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Dayang Chem (Hangzhou) Co.,Ltd.

Dayangchem’s R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantiti

Diphenylphosphoryl azide TOP1 supplier in China

Cas:26386-88-9

Min.Order:1 Kilogram

FOB Price: $3.0

Type:Lab/Research institutions

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Simagchem Corporation

Welcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our

High quality Diphenylphosphoryl Azide supplier in China

Cas:26386-88-9

Min.Order:0 Metric Ton

Negotiable

Type:Manufacturers

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Jinan Finer Chemical Co., Ltd

Product description: Product name Diphenylphosphoryl azide CAS number 26386-88-9 Assay ≥99% Appearance Colorless or yellowish liquid Capacity 500mt/year Application Widely us

Diphenylphosphoryl azide

Cas:26386-88-9

Min.Order:10 Gram

FOB Price: $12.0

Type:Lab/Research institutions

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Ality Chemical Corporation

The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi

Factory Supply Diphenyl azidophosphate

Cas:26386-88-9

Min.Order:1

Negotiable

Type:Other

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Enke Pharma-tech Co.,Ltd. (Cangzhou, China )

Cangzhou Enke Pharma Tech Co.,ltd. is located in Cangzhou City, Hebei province ,where is a famous petroleum chemical industry city in China. Enke Pharma a high-tech enterprise ,and we are dedicated to developing and manufacturing ne

Diphenylphosphoryl azide

Cas:26386-88-9

Min.Order:1 Kilogram

FOB Price: $5.0

Type:Manufacturers

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Chemwill Asia Co., Ltd.

Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block

Diphenylphosphoryl azide

Cas:26386-88-9

Min.Order:5 Kiloliter

FOB Price: $1.2 / 5.0

Type:Manufacturers

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Henan Tianfu Chemical Co., Ltd.

Diphenylphosphoryl azide Basic information Product Name: Diphenylphosphoryl azide Synonyms: DIPHENYLPHOSPHORYL AZIDE;DIPHENYLPHOSPHORYL AZIDE, POLYMER-BOUND;DIPHENYL PHOSPHORAZIDATE;DIPH

best offer Diphenylphosphoryl azide

Cas:26386-88-9

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

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Hebei Nengqian Chemical Import and Export Co., LTD

With our good experience, we offer detailed technical support and advice to assist customers. We communicate closely with customers to establish their quality requirements. Consistent Quality Our plant has strict quality control in each manufacturin

Diphenylphosphoryl azide

Cas:26386-88-9

Min.Order:1 Kilogram

FOB Price: $1.0 / 10.0

Type:Trading Company

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Zhuozhou Wenxi import and Export Co., Ltd

WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et

Manufacturer supply CAS 26386-88-9 with best quality

Cas:26386-88-9

Min.Order:1 Kilogram

FOB Price: $139.0 / 210.0

Type:Trading Company

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Shanghai Upbio Tech Co.,Ltd

1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized

Phosphorazidic acid,diphenyl ester 26386-88-9

Cas:26386-88-9

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

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Qingdao Beluga Import and Export Co., LTD

Beluga chemical professional supply High quality dppa CAS 26386-88-9 1. Beluga Chemical has a professional RESEARCH and development team and strong technical force to ensure technical support and research capabilities. 2. Made in China and expor

High quality dppa CAS 26386-88-9

Cas:26386-88-9

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

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Shandong Hanjiang Chemical Co., Ltd.

Hello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai

Phosphorazidic acid,diphenyl ester

Cas:26386-88-9

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

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Henan Wentao Chemical Product Co., Ltd.

Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

CAS NO.:26386-88-9

Cas:26386-88-9

Min.Order:0

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Xiamen Hisunny Chemical Co.,Ltd

Best quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia

Diphenylphosphoryl Azide

Cas:26386-88-9

Min.Order:0

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Type:Manufacturers

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Triumph International Development Limilted

Appearance:white powder Storage:Store in a cool,dry place and keep away from direct strong light Package:As customer request Application:Used for research and industrial manufacture. Transportation:Common products:Sea/Air/Couri

diphenyl azidophosphate

Cas:26386-88-9

Min.Order:100 Metric Ton

Negotiable

Type:Lab/Research institutions

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Afine Chemicals Limited

Company Introduction 1. Established in 2005, with two independent business divisions: Fine chemicals division; Pharmaceutical division. 2. Main product: Optical brightener Textile auxiliary Dye stuff Pigments

DIPHENYLPHOSPHORYL AZIDE

Cas:26386-88-9

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

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Hangzhou J&H Chemical Co., Ltd.

J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

Diphenyl azidophosphate

Cas:26386-88-9

Min.Order:0

Negotiable

Type:Lab/Research institutions

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SHANGHAI T&W PHARMACEUTICAL CO., LTD.

A substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc

Diphenylphosphoryl azide

Cas:26386-88-9

Min.Order:4 Kilogram

Negotiable

Type:Lab/Research institutions

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Hangzhou Lingrui Chemical Co.,Ltd.

Hot sale 26386-88-9 Diphenylphosphoryl azide in stock Supply diphenyl azophosphate is a safe and efficient azide reagent obtained by reacting diphenyl chlorophosphate with sodium azide, which can replace sodium azide with explosion risk for azide re

Hot sale 26386-88-9 Diphenylphosphoryl azide in stock Supply

Cas:26386-88-9

Min.Order:1 Gram

Negotiable

Type:Other

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Shaanxi Cuicheng Biomedical Technology Co., Ltd.

Why Choose Us: 1. Factory direct sales, so we can provide the competitive price and high quality product base on 8 years of production and R&D experience. 2. It is available in stock for quick shipment.Products could be packaged according to cu

Diphenylphosphoryl azide

Cas:26386-88-9

Min.Order:1 Gram

Negotiable

Type:Other

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Shanghai Massive Chemical Technology Co., Ltd.

Massive Chemical is certified with ISO9001 and ISO14001 manufacturer for this product. We will offer all documents as requirement for the materials which includes, Certificate of Analysis, Material Safety Data Sheet, and Method of Analysis and

Diphenylphosphoryl azide/High quality/Best price

Cas:26386-88-9

Min.Order:1 Gram

FOB Price: $1.0

Type:Lab/Research institutions

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Zibo Hangyu Biotechnology Development Co., Ltd

Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi

Diphenylphosphoryl azide

Cas:26386-88-9

Min.Order:10 Gram

FOB Price: $100.0

Type:Lab/Research institutions

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HANGZHOU YUNUO CHEMICAL CO.,LTD

moderate price & quick delivery Appearance:colorless to yellow liquid Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:100g/bottle,1kg/bottle,25kg/drum or as per your request Application:Used as Pharmac

Diphenylphosphoryl azide

Cas:26386-88-9

Min.Order:1 Kilogram

Negotiable

Type:Trading Company

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Zibo Dorne chemical technology co. LTD

Product Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,

Diphenylphosphoryl azide ,98%

Cas:26386-88-9

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

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Henan Sinotech Import&Export Corporation

Brief introduction: Chemical Name:Diphenylphosphoryl azide CAS Number:26386-88-9 Molecular Formula:C12H10N3O3P Molecular Weight:275.2 Properties: slightly yellow liquid Appearance: Clear yellow liquid Storage: RT. Package:25kg/drum Application:Synt

Diphenylphosphoryl azide

Cas:26386-88-9

Min.Order:1 Kilogram

FOB Price: $1.0

Type:Other

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Xiamen Jenny Chemical Technology Co., Ltd.

GMP standard, high purity, competitive price, in stock 1. Quick Response: within 6 hours after receiving your email. 2. Quality Guarantee: All products are strictly tested by our QC, confirmed by QA, and approved by a third-party lab in China, USA,

Diphenylphosphorylazide

Cas:26386-88-9

Min.Order:1 Milligram

Negotiable

Type:Trading Company

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Shanghai Minstar Chemical Co., Ltd

Product Name: Diphenylphosphoryl azide Synonyms: phosphorazidicacid,diphenylester;(PHO)2PO-N3;PHOSPHORIC ACID DIPHENYL ESTER AZIDE;PS-DPPA;Diphenylphosphorazindate(DPPA);Diphenylphosphonicazide,97%;DPPA polymer-bound, PS-DPPA;DPPA, Phosphoric

Diphenylphosphoryl azide 26386-88-9 C12H10N3O3P

Cas:26386-88-9

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

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Siwei Development Group Ltd.

Product name: DPPA CAS No.:26386-88-9 Molecule Formula:C12H10N3OP Molecule Weight:243.20 Purity: 98.0% Package: 25kg/drum Description:Pale yellow to yellow liquid Manufacture Standards:Enterprise Standard TESTING I

Best Quality DPPA

Cas:26386-88-9

Min.Order:1 Kilogram

Negotiable

Type:Trading Company

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Hangzhou Huarong Pharm Co., Ltd.

Hangzhou Huarong Pharm Co., Ltd.established since 2006 , has been actively developing specialty products for Finished Dosages, APIs, Intermediates, and Fine chemicals markets in North America, Europe, Korea, Japan, Mid-East and all over the World. Hu

Diphenyl phosporylazide

Cas:26386-88-9

Min.Order:0

Negotiable

Type:Trading Company

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KAISA GROUP INC

1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer

26386-88-9 CAS NO.26386-88-9

Cas:26386-88-9

Min.Order:1 Metric Ton

FOB Price: $7.0 / 8.0

Type:Trading Company

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Synthetic route

chlorophosphoric acid diphenyl ester
2524-64-3

chlorophosphoric acid diphenyl ester

diphenyl phosphoryl azide
26386-88-9

diphenyl phosphoryl azide

Conditions
ConditionsYield
With sodium azide In acetone at 25℃; for 4h;96%
With alkali metal azide at 60℃; for 0.0166667h; Microwave irradiation; neat (no solvent);95%
With sodium azide In water; acetone for 3h; Ambient temperature;90%
diphenyl hydrogen phosphite
4712-55-4

diphenyl hydrogen phosphite

diphenyl phosphoryl azide
26386-88-9

diphenyl phosphoryl azide

Conditions
ConditionsYield
With tetrachloromethane; sodium azide; triethylamine In acetonitrile at 20℃; for 0.5h; Atherton-Todd reaction;76%
phenol
108-95-2

phenol

phosphorous oxychloride

phosphorous oxychloride

diphenyl phosphoryl azide
26386-88-9

diphenyl phosphoryl azide

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 40 percent / POCl3 / 2 h / 180 °C
2: 90 percent / NaN3 / acetone; H2O / 3 h / Ambient temperature
View Scheme
phenol
108-95-2

phenol

diphenyl phosphoryl azide
26386-88-9

diphenyl phosphoryl azide

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: triethylamine; trichlorophosphate / dichloromethane / 5 h / 20 °C
2: sodium azide / acetone / 10 h / 25 °C
View Scheme
Multi-step reaction with 2 steps
1: magnesium chloride; trichlorophosphate / 24 h / 100 °C / Inert atmosphere
2: sodium azide / acetonitrile / 12 h / 0 - 25 °C / Inert atmosphere
View Scheme
diphenylphosphoroamidate
2015-56-7

diphenylphosphoroamidate

diphenyl phosphoryl azide
26386-88-9

diphenyl phosphoryl azide

Conditions
ConditionsYield
Stage #1: diphenylphosphoroamidate With sulfuric acid In 1,4-dioxane at -15℃; for 0.0833333h;
Stage #2: With sodium nitrite In 1,4-dioxane for 0.5h;
Stage #3: With sodium azide In 1,4-dioxane
diphenyl phosphoryl azide
26386-88-9

diphenyl phosphoryl azide

2',3'-isopropylidene adenosine
362-75-4

2',3'-isopropylidene adenosine

5'-diphenylphosphate-5'-deoxy-2',3'-isopropylidene adenosine
78111-39-4

5'-diphenylphosphate-5'-deoxy-2',3'-isopropylidene adenosine

Conditions
ConditionsYield
With 1,8-diazabicyclo[5.4.0]undec-7-ene In 1,4-dioxane at 20℃; for 3h;100%
With 1,8-diazabicyclo[5.4.0]undec-7-ene In 1,4-dioxane at 20℃;
(S)-2-((R)-2-Methyl-pentyl)-succinic Acid 4-tert-butyl Ester
313653-11-1

(S)-2-((R)-2-Methyl-pentyl)-succinic Acid 4-tert-butyl Ester

diphenyl phosphoryl azide
26386-88-9

diphenyl phosphoryl azide

C14H25NO3

C14H25NO3

Conditions
ConditionsYield
With triethylamine In tert-butyl methyl ether at 45℃; Curtius rearrangement;100%
diphenyl phosphoryl azide
26386-88-9

diphenyl phosphoryl azide

ent-11α,15α-Dihydroxykaur-16-en-19-oic acid
57719-76-3

ent-11α,15α-Dihydroxykaur-16-en-19-oic acid

4α-isocyanato-11β,15β-dihydroxykaur-16-ene
1391633-67-2

4α-isocyanato-11β,15β-dihydroxykaur-16-ene

Conditions
ConditionsYield
With triethylamine at 20 - 90℃; for 1.5h; Curtius Rearrangement;100%
(4-Nitrophenyl)acetylene
937-31-5

(4-Nitrophenyl)acetylene

diphenyl phosphoryl azide
26386-88-9

diphenyl phosphoryl azide

diisopropylamine
108-18-9

diisopropylamine

N1,N1-diisopropyl-N2-(diphenylphosphoryl)-2-(4-nitrophenyl)acetamidine

N1,N1-diisopropyl-N2-(diphenylphosphoryl)-2-(4-nitrophenyl)acetamidine

Conditions
ConditionsYield
With copper(l) iodide In tetrahydrofuran at 25℃; for 12h;99%
With copper(l) iodide In tetrahydrofuran at 20℃; Inert atmosphere;
N-t-butylbenzamide
5894-65-5

N-t-butylbenzamide

diphenyl phosphoryl azide
26386-88-9

diphenyl phosphoryl azide

diphenyl (2-(tert-butylcarbamoyl)phenyl)phosphoramidate

diphenyl (2-(tert-butylcarbamoyl)phenyl)phosphoramidate

Conditions
ConditionsYield
With bis[dichloro(pentamethylcyclopentadienyl)iridium(III)]; sodium acetate; silver(I) triflimide In 1,2-dichloro-ethane at 60℃; under 760.051 Torr; for 24h; Reagent/catalyst;99%
2,2-dimethylpropiophenone
938-16-9

2,2-dimethylpropiophenone

diphenyl phosphoryl azide
26386-88-9

diphenyl phosphoryl azide

diphenyl (2-pivaloylphenyl)phosphoramidate

diphenyl (2-pivaloylphenyl)phosphoramidate

Conditions
ConditionsYield
With bis[dichloro(pentamethylcyclopentadienyl)iridium(III)]; lithium carbonate; acetic acid; silver(I) triflimide In 1,2-dichloro-ethane at 60℃; under 760.051 Torr; for 24h;99%
diphenyl phosphoryl azide
26386-88-9

diphenyl phosphoryl azide

1-(4-methoxyphenyl)ethanone
100-06-1

1-(4-methoxyphenyl)ethanone

diphenyl (2-acetyl-5-methoxyphenyl)phosphoramidate

diphenyl (2-acetyl-5-methoxyphenyl)phosphoramidate

Conditions
ConditionsYield
With bis[dichloro(pentamethylcyclopentadienyl)iridium(III)]; lithium carbonate; acetic acid; silver(I) triflimide In 1,2-dichloro-ethane at 60℃; under 760.051 Torr; for 24h;99%
2-isopropyl-1-methyl-1,2-dihydro-isoquinoline
104860-90-4

2-isopropyl-1-methyl-1,2-dihydro-isoquinoline

diphenyl phosphoryl azide
26386-88-9

diphenyl phosphoryl azide

[2-Isopropyl-1-methyl-1,4-dihydro-2H-isoquinolin-(3E)-ylidene]-phosphoramidic acid diphenyl ester

[2-Isopropyl-1-methyl-1,4-dihydro-2H-isoquinolin-(3E)-ylidene]-phosphoramidic acid diphenyl ester

Conditions
ConditionsYield
for 4h; Ambient temperature;98%
1,2-diethyl-1,2-dihydro-isoquinoline
104860-92-6

1,2-diethyl-1,2-dihydro-isoquinoline

diphenyl phosphoryl azide
26386-88-9

diphenyl phosphoryl azide

[1,2-Diethyl-1,4-dihydro-2H-isoquinolin-(3E)-ylidene]-phosphoramidic acid diphenyl ester

[1,2-Diethyl-1,4-dihydro-2H-isoquinolin-(3E)-ylidene]-phosphoramidic acid diphenyl ester

Conditions
ConditionsYield
for 4h; Ambient temperature;98%
diphenyl phosphoryl azide
26386-88-9

diphenyl phosphoryl azide

benzyloxydiphenylphosphine
53772-44-4

benzyloxydiphenylphosphine

benzyl P,P-diphenyl-N-(diphenylphosphoryl)phosphinimidate
864298-72-6

benzyl P,P-diphenyl-N-(diphenylphosphoryl)phosphinimidate

Conditions
ConditionsYield
In tetrahydrofuran at 0℃; for 1h;98%
In 1,2-dichloro-ethane
carbon dioxide
124-38-9

carbon dioxide

diphenyl phosphoryl azide
26386-88-9

diphenyl phosphoryl azide

dibutylamine
111-92-2

dibutylamine

dibutylcarbamic (diphenyl phosphoric) anhydride
1016549-40-8

dibutylcarbamic (diphenyl phosphoric) anhydride

Conditions
ConditionsYield
With 1,1,3,3-tetramethyl-2-phenylguanidine In acetonitrile at 0 - 20℃; for 5h;98%
1-carboxy-1'-[(dimethylamino)carbonyl]ferrocene
165814-41-5

1-carboxy-1'-[(dimethylamino)carbonyl]ferrocene

diphenyl phosphoryl azide
26386-88-9

diphenyl phosphoryl azide

1-azidocarbonyl-1'-[(dimethylamino)carbonyl]ferrocene
165814-42-6

1-azidocarbonyl-1'-[(dimethylamino)carbonyl]ferrocene

Conditions
ConditionsYield
With triethylamine In dichloromethane; toluene (N2), stirring (room temp., 25 min), addn. of CH2Cl2, washing (HCl, NaHCO3) and drying of the org. layer; evapn. of the solvent;98%
1-Acetyl-2,3-dihydro-1H-indole
16078-30-1

1-Acetyl-2,3-dihydro-1H-indole

diphenyl phosphoryl azide
26386-88-9

diphenyl phosphoryl azide

diphenyl (1-acetylindolin-7-yl)phosphoramidate

diphenyl (1-acetylindolin-7-yl)phosphoramidate

Conditions
ConditionsYield
With bis[dichloro(pentamethylcyclopentadienyl)iridium(III)]; sodium acetate; silver(I) triflimide In 1,2-dichloro-ethane at 60℃; under 760.051 Torr; for 24h;98%
diphenyl phosphoryl azide
26386-88-9

diphenyl phosphoryl azide

acetophenone
98-86-2

acetophenone

diphenyl (2-acetylphenyl)phosphoramidate

diphenyl (2-acetylphenyl)phosphoramidate

Conditions
ConditionsYield
With bis[dichloro(pentamethylcyclopentadienyl)iridium(III)]; lithium carbonate; acetic acid; silver(I) triflimide In 1,2-dichloro-ethane at 60℃; under 760.051 Torr; for 24h;98%
6-ethoxy-6Η-dibenz[c,e][1,2]oxaphosphorin
194091-96-8

6-ethoxy-6Η-dibenz[c,e][1,2]oxaphosphorin

diphenyl phosphoryl azide
26386-88-9

diphenyl phosphoryl azide

diphenyl (6-ethoxy-6H-6λ5-dibenzo[c,e][1,2]oxaphosphinin-6-ylidene)phosphoramidate

diphenyl (6-ethoxy-6H-6λ5-dibenzo[c,e][1,2]oxaphosphinin-6-ylidene)phosphoramidate

Conditions
ConditionsYield
In dichloromethane at 20℃; Inert atmosphere;98%
diphenyl phosphoryl azide
26386-88-9

diphenyl phosphoryl azide

2-amino-5-(2-hydroxyethyl)-3,7-dihydro-7H-pyrrolo[2,3-d]pyrimidin-4-one
190771-48-3

2-amino-5-(2-hydroxyethyl)-3,7-dihydro-7H-pyrrolo[2,3-d]pyrimidin-4-one

2-(2-amino-4-oxo-4,7-dihydro-3H-pyrrolo[2,3-d]pyrimidin-5-yl)ethyl diphenylphosphate

2-(2-amino-4-oxo-4,7-dihydro-3H-pyrrolo[2,3-d]pyrimidin-5-yl)ethyl diphenylphosphate

Conditions
ConditionsYield
With 1,8-diazabicyclo[5.4.0]undec-7-ene In N,N-dimethyl-formamide at 20℃; for 16h;98%
2-ethyl-1-methyl-1,2-dihydro-isoquinoline
104860-89-1

2-ethyl-1-methyl-1,2-dihydro-isoquinoline

diphenyl phosphoryl azide
26386-88-9

diphenyl phosphoryl azide

[2-Ethyl-1-methyl-1,4-dihydro-2H-isoquinolin-(3E)-ylidene]-phosphoramidic acid diphenyl ester

[2-Ethyl-1-methyl-1,4-dihydro-2H-isoquinolin-(3E)-ylidene]-phosphoramidic acid diphenyl ester

Conditions
ConditionsYield
for 4h; Ambient temperature;97%
diphenyl phosphoryl azide
26386-88-9

diphenyl phosphoryl azide

triphenylphosphine
603-35-0

triphenylphosphine

N-(diphenoxyphosphinyl)-P,P,P-triphenylphosphine imide
2809-29-2

N-(diphenoxyphosphinyl)-P,P,P-triphenylphosphine imide

Conditions
ConditionsYield
In tetrahydrofuran Ambient temperature;97%
In diethyl ether
diphenyl phosphoryl azide
26386-88-9

diphenyl phosphoryl azide

4-trifluoromethylphenylacetylene
705-31-7

4-trifluoromethylphenylacetylene

diisopropylamine
108-18-9

diisopropylamine

N1,N1-diisopropyl-N2-(diphenylphosphoryl)-2-(4-trifluoromethylphenyl)acetamidine

N1,N1-diisopropyl-N2-(diphenylphosphoryl)-2-(4-trifluoromethylphenyl)acetamidine

Conditions
ConditionsYield
With copper(l) iodide In tetrahydrofuran at 25℃; for 12h;97%
diphenyl phosphoryl azide
26386-88-9

diphenyl phosphoryl azide

1,2-bis-(diphenylphosphino)ethane
1663-45-2

1,2-bis-(diphenylphosphino)ethane

CH2CH2[P{=NP(=O)(OPh)2}Ph2]2
1192175-67-9

CH2CH2[P{=NP(=O)(OPh)2}Ph2]2

Conditions
ConditionsYield
In toluene at 20℃;97%
In N,N-dimethyl-formamide at 20℃; Solvent; Staudinger Azide Reduction;
1-isopropyl-2-methyl-1,2-dihydroisoquinoline
104860-93-7

1-isopropyl-2-methyl-1,2-dihydroisoquinoline

diphenyl phosphoryl azide
26386-88-9

diphenyl phosphoryl azide

[1-Isopropyl-2-methyl-1,4-dihydro-2H-isoquinolin-(3E)-ylidene]-phosphoramidic acid diphenyl ester

[1-Isopropyl-2-methyl-1,4-dihydro-2H-isoquinolin-(3E)-ylidene]-phosphoramidic acid diphenyl ester

Conditions
ConditionsYield
for 4h; Ambient temperature;96%
diphenyl phosphoryl azide
26386-88-9

diphenyl phosphoryl azide

diphenyl(methyl)phosphine
1486-28-8

diphenyl(methyl)phosphine

C25H23NO3P2
225658-22-0

C25H23NO3P2

Conditions
ConditionsYield
In tetrahydrofuran Ambient temperature;96%
In tetrahydrofuran at 25℃; for 0.5h; Staudinger reaction;95%
at 0℃; for 2h;
diphenyl phosphoryl azide
26386-88-9

diphenyl phosphoryl azide

N1,N2-bis(diphenylphosphino)-N1,N2-dimethylethane-1,2-diamine

N1,N2-bis(diphenylphosphino)-N1,N2-dimethylethane-1,2-diamine

N,N'-dimethyl-N,N'-bis(diphenylphosphino)ethylenediamine

N,N'-dimethyl-N,N'-bis(diphenylphosphino)ethylenediamine

Conditions
ConditionsYield
96%
diphenyl phosphoryl azide
26386-88-9

diphenyl phosphoryl azide

1,1-dimethyl-3-phenylpropyl diphenylphosphinite
820961-79-3

1,1-dimethyl-3-phenylpropyl diphenylphosphinite

1,1-dimethyl-3-phenylpropyl N-(diphenoxyphosphoryl)diphenylphosphinimidate
913542-28-6

1,1-dimethyl-3-phenylpropyl N-(diphenoxyphosphoryl)diphenylphosphinimidate

Conditions
ConditionsYield
In tetrahydrofuran at 0℃; for 1h;96%
1,1'-bis-(diphenylphosphino)ferrocene
12150-46-8

1,1'-bis-(diphenylphosphino)ferrocene

diphenyl phosphoryl azide
26386-88-9

diphenyl phosphoryl azide

[C5H4P(C6H5)2(NPO(OC6H5)2)]2Fe
225658-24-2

[C5H4P(C6H5)2(NPO(OC6H5)2)]2Fe

Conditions
ConditionsYield
In tetrahydrofuran byproducts: N2; argon atmosphere, stirring at room temperature until N2 evolution ceases; concn. to dryness, washing (ether and pentane); elem. anal.;96%
propylamine
107-10-8

propylamine

diphenyl phosphoryl azide
26386-88-9

diphenyl phosphoryl azide

diphenyl propylamino phosphate
5756-03-6

diphenyl propylamino phosphate

Conditions
ConditionsYield
With sodium carbonate; zinc(II) acetylacetonate In 1,4-dioxane at 40℃; for 3.5h; Inert atmosphere;96%
In N,N-dimethyl-formamide at 120℃; for 12h; Solvent; Temperature; Schlenk technique; Green chemistry;84%
diphenyl phosphoryl azide
26386-88-9

diphenyl phosphoryl azide

N-butylamine
109-73-9

N-butylamine

N-butyl-P,P-diphenylphosphinic acid
5756-05-8

N-butyl-P,P-diphenylphosphinic acid

Conditions
ConditionsYield
With sodium carbonate; zinc(II) acetylacetonate In 1,4-dioxane at 40℃; for 3.5h; Inert atmosphere;96%
In N,N-dimethyl-formamide at 120℃; for 12h; Schlenk technique; Green chemistry;81%
1,1,1,3',3',3'-hexafluoro-propanol
920-66-1

1,1,1,3',3',3'-hexafluoro-propanol

diphenyl phosphoryl azide
26386-88-9

diphenyl phosphoryl azide

1,1,1,3,3,3-hexafluoropropan-2-yl diphenyl phosphate
22410-38-4

1,1,1,3,3,3-hexafluoropropan-2-yl diphenyl phosphate

Conditions
ConditionsYield
With sodium carbonate at 80℃; for 24h; Schlenk technique;96%
N-methyl-1,2,3,4-tetrahydroisoquinoline
14990-40-0

N-methyl-1,2,3,4-tetrahydroisoquinoline

diphenyl phosphoryl azide
26386-88-9

diphenyl phosphoryl azide

[2-Methyl-1,4-dihydro-2H-isoquinolin-(3Z)-ylidene]-phosphoramidic acid diphenyl ester

[2-Methyl-1,4-dihydro-2H-isoquinolin-(3Z)-ylidene]-phosphoramidic acid diphenyl ester

Conditions
ConditionsYield
for 4h; Ambient temperature;95%
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