°C, 0.5-1 h; filtrn. of excess MnO2, addn. of an equal vol. of cold ethanol, then standing for several hours at 0°C, washing with abs. ethanol, drying in vac. at room temp.; | 80% |
molar ratio of C14H22N2O8:Mn(NO3)2=2:1, 0°C, 0.5-1 h; filtrn. of excess MnO2, addn. of an equal vol. of cold ethanol, then standing for several hours at 0°C, washing with abs. ethanol; | |
molar ratio of C14H22N2O8:Mn(NO3)2=2:1, 0°C, 0.5-1 h; filtrn. of excess MnO2, addn. of an equal vol. of cold ethanol, then standing for several hours at 0°C, washing with abs. ethanol; |
Conditions | Yield |
---|---|
In isopropyl alcohol byproducts: acetone; by a react. of Yb2O3 with i-PrOH at 285°C for 20 h; according to Buslaeva et al. Zh. Neorg. Khim., 2001, vol. 46, no. 3, p. 380; Neorg. Mater., 2002, vol. 38, no. 6, p. 706; XRD studies; | A n/a B 80% C n/a |
Conditions | Yield |
---|---|
With isopropyl alcohol In isopropyl alcohol byproducts: (CH3)2CO, H2O; High Pressure; according to Buslaeva, E. Yu., et al., Zh. Neorg. Khim., 2001, vol. 46, p. 380; in glass ampule powdered oxide placed, i-PrOH added; placed intoautoclave; autoclave was pressurized; furnace temp. raised at 60-70 K/h ; heated at 300°C for 2-6 h; monitored by X-ray diffraction; | A 80% B 20% |
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