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Dayang Chem (Hangzhou) Co.,Ltd.

DayangChem exported this product to many countries and regions at best price. If you are looking for the material's manufacturer or supplier in China, DayangChem is your best choice. Pls contact with us freely for getting detailed product spe

2-Amino-6-chlorobenzoic acid

Cas:2148-56-3

Min.Order:1 Kilogram

FOB Price: $3.0

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Simagchem Corporation

Welcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our

High quality 2-Amino-6-Chlorobenzoic Acid supplier in China

Cas:2148-56-3

Min.Order:1 Metric Ton

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Hebei yanxi chemical co.,LTD.

hebei yanxi chemical co., LTD who registered capital of 10 million yuan, nearly to $2 million, we have a pharmaceutical raw materials factory production of pharmaceutical raw materials, and a reagent r&d center, and we do research and developm

2-Amino-6-chlorobenzoic acid CAS NO.2148-56-3

Cas:2148-56-3

Min.Order:1 Metric Ton

FOB Price: $1.0 / 3.0

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Henan Allgreen Chemical Co.,Ltd

Good price Good quality Appearance:powder Storage:dry condition Package:According to the demand of customer Application:intermediate Transportation:By sea or by air Port:Shanghai Port

2148-56-3,2-Amino-6-chlorobenzoic acid

Cas:2148-56-3

Min.Order:1 Gram

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Ality Chemical Corporation

The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi

Factory Supply 2-amino-6-chlorobenzoic acid

Cas:2148-56-3

Min.Order:1

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Type:Other

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COLORCOM LTD.

Colorcom is a global leader in industrial chemical manufacturing and is continuously innovating and transforming to exceed client expectations and industry standards. Colorcom prides itself on superior customer and technical focus, while focusing on

2-Amino-6-Chlorobenzoic Acid

Cas:2148-56-3

Min.Order:1 Metric Ton

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Type:Manufacturers

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Chemwill Asia Co., Ltd.

2-Amino-6-chlorobenzoic acid CAS 2148-56-3 In stock 6-Chloroanthranilic acid

Cas:2148-56-3

Min.Order:1 Metric Ton

FOB Price: $1.0

Type:Manufacturers

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Jinan Finer Chemical Co., Ltd

Product Description Product website: http://www.finerchem.com Product Name 2-Amino-6-chlorobenzoic acid CAS No. 2148-56-3

2-Amino-6-chlorobenzoic acid

Cas:2148-56-3

Min.Order:1 Gram

FOB Price: $12.0

Type:Lab/Research institutions

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Hebei Nengqian Chemical Import and Export Co., LTD

With our good experience, we offer detailed technical support and advice to assist customers. We communicate closely with customers to establish their quality requirements. Consistent Quality Our plant has strict quality control in each manufactu

2-Amino-6-Chlorobenzoic Acid CAS: 2148-56-3

Cas:2148-56-3

Min.Order:1 Kilogram

FOB Price: $1.0 / 10.0

Type:Trading Company

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Zhuozhou Wenxi import and Export Co., Ltd

WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et

Factory direct supply CAS 2148-56-3 with best quality

Cas:2148-56-3

Min.Order:1 Kilogram

FOB Price: $139.0 / 210.0

Type:Trading Company

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Henan Sinotech Import&Export Corporation

Product Type: 2-Amino-6-chlorobenzoic acid Cas: 2148-56-3 Molecular Formula: C7H6ClNO2 Purity:

2-Amino-6-chlorobenzoic acid CAS: 2148-56-3

Cas:2148-56-3

Min.Order:5 Metric Ton

FOB Price: $1.0 / 2.0

Type:Other

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Shijiazhuang Sdyano Fine Chemical Co., Ltd

1. Best prices with satisfied quality; 2. It's clients' right to choose the package's Courier (EMS, DHL, FedEx, UPS); 3.It's clients' right to choose the packing way for his produccts from many recent effective packing ways;

2-Amino-6-chlorobenzoic acid

Cas:2148-56-3

Min.Order:0 Metric Ton

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Shanghai Upbio Tech Co.,Ltd

1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized

2-Amino-6-chlorobenzoic acid 2148-56-3

Cas:2148-56-3

Min.Order:1 Kilogram

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Baoji Guokang Healthchem co.,ltd

Our company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At prese

Pharmaceutical Intermediate, 2-Amino-6-chlorobenzoic acid CAS:2148-56-3

Cas:2148-56-3

Min.Order:1 Kilogram

FOB Price: $61.2 / 65.8

Type:Trading Company

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Qingdao Beluga Import and Export Co., LTD

2-Amino-6-chlorobenzoic acid CAS:2148-56-3 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organ

2-Amino-6-chlorobenzoic acid CAS:2148-56-3

Cas:2148-56-3

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

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Shandong Hanjiang Chemical Co., Ltd.

Hello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai

2-Amino-6-chlorobenzoic acid

Cas:2148-56-3

Min.Order:1 Kilogram

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Henan Wentao Chemical Product Co., Ltd.

Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

CAS NO.:2148-56-3

Cas:2148-56-3

Min.Order:0

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Hebei Mojin Biotechnology Co.,Ltd

Hebei Mojin Biotechnology Co., Ltd, Our company is a professional in chemical raw materials and chemical reagents research and development production enterprises. Our business covers more than 30 countries, most of the big customers come from Europe,

2-Amino-6-chlorobenzoic acid cas 2148-56-3 2-amino-6-chloro-benzoic acid

Cas:2148-56-3

Min.Order:1 Kilogram

FOB Price: $80.0 / 100.0

Type:Trading Company

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Wuhan Zenuo Biological Medicine Technology Co Ltd

Product Name: 2-Amino-6-chlorobenzoic acid Synonyms: Benzoic acid, 2-amino-6-chloro-;RARECHEM AL BO 1514;TIMTEC-BB SBB001735;2-AMINO-6-CHLOROBENZOIC ACID;6-CHLOROANTHRANILIC ACID;6-AMINO-2-CHLOROBENZOIC ACID;2-Amino-6-chlorobenzoic acid 2148-56-3

2-Amino-6-chlorobenzoic acid big supplier with lower price

Cas:2148-56-3

Min.Order:1 Kilogram

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Wuhan Han Sheng New Material Technology Co.,Ltd

Our Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We

Top quality 2-Amino-6-chlorobenzoic acid CAS 2148-56-3 !

Cas:2148-56-3

Min.Order:10 Kilogram

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Win-Win chemical Co.Ltd

Stock products, own laboratory Product number 1329 English Name 2-Amino-6-Chlorobenzoic Acid CAS Number 2148-56-3 Purity 98% Molecular fo

2-Amino-6-Chlorobenzoic Acid cas no. 2148-56-3 98%

Cas:2148-56-3

Min.Order:1 Metric Ton

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Triumph International Development Limilted

Appearance:off-white to white solid Storage:Store in a cool,dry place and keep away from direct strong light Package:As customer request Application:Used for Synthesis API and Research Transportation:By Sea/Air/Courier Port:Qingdao

2-Amino-6-chlorobenzoic acid 2148-56-3

Cas:2148-56-3

Min.Order:0 Metric Ton

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Hubei Jiutian Bio-medical Technology Co., Ltd

1,we produce and sell good chemicals around the world. 2,our success rate is about 95%. this means, if customer order is accepted, the probability that the customer will obtain the ordered substances, is 95%. 3,our staff consists of highly qualifie

CAS 2148-56-3 2-Amino-6-chlorobenzoic acid

Cas:2148-56-3

Min.Order:1 Kilogram

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Type:Lab/Research institutions

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Hangzhou Keyingchem Co.,Ltd

Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det

2-Amino-6-chlorobenzoic acid

Cas:2148-56-3

Min.Order:0 Metric Ton

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Hangzhou J&H Chemical Co., Ltd.

J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

2-Amino-6-chlorobenzoic acid

Cas:2148-56-3

Min.Order:0

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Afine Chemicals Limited

Our Services 1. New Molecules R&D 2. Own test center HPLC NMR GC LC-MS 3. API and Intermediates from China reputed manufacturers 4. Documents support COA MOA MSDS DMF open part Our advantages 1. Government awarded company. Top 100 enter

2-AMINO-6-CHLOROBENZOIC ACID

Cas:2148-56-3

Min.Order:0

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Shanghai Massive Chemical Technology Co., Ltd.

Massive Chemical is certified with ISO9001 and ISO14001 manufacturer for this product. We will offer all documents as requirement for the materials which includes, Certificate of Analysis, Material Safety Data Sheet, and Method of Analysis and

2-Amino-6-chlorobenzoic acid/High quality/Best price

Cas:2148-56-3

Min.Order:1 Gram

FOB Price: $1.0

Type:Lab/Research institutions

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Zibo Hangyu Biotechnology Development Co., Ltd

Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi

High quality 2-Amino-6-Chlorobenzoic Acid

Cas:2148-56-3

Min.Order:10 Gram

FOB Price: $100.0

Type:Lab/Research institutions

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Henan Tianfu Chemical Co., Ltd.

Our company was built in 2009 with an ISO certificate.In the past 5 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so

TIANFU-CHEM CAS NO.2148-56-3 2-Amino-6-chlorobenzoic acid

Cas:2148-56-3

Min.Order:1 Kilogram

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Siwei Development Group Ltd.

Product name: 2-Amino-6-Chlorobenzoic Acid CAS No.: 2148-56-3 Molecule Formula:C7H5ClNO2 Molecule Weight:170.57 Purity: 99.0% Package: 25kg/drum Description:Light yellow crystalline powder Manufacture Standards:Enterprise Standard

Lower Price 2-Amino-6-Chlorobenzoic Acid

Cas:2148-56-3

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Synthetic route

2-chloro-6-nitrobenzoic acid
5344-49-0

2-chloro-6-nitrobenzoic acid

2-chloro-6-aminobenzoic acid
2148-56-3

2-chloro-6-aminobenzoic acid

Conditions
ConditionsYield
With potassium bisulfite; cerium(III) chloride; potassium chloride; 2-methoxy-phenol In ethanol at 65℃; for 8h; Time;90%
With platinum Hydrogenation;
With ammonium hydroxide; iron(II) sulfate
With iron(II) sulfate
2-[(tert-butoxycarbonyl)amino]-6-chlorobenzoic acid
616224-61-4

2-[(tert-butoxycarbonyl)amino]-6-chlorobenzoic acid

2-chloro-6-aminobenzoic acid
2148-56-3

2-chloro-6-aminobenzoic acid

Conditions
ConditionsYield
With hydrogenchloride In 1,4-dioxane; water at 90℃; under 760.051 Torr; for 1h; Temperature;99.5%
2-amino-6-chlorobenzonitrile
6575-11-7

2-amino-6-chlorobenzonitrile

2-chloro-6-aminobenzoic acid
2148-56-3

2-chloro-6-aminobenzoic acid

Conditions
ConditionsYield
With dihydrogen peroxide; potassium hydroxide Reflux;94%
With dihydrogen peroxide; potassium hydroxide In water for 12h; Reflux;94%
2-(acetylamino)-6-chlorobenzoic acid
19407-42-2

2-(acetylamino)-6-chlorobenzoic acid

2-chloro-6-aminobenzoic acid
2148-56-3

2-chloro-6-aminobenzoic acid

Conditions
ConditionsYield
With hydrogenchloride
With hydrogenchloride Zers. des entstandenen Hydrochlorids mit Natriumdicarbonat;
With hydrogenchloride at 80 - 90℃; for 1.5h;
N-(3-chloro-2-methylphenyl)acetamide
7463-35-6

N-(3-chloro-2-methylphenyl)acetamide

2-chloro-6-aminobenzoic acid
2148-56-3

2-chloro-6-aminobenzoic acid

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 65.7 percent / potassium permanganate; magnesium sulfate heptahydrate / H2O / 5 h / 135 - 160 °C
2: hydrochloric acid / 1.5 h / 80 - 90 °C
View Scheme
Multi-step reaction with 2 steps
1: potassium permanganate; magnesium sulfate
2: concentrated hydrochloric acid / Zers. des entstandenen Hydrochlorids mit Natriumdicarbonat
View Scheme
Multi-step reaction with 2 steps
1: potassium permanganate; magnesium sulfate; water
2: aqueous hydrochloric acid
View Scheme
4-chloroisatin
6344-05-4

4-chloroisatin

2-chloro-6-aminobenzoic acid
2148-56-3

2-chloro-6-aminobenzoic acid

Conditions
ConditionsYield
With sodium hydroxide; dihydrogen peroxide
2-benzoylamino-6-chloro-benzoic acid
19407-43-3

2-benzoylamino-6-chloro-benzoic acid

2-chloro-6-aminobenzoic acid
2148-56-3

2-chloro-6-aminobenzoic acid

Conditions
ConditionsYield
With sodium hydroxide
3-chloro-2-methyl-aniline; hydrochloride
6259-40-1

3-chloro-2-methyl-aniline; hydrochloride

2-chloro-6-aminobenzoic acid
2148-56-3

2-chloro-6-aminobenzoic acid

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: sodium acetate
2: potassium permanganate; magnesium sulfate; water
3: aqueous hydrochloric acid
View Scheme
3-chloro-2-methylbenzenamine
87-60-5

3-chloro-2-methylbenzenamine

2-chloro-6-aminobenzoic acid
2148-56-3

2-chloro-6-aminobenzoic acid

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: 90.2 percent / CH2Cl2
2: 65.7 percent / potassium permanganate; magnesium sulfate heptahydrate / H2O / 5 h / 135 - 160 °C
3: hydrochloric acid / 1.5 h / 80 - 90 °C
View Scheme
Multi-step reaction with 3 steps
1: fluorobenzene / 2 h / 50 °C
2: water / tetrahydrofuran / 9.17 h / 155 - 175 °C / 5320.36 - 7600.51 Torr / Inert atmosphere
3: hydrogenchloride / 1,4-dioxane; water / 1 h / 90 °C / 760.05 Torr
View Scheme
anthranilic acid
118-92-3

anthranilic acid

2-chloro-6-aminobenzoic acid
2148-56-3

2-chloro-6-aminobenzoic acid

Conditions
ConditionsYield
With D-glucose; Escherichia coli flavin reductase; Bacillus megaterium glucose dehydrogenase; Lechevalieria aerocolonigenes tryptophan-7-halogenase; flavin adenine dinucleotide; NADH; sodium chloride In aq. phosphate buffer; isopropyl alcohol pH=7.4; Enzymatic reaction;
4-chloro-isatin

4-chloro-isatin

2-chloro-6-aminobenzoic acid
2148-56-3

2-chloro-6-aminobenzoic acid

Conditions
ConditionsYield
With sodium azide; sulfuric acid
2-chloro-6-nitrobenzonitrile
6575-07-1

2-chloro-6-nitrobenzonitrile

2-chloro-6-aminobenzoic acid
2148-56-3

2-chloro-6-aminobenzoic acid

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: (i) H2SO4, (ii) aq. NaNO2
2: FeSO4
View Scheme
phosgene
75-44-5

phosgene

2-chloro-6-aminobenzoic acid
2148-56-3

2-chloro-6-aminobenzoic acid

5-chloro-1H-benzo[d][1,3]oxazine-2,4-dione
20829-96-3

5-chloro-1H-benzo[d][1,3]oxazine-2,4-dione

Conditions
ConditionsYield
In 1,4-dioxane at 12 - 20℃;99%
In 1,4-dioxane at 0 - 23℃; for 24h;93%
With potassium hydroxide In water; toluene91%
bis(trichloromethyl) carbonate
32315-10-9

bis(trichloromethyl) carbonate

2-chloro-6-aminobenzoic acid
2148-56-3

2-chloro-6-aminobenzoic acid

5-chloro-1H-benzo[d][1,3]oxazine-2,4-dione
20829-96-3

5-chloro-1H-benzo[d][1,3]oxazine-2,4-dione

Conditions
ConditionsYield
In 1,4-dioxane for 2h; Reflux;99%
In 1,4-dioxane Reflux;99%
With pyridine In dichloromethane; acetonitrile at 50℃; for 2h;97%
2-methyl-4-(piperidin-4-yl)-1-[1-(4-trifluoromethylphenyl)ethyl]piperazine
306296-91-3

2-methyl-4-(piperidin-4-yl)-1-[1-(4-trifluoromethylphenyl)ethyl]piperazine

2-chloro-6-aminobenzoic acid
2148-56-3

2-chloro-6-aminobenzoic acid

C26H32ClF3N4O

C26H32ClF3N4O

Conditions
ConditionsYield
With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine In dichloromethane at 20℃; for 16h;98%
With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine In dichloromethane at 20℃; for 16h;80%
2-chloro-6-aminobenzoic acid
2148-56-3

2-chloro-6-aminobenzoic acid

acetyl chloride
75-36-5

acetyl chloride

5-chloro-1H-benzo[d][1,3]oxazine-2,4-dione
20829-96-3

5-chloro-1H-benzo[d][1,3]oxazine-2,4-dione

Conditions
ConditionsYield
With chloroformic acid ethyl ester In 1,4-dioxane at 50℃; for 11h; Heating / reflux;97%
2-chloro-6-aminobenzoic acid
2148-56-3

2-chloro-6-aminobenzoic acid

acetyl chloride
75-36-5

acetyl chloride

5-Chloroisatoic anhydride
4743-17-3

5-Chloroisatoic anhydride

Conditions
ConditionsYield
Stage #1: 2-chloro-6-aminobenzoic acid With chloroformic acid ethyl ester In 1,4-dioxane for 1h; Heating / reflux;
Stage #2: acetyl chloride In 1,4-dioxane at 50℃; for 10h;
97%
2-chloro-6-aminobenzoic acid
2148-56-3

2-chloro-6-aminobenzoic acid

(2-amino-6-chlorophenyl)methanol
39885-08-0

(2-amino-6-chlorophenyl)methanol

Conditions
ConditionsYield
With lithium aluminium tetrahydride In tetrahydrofuran at 0 - 20℃;95%
With borane-THF In tetrahydrofuran at 0 - 30℃; for 1.66667h; Inert atmosphere;88%
With lithium aluminium tetrahydride In tetrahydrofuran at 0 - 20℃; for 2h;87%
1,1-dichloro-2-nitro ethylene
6061-04-7

1,1-dichloro-2-nitro ethylene

2-chloro-6-aminobenzoic acid
2148-56-3

2-chloro-6-aminobenzoic acid

2-chloro-6-(2-nitroacetamido)benzoic acid

2-chloro-6-(2-nitroacetamido)benzoic acid

Conditions
ConditionsYield
In water at 50℃; for 6h; Temperature; Green chemistry;95%
2-chloro-6-aminobenzoic acid
2148-56-3

2-chloro-6-aminobenzoic acid

2-amino-3,5,6-trichloro-benzoic acid
731007-25-3

2-amino-3,5,6-trichloro-benzoic acid

Conditions
ConditionsYield
With N-chloro-succinimide In N,N-dimethyl-formamide at 80 - 90℃;95%
{(1S)-1-[4-phenyl-1-(propylsulfonyl)piperidin-4-yl]ethyl}amine
852029-79-9

{(1S)-1-[4-phenyl-1-(propylsulfonyl)piperidin-4-yl]ethyl}amine

2-chloro-6-aminobenzoic acid
2148-56-3

2-chloro-6-aminobenzoic acid

2-amino-6-chloro-N-((4-phenyl-1-(propylsulfonyl)piperidin-4-yl)methyl)benzamide
852029-50-6

2-amino-6-chloro-N-((4-phenyl-1-(propylsulfonyl)piperidin-4-yl)methyl)benzamide

Conditions
ConditionsYield
With benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine; dicyclohexyl-carbodiimide In dichloromethane at 20℃; Polystyrene;94%
2-chloro-6-aminobenzoic acid
2148-56-3

2-chloro-6-aminobenzoic acid

methyl iodide
74-88-4

methyl iodide

methyl 6-chloroanthranilate
41632-04-6

methyl 6-chloroanthranilate

Conditions
ConditionsYield
With potassium carbonate In N,N-dimethyl-formamide at 20℃;93%
With potassium carbonate In N,N-dimethyl-formamide at 20℃;93%
With potassium carbonate In N,N-dimethyl-formamide at 20℃; for 18h; Inert atmosphere;82%
With potassium carbonate In N,N-dimethyl-formamide at 20℃; for 18h;82%
With potassium carbonate In DMF (N,N-dimethyl-formamide) at 20℃; for 18h;56%
2-chloro-6-aminobenzoic acid
2148-56-3

2-chloro-6-aminobenzoic acid

diazomethyl-trimethyl-silane
18107-18-1

diazomethyl-trimethyl-silane

methyl 6-chloroanthranilate
41632-04-6

methyl 6-chloroanthranilate

Conditions
ConditionsYield
In methanol; hexane; benzene at 20℃; for 1h;91%
2-chloro-6-aminobenzoic acid
2148-56-3

2-chloro-6-aminobenzoic acid

chloroacetyl chloride
79-04-9

chloroacetyl chloride

6-Chloro-4,1-benzoxazepin-2,5-dione
127603-58-1

6-Chloro-4,1-benzoxazepin-2,5-dione

Conditions
ConditionsYield
With sodium hydroxide In N-methyl-acetamide; water91%
C19H28F3N3
306297-33-6

C19H28F3N3

2-chloro-6-aminobenzoic acid
2148-56-3

2-chloro-6-aminobenzoic acid

C26H32ClF3N4O

C26H32ClF3N4O

Conditions
ConditionsYield
With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine90%
tetrahydrobetacarboline
16502-01-5

tetrahydrobetacarboline

2-chloro-6-aminobenzoic acid
2148-56-3

2-chloro-6-aminobenzoic acid

(2-amino-6-chlorophenyl)(1,3,4,9-tetrahydro-2H-pyrido[3,4-b]indol-2-yl)methanone

(2-amino-6-chlorophenyl)(1,3,4,9-tetrahydro-2H-pyrido[3,4-b]indol-2-yl)methanone

Conditions
ConditionsYield
With triethylamine; HATU89%
2-chloro-6-aminobenzoic acid
2148-56-3

2-chloro-6-aminobenzoic acid

4-chloro-1,3-dihydro-2H-benzoimidazol-2-one
5918-97-8

4-chloro-1,3-dihydro-2H-benzoimidazol-2-one

Conditions
ConditionsYield
With sodium azide; ammonium chloride; trichlorophosphate; N,N-dimethyl-formamide at 0 - 20℃; Curtius rearrangement;88%
2-chloro-6-aminobenzoic acid
2148-56-3

2-chloro-6-aminobenzoic acid

acetic anhydride
108-24-7

acetic anhydride

5-chloro-2-methyl-4-oxo-4H-benzo[d][1,3]oxazine
5627-73-6

5-chloro-2-methyl-4-oxo-4H-benzo[d][1,3]oxazine

Conditions
ConditionsYield
at 130℃; for 6h; Inert atmosphere;87%
at 130℃;78%
Reflux;76%
for 0.666667h; cyclocondensation; Heating;32%
for 2h; Reflux;
1-(tert-butoxycarbonyl)-L-proline
15761-39-4

1-(tert-butoxycarbonyl)-L-proline

2-chloro-6-aminobenzoic acid
2148-56-3

2-chloro-6-aminobenzoic acid

aniline
62-53-3

aniline

tert-butyl (S)-2-(5-chloro-4-oxo-3-phenyl-3,4-dihydroquinazoline-2-yl)pyrrolidine-1-carboxylate
1615680-13-1

tert-butyl (S)-2-(5-chloro-4-oxo-3-phenyl-3,4-dihydroquinazoline-2-yl)pyrrolidine-1-carboxylate

Conditions
ConditionsYield
Stage #1: 1-(tert-butoxycarbonyl)-L-proline; 2-chloro-6-aminobenzoic acid With triphenyl phosphite In pyridine at 70℃; for 2h;
Stage #2: aniline In pyridine at 70℃; for 2h;
86%
Stage #1: 1-(tert-butoxycarbonyl)-L-proline; 2-chloro-6-aminobenzoic acid With pyridine; triphenyl phosphite at 70℃;
Stage #2: aniline at 70 - 80℃;
2-chloro-6-aminobenzoic acid
2148-56-3

2-chloro-6-aminobenzoic acid

dimethyl sulfate
77-78-1

dimethyl sulfate

methyl 6-chloroanthranilate
41632-04-6

methyl 6-chloroanthranilate

Conditions
ConditionsYield
With potassium carbonate In N,N-dimethyl-formamide at 20℃; Inert atmosphere;86%
With sodium carbonate In N,N-dimethyl-formamide at 20℃; for 0.5h;75.8%
hex-5-in-carboxyl chloride
55183-45-4

hex-5-in-carboxyl chloride

2-chloro-6-aminobenzoic acid
2148-56-3

2-chloro-6-aminobenzoic acid

5-chloro-2-(pent-4-yn-1-yl)-4H-3,1-benzoxazin-4-one

5-chloro-2-(pent-4-yn-1-yl)-4H-3,1-benzoxazin-4-one

Conditions
ConditionsYield
With triethylamine In dichloromethane at 0 - 20℃; for 2.5h;86%
ethyl 2-phenyldiazoacetate
22065-57-2

ethyl 2-phenyldiazoacetate

2-chloro-6-aminobenzoic acid
2148-56-3

2-chloro-6-aminobenzoic acid

2-chloro-6-((2-ethoxy-2-oxo-1-phenylethyl)amino)benzoic acid

2-chloro-6-((2-ethoxy-2-oxo-1-phenylethyl)amino)benzoic acid

Conditions
ConditionsYield
With C43H37Br2CuN3P2(1+)*ClO4(1-) In methanol at 0 - 20℃; for 8h; Schlenk technique; Inert atmosphere; chemoselective reaction;85%
2-chloro-6-aminobenzoic acid
2148-56-3

2-chloro-6-aminobenzoic acid

isobutyryl chloride
79-30-1

isobutyryl chloride

5-chloro-2-isopropyl-4H-3,1-benzoxazin-4-one
57334-25-5

5-chloro-2-isopropyl-4H-3,1-benzoxazin-4-one

Conditions
ConditionsYield
With triethylamine In dichloromethane at 0 - 20℃; for 2.5h;85%
[1,1'-biphenyl]-2,2'-iodonium trifluoromethanesulfonate
189999-35-7

[1,1'-biphenyl]-2,2'-iodonium trifluoromethanesulfonate

2-chloro-6-aminobenzoic acid
2148-56-3

2-chloro-6-aminobenzoic acid

2′-iodo-[1,1′-biphenyl]-2-yl 2-amino-6-chlorobenzoate

2′-iodo-[1,1′-biphenyl]-2-yl 2-amino-6-chlorobenzoate

Conditions
ConditionsYield
With copper(l) iodide; 1,10-Phenanthroline; sodium carbonate In 1,4-dioxane at 95℃; for 17h; Molecular sieve; Green chemistry;84%
With copper(l) iodide; 1,10-Phenanthroline; sodium carbonate In 1,4-dioxane at 95℃; for 17h; Sealed tube;
2-chloro-6-aminobenzoic acid
2148-56-3

2-chloro-6-aminobenzoic acid

2-amino-6-chlorobenzamide
54166-95-9

2-amino-6-chlorobenzamide

Conditions
ConditionsYield
Stage #1: 2-chloro-6-aminobenzoic acid With 4-methyl-morpholine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In tetrahydrofuran at 20℃; for 0.5h;
Stage #2: With ammonium hydroxide In tetrahydrofuran at 20℃; for 23h;
83%
Stage #1: 2-chloro-6-aminobenzoic acid With 4-methyl-morpholine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In tetrahydrofuran at 20℃; for 0.5h;
Stage #2: With ammonium hydroxide at 20℃; for 23h;
83%
Multi-step reaction with 2 steps
1: pyridine / dichloromethane; acetonitrile / Inert atmosphere
2: ethanol; ammonia / 2 h / 20 °C
View Scheme
(phenylthio)acetic acid chloride
7031-27-8

(phenylthio)acetic acid chloride

2-chloro-6-aminobenzoic acid
2148-56-3

2-chloro-6-aminobenzoic acid

2-chloro-6-(2-phenylsulfanyl-acetylamino)benzoic acid
1265087-53-3

2-chloro-6-(2-phenylsulfanyl-acetylamino)benzoic acid

Conditions
ConditionsYield
Stage #1: (phenylthio)acetic acid chloride; 2-chloro-6-aminobenzoic acid With sodium hydroxide In water at 0 - 20℃; for 3h;
Stage #2: With hydrogenchloride In water pH=4 - 5;
82%
2-chloro-6-aminobenzoic acid
2148-56-3

2-chloro-6-aminobenzoic acid

2-amino-5-bromo-6-chlorobenzoic acid
3030-19-1

2-amino-5-bromo-6-chlorobenzoic acid

Conditions
ConditionsYield
With N-Bromosuccinimide In N,N-dimethyl-formamide at 0 - 20℃; for 16h;82%
2-chloro-6-aminobenzoic acid
2148-56-3

2-chloro-6-aminobenzoic acid

2-methoxy-phenylamine
90-04-0

2-methoxy-phenylamine

2-Amino-6-chloro-N-(2-methoxyphenyl)benzamide
371243-74-2

2-Amino-6-chloro-N-(2-methoxyphenyl)benzamide

Conditions
ConditionsYield
With thionyl chloride In dichloromethane; chloroform; benzene81%
Stage #1: 2-chloro-6-aminobenzoic acid With sulfuryl dichloride In benzene for 24h; Heating / reflux;
Stage #2: 2-methoxy-phenylamine In chloroform at 65℃; for 2h;
2-chloro-6-aminobenzoic acid
2148-56-3

2-chloro-6-aminobenzoic acid

ethyl iodide
75-03-6

ethyl iodide

ethyl 2-amino-6-chlorobenzoate
172217-11-7

ethyl 2-amino-6-chlorobenzoate

Conditions
ConditionsYield
Stage #1: 2-chloro-6-aminobenzoic acid With sodium hydride In N,N-dimethyl-formamide at 20℃; for 0.5h;
Stage #2: ethyl iodide In N,N-dimethyl-formamide at 20℃; for 48h;
80%
In N,N-dimethyl-formamide; mineral oil; Petroleum ether
In N,N-dimethyl-formamide; mineral oil; Petroleum ether

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