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Dayang Chem (Hangzhou) Co.,Ltd.

Dayangchem's R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantities

3-MEHTOXYPROPIONALDEHYDE

Cas:2806-84-0

Min.Order:1 Kilogram

FOB Price: $3.0

Type:Lab/Research institutions

inquiry

Chemwill Asia Co., Ltd.

Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block

3-Methoxypropionaldehyde

Cas:2806-84-0

Min.Order:5 Kiloliter

FOB Price: $1.2 / 5.0

Type:Manufacturers

inquiry

Hebei Nengqian Chemical Import and Export Co., LTD

With our good experience, we offer detailed technical support and advice to assist customers. We communicate closely with customers to establish their quality requirements. Consistent Quality Our plant has strict quality control in each manufacturin

3-METHOXY-PROPIONALDEHYDE CAS:2806-84-0

Cas:2806-84-0

Min.Order:1 Kilogram

FOB Price: $8.0 / 16.0

Type:Trading Company

inquiry

Shanghai Upbio Tech Co.,Ltd

1.In No Less 10 years exporting experience. you can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specializ

Propanal, 3-methoxy-

Cas:2806-84-0

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Shandong Hanjiang Chemical Co., Ltd.

Hello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai

Propanal, 3-methoxy-

Cas:2806-84-0

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Hangzhou J&H Chemical Co., Ltd.

J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

Propanal, 3-methoxy-

Cas:2806-84-0

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Siwei Development Group Ltd.

Product name: 3-Methoxypropionaldehyde CAS No.:2806-84-0 Molecule Formula:C4H8O2 Molecule Weight:88.10 Purity: 99% Package: 25kg/drum Description:Colorless transparent liquid Manufacture Standards:Enterprise Standard TESTING ITEM

High Quality 3-Methoxypropionaldehyde in stock

Cas:2806-84-0

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

TAIZHOU ZHENYU BIOTECHNOLOGY CO., LTD

Zhenyu biotech exported this product to many countries and regions at best price. if you are looking for the material's manufacturer or supplier in china, zhenyu biotech is your best choice. pls contact with us freely for getting detailed

3-METHOXY-PROPIONALDEHYDE

Cas:2806-84-0

Min.Order:1 Kilogram

FOB Price: $2.0

Type:Lab/Research institutions

inquiry

KAISA GROUP INC

1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer

2806-84-0 CAS NO.2806-84-0

Cas:2806-84-0

Min.Order:1 Metric Ton

FOB Price: $7.0 / 8.0

Type:Trading Company

inquiry

Suzhou Health Chemicals Co., Ltd.

High quality,stable supply chain.Appearance:white/off-white or light yellow Storage:Store in cool and dry place, keep away from strong light and heat. Package:aluminum bottle,glass bottle,PTFE bottle,cardboard drum Application:This product can be use

2806-84-0

Cas:2806-84-0

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Win-Win chemical Co.Ltd

Stock products, own laboratory Package:Grams, Kilograms Application:For R&D Transportation:According to customer request Port:Shanghai

3-METHOXY-PROPIONALDEHYDE Cas no.2806-84-0 98%

Cas:2806-84-0

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Henan Tianfu Chemical Co., Ltd.

1.Our services:A.Supply sampleB.The packing also can be according the customers` requirmentC.Any inquiries will be replied within 24 hoursD.we provide Commerical Invoice, Packing List, Bill of loading, COA , Health certificate and Origin certificate.

Propanal, 3-methoxy-

Cas:2806-84-0

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Antimex Chemical Limied

Ansciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali

Propanal, 3-methoxy-

Cas:2806-84-0

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Hangzhou Ocean Chemical Co., Ltd.

★.Best quality according to requirement ★.Competitive price in China market ★.Mature Technical support ★.Professional logistic support

3-METHOXY-PROPIONALDEHYDE

Cas:2806-84-0

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

BOC Sciences

We are committed to providing our customers with the best products and services at the most competitive prices.Appearance:light beige powder Storage:Room temperature with sealed well Package:according to the clients requirement Application:Use as pri

3-METHOXY-PROPIONALDEHYDE

Cas:2806-84-0

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Changchun Artel lmport and Export trade company

Supply top quality products with a reasonable price Application:api

2806-84-0

Cas:2806-84-0

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Hangzhou Fandachem Co.,Ltd

Propanal, 3-methoxy-Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express

Propanal, 3-methoxy-

Cas:2806-84-0

Min.Order:0

Negotiable

Type:Other

inquiry

Hunan Longxianng Runhui Trading Co.,Ltd

R & D enterprises have their own stock in stockAppearance:To be subject to the object Package:Customized Application:pharmaceutical intermediates Transportation:Air Port:Shanghai;Guangzhou

3-Methoxy-propionaldehyde

Cas:2806-84-0

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Chemlyte Solutions

Stock products, own laboratory Package:Grams, Kilograms Application:For R&D Transportation:According to customer request Port:Shanghai

3-Methoxy-propionaldehyde

Cas:2806-84-0

Min.Order:0

Negotiable

Type:Other

inquiry

ZHEJIANG JIUZHOU CHEM CO.,LTD

factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin

3-METHOXY-PROPIONALDEHYDE

Cas:2806-84-0

Min.Order:0

Negotiable

Type:Trading Company

inquiry

LEAP CHEM Co., Ltd.

Best Seller, High Quality, Competitive Price, Fast Delivery, Quick ResponseAppearance:powder, or liquid Storage:Stored in room temperature, ventilated place Package:Bottle, barrel, cargo, container, etc. Application:Pharmaceuticals, intermediates, AP

3-METHOXY-PROPIONALDEHYDE

Cas:2806-84-0

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Amadis Chemical Co., Ltd.

1.Professional synthesis laboratory and production base. 2.Strong synthesis team and service team. 3.Professional data management system. 4.We provide the professional test date and product information ,ex. HNMR ,CNMR,FNMR, HPLC/G

3-Methoxypropanal

Cas:2806-84-0

Min.Order:10 Milligram

Negotiable

Type:Lab/Research institutions

inquiry

Jilin haofei import and export trade Co.,Ltd

Price, service, company and transport advantage: 1. Best service, place of origin China, high quality, and reasonable price. 2. It's customers' right to choose the package (EMS, DHL, FEDEX, UPS). 3. It's customers' right

2806-84-0 CAS NO.2806-84-0

Cas:2806-84-0

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Henan Wising Chem Co., Ltd

Henan Wising Chem specializes in sourcing chemicals in China. We are associated with many trusted manufacturers each having different areas of expertise required for meeting the needs of our local as well as overseas buyers. We have access to custom

3-METHOXY-PROPIONALDEHYDE

Cas:2806-84-0

Min.Order:10 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Nanjing Norris Pharm Technology Co., Ltd.

R & D enterprises have their own stock in stockAppearance:To be subject to the object Package:Customized Application:pharmaceutical intermediates Transportation:Air Port:Shanghai;Guangzhou

3-Methoxy-propionaldehyde

Cas:2806-84-0

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Shanghai united Scientific Co.,Ltd.

United Scientific Company Located in Shanghai of China , is a competitive player in the global specialty and fine chemical market. Fenghua has both the expertise and flexibility to produce a wide range of chemicals. Focusing on developing the innovat

Propanal, 3-methoxy-

Cas:2806-84-0

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Capot Chemical Co., Ltd.

At Capot,We can synthesize and purify your complex molecules from 100 gram to 10 tons.Appearance:Clear colorless to light yellow liquid Storage:Dry,Seal and Cool place Package:1G,5G,10G,25G,100G,250G,500G,1KG,5KG,10KG,25KG,50KG,100KG,150KG,200KG. App

3-Methoxy propionaldehyde

Cas:2806-84-0

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Finetech Industry Limited

FINETECH INDUSTRY LIMITED is a LONDON based CRO company providing drug discovery & development services to worldwide clients. FINETECH INDUSTRY LIMITED supplies the 3-METHOXY-PROPIONALDEHYDE, CAS:2806-84-0 with the most competitive price and the best

3-METHOXY-PROPIONALDEHYDE

Cas:2806-84-0

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Nanjing Raymon Biotech Co., Ltd.

Propanal, 3-methoxy- Storage:keep in dry and cool condition Package:25kg or according to cutomer's demand Application:Chemical research/pharma intermediate Transportation:By Sea,by Air,By courier like DHL or Fedx. Port:Shanghai/Shenzhen

Propanal, 3-methoxy-

Cas:2806-84-0

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Debye Scientific

Debyesci is here who supplied several kinds of chemical products to global pharmaceutical, drug discovery, agrochemical and biotechnology industries for four yearsOur key scientific leadership team has gained experience in top research and developmen

3-METHOXY-PROPIONALDEHYDE

Cas:2806-84-0

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Synthetic route

1-Chloro-3-methoxypropane
36215-07-3

1-Chloro-3-methoxypropane

3-methoxy-1-propanal
2806-84-0

3-methoxy-1-propanal

Conditions
ConditionsYield
With C30H38Cl2Ir2N4 In dimethyl sulfoxide at 30℃; for 4h;95%
methoxypropanol
1589-49-7

methoxypropanol

3-methoxy-1-propanal
2806-84-0

3-methoxy-1-propanal

Conditions
ConditionsYield
With 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione In ethyl acetate Reflux;85%
With pyridinium chlorochromate In dichloromethane at 20℃; for 12h; Inert atmosphere;65%
With PyCrO3*HCl In dichloromethane at 20℃; for 2h;36.8%
glycerol 1-monomethyl ether
623-39-2, 36887-04-4

glycerol 1-monomethyl ether

3-methoxy-1-propanal
2806-84-0

3-methoxy-1-propanal

Conditions
ConditionsYield
With copper(II) sulfate at 200℃; under 760.051 Torr;39%
acrolein
107-02-8

acrolein

/PBUVC009---40/

/PBUVC009---40/

A

3-methoxy-1-propanal
2806-84-0

3-methoxy-1-propanal

B

methyl (Z)-2,4-pentadienoate
35694-23-6

methyl (Z)-2,4-pentadienoate

C

5-methoxy-2-pentenoate
58185-67-4

5-methoxy-2-pentenoate

D

methyl (2E)-penta-2,4-dienoate
2409-87-2

methyl (2E)-penta-2,4-dienoate

Conditions
ConditionsYield
In methanol 1.) 3 h, 2.) room temperature, 14 h, 3.) 45 deg C, 8 h; Further byproducts given;A 0.14%
B 2.7%
C 10%
D 20%
1,1,3-trimethoxypropane
14315-97-0

1,1,3-trimethoxypropane

3-methoxy-1-propanal
2806-84-0

3-methoxy-1-propanal

Conditions
ConditionsYield
With sulfuric acid
With hydrogen at 30℃; under 50.255 Torr;
With hydrogenchloride In tetrahydrofuran; water at 20℃; for 1h; Cooling;
methanol
67-56-1

methanol

acrolein
107-02-8

acrolein

3-methoxy-1-propanal
2806-84-0

3-methoxy-1-propanal

Conditions
ConditionsYield
With potassium hydroxide
With propionic acid; diethylamine
With sulfuric acid und Behandeln der mit Bariumhydroxid neutralisierten Reaktionsloesung mit Oxalsaeure;
With piperidine
With sodium hydroxide at 0 - 6℃; for 0.5h;
sodium methylate
124-41-4

sodium methylate

acrolein
107-02-8

acrolein

3-methoxy-1-propanal
2806-84-0

3-methoxy-1-propanal

methoxyethene
107-25-5

methoxyethene

carbon monoxide
201230-82-2

carbon monoxide

A

2-methoxypropanal
6142-38-7

2-methoxypropanal

B

3-methoxy-1-propanal
2806-84-0

3-methoxy-1-propanal

Conditions
ConditionsYield
With hydrogen; dodecacarbonyltetrarhodium(0) In benzene at 100℃; under 76000 Torr;
C7H14N2O4

C7H14N2O4

A

methanol
67-56-1

methanol

B

3-methoxy-1-propanal
2806-84-0

3-methoxy-1-propanal

Conditions
ConditionsYield
With sodium perchlorate In acetonitrile at 25℃; Rate constant;
1,3-dioxane
505-22-6

1,3-dioxane

A

methoxypropanol
1589-49-7

methoxypropanol

B

3-methoxy-1-propanal
2806-84-0

3-methoxy-1-propanal

C

alkoxyalkyl substd. 1,3-dioxanes, H2, CO, CO2

alkoxyalkyl substd. 1,3-dioxanes, H2, CO, CO2

Conditions
ConditionsYield
Mechanism; Product distribution; Quantum yield; Irradiation; 185 nm vacuum-ultraviolet photolysis;
hydrogenchloride
7647-01-0

hydrogenchloride

methanol
67-56-1

methanol

acrolein
107-02-8

acrolein

A

3,3-dimethoxyprop-1-ene
6044-68-4

3,3-dimethoxyprop-1-ene

B

3-methoxy-1-propanal
2806-84-0

3-methoxy-1-propanal

Conditions
ConditionsYield
at 25 - 40℃; Kinetics;
glycidyl methyl ether
930-37-0

glycidyl methyl ether

A

Methoxyacetone
5878-19-3

Methoxyacetone

B

3-methoxy-1-propanal
2806-84-0

3-methoxy-1-propanal

Conditions
ConditionsYield
With erbium(III) triflate In dichloromethane for 4h; Heating; Title compound not separated from byproducts;
methanol
67-56-1

methanol

acrolein
107-02-8

acrolein

A

malonaldehydebis(dimethylacetal)
102-52-3

malonaldehydebis(dimethylacetal)

B

1,1,3-trimethoxypropane
14315-97-0

1,1,3-trimethoxypropane

C

3-methoxy-1-propanal
2806-84-0

3-methoxy-1-propanal

Conditions
ConditionsYield
With carbon dioxide; oxygen; sodium phosphate; copper(l) chloride; palladium dichloride at 50℃; under 90007.2 Torr; for 24h; Michael addition;A 17.5 % Chromat.
B 54.6 % Chromat.
C 26.2 % Chromat.
methanol
67-56-1

methanol

acrolein
107-02-8

acrolein

A

1,1,3-trimethoxypropane
14315-97-0

1,1,3-trimethoxypropane

B

3-methoxy-1-propanal
2806-84-0

3-methoxy-1-propanal

Conditions
ConditionsYield
With carbon dioxide; oxygen; copper dichloride; palladium dichloride at 50℃; under 90007.2 Torr; for 24h; Michael addition;A 12.7 % Chromat.
B 62.5 % Chromat.
Stage #1: methanol; acrolein; Mitsubishi Chemical's Diaion SK104 In water at 50℃; for 5h;
Stage #2: With water at 25 - 36℃; under 50.255 Torr;
methanol
67-56-1

methanol

acrolein
107-02-8

acrolein

A

malonaldehydebis(dimethylacetal)
102-52-3

malonaldehydebis(dimethylacetal)

B

1,1,3-trimethoxypropane
14315-97-0

1,1,3-trimethoxypropane

C

3-methoxy-1-propanal
2806-84-0

3-methoxy-1-propanal

D

3,3-dimethoxypropanal
19060-10-7

3,3-dimethoxypropanal

Conditions
ConditionsYield
With carbon dioxide; polystyrene-supported benzoquinone; oxygen; palladium dichloride at 50℃; under 67505.4 Torr; for 12h;A 46.7 % Chromat.
B 12.9 % Chromat.
C 3.9 % Chromat.
D 20.4 % Chromat.
methanol
67-56-1

methanol

acrylic acid
79-10-7

acrylic acid

acrolein
107-02-8

acrolein

3-methoxy-1-propanal
2806-84-0

3-methoxy-1-propanal

Conditions
ConditionsYield
With acetic acid; Mitsubishi Chemical's Diaion SK104 In water at 50℃; for 5h;
acrylic acid
79-10-7

acrylic acid

acrolein
107-02-8

acrolein

3-methoxy-1-propanal
2806-84-0

3-methoxy-1-propanal

Conditions
ConditionsYield
With acetic acid In methanol; water85 mol %
glycerol
56-81-5

glycerol

A

glycerol formal
4740-78-7

glycerol formal

B

3-methoxy-1-propanal
2806-84-0

3-methoxy-1-propanal

C

acetaldehyde
75-07-0

acetaldehyde

D

hydroxy-2-propanone
116-09-6

hydroxy-2-propanone

E

acrolein
107-02-8

acrolein

Conditions
ConditionsYield
With H-ZSM5 In water at 340℃; under 760.051 Torr; for 6h; Reagent/catalyst; Inert atmosphere;
methyl propyl ether
557-17-5

methyl propyl ether

A

Methoxyacetone
5878-19-3

Methoxyacetone

B

Methyl formate
107-31-3

Methyl formate

C

propanoic acid methyl ester
554-12-1

propanoic acid methyl ester

D

methoxyacetaldehyde
10312-83-1

methoxyacetaldehyde

E

propyl methanoate
110-74-7

propyl methanoate

F

3-methoxy-1-propanal
2806-84-0

3-methoxy-1-propanal

G

acetaldehyde
75-07-0

acetaldehyde

Conditions
ConditionsYield
With hydroxyl; oxygen at 19.84℃; under 760.051 Torr; Kinetics; Gas phase;
3-methoxy-1-propanal
2806-84-0

3-methoxy-1-propanal

7-bromo-5-phenyl-1,3-dihydro-2H-benzo[e][1,4]diazepin-2-one
2894-61-3

7-bromo-5-phenyl-1,3-dihydro-2H-benzo[e][1,4]diazepin-2-one

C19H21BrN2O2

C19H21BrN2O2

Conditions
ConditionsYield
Stage #1: 7-bromo-5-phenyl-1,3-dihydro-2H-benzo[e][1,4]diazepin-2-one With sodium cyanoborohydride; acetic acid In methanol at 20℃; for 4h;
Stage #2: 3-methoxy-1-propanal In methanol at 20℃;
100%
3-methoxy-1-propanal
2806-84-0

3-methoxy-1-propanal

(R)-2-methylpropane-2-sulfinamide
196929-78-9

(R)-2-methylpropane-2-sulfinamide

C8H17NO2S

C8H17NO2S

Conditions
ConditionsYield
With copper(II) sulfate In dichloromethane at 20℃; for 48h; Inert atmosphere;92%
3-methoxy-1-propanal
2806-84-0

3-methoxy-1-propanal

(S)-2-methylpropane-2-sulfinamide
343338-28-3

(S)-2-methylpropane-2-sulfinamide

(S,E)-N-(3-methoxypropylidene)-2-methylpropane-2-sulfinamide

(S,E)-N-(3-methoxypropylidene)-2-methylpropane-2-sulfinamide

Conditions
ConditionsYield
With pyridine; magnesium sulfate; toluene-4-sulfonic acid In dichloromethane at 20℃; for 72h;76%
diethoxyphosphoryl-acetic acid ethyl ester
867-13-0

diethoxyphosphoryl-acetic acid ethyl ester

3-methoxy-1-propanal
2806-84-0

3-methoxy-1-propanal

(E)-ethyl 5-methoxypent-2-enoate

(E)-ethyl 5-methoxypent-2-enoate

Conditions
ConditionsYield
Stage #1: diethoxyphosphoryl-acetic acid ethyl ester With sodium hydride In tetrahydrofuran; mineral oil at 0℃; for 0.5h;
Stage #2: 3-methoxy-1-propanal In tetrahydrofuran; mineral oil at 0℃; for 1.5h; Horner-Wadsworth-Emmons Olefination; diastereoselective reaction;
75%
3-methoxy-1-propanal
2806-84-0

3-methoxy-1-propanal

phenylacetylene
536-74-3

phenylacetylene

5-methoxy-1-phenylpent-1-yn-3-ol

5-methoxy-1-phenylpent-1-yn-3-ol

Conditions
ConditionsYield
Stage #1: phenylacetylene With n-butyllithium In tetrahydrofuran; hexane at -78℃; for 0.5h; Inert atmosphere;
Stage #2: 3-methoxy-1-propanal In tetrahydrofuran; hexane at -78 - 20℃; Inert atmosphere;
75%
1,3-dimethyl-7-methylthiolumazine
70673-90-4

1,3-dimethyl-7-methylthiolumazine

3-methoxy-1-propanal
2806-84-0

3-methoxy-1-propanal

6-(β-methoxypropionyl)-1,3-dimethyl-7-methylthiolumazine

6-(β-methoxypropionyl)-1,3-dimethyl-7-methylthiolumazine

Conditions
ConditionsYield
With di-tert-butyl peroxide; iron(II) sulfate In acetic acid for 0.333333h; Ambient temperature;74%
tetrachloromethane
56-23-5

tetrachloromethane

chloroform
67-66-3

chloroform

3-methoxy-1-propanal
2806-84-0

3-methoxy-1-propanal

4-methoxy-1,1,1-trichlorobutan-2-ol
85363-86-6

4-methoxy-1,1,1-trichlorobutan-2-ol

Conditions
ConditionsYield
cathodic reduction;62%
chloroform
67-66-3

chloroform

3-methoxy-1-propanal
2806-84-0

3-methoxy-1-propanal

4-methoxy-1,1,1-trichlorobutan-2-ol
85363-86-6

4-methoxy-1,1,1-trichlorobutan-2-ol

Conditions
ConditionsYield
With tetrachloromethane In N,N-dimethyl-formamide electroreduction;62%
3-methoxy-1-propanal
2806-84-0

3-methoxy-1-propanal

2-amino-3-bromo-5-chlorobenzaldehyde
166527-09-9

2-amino-3-bromo-5-chlorobenzaldehyde

8-bromo-6-chloro-3-(methoxymethyl)quinoline

8-bromo-6-chloro-3-(methoxymethyl)quinoline

Conditions
ConditionsYield
With sodium methylate In methanol for 3h; Reflux;57%
3-methoxy-1-propanal
2806-84-0

3-methoxy-1-propanal

1,1-Dichloro-3-methoxypropane
2806-74-8

1,1-Dichloro-3-methoxypropane

Conditions
ConditionsYield
With pyridine; phosphorus pentachloride In dichloromethane for 10h; Ambient temperature;55%
cyclopent-2-enone
930-30-3

cyclopent-2-enone

3-methoxy-1-propanal
2806-84-0

3-methoxy-1-propanal

2-(1-hydroxy-3-methoxypropyl)cyclopent-2-en-1-one

2-(1-hydroxy-3-methoxypropyl)cyclopent-2-en-1-one

Conditions
ConditionsYield
With tributylphosphine; 1,1'-bi-2-naphthol In tetrahydrofuran at 20℃; Baylis-Hillman reaction;53%
3-methoxy-1-propanal
2806-84-0

3-methoxy-1-propanal

n-propylmagnesium bromide
927-77-5

n-propylmagnesium bromide

1-methoxyhexan-3-ol

1-methoxyhexan-3-ol

Conditions
ConditionsYield
In diethyl ether for 0.5h; Heating;49%
3-methoxy-1-propanal
2806-84-0

3-methoxy-1-propanal

3,5-dichloro-N-(4-fluoro-2-(3-(methylamino)pyrrolidin-1-yl)-5-(2-morpholinopyrimidin-5-yl)phenyl)benzamide

3,5-dichloro-N-(4-fluoro-2-(3-(methylamino)pyrrolidin-1-yl)-5-(2-morpholinopyrimidin-5-yl)phenyl)benzamide

3,5-dichloro-N-[4-fluoro-2-[3-[3-methoxypropyl(methyl)amino]pyrrolidin-1-yl]-5-(2-morpholin-4-ylpyrimidin-5-yl)phenyl]benzamide

3,5-dichloro-N-[4-fluoro-2-[3-[3-methoxypropyl(methyl)amino]pyrrolidin-1-yl]-5-(2-morpholin-4-ylpyrimidin-5-yl)phenyl]benzamide

Conditions
ConditionsYield
Stage #1: 3-methoxy-1-propanal; 3,5-dichloro-N-(4-fluoro-2-(3-(methylamino)pyrrolidin-1-yl)-5-(2-morpholinopyrimidin-5-yl)phenyl)benzamide With acetic acid In cis-1,2-Dichloroethylene at 20℃; for 0.25h;
Stage #2: With sodium tris(acetoxy)borohydride In cis-1,2-Dichloroethylene at 20℃; for 1.5h;
48.2%
3-methoxy-1-propanal
2806-84-0

3-methoxy-1-propanal

4-Bromo-3-methyl-1-butene
31950-55-7

4-Bromo-3-methyl-1-butene

1-methoxy-5-methylhept-6-en-3-ol

1-methoxy-5-methylhept-6-en-3-ol

Conditions
ConditionsYield
Stage #1: 4-Bromo-3-methyl-1-butene With iodine; magnesium; ethylene dibromide In tetrahydrofuran at 20 - 50℃; for 2h;
Stage #2: 3-methoxy-1-propanal In tetrahydrofuran at -15 - 20℃;
46%
2-bromoprop-1-ene
557-93-7

2-bromoprop-1-ene

3-methoxy-1-propanal
2806-84-0

3-methoxy-1-propanal

2-methyl-5-methoxy-1(E)-penten-3-ol
477251-09-5

2-methyl-5-methoxy-1(E)-penten-3-ol

Conditions
ConditionsYield
Stage #1: 2-bromoprop-1-ene With iodine; magnesium In tetrahydrofuran for 1h; Heating;
Stage #2: 3-methoxy-1-propanal In tetrahydrofuran at 0 - 20℃;
40.5%
3-methoxy-1-propanal
2806-84-0

3-methoxy-1-propanal

4-methoxybenzoic acid hydrazide
3290-99-1

4-methoxybenzoic acid hydrazide

methyl iodide
74-88-4

methyl iodide

4-methoxy-N’-3-methoxypropylidene-N-methylbenzohydrazide

4-methoxy-N’-3-methoxypropylidene-N-methylbenzohydrazide

Conditions
ConditionsYield
Stage #1: 3-methoxy-1-propanal; 4-methoxybenzoic acid hydrazide In ethanol
Stage #2: methyl iodide With potassium carbonate In acetonitrile at 60℃; Sealed tube;
40%
3-methoxy-1-propanal
2806-84-0

3-methoxy-1-propanal

acrylic acid methyl ester
292638-85-8

acrylic acid methyl ester

methyl 3-hydroxy-5-methoxy-2-methylenepentanoate
115204-91-6

methyl 3-hydroxy-5-methoxy-2-methylenepentanoate

Conditions
ConditionsYield
With 1,4-diaza-bicyclo[2.2.2]octane Ambient temperature;36%
3-methoxy-1-propanal
2806-84-0

3-methoxy-1-propanal

3-amino-2-(benzyloxy)-6-methylisonicotinaldehyde

3-amino-2-(benzyloxy)-6-methylisonicotinaldehyde

8-(benzyloxy)-3-(methoxymethyl)-6-methyl-1,7-naphthyridine

8-(benzyloxy)-3-(methoxymethyl)-6-methyl-1,7-naphthyridine

Conditions
ConditionsYield
With sodium methylate In methanol for 3.5h; Reflux;30.9%
3-methoxy-1-propanal
2806-84-0

3-methoxy-1-propanal

N-[4-fluoro-2-[3-(methylamino)pyrrolidin1-yl]-5-(2-morpholin-4-ylpyrimidin-5-yl)phenyl]-6-oxo-4-(trifluoromethyl)-1H-pyridine-3-carboxamide

N-[4-fluoro-2-[3-(methylamino)pyrrolidin1-yl]-5-(2-morpholin-4-ylpyrimidin-5-yl)phenyl]-6-oxo-4-(trifluoromethyl)-1H-pyridine-3-carboxamide

N-[4-fluoro-2-[3-[3-methoxypropyl(methyl)amino]pyrrolidin-1-yl]-5-(2-morpholin-4-ylpyrimidin-5-yl)phenyl]-6-oxo-4-(trifluoromethyl)-1H-pyridine-3-carboxamide

N-[4-fluoro-2-[3-[3-methoxypropyl(methyl)amino]pyrrolidin-1-yl]-5-(2-morpholin-4-ylpyrimidin-5-yl)phenyl]-6-oxo-4-(trifluoromethyl)-1H-pyridine-3-carboxamide

Conditions
ConditionsYield
Stage #1: 3-methoxy-1-propanal; N-[4-fluoro-2-[3-(methylamino)pyrrolidin1-yl]-5-(2-morpholin-4-ylpyrimidin-5-yl)phenyl]-6-oxo-4-(trifluoromethyl)-1H-pyridine-3-carboxamide With acetic acid In cis-1,2-Dichloroethylene at 20℃; for 0.25h;
Stage #2: With sodium tris(acetoxy)borohydride In cis-1,2-Dichloroethylene at 20℃; for 0.333333h;
29.9%
3-methoxy-1-propanal
2806-84-0

3-methoxy-1-propanal

methyl 4-[2-[4-[[2-[[3-[(2,2-dimethylpiperazin-1-yl)methyl]benzoyl]amino]-4,5,6,7-tetrahydrobenzothiophene-3-carbonyl]amino]-2,6-difluorophenyl]ethyl]benzoate dihydrochloride

methyl 4-[2-[4-[[2-[[3-[(2,2-dimethylpiperazin-1-yl)methyl]benzoyl]amino]-4,5,6,7-tetrahydrobenzothiophene-3-carbonyl]amino]-2,6-difluorophenyl]ethyl]benzoate dihydrochloride

methyl 4-[2-[2,6-difluoro-4-[[2-[[3-[[4-(3-methoxypropyl)-2,2-dimethylpiperazin-1-yl]methyl]benzoyl]amino]-4,5,6,7-tetrahydrobenzothiophene-3-carbonyl]amino]phenyl]ethyl]benzoate

methyl 4-[2-[2,6-difluoro-4-[[2-[[3-[[4-(3-methoxypropyl)-2,2-dimethylpiperazin-1-yl]methyl]benzoyl]amino]-4,5,6,7-tetrahydrobenzothiophene-3-carbonyl]amino]phenyl]ethyl]benzoate

Conditions
ConditionsYield
With sodium tris(acetoxy)borohydride; acetic acid; N-ethyl-N,N-diisopropylamine In dichloromethane at 20℃; for 12h;27.6%
3-methoxy-1-propanal
2806-84-0

3-methoxy-1-propanal

erythromycylamine
26116-56-3

erythromycylamine

9-N-(3-methoxy-1-propyl)erythromycylamine
112452-16-1

9-N-(3-methoxy-1-propyl)erythromycylamine

Conditions
ConditionsYield
With sodium phosphate buffer; sodium cyanoborohydride In acetonitrile for 1h; Ambient temperature;22%
3-methoxy-1-propanal
2806-84-0

3-methoxy-1-propanal

(carbobenzyloxymethylene)triphenylphosphorane
15097-38-8

(carbobenzyloxymethylene)triphenylphosphorane

(E)-benzyl-5-methoxypent-2-enoate

(E)-benzyl-5-methoxypent-2-enoate

Conditions
ConditionsYield
In dichloromethane for 3h; Reflux;19.04%
3-methoxy-1-propanal
2806-84-0

3-methoxy-1-propanal

N-(4-fluorophenyl)-2-(7-methoxy-1-methyl-1H-pyrrolo[2,3-c]pyridin-3-yl)-4-((methylsulfonyl)methyl)aniline

N-(4-fluorophenyl)-2-(7-methoxy-1-methyl-1H-pyrrolo[2,3-c]pyridin-3-yl)-4-((methylsulfonyl)methyl)aniline

5-(4-fluorophenyl)-4-(2-methoxyethyl)-11-methyl-8-((methylsulfonyl)methyl)-2,4,5,11-tetrahydro-1H-2,5,11-triazadibenzo[cd,h]azulen-1-one

5-(4-fluorophenyl)-4-(2-methoxyethyl)-11-methyl-8-((methylsulfonyl)methyl)-2,4,5,11-tetrahydro-1H-2,5,11-triazadibenzo[cd,h]azulen-1-one

Conditions
ConditionsYield
With hydrogenchloride; water In 1,4-dioxane; methanol at 90℃; for 2h;12%
3-methoxy-1-propanal
2806-84-0

3-methoxy-1-propanal

N-(6-(4-isopropyl-4H-1,2,4-triazol-3-yl)pyridin-2-yl)-1,2,3,4-tetrahydroisoquinoline-7-carboxamide

N-(6-(4-isopropyl-4H-1,2,4-triazol-3-yl)pyridin-2-yl)-1,2,3,4-tetrahydroisoquinoline-7-carboxamide

N-(6-(4-isopropyl-4H-1,2,4-triazol-3-yl)pyridin-2-yl)-2-(3-methoxypropyl)-1,2,3,4-tetrahydroisoquinoline-7-carboxamide

N-(6-(4-isopropyl-4H-1,2,4-triazol-3-yl)pyridin-2-yl)-2-(3-methoxypropyl)-1,2,3,4-tetrahydroisoquinoline-7-carboxamide

Conditions
ConditionsYield
With sodium tris(acetoxy)borohydride In 1,2-dichloro-ethane12%
3-methoxy-1-propanal
2806-84-0

3-methoxy-1-propanal

(S)-N-(2-amino-5-(3,5-dimethylisoxazol-4-yl)phenyl)-1-(3,4-difluorophenyl)-5-oxopyrrolidine-2-carboxamide

(S)-N-(2-amino-5-(3,5-dimethylisoxazol-4-yl)phenyl)-1-(3,4-difluorophenyl)-5-oxopyrrolidine-2-carboxamide

(S)-1-(3,4-difluorophenyl)-5-(5-(3,5-dimethylisoxazol-4-yl)-1-(3-methoxypropyl)-1H-benzo[d]imidazol-2-yl)pyrrolidin-2-one

(S)-1-(3,4-difluorophenyl)-5-(5-(3,5-dimethylisoxazol-4-yl)-1-(3-methoxypropyl)-1H-benzo[d]imidazol-2-yl)pyrrolidin-2-one

Conditions
ConditionsYield
Stage #1: 3-methoxy-1-propanal; (S)-N-(2-amino-5-(3,5-dimethylisoxazol-4-yl)phenyl)-1-(3,4-difluorophenyl)-5-oxopyrrolidine-2-carboxamide In tetrahydrofuran at 20℃; for 1h;
Stage #2: With sodium tris(acetoxy)borohydride In tetrahydrofuran at 20℃; for 4h;
Stage #3: With acetic acid at 80℃; for 18h;
7%
3-methoxy-1-propanal
2806-84-0

3-methoxy-1-propanal

Diethyl maleate
141-05-9

Diethyl maleate

(3-methoxy-propionyl)-succinic acid diethyl ester

(3-methoxy-propionyl)-succinic acid diethyl ester

Conditions
ConditionsYield
Im UV-Licht.;

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