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Dayang Chem (Hangzhou) Co.,Ltd.

Dayangchem's R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantities

1-bromo-6-phenylhexane

Cas:27976-27-8

Min.Order:1 Kilogram

FOB Price: $3.0

Type:Lab/Research institutions

inquiry

Henan Tianfu Chemical Co., Ltd.

TIANFUCHEM--27976-27-8--1-BROMO-6-PHENYLHEXANE in stock Our company was built in 2009 with an ISO certificate.In the past 10 years, we have grown up as a famous fine chemicals supplier in China And we had established stable business re

TIANFUCHEM--27976-27-8--1-BROMO-6-PHENYLHEXANE in stock

Cas:27976-27-8

Min.Order:1 Metric Ton

FOB Price: $2000.0

Type:Lab/Research institutions

inquiry

Ality Chemical Corporation

The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi

Factory Supply 1-Bromo-6-phenylhexane

Cas:27976-27-8

Min.Order:0 Metric Ton

Negotiable

Type:Other

inquiry

Hangzhou J&H Chemical Co., Ltd.

J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

1-Bromo-6-phenylhexane

Cas:27976-27-8

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Suzhou Health Chemicals Co., Ltd.

High quality,stable supply chain.Appearance:white/off-white or light yellow Storage:Store in cool and dry place, keep away from strong light and heat. Package:aluminum bottle,glass bottle,PTFE bottle,cardboard drum Application:This product can be use

1-Bromo-6-phenylhexane

Cas:27976-27-8

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Hangzhou Dingyan Chem Co., Ltd

R & D enterprises have their own stock in stockAppearance:To be subject to the object Package:Customized Application:pharmaceutical intermediates Transportation:Air Port:Shanghai;Guangzhou

(6-BroMohexyl)benzene

Cas:27976-27-8

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Shanghai Finebiotech Co.,Ltd.

Shanghai Finebiotech Co.,Ltd.was established in 2020, which providing professional chemical services. As a customer-oriented company, we have distinguished ourself from others in providing worldwide customers with cost-effective and efficient service

1-BroMo-6-phenylhexane

Cas:27976-27-8

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Antimex Chemical Limied

1-bromo-6-phenylhexaneAppearance:detailed see specifications Storage:Keep away of light, cool place Package:25kg/drum;200kg/drum Application:An important raw material and intermediate used in Organic Synthesis, Pharmaceuticals Transportation:Sea/air/

1-bromo-6-phenylhexane

Cas:27976-27-8

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

ZHEJIANG JIUZHOU CHEM CO.,LTD

factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin

1-Bromo-6-phenylhexane

Cas:27976-27-8

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Amadis Chemical Co., Ltd.

1.Professional synthesis laboratory and production base. 2.Strong synthesis team and service team. 3.Professional data management system. 4.We provide the professional test date and product information ,ex. HNMR ,CNMR,FNMR, HPLC/G

6-bromohexylbenzene

Cas:27976-27-8

Min.Order:10 Milligram

Negotiable

Type:Lab/Research institutions

inquiry

Xi'an Harmonious Natural Bio-Technology Co., Ltd.

Before-Sale Service:---Any inquiries will be replied within 12 hours.---Golden Manufactory under?ISO/GMP?with?large stock.---Dedication to quality,We?have?strict?quality?control?system.?---OEM/ODM Available.---Sample is available for your evaluation

1-BROMO-6-PHENYLHEXANE

Cas:27976-27-8

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Jilin haofei import and export trade Co.,Ltd

Price, service, company and transport advantage: 1. Best service, place of origin China, high quality, and reasonable price. 2. It's customers' right to choose the package (EMS, DHL, FEDEX, UPS). 3. It's customers' right

1-bromo-6-phenylhexane CAS NO.27976-27-8

Cas:27976-27-8

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Yinghao Pharm Co.,Ltd.

Yinghao Pharm products include: leader molecule, heterocyclic compounds,chiral compounds, photoelectric materials, biochemical reagents etc. For example:benzene, pyrimidine, boricacid,pyridine, pyrazole, imidazole, pyrrole, fluorine and other derivat

1-BROMO-6-PHENYLHEXANE

Cas:27976-27-8

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Hangzhou Share Chemical Co., Ltd

At Share Chemical Company, we scrupulously abide by our policy of “Excellent Quality at a Reasonable Price”. We strive to satisfy all of our customers by providing the finest quality products supported by the finest in customer servi

1-BroMo-6-phenylhexane

Cas:27976-27-8

Min.Order:1 Gram

Negotiable

Type:Other

inquiry

Chemical Technology Co.,LTD

1. Production capacity: we have three production base with high-tech production equipment and instruments, equipped with professional production personnel, meet your requirements.2. Quality assurance: we have a first-class testing equipment and testi

1-BROMO-6-PHENYLHEXANE

Cas:27976-27-8

Min.Order:0

Negotiable

Type:Other

inquiry

Shanghai Run-Biotech Co., Ltd.

Shanghai, Run-Biotech Co., Ltd is a leading domestic pharmaceutical, biopharmaceutical, and health care products R & D outsourcing services company. As an innovation-driven and customer-focused company, Run Biotech provides a broad and integrated por

1-BroMo-6-phenylhexane

Cas:27976-27-8

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Finetech Industry Limited

FINETECH INDUSTRY LIMITED is a LONDON based CRO company providing drug discovery & development services to worldwide clients. FINETECH INDUSTRY LIMITED supplies the 1-BROMO-6-PHENYLHEXANE, CAS:27976-27-8 with the most competitive price and the best q

1-BROMO-6-PHENYLHEXANE

Cas:27976-27-8

Min.Order:0

Negotiable

Type:Trading Company

inquiry

GZ HONESTCHEM CO., LTD

R & D enterprises have their own stock in stockAppearance:To be subject to the object Package:Customized Application:pharmaceutical intermediates Transportation:Air Port:Shanghai;Guangzhou

(6-BroMohexyl)benzene

Cas:27976-27-8

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Skyrun Industrial Co.,Ltd

Adequate stocks available,prompt shipment,Strictly control on quality,Timely after-sales

1-BroMo-6-phenylhexane, 97%

Cas:27976-27-8

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Debye Scientific

Debyesci is here who supplied several kinds of chemical products to global pharmaceutical, drug discovery, agrochemical and biotechnology industries for four yearsOur key scientific leadership team has gained experience in top research and developmen

1-BROMO-6-PHENYLHEXANE

Cas:27976-27-8

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Shanghai chamflyer chemicals Co., Ltd

High quality Application:Pharmaceutial

(6-BroMohexyl)benzene

Cas:27976-27-8

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Wuhan Chemwish Technology Co., Ltd

High quality Products with prompt delivery Package:based on customer requirement Application:organic intermediates Transportation:By air or By sea Port:any port or China

1-Bromo-6-phenylhexane

Cas:27976-27-8

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

CHESS GmbH

more information,please contact us

1-Bromo-6-phenylhexane

Cas:27976-27-8

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Synthon Chemicals GmbH & Co. KG

1-Bromo-6-phenylhexane

1-Bromo-6-phenylhexane

Cas:27976-27-8

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Synthetic route

6-phenyl-1-hexanol
2430-16-2

6-phenyl-1-hexanol

(6-bromohexyl)benzene
27976-27-8

(6-bromohexyl)benzene

Conditions
ConditionsYield
With carbon tetrabromide; triphenylphosphine In dichloromethane for 1h;77%
With phosphorus tribromide In diethyl ether at 0 - 20℃; for 15h;34%
With phosphorus; sulfuric acid; hydrogen bromide
1 ,6-dibromohexane
629-03-8

1 ,6-dibromohexane

phenyllithium
591-51-5

phenyllithium

(6-bromohexyl)benzene
27976-27-8

(6-bromohexyl)benzene

Conditions
ConditionsYield
In tetrahydrofuran; diethyl ether; hexane at -14 - 20℃; for 7h; Inert atmosphere;70%
In tetrahydrofuran
In tetrahydrofuran; diethyl ether at -10℃; for 0.5h;
phenylmagnesium bromide

phenylmagnesium bromide

6-bromohexyl 4-methylbenzenesulfonate

6-bromohexyl 4-methylbenzenesulfonate

A

1,6-diphenylhexane
1087-49-6

1,6-diphenylhexane

B

(6-bromohexyl)benzene
27976-27-8

(6-bromohexyl)benzene

Conditions
ConditionsYield
With buta-1,3-diene; palladium(II) acetylacetonate In tetrahydrofuran at 20℃; for 3h;A 8%
B 69%
With buta-1,3-diene; nickel dichloride In tetrahydrofuran at 20℃; for 3h;A 20%
B 27%
1 ,6-dibromohexane
629-03-8

1 ,6-dibromohexane

phenylmagnesium bromide

phenylmagnesium bromide

(6-bromohexyl)benzene
27976-27-8

(6-bromohexyl)benzene

Conditions
ConditionsYield
With 1,8-diazabicyclo[2.2.2.]octane; (1,2,3,4,5-pentamethyl-cyclopenta-2,4-dienylmethyl)PPh2*BH3; nickel dichloride In tetrahydrofuran; diethyl ether; toluene at 25℃; for 3h;68%
1 ,6-dibromohexane
629-03-8

1 ,6-dibromohexane

benzene
71-43-2

benzene

A

(5-bromo-1-methylpentyl)benzene
28591-23-3

(5-bromo-1-methylpentyl)benzene

B

1,2,3,4-tetrahydro-1,4-dimethylnaphthalene
4175-54-6

1,2,3,4-tetrahydro-1,4-dimethylnaphthalene

C

(6-bromohexyl)benzene
27976-27-8

(6-bromohexyl)benzene

D

1-ethyltetralin
13556-58-6

1-ethyltetralin

Conditions
ConditionsYield
With silver trifluoromethanesulfonate for 20h; Heating; Further byproducts given;A 21%
B 24%
C 6%
D 25%
5-hexen-2-ylbenzene
30134-52-2

5-hexen-2-ylbenzene

(6-bromohexyl)benzene
27976-27-8

(6-bromohexyl)benzene

Conditions
ConditionsYield
With hydrogen bromide; dihydrogen peroxide
6-phenylhexyl acetate
296282-60-5

6-phenylhexyl acetate

(6-bromohexyl)benzene
27976-27-8

(6-bromohexyl)benzene

Conditions
ConditionsYield
With hydrogen bromide Heating; Yield given;
With hydrogen bromide Reflux;
6-phenyl-1-hexene
1588-44-9

6-phenyl-1-hexene

hydrogen bromide
10035-10-6, 12258-64-9

hydrogen bromide

peroxide/s

peroxide/s

(6-bromohexyl)benzene
27976-27-8

(6-bromohexyl)benzene

(E/Z)-6-Phenylhex-5-enoic acid
16424-56-9, 81077-22-7, 5771-67-5

(E/Z)-6-Phenylhex-5-enoic acid

(6-bromohexyl)benzene
27976-27-8

(6-bromohexyl)benzene

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: diethyl ether; methanol
2: DIBAL-H / CH2Cl2 / 0.5 h / 0 °C
3: H2 / PtO2 / methanol / 2585.7 Torr
4: NBS, Ph3P / CH2Cl2 / 0.42 h / 0 - 20 °C
View Scheme
(4-carboxybutyl)triphenylphosphonium bromide
17814-85-6

(4-carboxybutyl)triphenylphosphonium bromide

(6-bromohexyl)benzene
27976-27-8

(6-bromohexyl)benzene

Conditions
ConditionsYield
Multi-step reaction with 5 steps
1: 1.) NaCH2SOCH3 / 1.) DMSO, RT, 30 min, 2.) DMSO, RT, 1 h
2: diethyl ether; methanol
3: DIBAL-H / CH2Cl2 / 0.5 h / 0 °C
4: H2 / PtO2 / methanol / 2585.7 Torr
5: NBS, Ph3P / CH2Cl2 / 0.42 h / 0 - 20 °C
View Scheme
6-phenylhex-5-en-1-ol
98078-15-0

6-phenylhex-5-en-1-ol

(6-bromohexyl)benzene
27976-27-8

(6-bromohexyl)benzene

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: H2 / PtO2 / methanol / 2585.7 Torr
2: NBS, Ph3P / CH2Cl2 / 0.42 h / 0 - 20 °C
View Scheme
benzaldehyde
100-52-7

benzaldehyde

C-phenyl-C-<2-methoxy-naphthyl-(1)>-methylamine

C-phenyl-C-<2-methoxy-naphthyl-(1)>-methylamine

(6-bromohexyl)benzene
27976-27-8

(6-bromohexyl)benzene

Conditions
ConditionsYield
Multi-step reaction with 5 steps
1: 1.) NaCH2SOCH3 / 1.) DMSO, RT, 30 min, 2.) DMSO, RT, 1 h
2: diethyl ether; methanol
3: DIBAL-H / CH2Cl2 / 0.5 h / 0 °C
4: H2 / PtO2 / methanol / 2585.7 Torr
5: NBS, Ph3P / CH2Cl2 / 0.42 h / 0 - 20 °C
View Scheme
(E)-6-phenyl-5-hexenoic acid methyl ester
85396-64-1

(E)-6-phenyl-5-hexenoic acid methyl ester

(6-bromohexyl)benzene
27976-27-8

(6-bromohexyl)benzene

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: DIBAL-H / CH2Cl2 / 0.5 h / 0 °C
2: H2 / PtO2 / methanol / 2585.7 Torr
3: NBS, Ph3P / CH2Cl2 / 0.42 h / 0 - 20 °C
View Scheme
6-phenyl-hexanoic acid methyl ester
5581-76-0

6-phenyl-hexanoic acid methyl ester

(6-bromohexyl)benzene
27976-27-8

(6-bromohexyl)benzene

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: LiBH4
2: sulfuric acid; red phosphorus; aqueous hydrobromic acid
View Scheme
2,3-dichlorotetrahydro-2H-pyran
5631-95-8

2,3-dichlorotetrahydro-2H-pyran

aqueous alkaline solution

aqueous alkaline solution

(6-bromohexyl)benzene
27976-27-8

(6-bromohexyl)benzene

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: (i) Mg, Et2O, (ii) Na
2: H2 / Raney-Ni
3: aq. HBr, H2SO4
View Scheme
Multi-step reaction with 2 steps
2: aq. HBr
View Scheme
trans-6-phenyl-4-hexen-1-ol
136054-69-8

trans-6-phenyl-4-hexen-1-ol

(6-bromohexyl)benzene
27976-27-8

(6-bromohexyl)benzene

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: H2 / Raney-Ni
2: aq. HBr, H2SO4
View Scheme
benzyl chloride
100-44-7

benzyl chloride

sodium compound of α-naphthol

sodium compound of α-naphthol

(6-bromohexyl)benzene
27976-27-8

(6-bromohexyl)benzene

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: (i) Mg, Et2O, (ii) Na
2: H2 / Raney-Ni
3: aq. HBr, H2SO4
View Scheme
benzylmagnesium chloride
6921-34-2

benzylmagnesium chloride

d(-)-mandelic acidamide

d(-)-mandelic acidamide

(6-bromohexyl)benzene
27976-27-8

(6-bromohexyl)benzene

Conditions
ConditionsYield
Multi-step reaction with 2 steps
2: aq. HBr
View Scheme
carbon tetrabromide
558-13-4

carbon tetrabromide

hexan-1-ol
111-27-3

hexan-1-ol

(6-bromohexyl)benzene
27976-27-8

(6-bromohexyl)benzene

Conditions
ConditionsYield
With triphenylphosphine In dichloromethane
With triphenylphosphine In dichloromethane
With triphenylphosphine In dichloromethane
(E)-(6-bromohex-3-en1-yl)benzene

(E)-(6-bromohex-3-en1-yl)benzene

(6-bromohexyl)benzene
27976-27-8

(6-bromohexyl)benzene

6-bromohexanoyl chloride
22809-37-6

6-bromohexanoyl chloride

(6-bromohexyl)benzene
27976-27-8

(6-bromohexyl)benzene

Conditions
ConditionsYield
With triethylsilane; aluminium chloride In hexane; dichloromethane; water; benzene
1-phenyl-2-bromoethane
103-63-9

1-phenyl-2-bromoethane

(6-bromohexyl)benzene
27976-27-8

(6-bromohexyl)benzene

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: iodine; magnesium / tetrahydrofuran / Inert atmosphere; Reflux
1.2: 1 h / 5 - 10 °C / Inert atmosphere
2.1: hydrogen bromide / Reflux
View Scheme
1 ,6-dibromohexane
629-03-8

1 ,6-dibromohexane

bromobenzene
108-86-1

bromobenzene

(6-bromohexyl)benzene
27976-27-8

(6-bromohexyl)benzene

Conditions
ConditionsYield
With n-butyllithium In diethyl ether; hexane at 0℃; for 2h; Inert atmosphere;
1 ,6-dibromohexane
629-03-8

1 ,6-dibromohexane

phenylmagnesium bromide
100-58-3

phenylmagnesium bromide

(6-bromohexyl)benzene
27976-27-8

(6-bromohexyl)benzene

Conditions
ConditionsYield
With Cl2CuI(2-)*2Li(1+) In tetrahydrofuran at 20℃; for 2h;
benzyl boronic acid
4463-42-7

benzyl boronic acid

5-bromopentyl trifluoromethanesulfonate
103935-50-8

5-bromopentyl trifluoromethanesulfonate

(6-bromohexyl)benzene
27976-27-8

(6-bromohexyl)benzene

Conditions
ConditionsYield
With potassium phosphate In toluene at 60℃; for 12h;13 mg
5-bromopentan-1-ol
34626-51-2

5-bromopentan-1-ol

(6-bromohexyl)benzene
27976-27-8

(6-bromohexyl)benzene

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 2,6-dimethylpyridine / dichloromethane / 0.33 h / -78 °C / Inert atmosphere
2: potassium phosphate / toluene / 12 h / 60 °C
View Scheme
2-Phenylethyl cyclopropyl carbinol
662143-14-8

2-Phenylethyl cyclopropyl carbinol

(6-bromohexyl)benzene
27976-27-8

(6-bromohexyl)benzene

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: lithium bromide; phosphorus tribromide; zinc dibromide
View Scheme
6-bromohexanoyl chloride
22809-37-6

6-bromohexanoyl chloride

benzene
71-43-2

benzene

(6-bromohexyl)benzene
27976-27-8

(6-bromohexyl)benzene

Conditions
ConditionsYield
With triethylsilane; aluminium chloride In hexane; dichloromethane; water; benzene
(6-bromohexyl)benzene
27976-27-8

(6-bromohexyl)benzene

6-phenyl-1-hexyl iodide
52121-98-9

6-phenyl-1-hexyl iodide

Conditions
ConditionsYield
In acetone99%
With sodium iodide In acetone99%
(6-bromohexyl)benzene
27976-27-8

(6-bromohexyl)benzene

sodium 6-phenylhexane-1-sulfonate

sodium 6-phenylhexane-1-sulfonate

Conditions
ConditionsYield
With sodium sulfite In ethanol; water for 24h; Heating;96%
With sodium sulfite In tetrahydrofuran; ethanol; water at 160℃; for 0.25h; Microwave irradiation;
(6-bromohexyl)benzene
27976-27-8

(6-bromohexyl)benzene

6-phenylhexane-1-thiol
192182-85-7

6-phenylhexane-1-thiol

Conditions
ConditionsYield
Stage #1: (6-bromohexyl)benzene With hexamethyldisilathiane; tetrabutyl ammonium fluoride In tetrahydrofuran at -20 - 20℃; for 12h; Darkness;
Stage #2: With ammonium chloride In dichloromethane; water
91%
Multi-step reaction with 2 steps
1: 0.48 g / NaOH
View Scheme
With ammonia; thiourea In ethanol; dichloromethane
(6-bromohexyl)benzene
27976-27-8

(6-bromohexyl)benzene

2-(pyrimidin-5-yl)phenol

2-(pyrimidin-5-yl)phenol

5-(2-((6-phenylhexyl)oxy)phenyl)pyrimidine

5-(2-((6-phenylhexyl)oxy)phenyl)pyrimidine

Conditions
ConditionsYield
With potassium carbonate In acetone at 70℃; for 24h; Inert atmosphere; Sealed tube;85%
(6-bromohexyl)benzene
27976-27-8

(6-bromohexyl)benzene

1,4-dideoxy-2,3:5,6-di-O-isopropylidene-1,4-imino-D-mannitol

1,4-dideoxy-2,3:5,6-di-O-isopropylidene-1,4-imino-D-mannitol

N-(phenylhexyl)-1,4-dideoxy-2,3:5,6-di-O-isopropylidene-1,4-imino-D-mannitol

N-(phenylhexyl)-1,4-dideoxy-2,3:5,6-di-O-isopropylidene-1,4-imino-D-mannitol

Conditions
ConditionsYield
With potassium carbonate In N,N-dimethyl-formamide for 10h; Heating;81%
(6-bromohexyl)benzene
27976-27-8

(6-bromohexyl)benzene

hexylbenzene
1077-16-3

hexylbenzene

Conditions
ConditionsYield
With n-butyllithium; samarium diiodide; dipyrrolidinomethylaminophosphoric acid triamide; tert-butyl alcohol In tetrahydrofuran; hexane at -66 - 21℃;80%
4-[2-(4-benzyloxyphenyl)-5-methyl-1H-pyrrol-1-yl]phenol
376642-19-2

4-[2-(4-benzyloxyphenyl)-5-methyl-1H-pyrrol-1-yl]phenol

(6-bromohexyl)benzene
27976-27-8

(6-bromohexyl)benzene

2-(4-Benzyloxyphenyl)-5-methyl-1-[4-(6-phenylhexyloxy)-phenyl]-1H-pyrrole
376642-36-3

2-(4-Benzyloxyphenyl)-5-methyl-1-[4-(6-phenylhexyloxy)-phenyl]-1H-pyrrole

Conditions
ConditionsYield
With potassium carbonate In N,N-dimethyl-formamide79.4%
(6-bromohexyl)benzene
27976-27-8

(6-bromohexyl)benzene

C16H16N4O*2ClH

C16H16N4O*2ClH

C28H32N4O
1426156-40-2

C28H32N4O

Conditions
ConditionsYield
With triethylamine In acetonitrile for 15h; Reflux;77%
4-phenyl-4-cyanopiperidine
40481-13-8

4-phenyl-4-cyanopiperidine

(6-bromohexyl)benzene
27976-27-8

(6-bromohexyl)benzene

4-Cyano-1-(6-phenylhexyl)-4-phenylpiperidin

4-Cyano-1-(6-phenylhexyl)-4-phenylpiperidin

Conditions
ConditionsYield
75%
(6-bromohexyl)benzene
27976-27-8

(6-bromohexyl)benzene

4-Piperazin-1-yl-pyrrolo[1,2-a]quinoxaline
195711-50-3

4-Piperazin-1-yl-pyrrolo[1,2-a]quinoxaline

4-(4-(6-phenylhexyl)piperazin-1-yl)pyrrolo[1,2-a]quinoxaline

4-(4-(6-phenylhexyl)piperazin-1-yl)pyrrolo[1,2-a]quinoxaline

Conditions
ConditionsYield
With triethylamine In acetonitrile Reflux;75%
4-bromo-phenol
106-41-2

4-bromo-phenol

(6-bromohexyl)benzene
27976-27-8

(6-bromohexyl)benzene

6-(p-bromophenoxy)-1-phenylhexane

6-(p-bromophenoxy)-1-phenylhexane

Conditions
ConditionsYield
With sodium hydroxide In dimethyl sulfoxide at 100℃; for 5h; Etherification;72%
7-hydroxy-8-nitrochromone
101870-11-5

7-hydroxy-8-nitrochromone

(6-bromohexyl)benzene
27976-27-8

(6-bromohexyl)benzene

8-nitro-7-<(6-phenylhexyl)oxy>chromone
166529-53-9

8-nitro-7-<(6-phenylhexyl)oxy>chromone

Conditions
ConditionsYield
With potassium carbonate; lithium iodide In N,N-dimethyl-formamide at 90℃; for 24h;68%
4-{2-[2-(4-benzyloxyphenyl)-5-methyl-1H-pyrrol-1-yl]ethyl}phenol
376641-68-8

4-{2-[2-(4-benzyloxyphenyl)-5-methyl-1H-pyrrol-1-yl]ethyl}phenol

(6-bromohexyl)benzene
27976-27-8

(6-bromohexyl)benzene

2-(4-benzyloxyphenyl)-5-methyl-1-{2-[4-(6-phenylhexyloxy)phenyl]ethyl}-1H-pyrrole
376642-23-8

2-(4-benzyloxyphenyl)-5-methyl-1-{2-[4-(6-phenylhexyloxy)phenyl]ethyl}-1H-pyrrole

Conditions
ConditionsYield
With potassium carbonate In N,N-dimethyl-formamide67.1%
phenyl sulfamate
19792-91-7

phenyl sulfamate

(6-bromohexyl)benzene
27976-27-8

(6-bromohexyl)benzene

phenyl (6-bromo-1-phenylhexyl)sulfamate

phenyl (6-bromo-1-phenylhexyl)sulfamate

Conditions
ConditionsYield
Stage #1: phenyl sulfamate; (6-bromohexyl)benzene With aluminum oxide; tert-butyl isocyanide; bis{rhodium[3,3'-(1,3-phenylene)bis(2,2-dimethylpropanoic acid)]} for 0.166667h;
Stage #2: With (PhI(OtBu)2) for 6h; Sealed tube;
65%
Dichloromethyl methyl ether
4885-02-3

Dichloromethyl methyl ether

(6-bromohexyl)benzene
27976-27-8

(6-bromohexyl)benzene

4-(6-Bromo-hexyl)-benzaldehyde

4-(6-Bromo-hexyl)-benzaldehyde

Conditions
ConditionsYield
With titanium tetrachloride In dichloromethane at 35℃; for 1h; Cooling with ice;60%
With titanium tetrachloride In dichloromethane at 0 - 35℃; for 0.666667h;
methyl 5-(furan-2-yl)-1,3,4-oxadiazole-2-carboxylate
35403-85-1

methyl 5-(furan-2-yl)-1,3,4-oxadiazole-2-carboxylate

(6-bromohexyl)benzene
27976-27-8

(6-bromohexyl)benzene

7-phenyl-1-(5-(furan-2-yl)-1,3,4-oxadiazol-2-yl)-heptan-1-one

7-phenyl-1-(5-(furan-2-yl)-1,3,4-oxadiazol-2-yl)-heptan-1-one

Conditions
ConditionsYield
Stage #1: (6-bromohexyl)benzene With magnesium In tetrahydrofuran; ethylene dibromide at 23℃; Grignard reaction; Inert atmosphere; Sonication;
Stage #2: methyl 5-(furan-2-yl)-1,3,4-oxadiazole-2-carboxylate In tetrahydrofuran; ethylene dibromide at -40℃; for 2h;
57%
methyl 5-(thiophen-2-yl)-1,3,4-oxadiazole-2-carboxylate
35403-82-8

methyl 5-(thiophen-2-yl)-1,3,4-oxadiazole-2-carboxylate

(6-bromohexyl)benzene
27976-27-8

(6-bromohexyl)benzene

7-phenyl-1-(5-(thien-2-yl)-1,3,4-oxadiazol-2-yl)-heptan-1-one
1042151-27-8

7-phenyl-1-(5-(thien-2-yl)-1,3,4-oxadiazol-2-yl)-heptan-1-one

Conditions
ConditionsYield
Stage #1: (6-bromohexyl)benzene With magnesium In tetrahydrofuran; ethylene dibromide at 23℃; Grignard reaction; Inert atmosphere; Sonication;
Stage #2: methyl 5-(thiophen-2-yl)-1,3,4-oxadiazole-2-carboxylate In tetrahydrofuran; ethylene dibromide at -40℃; for 2h;
57%
(+/-)-5-benzyl-5-ethyl-4-oxo-1,2-oxathiolane-2,2-dioxide
1097642-11-9

(+/-)-5-benzyl-5-ethyl-4-oxo-1,2-oxathiolane-2,2-dioxide

(6-bromohexyl)benzene
27976-27-8

(6-bromohexyl)benzene

(+/-)-5-benzyl-5-ethyl-4-(6'-phenylhexyloxy)-5H-1,2-oxathiole-2,2-dioxide
1127304-80-6

(+/-)-5-benzyl-5-ethyl-4-(6'-phenylhexyloxy)-5H-1,2-oxathiole-2,2-dioxide

Conditions
ConditionsYield
With tetra-(n-butyl)ammonium iodide; potassium carbonate In acetonitrile at 40℃; for 4h;56%
methyl 3-(6-bromopyridin-2-yl)-1,2,4-oxadiazole-5-carboxylate
1042151-20-1

methyl 3-(6-bromopyridin-2-yl)-1,2,4-oxadiazole-5-carboxylate

(6-bromohexyl)benzene
27976-27-8

(6-bromohexyl)benzene

1-(3-(6-bromopyridin-2-yl)-1,2,4-oxadiazol-5-yl)-7-phenylheptan-1-one
1042151-37-0

1-(3-(6-bromopyridin-2-yl)-1,2,4-oxadiazol-5-yl)-7-phenylheptan-1-one

Conditions
ConditionsYield
Stage #1: (6-bromohexyl)benzene With magnesium In tetrahydrofuran; ethylene dibromide at 23℃; Grignard reaction; Inert atmosphere; Sonication;
Stage #2: methyl 3-(6-bromopyridin-2-yl)-1,2,4-oxadiazole-5-carboxylate In tetrahydrofuran; ethylene dibromide at -40℃; for 2h;
55%
(6-bromohexyl)benzene
27976-27-8

(6-bromohexyl)benzene

dimethyl amine
124-40-3

dimethyl amine

N,N-dimethyl-6-phenylhexylamine
106291-63-8

N,N-dimethyl-6-phenylhexylamine

Conditions
ConditionsYield
In tetrahydrofuran; diethyl ether for 50h; Ambient temperature;51%
(6-bromohexyl)benzene
27976-27-8

(6-bromohexyl)benzene

methyl 5-(pyridin-2-yl)-1,3,4-oxadiazole-2-carboxylate
849798-86-3

methyl 5-(pyridin-2-yl)-1,3,4-oxadiazole-2-carboxylate

7-phenyl-1-(5-(pyridin-2-yl)-1,3,4-oxadiazol-2-yl)-heptan-1-one

7-phenyl-1-(5-(pyridin-2-yl)-1,3,4-oxadiazol-2-yl)-heptan-1-one

Conditions
ConditionsYield
Stage #1: (6-bromohexyl)benzene With magnesium In tetrahydrofuran; ethylene dibromide at 23℃; Grignard reaction; Inert atmosphere; Sonication;
Stage #2: methyl 5-(pyridin-2-yl)-1,3,4-oxadiazole-2-carboxylate In tetrahydrofuran; ethylene dibromide at -40℃; for 2h;
51%
Stage #1: (6-bromohexyl)benzene With magnesium; ethylene dibromide In tetrahydrofuran at 23℃; Inert atmosphere of Ar; Heating; Sonication;
Stage #2: methyl 5-(pyridin-2-yl)-1,3,4-oxadiazole-2-carboxylate In tetrahydrofuran at -40℃; for 2h;
51%
Stage #1: (6-bromohexyl)benzene With iodine; magnesium In tetrahydrofuran at 60℃; for 2h;
Stage #2: methyl 5-(pyridin-2-yl)-1,3,4-oxadiazole-2-carboxylate In tetrahydrofuran at -40℃; for 4h;
51%
(6-bromohexyl)benzene
27976-27-8

(6-bromohexyl)benzene

p-aminoethylbenzoate
94-09-7

p-aminoethylbenzoate

ethyl 4-(6-phenylhexylamino)benzoate
61440-49-1

ethyl 4-(6-phenylhexylamino)benzoate

Conditions
ConditionsYield
In N,N,N,N,N,N-hexamethylphosphoric triamide at 125℃; for 24h;50%
(6-bromohexyl)benzene
27976-27-8

(6-bromohexyl)benzene

trioctylaluminum
1070-00-4

trioctylaluminum

tetradecylbenzene
1459-10-5

tetradecylbenzene

Conditions
ConditionsYield
With potassium fluoride; benzylnixantphos; iron(II) acetate In tetrahydrofuran at 0 - 40℃; for 12h; Negishi Coupling; Inert atmosphere;50%
(6-bromohexyl)benzene
27976-27-8

(6-bromohexyl)benzene

triphenylphosphine
603-35-0

triphenylphosphine

triphenyl(6-phenylhexyl)phosphonium iodide

triphenyl(6-phenylhexyl)phosphonium iodide

Conditions
ConditionsYield
With potassium iodide In acetonitrile at 85℃;43%
(6-bromohexyl)benzene
27976-27-8

(6-bromohexyl)benzene

5-methyl-4-mercaptomethylimidazole hydrochloride
70826-45-8

5-methyl-4-mercaptomethylimidazole hydrochloride

5-Methyl-4-(6-phenyl-hexylsulfanylmethyl)-1H-imidazole
131028-48-3

5-Methyl-4-(6-phenyl-hexylsulfanylmethyl)-1H-imidazole

Conditions
ConditionsYield
With N-benzyl-N,N,N-triethylammonium chloride In water; isopropyl alcohol at 80℃; for 4h;41%
dibenzyl methylphosphonate
19236-58-9

dibenzyl methylphosphonate

(6-bromohexyl)benzene
27976-27-8

(6-bromohexyl)benzene

dibenzyl 6-phenylhexylphosphonate
790699-80-8

dibenzyl 6-phenylhexylphosphonate

Conditions
ConditionsYield
With n-butyllithium In tetrahydrofuran; hexane at -78 - 20℃;38.5%

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