1-Phenyloxindole CAS: 3335-98-6 Linopirdine intermediate Company Profile: Synchem is dedicated to custom synthesis and manufacturing services for small molecules. We serve the needs of customers in the pharmaceutical, agrochemical, and elect
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inquiryGood quality of 1-Phenyloxindole at competitive price from Henan Tianfu Chemical: Henan Tianfu Chemical Co.,LTD was built in 2009 with an ISO certificate in the past 5 years, we have grown up as a famous fine chemicals supplier in china and we ha
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inquiry1-Phenyloxindole Category: Pharmaceutical intermediates CAS NO.: 3335-98-6 Molecular formula: C14H11NO
With our good experience, we offer detailed technical support and advice to assist customers. We communicate closely with customers to establish their quality requirements. Consistent Quality Our plant has strict quality control in each manufacturin
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inquiry1-Phenyloxindole CAS:3335-98-6 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic intermedi
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
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inquiryEstablished in May 2015, TaiChem Ltd. is initially invested by a British research and development company and started by PhDs back from aboard. The company is registered in China Medical City (CMC), Taizhou, Jiangsu Province, and the production site
Product name: 1-Phenyloxindole CAS No.: 3335-98-6 Molecule Formula:C14H11NO Molecule Weight:209.24 Purity: 99.0% Package: 25kg/drum Description:White powder Manufacture Standards:Enterprise Standard TESTING ITEMS
Cas:3335-98-6
Min.Order:1 Kilogram
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inquiry1-Phenyloxindole Basic information Product Name: 1-Phenyloxindole Synonyms: 1,3-Dihydro-1-phenyl-2H-indol-2-one 98%;1-Phenyl-2-indolinone;2-Oxo-1-phenylindoline;1-phenyl-3H-indol-2-one;1-phenyl-2(1H,3H)-indolone;N-phenyl-indole ketone;1-phenox
factory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B
Cas:3335-98-6
Min.Order:1 Kilogram
FOB Price: $18.0 / 20.0
Type:Trading Company
inquiryShandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W
1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer
Cas:3335-98-6
Min.Order:1 Metric Ton
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Type:Trading Company
inquiryAppearance:95%+ Package:R&D,Pilot run Transportation:per client require Port:Express ,Air, Sea
High quality,stable supply chain.Appearance:white/off-white or light yellow Storage:Store in cool and dry place, keep away from strong light and heat. Package:aluminum bottle,glass bottle,PTFE bottle,cardboard drum Application:This product can be use
We are a Union of chemistry in China, consists of chemists,engineers, laboratories,factories in China. We organize surplus capacity of R&D and production as well as custom synthesis for chemical products and chemical business project. We are supp
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inquiryStock products, own laboratoryAppearance:off-white crystal powder Package:Grams, Kilograms Application:For R&D Transportation:According to customer request Port:Shanghai
Cas:3335-98-6
Min.Order:0
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inquiryhigh purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou
1-phenyl-1,3-dihydro-indol-2-one
Conditions | Yield |
---|---|
With trifluoroacetic anhydride Product distribution; Further Variations:; Reagents; | 100% |
Multi-step reaction with 4 steps 1: 98 percent / dimethylformamide / 4 h / 24 °C 2: 98 percent / Et3N; DMAP / CH2Cl2 / 3.5 h / 20 - 40 °C 3: 95 percent / hydrogen / Pd/C / methanol / 3 h / 30 °C 4: polyphosphoric acid / toluene / 11 h / 110 °C View Scheme |
2-diazo-N,N-diphenyl-acetamide
1-phenyl-1,3-dihydro-indol-2-one
Conditions | Yield |
---|---|
With [(S)-(2-phenyl-4-pheox)Ru(CH3CN)4]PF6 In dichloromethane at 20℃; for 0.0166667h; Inert atmosphere; regioselective reaction; | 99% |
Conditions | Yield |
---|---|
With palladium diacetate; triethylamine; johnphos In toluene at 80℃; for 3h; | 95% |
With aluminium trichloride at 180 - 190℃; for 0.166667h; | 81.5% |
With aluminium trichloride at 180 - 190℃; for 1h; | 75% |
Conditions | Yield |
---|---|
With hydrazine hydrate for 0.25h; Heating; | 92% |
Stage #1: 1-phenyl-indole-2,3-dione With potassium hydroxide; hydrazine In water; ethylene glycol at 160℃; for 1.5h; Stage #2: With hydrogenchloride In water; ethylene glycol | 90% |
With hydrazine hydrate In ethanol for 6h; Wolff-Kishner reduction; Heating; | 58% |
3-(methylthio)-1-phenylindolin-2-one
1-phenyl-1,3-dihydro-indol-2-one
Conditions | Yield |
---|---|
With nickel In ethanol for 2h; Heating; | 85% |
1-phenyl-1,3-dihydro-indol-2-one
Conditions | Yield |
---|---|
With sulfuric acid; tetrabutylammomium bromide In 5,5-dimethyl-1,3-cyclohexadiene at 100℃; for 16h; Solvent; Reagent/catalyst; | 84% |
Conditions | Yield |
---|---|
With copper(l) iodide; potassium carbonate; N,N`-dimethylethylenediamine In 1,4-dioxane for 24h; Reflux; | 83% |
With copper(l) iodide; potassium carbonate; N,N`-dimethylethylenediamine In acetonitrile Reflux; Inert atmosphere; | 82% |
With potassium phosphate; copper(l) iodide In dimethyl sulfoxide at 130℃; for 24h; Ullmann Condensation; Inert atmosphere; Glovebox; | 41 %Chromat. |
With potassium phosphate; copper(l) iodide; 3-azapentane-1,5-diamine In dimethyl sulfoxide at 50℃; for 24h; Reagent/catalyst; Inert atmosphere; Glovebox; Sealed tube; | 27 %Chromat. |
2-(2-bromophenyl)-N-phenylacetamide
1-phenyl-1,3-dihydro-indol-2-one
Conditions | Yield |
---|---|
With caesium carbonate; XPhos; palladium diacetate In toluene at 100℃; for 0.5h; microwave irradiation; | 82% |
2-(2-chlorophenyl)-N-phenylacetamide
1-phenyl-1,3-dihydro-indol-2-one
Conditions | Yield |
---|---|
With caesium carbonate; XPhos; palladium diacetate In toluene at 100℃; for 0.5h; microwave irradiation; | 80% |
methyl (2-nitrophenyl)acetate
phenylboronic acid
1-phenyl-1,3-dihydro-indol-2-one
Conditions | Yield |
---|---|
With 1,2,2,3,4,4-hexamethylphosphetane 1-oxide; diphenylsilane In m-xylene at 120℃; for 4h; Catalytic behavior; Reagent/catalyst; Solvent; Inert atmosphere; Schlenk technique; Sealed tube; | 80% |
Conditions | Yield |
---|---|
With montmorillonite KSF at 20℃; for 1.08333h; Stolle synthesis; Sonication; Neat (no solvent); | 76% |
2-bromo-N,N-diphenylacetamide
A
1-phenyl-1,3-dihydro-indol-2-one
B
N,N-diphenylacetamide
Conditions | Yield |
---|---|
With tri-n-butyl-tin hydride; 2,2'-azobis(isobutyronitrile) In toluene for 14h; Heating; | A 8% B 75% |
2-chloro-N,N-diphenylacetamide
A
1-phenyl-1,3-dihydro-indol-2-one
B
N,N-diphenylacetamide
Conditions | Yield |
---|---|
With tri-n-butyl-tin hydride; 2,2'-azobis(isobutyronitrile) In toluene for 14h; Heating; | A 11% B 74% |
2-[(methoxycarbonyl)phenylamino]benzeneacetic acid
A
1-phenyl-1,3-dihydro-indol-2-one
B
10,11-dihydro-10-oxo-5H-dibenz[b,f]azepine-5-carboxylic acid methyl ester
Conditions | Yield |
---|---|
With PPA at 95℃; for 3h; | A n/a B 70% |
1-phenyl-1,3-dihydro-indol-2-one
Conditions | Yield |
---|---|
at 120℃; for 60h; | 68% |
1-phenyl-1H-indole
1-phenyl-1,3-dihydro-indol-2-one
Conditions | Yield |
---|---|
With water; iodine In N,N-dimethyl-formamide for 12h; Reflux; | 62% |
With 1-fluoro-1,2-phenyliodohydrin-3-(1H)-one In 1,4-dioxane; water at 140℃; for 5h; | 61% |
With 1-fluoro-1,2-phenyliodohydrin-3-(1H)-one In 1,4-dioxane; water at 140℃; for 5h; | 61% |
2-oxoindole
2-(trimethylsilyl)phenyl trifluoromethanesulfonate
A
1-phenyl-1,3-dihydro-indol-2-one
B
N-phenyl-1,3-dihydro-3,3-diphenyl-2H-indol-2-one
Conditions | Yield |
---|---|
With cesium fluoride In acetonitrile at 20℃; for 6h; | A 45% B 26% |
With cesium fluoride In acetonitrile at 75℃; for 6h; Reagent/catalyst; | A 22% B 39% |
Conditions | Yield |
---|---|
With potassium carbonate; N,N`-dimethylethylenediamine; copper(l) iodide In acetonitrile Heating; | 43% |
{2-[Phenyl-(2,2,2-trifluoro-acetyl)-amino]-phenyl}-acetic acid
A
1-phenyl-1,3-dihydro-indol-2-one
B
5-trifluoroacetyl-5,11-dihydro-dibenzo[b,f]azepin-10-one
Conditions | Yield |
---|---|
With PPA In toluene at 110℃; for 11h; | A n/a B 40% |
Conditions | Yield |
---|---|
Multistep reaction.; | 39% |
In acetonitrile Cyclization; Dehydrobromination; Irradiation; | 26% |
Multistep reaction; | 24 mg |
Multi-step reaction with 2 steps 1: N,N'-ditosylhydrazine; 1,8-diazabicyclo[5.4.0]undec-7-ene / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere 2: [(S)-(2-phenyl-4-pheox)Ru(CH3CN)4]PF6 / dichloromethane / 0.02 h / 20 °C / Inert atmosphere View Scheme |
2-oxoindole
2-(trimethylsilyl)phenyl trifluoromethanesulfonate
A
1-phenyl-1,3-dihydro-indol-2-one
C
N-phenyl-1,3-dihydro-3,3-diphenyl-2H-indol-2-one
Conditions | Yield |
---|---|
With cesium fluoride In acetonitrile at 20℃; for 6h; | A 15% B 8% C 32% |
3-hydroxy-1-phenyl-1,4,5,6-tetrahydro-indol-2-one
1-phenyl-1,3-dihydro-indol-2-one
Conditions | Yield |
---|---|
With pyridine hydrochloride at 230℃; for 1h; | 12.4% |
With pyridine hydrochloride at 230℃; for 1h; Product distribution; other time, temperature; | 12.4% |
Conditions | Yield |
---|---|
With aluminium trichloride |
1-phenyl-1,3-dihydro-indol-2-one
Conditions | Yield |
---|---|
With calcium hypochlorite; water |
2-[2-(phenylamino)phenyl]acetic acid
1-phenyl-1,3-dihydro-indol-2-one
Conditions | Yield |
---|---|
With PPA In toluene at 110℃; for 11h; Product distribution; Further Variations:; Reagents; Solvents; Temperatures; |
[2-(acetyl-phenyl-amino)-phenyl]-acetic acid
A
1-phenyl-1,3-dihydro-indol-2-one
Conditions | Yield |
---|---|
With PPA at 95℃; for 3h; Product distribution; | A n/a B 35 % Chromat. |
[2-(benzyl-phenyl-amino)-phenyl]-acetic acid
1-phenyl-1,3-dihydro-indol-2-one
Conditions | Yield |
---|---|
With PPA In chlorobenzene at 90℃; for 2h; Product distribution; |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 42 percent / NEt3 / CH2Cl2 / 16 h / 20 °C View Scheme | |
Multi-step reaction with 3 steps 1: 98 percent / 2 h / 20 °C 2: 83 percent / AlCl3 / CS2 / 2 h / 20 °C 3: 58 percent / hydrazine hydrate / ethanol / 6 h / Heating View Scheme | |
Multi-step reaction with 2 steps 1: 97 percent / dimethylformamide / 2 h / 80 °C 2: 75 percent / AlCl3 / 1 h / 180 - 190 °C View Scheme |
(N,N-diphenylcarbamoyl) formyl chloride
1-phenyl-1,3-dihydro-indol-2-one
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 83 percent / AlCl3 / CS2 / 2 h / 20 °C 2: 58 percent / hydrazine hydrate / ethanol / 6 h / Heating View Scheme |
1-phenyl-1,3-dihydro-indol-2-one
Conditions | Yield |
---|---|
With sodium hydroxide at 100℃; for 6h; | 97% |
Conditions | Yield |
---|---|
With potassium fluoride; 2-[2-(dicyclohexylphosphino)-phenyl]-1-methyl-1H-indole; palladium diacetate In tert-butyl alcohol at 20 - 120℃; for 18.0833h; Inert atmosphere; Schlenk technique; | 97% |
Conditions | Yield |
---|---|
With oxygen; sodium hydroxide In N,N-dimethyl-formamide at 0℃; for 6h; Green chemistry; | 97% |
1-phenyl-1,3-dihydro-indol-2-one
trifluoromethylsulfonic anhydride
1-phenyl-1H-indol-2-yl trifluoromethanesulfonate
Conditions | Yield |
---|---|
With 2,4,6-tri-tertbutylpyridine In 1,2-dichloro-ethane at 0 - 20℃; Inert atmosphere; | 96% |
Conditions | Yield |
---|---|
With triphenylphosphine In 5,5-dimethyl-1,3-cyclohexadiene at 50℃; for 24h; Inert atmosphere; | 96% |
1-phenyl-1,3-dihydro-indol-2-one
Conditions | Yield |
---|---|
Stage #1: 1-phenyl-1,3-dihydro-indol-2-one With lithium diisopropyl amide In hexane; dichloromethane at -78℃; for 1h; Inert atmosphere; Stage #2: (SS)-2-methyl-N-(2,2,2-trifluoroethylidene)-propane-2-sulfinamide In hexane; dichloromethane at -78℃; for 5h; Inert atmosphere; Stage #3: With ammonium chloride In hexane; dichloromethane; water at -78℃; Inert atmosphere; diastereoselective reaction; | A n/a B 95% |
1-phenyl-1,3-dihydro-indol-2-one
chlorobenzene
1,3-dihydro-1,3-diphenyl-2H-indol-2-one
Conditions | Yield |
---|---|
With copper(II) ferrite; potassium carbonate In 1,4-dioxane at 70℃; for 1.33333h; Reagent/catalyst; | 95% |
1-phenyl-1,3-dihydro-indol-2-one
chlorobenzene
A
1,3-dihydro-1,3-diphenyl-2H-indol-2-one
B
N-phenyl-1,3-dihydro-3,3-diphenyl-2H-indol-2-one
Conditions | Yield |
---|---|
With cobalt ferrite; potassium carbonate In 1,4-dioxane at 70℃; for 4h; | A 95% B 8% |
1-phenyl-1,3-dihydro-indol-2-one
malononitrile
2-(2-oxo-1-phenylindolin-3-ylidene)malononitrile
Conditions | Yield |
---|---|
With iron(III) chloride hexahydrate; oxygen In N,N-dimethyl-formamide at 50℃; for 2h; Green chemistry; | 95% |
Conditions | Yield |
---|---|
In 1,3,5-trimethyl-benzene at 170℃; for 24h; Inert atmosphere; | 94% |
1-phenyl-1,3-dihydro-indol-2-one
5-chloroindole 2,3-dione
Conditions | Yield |
---|---|
With zirconium(IV) chloride In ethanol for 10h; Reflux; | 94% |
Conditions | Yield |
---|---|
With potassium tert-butylate In ethanol at 80℃; for 0.0833333h; | 93% |
In ethanol |
Conditions | Yield |
---|---|
With nickel(II) ferrite; potassium carbonate In 1,4-dioxane at 70℃; for 1.66667h; Reagent/catalyst; | 93% |
1-phenyl-1,3-dihydro-indol-2-one
Conditions | Yield |
---|---|
With iodine In methanol at 20℃; for 0.416667h; | 92% |
1-phenyl-1,3-dihydro-indol-2-one
benzyl alcohol
3-benzyl-1,3-dihydro-1-phenyl-2H-indol-2-one
Conditions | Yield |
---|---|
In 1,3,5-trimethyl-benzene at 170℃; for 24h; Inert atmosphere; | 92% |
With (1,4-dimethyl-5,7-diphenyl-1,2,3,4-tetrahydro-6H-cyclopenta[b]pyrazin-6-one) irontricarbonyl complex3; potassium carbonate; triphenylphosphine In 5,5-dimethyl-1,3-cyclohexadiene at 150℃; for 24h; | 75% |
Conditions | Yield |
---|---|
With iron(III) chloride; potassium carbonate In dimethyl sulfoxide at 50℃; for 1h; Green chemistry; | 92% |
Conditions | Yield |
---|---|
With zirconium(IV) chloride In ethanol Reflux; | 91% |
With zirconium(IV) chloride In ethanol for 9h; Reflux; | 91% |
With hydrogenchloride; acetic acid |
Conditions | Yield |
---|---|
With copper(II) ferrite; potassium carbonate In 1,4-dioxane at 70℃; for 2h; Reagent/catalyst; | 91% |
Conditions | Yield |
---|---|
With nickel(II) ferrite; potassium carbonate In 1,4-dioxane at 70℃; for 1.66667h; Reagent/catalyst; | 91% |
1-phenyl-1,3-dihydro-indol-2-one
1-isopropyl-1H-indole-2,3-dione
Conditions | Yield |
---|---|
With zirconium(IV) chloride In ethanol Reflux; | 91% |
1-phenyl-1,3-dihydro-indol-2-one
anthranilic acid amide
1-phenyl-1'H-spiro[indoline-3,2'-quinazoline]-2,4'(3'H)-dione
Conditions | Yield |
---|---|
With iron(III) chloride; toluene-4-sulfonic acid In N,N-dimethyl-formamide at 80℃; for 3.5h; | 91% |
Conditions | Yield |
---|---|
With iron(III) chloride; toluene-4-sulfonic acid In N,N-dimethyl-formamide at 80℃; for 1h; | 91% |
1-phenyl-1,3-dihydro-indol-2-one
2-[2-(phenylamino)phenyl]acetic acid
Conditions | Yield |
---|---|
With sodium hydroxide In ethanol for 4h; Heating; | 90% |
With sodium hydroxide In ethanol for 4h; Heating; | 88% |
With sodium hydroxide In ethanol; water for 4h; Heating; Yield given; | |
Multi-step reaction with 2 steps 1: 97 percent / aq. NaOH / 6 h / 100 °C 2: acid / pH 2 View Scheme |
1-phenyl-1,3-dihydro-indol-2-one
4-picolylchloride hydrochloride
linopirdine
Conditions | Yield |
---|---|
With potassium fluoride on basic alumina for 0.05h; microwave irradiation; | 90% |
Conditions | Yield |
---|---|
With oxygen; sodium iodide In tetrahydrofuran at 60℃; for 12h; Schlenk technique; chemoselective reaction; | 90% |
With tert.-butylhydroperoxide In 1,2-dichloro-ethane at 85℃; for 24h; Schlenk technique; | 84% |
With tert.-butylnitrite; oxygen In tetrahydrofuran at 50℃; under 760.051 Torr; for 24h; Schlenk technique; Inert atmosphere; | 80% |
With tert.-butylnitrite In tetrahydrofuran at 25℃; under 1520.1 Torr; | 66% |
Conditions | Yield |
---|---|
With zirconium(IV) chloride In ethanol for 10h; Reflux; | 90% |
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