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inquiryHigh quality Imidazol-1-yl-acetic acid CAS 22884-10-2 with factory price Company profile Wuhan Fortuna Chemical Co.,Ltd established in 2006, is a big integrative chemical enterprise being engaged in Pharmaceutical & its intermediates, Food/F
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inquiryImidazol-1-yl-acetic acid CAS 22884-10-2 2-(1H-Imidazol-1-yl)acetic acid CAS no 22884-10-2 Imidazole-1-acetic acid Imidazol-1-yl-acetic acid 2-(1H-Imidazol-1-yl)acetic acid Imidazole-1-acetic acid Imidazol-1-yl-acetic acid CAS 22884-10-2 2-(1
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
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inquiryBest quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia
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inquiryImidazol-1-yl-acetic acid Basic information Product Name: Imidazol-1-yl-acetic acid Synonyms: 1H-Imidazole-1-acetic acid≥ 99% (HPLC);AKOS MSC-0001;2-(IMIDAZOLE-1-YL)-ACETIC ACID;2-(1H-IMIDAZOL-1-YL)ACETIC ACID;2-(1-IMIDAZOLYL)ACETIC ACID;1-
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inquiryProduct name:1H-imidazole-1-Acetic Acid CAS No.:22884-10-2 Molecule Formula:C5H6N2O2 Molecule Weight:126.11 Purity: 99.0% Package: 25kg/drum Description:White powder Manufacture Standards:Enterprise Standard TESTIN
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inquiryHangzhou Huarong Pharm Co., Ltd.established since 2006 , has been actively developing specialty products for Finished Dosages, APIs, Intermediates, and Fine chemicals markets in North America, Europe, Korea, Japan, Mid-East and all over the World. Hu
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Min.Order:1 Kilogram
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inquirymethyl 2-(1H-imidazol-1-yl)acetate
imidazol-1-ylacetic acid
Conditions | Yield |
---|---|
In water | 97% |
With water-d2 at 80℃; for 12h; Rate constant; | |
With water for 6h; Heating; | |
With hydrogenchloride; water at -2 - 2℃; for 2h; pH=4 - 5; | |
With water In water for 5h; Reflux; |
tert-butyl imidazol-1-ylaceatate
imidazol-1-ylacetic acid
Conditions | Yield |
---|---|
With water at 60 - 115℃; Product distribution / selectivity; | 82.2% |
N-ethylglycine
isothiocyanoacetaldehyde diethyl acetal
imidazol-1-ylacetic acid
Conditions | Yield |
---|---|
With sulfuric acid; nitric acid |
ethyl 2-(1H-imidazol-1-yl)acetate
imidazol-1-ylacetic acid
Conditions | Yield |
---|---|
hydrolysis; | |
With hydrogenchloride In water at 100℃; for 7h; pH=1.5; | |
With water | |
With ethanol In acetonitrile for 1h; Reflux; | 12.78 g |
chloroacetic acid ethyl ester
1-(Trimethylsilyl)imidazole
B
imidazol-1-ylacetic acid
Conditions | Yield |
---|---|
Stage #1: chloroacetic acid ethyl ester; 1-(Trimethylsilyl)imidazole at 90 - 100℃; Stage #2: With water Further stages.; | |
Stage #1: chloroacetic acid ethyl ester; 1-(Trimethylsilyl)imidazole at 67 - 70℃; Stage #2: With water Further stages.; |
methyl chloroacetate
1-(Trimethylsilyl)imidazole
B
imidazol-1-ylacetic acid
Conditions | Yield |
---|---|
Stage #1: methyl chloroacetate; 1-(Trimethylsilyl)imidazole at 90 - 100℃; Stage #2: With water Further stages.; | |
Stage #1: methyl chloroacetate; 1-(Trimethylsilyl)imidazole at 67 - 70℃; Stage #2: With water Further stages.; |
trimethylsilyl chloroacetate
1-(Trimethylsilyl)imidazole
B
imidazol-1-ylacetic acid
Conditions | Yield |
---|---|
Stage #1: trimethylsilyl chloroacetate; 1-(Trimethylsilyl)imidazole at 90 - 100℃; Stage #2: With water Further stages.; | |
Stage #1: trimethylsilyl chloroacetate; 1-(Trimethylsilyl)imidazole at 67 - 70℃; Stage #2: With water Further stages.; |
imidazol-1-ylacetic acid
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: Na2CO3 / H2O 2: hydrolysis View Scheme |
Conditions | Yield |
---|---|
With potassium carbonate; potassium iodide In DMF (N,N-dimethyl-formamide); toluene at 25 - 65℃; for 3.66667 - 5.16667h; Stirring; | |
Stage #1: 1H-imidazole With potassium tert-butylate In tetrahydrofuran at 0 - 7℃; Inert atmosphere; Stage #2: methyl chloroacetate In tetrahydrofuran at 7 - 25℃; Inert atmosphere; Stage #3: With hydrogenchloride; water In methanol at 25℃; pH=4 - 5; Product distribution / selectivity; |
Benzyl imidazol-1-ylacetate
imidazol-1-ylacetic acid
Conditions | Yield |
---|---|
With hydrogen; 5%-palladium/activated carbon In isopropyl alcohol at 20℃; for 2h; Product distribution / selectivity; | |
With hydrogenchloride; water at 65℃; for 4h; Product distribution / selectivity; |
Conditions | Yield |
---|---|
In tetrahydrofuran; ethanol; water | 1.22 g (7.5 mmol, 30%) |
imidazol-1-ylacetic acid
Conditions | Yield |
---|---|
With water for 4 - 8h; Heating / reflux; |
Conditions | Yield |
---|---|
Stage #1: 1H-imidazole With potassium carbonate; potassium iodide In N,N-dimethyl-formamide; toluene Stage #2: methyl chloroacetate In N,N-dimethyl-formamide; toluene at 25 - 65℃; Stage #3: With water for 0.5h; |
Conditions | Yield |
---|---|
Stage #1: 1H-imidazole; ethyl bromoacetate Stage #2: With water |
imidazol-1-ylacetic acid
1-hydroxy-2-(imidazol-1-yl)ethylidene-1,1-bisphosphonic acid
Conditions | Yield |
---|---|
Stage #1: imidazol-1-ylacetic acid With phosphoric acid; phosphorus trichloride In 1,2-propylene cyclic carbonate; PEG 600 (polyethylene glycol) at 40 - 60℃; Stage #2: With water In 1,2-propylene cyclic carbonate; PEG 600 (polyethylene glycol) at 85℃; for 18h; Product distribution / selectivity; | 99% |
Stage #1: imidazol-1-ylacetic acid With phosphorous acid; phosphorus trichloride In 1,2-propylene cyclic carbonate; PEG 600 at 40 - 60℃; Stage #2: With water In 1,2-propylene cyclic carbonate; PEG 600 at 85℃; for 18h; Product distribution / selectivity; | 99% |
With sulfolane; phosphonic Acid; 1-butyl-3-methylimidazolium Tetrafluoroborate; phosphorus trichloride at 75℃; for 3h; Reagent/catalyst; Green chemistry; | 93% |
imidazol-1-ylacetic acid
Fmoc-Pro-OH
N-Fmoc L-Phe
Fmoc-Asn-OH
Fmoc-L-Arg-OH
trifluoroacetic acid
Conditions | Yield |
---|---|
Stage #1: Fmoc-Asn-OH With benzotriazol-1-ol; diisopropyl-carbodiimide In N,N-dimethyl-formamide for 2h; Stage #2: With piperidine In N,N-dimethyl-formamide for 0.333333h; Stage #3: imidazol-1-ylacetic acid; Fmoc-Pro-OH; N-Fmoc L-Phe; Fmoc-L-Arg-OH; trifluoroacetic acid Further stages; | 97% |
imidazol-1-ylacetic acid
Conditions | Yield |
---|---|
Stage #1: imidazol-1-ylacetic acid With 1-butyl-3-methylimidazolium Tetrafluoroborate; phosphorous acid; phosphorus trichloride In sulfolane at 75℃; for 0.5h; Ionic liquid; Stage #2: With water at 105℃; for 1h; pH=1.8; Reagent/catalyst; | 93% |
Conditions | Yield |
---|---|
With thionyl chloride In methanol | 90% |
imidazol-1-ylacetic acid
(E)-5-[2-4-(hydroxyphenyl)ethenyl]-1,3-benzenediol
Conditions | Yield |
---|---|
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane; N,N-dimethyl-formamide at 60℃; for 3h; | 90% |
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane; N,N-dimethyl-formamide at 60℃; for 3h; | 90% |
imidazol-1-ylacetic acid
2-nitro-1,4-phenylenediamine
N-(4-amino-3-nitrophenyl)-2-(1H-imidazol-1-yl)acetamide
Conditions | Yield |
---|---|
With triethylamine; 3-[(diethoxyphosphinyl)oxy]-1,2,3-benzotriazin-4(3H)-one In acetonitrile at 20℃; for 96h; | 88% |
imidazol-1-ylacetic acid
Conditions | Yield |
---|---|
In water aq. soln. of Pb(NO3)2 added to aq. soln. of 2-(1H-imidazole-1-yl)acetic acid with stirring; filtered, allowed to stand at room temp. for several d; elem. anal.; | 80% |
imidazol-1-ylacetic acid
5-[9-(cyclopropylmethyl)-6-morpholin-4-yl-8-piperazin-1-yl-9H-purin-2-yl]pyrimidin-2-amine
5-{9-(Cyclopropylmethyl)-8-[4-(1H-imidazol-1-ylacetyl)piperazin-1-yl]-6-morpholin-4-yl-9H-purin-2-yl}pyrimidin-2-amine
Conditions | Yield |
---|---|
With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine In N,N-dimethyl-formamide at 20℃; for 17.5h; | 79% |
Conditions | Yield |
---|---|
In water aq. soln. of AgNO3 added to aq. soln. of 2-(1H-imidazole-1-yl)acetic acid, stirred for 30 min at room temp.; filtered, allowed to stand at room temp. for wk; elem. anal.; | 78% |
imidazol-1-ylacetic acid
cadmium(II) chloride
Conditions | Yield |
---|---|
With NaOH In water aq. soln. of ligand added to aq. soln. of CdCl2, aq. soln. of NaOH addedto pH 7, stirred for 30 min; filtered, left to stand at room temp., slow evapd. for 3 d; elem. anal.; | 75% |
imidazol-1-ylacetic acid
zinc(II) nitrate
Conditions | Yield |
---|---|
With NaOH In water aq. soln. of ligand added to aq. soln. of Zn(NO3)2, stirred for 30 min, aq. soln. of NaOH added to pH 7; filtered, left to stand at room temp., slow evapd. for 5 d; elem. anal.; | 72% |
imidazol-1-ylacetic acid
C2HF3O2*C21H27N3O4
1-(4-(4-(3-(benzyloxy)-2-nitrophenoxy)butyl)piperazin-1-yl)-2-(1H-imidazol-1-yl)ethanone
Conditions | Yield |
---|---|
Stage #1: C2HF3O2*C21H27N3O4 With N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 25℃; for 0.166667h; Inert atmosphere; Stage #2: imidazol-1-ylacetic acid With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In N,N-dimethyl-formamide at 25℃; for 16h; Inert atmosphere; | 72% |
With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide for 16h; Inert atmosphere; | 72% |
imidazol-1-ylacetic acid
[2,2]bipyridinyl
Conditions | Yield |
---|---|
In ethanol; water at 20 - 120℃; for 72h; pH=4; Autoclave; | 72% |
Conditions | Yield |
---|---|
With benzotriazol-1-ol; dicyclohexyl-carbodiimide In N,N-dimethyl-formamide | 65.9% |
imidazol-1-ylacetic acid
(2AS,3AS)-3A-amino-3A-deoxy-3A-β-cyclodextrin
Conditions | Yield |
---|---|
With benzotriazol-1-ol; dicyclohexyl-carbodiimide In N,N-dimethyl-formamide | 65.7% |
Conditions | Yield |
---|---|
With NaOH In water aq. soln. of NaOH added to aq. soln. of ligand to pH 7, aq. soln. of AgNO3 added slowly; filtered, slow evapd. for 1 wk; elem. anal.; | 65% |
2-Aminomethylthiophene
imidazol-1-ylacetic acid
Cyclohexyl isocyanide
2-methylphenyl aldehyde
C25H30N4O2S
Conditions | Yield |
---|---|
Stage #1: 2-Aminomethylthiophene; 2-methylphenyl aldehyde In methanol at 20℃; for 0.5h; Stage #2: imidazol-1-ylacetic acid In methanol at 20℃; for 0.166667h; Stage #3: Cyclohexyl isocyanide In methanol at 20℃; | 64% |
imidazol-1-ylacetic acid
Conditions | Yield |
---|---|
With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 20℃; for 16h; | 61.2% |
imidazol-1-ylacetic acid
3,4-bis((4-methoxybenzyl)oxy)aniline
C27H27N3O5
Conditions | Yield |
---|---|
Stage #1: imidazol-1-ylacetic acid; 3,4-bis((4-methoxybenzyl)oxy)aniline With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 0 - 20℃; for 2h; Stage #2: In N,N-dimethyl-formamide for 1h; | 58% |
imidazol-1-ylacetic acid
1,2-diamino-benzene
Conditions | Yield |
---|---|
With polyphosphoric acid | 57% |
imidazol-1-ylacetic acid
N-[1-(1H-imidazol-1-ylacetyl)piperidin-4-yl]-5-(phenylsulfonyl)-2-(trifluoromethyl)benzenesulfonamide hydrochloride
Conditions | Yield |
---|---|
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 20℃; for 72h; | 55% |
imidazol-1-ylacetic acid
Conditions | Yield |
---|---|
With NaOH In water byproducts: NaNO3; equimol., to a Soln. of N compd. (pH ca. 7-8 by NaOH) slowly added a soln. of metal salt, refluxed for 4 h; ppt. extd. (water), filtered, stored at room temp.; elem. anal., TGA, powder XRD; | 51% |
imidazol-1-ylacetic acid
3-amino-1-[2-(2,3-dihydro-1H-inden-2-ylamino)-7,8-dihydropyrido[4,3-d]pyrimidin-6(5H)-yl]propan-1-one
N-{3-[2-(2,3-dihydro-1H-inden-2-ylamino)-7,8-dihydropyrido[4,3-d]pyrimidin-6(5H)-yl]-3-oxopropyl}-2-(1H-imidazol-1-yl)acetamide
Conditions | Yield |
---|---|
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane for 16h; | 49% |
imidazol-1-ylacetic acid
4-(thiophen-3-yl)aniline
Conditions | Yield |
---|---|
With triethylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate In dichloromethane at 20℃; for 16h; | 42% |
Conditions | Yield |
---|---|
With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 20℃; for 36h; | 40% |
imidazol-1-ylacetic acid
(6Z,9Z,28Z,31Z)-heptatriaconta-6,9,28,31-tetraen-19-yl 2-(1H-imidazol-1-yl)acetate
Conditions | Yield |
---|---|
With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap In dichloromethane for 16h; Inert atmosphere; Reflux; | 39% |
imidazol-1-ylacetic acid
(6Z,9Z,28Z,31Z)-heptatriacont-6,9,28,31-tetraene-19-ol
(6Z,9Z,28Z,31Z)-heptatriaconta-6,9,28,31-tetraen-19-yl 2-(1H-imidazol-1-yl)acetate
Conditions | Yield |
---|---|
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine In dichloromethane for 16h; Inert atmosphere; Reflux; | 39% |
Conditions | Yield |
---|---|
Stage #1: imidazol-1-ylacetic acid; benzaldehyde With acetic anhydride; triethylamine at 100 - 170℃; Microwave irradiation; Stage #2: With sodium hydroxide In methanol; water at 20℃; | 39% |
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