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Dayang Chem (Hangzhou) Co.,Ltd.

As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem’s R&D center offer custom synthesis according to the contract research and development services for the fine c

1,3-Dioxane-5,5-dimethanol,2-phenyl-

Cas:2425-41-4

Min.Order:1 Kilogram

FOB Price: $3.0

Type:Lab/Research institutions

inquiry

Chemwill Asia Co., Ltd.

Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block

2-Phenyl-1,3-dioxane-5,5-dimethanol

Cas:2425-41-4

Min.Order:5 Kiloliter

FOB Price: $1.2 / 5.0

Type:Manufacturers

inquiry

Zhuozhou Wenxi import and Export Co., Ltd

WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et

Pharmaceutical Grade CAS 2425-41-4 with competitive price

Cas:2425-41-4

Min.Order:1 Kilogram

FOB Price: $139.0 / 210.0

Type:Trading Company

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Shanghai Upbio Tech Co.,Ltd

1.In No Less 10 years exporting experience. you can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specializ

1,3-Dioxane-5,5-dimethanol,2-phenyl-

Cas:2425-41-4

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Qingdao Beluga Import and Export Co., LTD

5,5-BIS(HYDROXYMETHYL)-2-PHENYL-1,3-DIOXANE CAS:2425-41-4 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in hi

5,5-BIS(HYDROXYMETHYL)-2-PHENYL-1,3-DIOXANE CAS:2425-41-4

Cas:2425-41-4

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Zibo Hangyu Biotechnology Development Co., Ltd

Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi

2,2-bis(hydroxymethyl)-4-phenyl-3-butene-1,3-diol CAS NO.2425-41-4

Cas:2425-41-4

Min.Order:10 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Shandong Mopai Biotechnology Co., LTD

Shandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W

5,5-BIS(HYDROXYMETHYL)-2-PHENYL-1,3-DIOXANE

Cas:2425-41-4

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Hunan chemfish Pharmaceutical co.,Ltd

Appearance:95%+ Package:R&D,Pilot run Transportation:per client require Port:Express ,Air, Sea

Monobenzalpentaerythritol

Cas:2425-41-4

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Suzhou Health Chemicals Co., Ltd.

High quality,stable supply chain.Appearance:white/off-white or light yellow Storage:Store in cool and dry place, keep away from strong light and heat. Package:aluminum bottle,glass bottle,PTFE bottle,cardboard drum Application:This product can be use

2425-41-4

Cas:2425-41-4

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Henan Allgreen Chemical Co.,Ltd

high quality Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea

5,5-Bis(hydroxyMethyl)-2-phenyl-1,3-dioxane

Cas:2425-41-4

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Antimex Chemical Limied

Ansciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali

5,5-Bis(hydroxyMethyl)-2-phenyl-1,3-dioxane

Cas:2425-41-4

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Baoji Guokang Healthchem co.,ltd

Our?company?has?been?in?existence?for?10?years?since?its?establishment.?We?have?our?own?unique?team.?The??company?integrates?independent?research?and?development,?production?and?sales.?We?have?established?famous??brands?at?home?and?abroad.?At?present

(2-Phenyl-1,3-dioxane-5,5-diyl)dimethanol

Cas:2425-41-4

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Hangzhou Fandachem Co.,Ltd

1,3-Dioxane-5,5-dimethanol,2-phenyl- cas 2425-41-4Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express

1,3-Dioxane-5,5-dimethanol,2-phenyl- cas 2425-41-4

Cas:2425-41-4

Min.Order:0

Negotiable

Type:Other

inquiry

Chemlyte Solutions

Stock products, own laboratory Package:Grams, Kilograms Application:For R&D Transportation:According to customer request Port:Shanghai

[5-(hydroxymethyl)-2-phenyl-1,3-dioxan-5-yl]methanol

Cas:2425-41-4

Min.Order:0

Negotiable

Type:Other

inquiry

Hunan Russell Chemicals Technology Co.,Ltd

high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:Foil bag; Drum; Plastic bottle Application:Pharma;Industry;Agricultural Transportation:by sea or air Port:any port in China

Monobenzalpentaerythritol 2425-41-4

Cas:2425-41-4

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Shenzhen Foris Technology Co. LTD

high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:Foil bag; Drum; Plastic bottle Application:Pharma;Industry;Agricultural Transportation:by sea or air Port:any port in China

Monobenzalpentaerythritol 2425-41-4

Cas:2425-41-4

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

ZHEJIANG JIUZHOU CHEM CO.,LTD

factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin

5,5-BIS(HYDROXYMETHYL)-2-PHENYL-1,3-DIOXANE

Cas:2425-41-4

Min.Order:0

Negotiable

Type:Trading Company

inquiry

NUTROCHEM- MANUFACTURE PLACE

best seller Application:API

5,5-BIS(HYDROXYMETHYL)-2-PHENYL-1,3-DIOXANE

Cas:2425-41-4

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Amadis Chemical Co., Ltd.

1.Professional synthesis laboratory and production base. 2.Strong synthesis team and service team. 3.Professional data management system. 4.We provide the professional test date and product information ,ex. HNMR ,CNMR,FNMR, HPLC/G

2,2-bis(hydroxymethyl)-4-phenyl-3-butene-1,3-diol

Cas:2425-41-4

Min.Order:10 Milligram

Negotiable

Type:Lab/Research institutions

inquiry

Nanjing Chemlin Chemical Co., Ltd.

Nanjing Chemlin Chemical Industry Co., Ltd was established in Aug,1999, located in the industrial park of Nanjing University of Technology, It is a private enterprises in Jiangsu Province with 1200 square meters’ R&D center. Our R&D center has a well

2425-41-4

Cas:2425-41-4

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Pure Chemistry Scientific Inc.

Monobenzalpentaerythritol Application:80084644

Monobenzalpentaerythritol

Cas:2425-41-4

Min.Order:1 Gram

FOB Price: $500.0

Type:Trading Company

inquiry

Beyond Pharmaceutical Co., Ltd

Used in medicine Application:Used in medicine

5,5-Bis(hydroxymethyl)-2-phenyl-1,3-dioxane

Cas:2425-41-4

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Shuanghe Bio-Technology Limited

5,5-BIS(HYDROXYMETHYL)-2-PHENYL-1,3-DIOXANE

1,3-Dioxane-5,5-dimethanol,2-phenyl-

Cas:2425-41-4

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

NovaChemistry

high purity Application:Drug intermediates Materials intermediates and active molecules

[5-(hydroxymethyl)-2-phenyl-1,3-dioxan-5-yl]methanol

Cas:2425-41-4

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Synthetic route

Pentaerythritol
115-77-5

Pentaerythritol

benzaldehyde
100-52-7

benzaldehyde

5,5-dihydroxymethyl-2-phenyl-1,3-dioxane
2425-41-4

5,5-dihydroxymethyl-2-phenyl-1,3-dioxane

Conditions
ConditionsYield
With hydrogenchloride In water at 40℃; for 6h;81%
With hydrogenchloride In water at 20℃; for 5h; Temperature;80%
With hydrogenchloride In water at 20℃; for 3h;80%
Pentaerythritol
115-77-5

Pentaerythritol

benzaldehyde
100-52-7

benzaldehyde

A

5,5-dihydroxymethyl-2-phenyl-1,3-dioxane
2425-41-4

5,5-dihydroxymethyl-2-phenyl-1,3-dioxane

B

3,9-diphenyl-2,4,8,10-tetraoxa-spiro[5,5]undecane
2064-95-1

3,9-diphenyl-2,4,8,10-tetraoxa-spiro[5,5]undecane

Conditions
ConditionsYield
With hydrogenchloride at 25℃;A 68%
B n/a
5,5-dihydroxymethyl-2-phenyl-1,3-dioxane
2425-41-4

5,5-dihydroxymethyl-2-phenyl-1,3-dioxane

3,4-didodecyloxybenzoic acid
131525-58-1

3,4-didodecyloxybenzoic acid

(2-phenyl-1,3-dioxane-5,5-diyl)bis(methylene) bis(3,4-bis(dodecyloxy)benzoate)
1235584-42-5

(2-phenyl-1,3-dioxane-5,5-diyl)bis(methylene) bis(3,4-bis(dodecyloxy)benzoate)

Conditions
ConditionsYield
With S-phenyl 4-methoxybenzenesulfinothioate; dicyclohexyl-carbodiimide In dichloromethane at 25℃; for 12h; Inert atmosphere;98%
With dicyclohexyl-carbodiimide; 4-(dimethylamino)pyridinium tosylate In dichloromethane at 20℃; for 12h; Inert atmosphere;98%
5,5-dihydroxymethyl-2-phenyl-1,3-dioxane
2425-41-4

5,5-dihydroxymethyl-2-phenyl-1,3-dioxane

3,5-didodecyloxybenzoic acid
123126-40-9

3,5-didodecyloxybenzoic acid

(2-phenyl-1,3-dioxane-5,5-diyl)bis(methylene) bis(3,5-bis(dodecyloxy)benzoate)
1235584-43-6

(2-phenyl-1,3-dioxane-5,5-diyl)bis(methylene) bis(3,5-bis(dodecyloxy)benzoate)

Conditions
ConditionsYield
With S-phenyl 4-methoxybenzenesulfinothioate; dicyclohexyl-carbodiimide In dichloromethane at 25℃; for 12h; Inert atmosphere;97%
With dicyclohexyl-carbodiimide; 4-(dimethylamino)pyridinium tosylate In dichloromethane at 20℃; for 12h; Inert atmosphere;97%
5,5-dihydroxymethyl-2-phenyl-1,3-dioxane
2425-41-4

5,5-dihydroxymethyl-2-phenyl-1,3-dioxane

2,2,5-trimethyl-1,3-dioxane-5-carboxylic acid
16837-14-2

2,2,5-trimethyl-1,3-dioxane-5-carboxylic acid

C28H40O10

C28H40O10

Conditions
ConditionsYield
With dicyclohexyl-carbodiimide; 4-(dimethylamino)pyridinium tosylate In dichloromethane at 20℃; for 20h;96.5%
5,5-dihydroxymethyl-2-phenyl-1,3-dioxane
2425-41-4

5,5-dihydroxymethyl-2-phenyl-1,3-dioxane

1-bromo-octane
111-83-1

1-bromo-octane

5,5'-bis(octyloxymethyl)-2-phenyl-1,3-dioxane
1191028-17-7

5,5'-bis(octyloxymethyl)-2-phenyl-1,3-dioxane

Conditions
ConditionsYield
Stage #1: 5,5-dihydroxymethyl-2-phenyl-1,3-dioxane With sodium hydride In N,N-dimethyl-formamide; mineral oil Inert atmosphere; Cooling with ice;
Stage #2: 1-bromo-octane In N,N-dimethyl-formamide; mineral oil for 26h;
93%
Stage #1: 5,5-dihydroxymethyl-2-phenyl-1,3-dioxane With sodium hydride In N,N-dimethyl-formamide Williamson synthesis; Inert atmosphere; Cooling with ice;
Stage #2: 1-bromo-octane In N,N-dimethyl-formamide Cooling with ice;
85%
5,5-dihydroxymethyl-2-phenyl-1,3-dioxane
2425-41-4

5,5-dihydroxymethyl-2-phenyl-1,3-dioxane

propargyl bromide
106-96-7

propargyl bromide

2-phenyl-5,5-bis(prop-2-ynyloxymethyl)-1,3-dioxane

2-phenyl-5,5-bis(prop-2-ynyloxymethyl)-1,3-dioxane

Conditions
ConditionsYield
With sodium hydride In N,N-dimethyl-formamide; toluene at 20℃; for 4h;92%
Stage #1: 5,5-dihydroxymethyl-2-phenyl-1,3-dioxane With sodium hydride In tetrahydrofuran; mineral oil at 0 - 20℃; for 1h; Inert atmosphere;
Stage #2: propargyl bromide In tetrahydrofuran at 0 - 40℃;
89.5%
Stage #1: 5,5-dihydroxymethyl-2-phenyl-1,3-dioxane With sodium hydride In tetrahydrofuran; mineral oil at 0 - 20℃; for 1h; Inert atmosphere;
Stage #2: propargyl bromide In tetrahydrofuran; mineral oil at 0 - 40℃;
89.5%
5,5-dihydroxymethyl-2-phenyl-1,3-dioxane
2425-41-4

5,5-dihydroxymethyl-2-phenyl-1,3-dioxane

dimethyl sulfate
77-78-1

dimethyl sulfate

5,5-bis(methoxymethyl)-2-phenyl-1,3-dioxane
2209-91-8

5,5-bis(methoxymethyl)-2-phenyl-1,3-dioxane

Conditions
ConditionsYield
Stage #1: 5,5-dihydroxymethyl-2-phenyl-1,3-dioxane With sodium hydride In tetrahydrofuran at 25 - 30℃; for 2h;
Stage #2: dimethyl sulfate In tetrahydrofuran at 0 - 20℃; for 8h; Reflux;
92%
5,5-dihydroxymethyl-2-phenyl-1,3-dioxane
2425-41-4

5,5-dihydroxymethyl-2-phenyl-1,3-dioxane

methyl iodide
74-88-4

methyl iodide

5,5-bis(methoxymethyl)-2-phenyl-1,3-dioxane
2209-91-8

5,5-bis(methoxymethyl)-2-phenyl-1,3-dioxane

Conditions
ConditionsYield
With sodium hydride In tetrahydrofuran at 20℃; Methylation;91%
With sodium hydride In N,N-dimethyl-formamide at 0 - 20℃;82%
5,5-dihydroxymethyl-2-phenyl-1,3-dioxane
2425-41-4

5,5-dihydroxymethyl-2-phenyl-1,3-dioxane

2,2,5-trimethyl-1,3-dioxane-5-carboxylic anhydride
408322-03-2

2,2,5-trimethyl-1,3-dioxane-5-carboxylic anhydride

C28H40O10

C28H40O10

Conditions
ConditionsYield
With pyridine; dmap In dichloromethane at 20℃;90%
5,5-dihydroxymethyl-2-phenyl-1,3-dioxane
2425-41-4

5,5-dihydroxymethyl-2-phenyl-1,3-dioxane

3,4,5-tridodecyloxy benzoic acid
117241-31-3

3,4,5-tridodecyloxy benzoic acid

(2-phenyl-1,3-dioxane-5,5-diyl)bis(methylene) bis(3,4,5-tris(dodecyloxy)benzoate)
1235584-44-7

(2-phenyl-1,3-dioxane-5,5-diyl)bis(methylene) bis(3,4,5-tris(dodecyloxy)benzoate)

Conditions
ConditionsYield
With S-phenyl 4-methoxybenzenesulfinothioate; dicyclohexyl-carbodiimide In dichloromethane at 25℃; for 12h; Inert atmosphere;90%
With dicyclohexyl-carbodiimide; 4-(dimethylamino)pyridinium tosylate In dichloromethane at 20℃; for 12h; Inert atmosphere;90%
5,5-dihydroxymethyl-2-phenyl-1,3-dioxane
2425-41-4

5,5-dihydroxymethyl-2-phenyl-1,3-dioxane

2-propynyl chloride
624-65-7

2-propynyl chloride

2-phenyl-5,5-bis(prop-2-ynyloxymethyl)-1,3-dioxane

2-phenyl-5,5-bis(prop-2-ynyloxymethyl)-1,3-dioxane

Conditions
ConditionsYield
Stage #1: 5,5-dihydroxymethyl-2-phenyl-1,3-dioxane With sodium hydride In N,N-dimethyl-formamide; mineral oil at 0℃; for 0.5h;
Stage #2: 2-propynyl chloride In N,N-dimethyl-formamide; mineral oil at 20℃; for 10h;
90%
5,5-dihydroxymethyl-2-phenyl-1,3-dioxane
2425-41-4

5,5-dihydroxymethyl-2-phenyl-1,3-dioxane

benzyl chloride
100-44-7

benzyl chloride

2-phenyl-5,5-bis<(benzyloxy)methyl>-1,3-dioxane
82265-10-9

2-phenyl-5,5-bis<(benzyloxy)methyl>-1,3-dioxane

Conditions
ConditionsYield
With potassium hydroxide In benzene for 16h; Heating;89%
5,5-dihydroxymethyl-2-phenyl-1,3-dioxane
2425-41-4

5,5-dihydroxymethyl-2-phenyl-1,3-dioxane

1-Bromotetradecane
112-71-0

1-Bromotetradecane

2-phenyl-5,5'-bis(tetradecyloxymethyl)-1,3-dioxane

2-phenyl-5,5'-bis(tetradecyloxymethyl)-1,3-dioxane

Conditions
ConditionsYield
Stage #1: 5,5-dihydroxymethyl-2-phenyl-1,3-dioxane With sodium hydride In N,N-dimethyl-formamide Williamson synthesis; Inert atmosphere; Cooling with ice;
Stage #2: 1-Bromotetradecane In N,N-dimethyl-formamide Cooling with ice;
89%
With sodium hydroxide; tetrabutylammomium bromide at 80℃; for 8.5h;84%
5,5-dihydroxymethyl-2-phenyl-1,3-dioxane
2425-41-4

5,5-dihydroxymethyl-2-phenyl-1,3-dioxane

1-bromo dodecane
112-29-8

1-bromo dodecane

5,5'-bis(decyloxymethyl)-2-phenyl-1,3-dioxane
1191028-21-3

5,5'-bis(decyloxymethyl)-2-phenyl-1,3-dioxane

Conditions
ConditionsYield
Stage #1: 5,5-dihydroxymethyl-2-phenyl-1,3-dioxane With sodium hydride In N,N-dimethyl-formamide Williamson synthesis; Inert atmosphere; Cooling with ice;
Stage #2: 1-bromo dodecane In N,N-dimethyl-formamide Cooling with ice;
89%
5,5-dihydroxymethyl-2-phenyl-1,3-dioxane
2425-41-4

5,5-dihydroxymethyl-2-phenyl-1,3-dioxane

benzyl bromide
100-39-0

benzyl bromide

2-phenyl-5,5-bis<(benzyloxy)methyl>-1,3-dioxane
82265-10-9

2-phenyl-5,5-bis<(benzyloxy)methyl>-1,3-dioxane

Conditions
ConditionsYield
With sodium hydride In N,N-dimethyl-formamide at 0 - 20℃; for 12h;86%
5,5-dihydroxymethyl-2-phenyl-1,3-dioxane
2425-41-4

5,5-dihydroxymethyl-2-phenyl-1,3-dioxane

N-3-benzoylthymine
4330-20-5

N-3-benzoylthymine

5,5-bis-[(3-benzoyl-thymin-1-yl)methyl]-2-phenyl-1,3-dioxane
650619-69-5

5,5-bis-[(3-benzoyl-thymin-1-yl)methyl]-2-phenyl-1,3-dioxane

Conditions
ConditionsYield
With triphenylphosphine; diethylazodicarboxylate In tetrahydrofuran at 20℃; Mitsunobu reaction;85%
5,5-dihydroxymethyl-2-phenyl-1,3-dioxane
2425-41-4

5,5-dihydroxymethyl-2-phenyl-1,3-dioxane

2-<(benzyloxy)methyl>-2-(hydroxymethyl)-1,3-propanediol
130147-42-1

2-<(benzyloxy)methyl>-2-(hydroxymethyl)-1,3-propanediol

Conditions
ConditionsYield
With triethylsilane; ethylaluminum dichloride In dichloromethane; toluene at -78℃; for 0.666667h;85%
5,5-dihydroxymethyl-2-phenyl-1,3-dioxane
2425-41-4

5,5-dihydroxymethyl-2-phenyl-1,3-dioxane

1-bromo-hexane
111-25-1

1-bromo-hexane

O-benzylidene-di-O-hexyl pentaerythritol

O-benzylidene-di-O-hexyl pentaerythritol

Conditions
ConditionsYield
With sodium hydroxide; tetrabutylammomium bromide at 80℃; for 8.5h;83%
5,5-dihydroxymethyl-2-phenyl-1,3-dioxane
2425-41-4

5,5-dihydroxymethyl-2-phenyl-1,3-dioxane

p-toluenesulfonyl chloride
98-59-9

p-toluenesulfonyl chloride

(2-phenyl-1,3-dioxane-5,5-diyl)di(methylene) bis(4-methylbenzenesulfonate)
2209-89-4

(2-phenyl-1,3-dioxane-5,5-diyl)di(methylene) bis(4-methylbenzenesulfonate)

Conditions
ConditionsYield
With pyridine for 10h; Ambient temperature;81%
With pyridine at 25℃; for 10h;78%
With pyridine at 20℃;
polytetrafluoroethylene
116-14-3

polytetrafluoroethylene

5,5-dihydroxymethyl-2-phenyl-1,3-dioxane
2425-41-4

5,5-dihydroxymethyl-2-phenyl-1,3-dioxane

2-phenyl-5,5-bis(1,1,2,2-tetrafluoroethoxymethyl)-1,3-dioxane

2-phenyl-5,5-bis(1,1,2,2-tetrafluoroethoxymethyl)-1,3-dioxane

Conditions
ConditionsYield
With potassium hydroxide In 1-methyl-pyrrolidin-2-one at 40℃; under 6750.68 Torr; Autoclave; Inert atmosphere;80.1%
5,5-dihydroxymethyl-2-phenyl-1,3-dioxane
2425-41-4

5,5-dihydroxymethyl-2-phenyl-1,3-dioxane

hexadecanyl bromide
112-82-3

hexadecanyl bromide

O-benzylidene-di-O-hexadecyl pentaerythritol
194930-71-7

O-benzylidene-di-O-hexadecyl pentaerythritol

Conditions
ConditionsYield
With sodium hydroxide; tetrabutylammomium bromide at 80℃; for 8h;80%
With sodium hydroxide; tetrabutylammomium bromide at 80℃; for 8.5h;80%
5,5-dihydroxymethyl-2-phenyl-1,3-dioxane
2425-41-4

5,5-dihydroxymethyl-2-phenyl-1,3-dioxane

2,3,5,6,8,9,11,12,14,15,17,18-dodecahydrobenzo[b][1,4,7,10,13,16,19]-heptaoxacyclohenicosine-21-carboxylic acid
1207563-98-1

2,3,5,6,8,9,11,12,14,15,17,18-dodecahydrobenzo[b][1,4,7,10,13,16,19]-heptaoxacyclohenicosine-21-carboxylic acid

C50H68O20

C50H68O20

Conditions
ConditionsYield
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 20℃; for 24h;79%
5,5-dihydroxymethyl-2-phenyl-1,3-dioxane
2425-41-4

5,5-dihydroxymethyl-2-phenyl-1,3-dioxane

benzoyl chloride
98-88-4

benzoyl chloride

5,5-bis-benzoyloximethyl-2-phenyl-[1,3]dioxane
2425-36-7

5,5-bis-benzoyloximethyl-2-phenyl-[1,3]dioxane

Conditions
ConditionsYield
In pyridine77%
With pyridine
5,5-dihydroxymethyl-2-phenyl-1,3-dioxane
2425-41-4

5,5-dihydroxymethyl-2-phenyl-1,3-dioxane

3-nitrobenzene-1,2-dicarbonitrile
51762-67-5

3-nitrobenzene-1,2-dicarbonitrile

5,5-bis(2',3'-dicyanophenoxymethyl)-2-phenyl-1,3-dioxane

5,5-bis(2',3'-dicyanophenoxymethyl)-2-phenyl-1,3-dioxane

Conditions
ConditionsYield
With potassium carbonate In dimethyl sulfoxide under 20 Torr; for 384h; Ambient temperature;77%
5,5-dihydroxymethyl-2-phenyl-1,3-dioxane
2425-41-4

5,5-dihydroxymethyl-2-phenyl-1,3-dioxane

methanesulfonyl chloride
124-63-0

methanesulfonyl chloride

2-phenyl-5,5-bis(methylsulfonyloxymethyl)-1,3-dioxane
582300-87-6

2-phenyl-5,5-bis(methylsulfonyloxymethyl)-1,3-dioxane

Conditions
ConditionsYield
With pyridine at 0℃; for 20h;77%
With triethylamine In dichloromethane at 5 - 20℃; for 25h;
5,5-dihydroxymethyl-2-phenyl-1,3-dioxane
2425-41-4

5,5-dihydroxymethyl-2-phenyl-1,3-dioxane

1-dodecylbromide
143-15-7

1-dodecylbromide

5,5'-bis(dodecyloxymethyl)-2-phenyl-1,3-dioxane

5,5'-bis(dodecyloxymethyl)-2-phenyl-1,3-dioxane

Conditions
ConditionsYield
Stage #1: 5,5-dihydroxymethyl-2-phenyl-1,3-dioxane With sodium hydride In N,N-dimethyl-formamide Williamson synthesis; Inert atmosphere; Cooling with ice;
Stage #2: 1-dodecylbromide In N,N-dimethyl-formamide Cooling with ice;
77%
With sodium hydride In N,N-dimethyl-formamide77%
With sodium hydroxide; tetrabutylammomium bromide at 80℃; for 8.5h;75%
5,5-dihydroxymethyl-2-phenyl-1,3-dioxane
2425-41-4

5,5-dihydroxymethyl-2-phenyl-1,3-dioxane

1,3,5-benzenetricarbaldehyde hexamethylacetal
107384-02-1

1,3,5-benzenetricarbaldehyde hexamethylacetal

C45H48O12

C45H48O12

Conditions
ConditionsYield
70%
5,5-dihydroxymethyl-2-phenyl-1,3-dioxane
2425-41-4

5,5-dihydroxymethyl-2-phenyl-1,3-dioxane

hexadecanyl bromide
112-82-3

hexadecanyl bromide

O-benzylidene-O-hexadecyl pentaerythritol
301329-67-9

O-benzylidene-O-hexadecyl pentaerythritol

Conditions
ConditionsYield
Stage #1: 5,5-dihydroxymethyl-2-phenyl-1,3-dioxane With di(n-butyl)tin oxide In methanol at 80℃; for 6h;
Stage #2: hexadecanyl bromide With cesium fluoride In N,N-dimethyl-formamide at 20℃; for 24h; Further stages.;
68%
With potassium tert-butylate; tetra-(n-butyl)ammonium iodide In tetrahydrofuran at 65℃; for 12h; Etherification;
5,5-dihydroxymethyl-2-phenyl-1,3-dioxane
2425-41-4

5,5-dihydroxymethyl-2-phenyl-1,3-dioxane

acetic anhydride
108-24-7

acetic anhydride

5,5-bis(acetyloxymethyl)-2-phenyl-1,3-dioxane
107058-94-6

5,5-bis(acetyloxymethyl)-2-phenyl-1,3-dioxane

Conditions
ConditionsYield
With pyridine for 20h;67%

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