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Name:FMOC-Ala-OH CAS NO: 35661-39-3 Grade:Medical scientific research and export Molecular formula:C18H17NO4 Molecular weight:311.33 Product Quality 12 years of chemical raw materials Mature operation of the industry System stability Data
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inquiryProduct Name Fmoc-Ala-OH CAS No. 35661-39-3 Synonyms N-[(9H-fluoren-9-ylmethoxy)carbonyl]-L-alanine Purity 98.0% min Molecular Formula C18H17NO4 Molecular Weight 311.33 Ap
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inquiryN-[(9H-fluoren-9-ylmethoxy)carbonyl]-L-alanine
Conditions | Yield |
---|---|
With potassium phosphate; tris(2,2-bipyridine)ruthenium(II) hexafluorophosphate; ascorbic acid In water; acetonitrile at 20℃; for 1h; Irradiation; | 100% |
L-alanin
N-(9H-fluoren-2-ylmethoxycarbonyloxy)succinimide
N-[(9H-fluoren-9-ylmethoxy)carbonyl]-L-alanine
Conditions | Yield |
---|---|
With sodium carbonate In 1,4-dioxane; water at 20℃; for 18h; | 99% |
With sodium carbonate In N,N-dimethyl-formamide for 0.166667h; Ambient temperature; | 96% |
With sodium carbonate In 1,4-dioxane; water at 20℃; for 18h; |
L-alanin
(fluorenylmethoxy)carbonyl chloride
N-[(9H-fluoren-9-ylmethoxy)carbonyl]-L-alanine
Conditions | Yield |
---|---|
In water at 110℃; for 0.0833333h; Microwave irradiation; Green chemistry; chemoselective reaction; | 96% |
In ethanol; water at 60℃; for 4h; chemoselective reaction; | 86% |
L-alanin
N-[(9H-fluoren-9-ylmethoxy)carbonyl]-L-alanine
Conditions | Yield |
---|---|
With potassium carbonate In acetone at 20℃; for 24h; | 95% |
L-alanin
N-(((9H-fluoren-9-yl)methoxy)carbonyloxy)-2-oxo-2-(piperidin-1-yl)acetimidoyl cyanide
N-[(9H-fluoren-9-ylmethoxy)carbonyl]-L-alanine
Conditions | Yield |
---|---|
With sodium hydrogencarbonate In water; acetone | 93.2% |
L-alanin
(9-fluorenyl)methyl pentafluorophenyl carbonate
N-[(9H-fluoren-9-ylmethoxy)carbonyl]-L-alanine
Conditions | Yield |
---|---|
With sodium hydrogencarbonate In water; acetone Ambient temperature; | 93% |
L-alanin
N-(((9H-fluoren-9-yl)methoxy)carbonyloxy)-2-(ethylamino)-2-oxoacetimidoyl cyanide
N-[(9H-fluoren-9-ylmethoxy)carbonyl]-L-alanine
Conditions | Yield |
---|---|
With sodium hydrogencarbonate In water; acetone | 92.6% |
L-alanin
Carbonic acid 3,5-dioxo-4-aza-tricyclo[5.2.1.02,6]dec-8-en-4-yl ester 9H-fluoren-9-ylmethyl ester
N-[(9H-fluoren-9-ylmethoxy)carbonyl]-L-alanine
Conditions | Yield |
---|---|
With tertiary amine In 1,4-dioxane; water for 3h; | 91% |
L-alanin
N-[(9H-fluoren-9-ylmethoxy)carbonyl]-L-alanine
Conditions | Yield |
---|---|
With potassium carbonate In acetonitrile at 20℃; for 2h; | 91% |
L-alanin
(fluorenylmethoxy)carbonyl chloride
N-[(9H-fluoren-9-ylmethoxy)carbonyl]-L-alanine
Conditions | Yield |
---|---|
In 1,4-dioxane; sodium carbonate | 90.2% |
L-alanin
9-fluorenylmethyl N-succinimidyl carbonate
N-[(9H-fluoren-9-ylmethoxy)carbonyl]-L-alanine
Conditions | Yield |
---|---|
With triethylamine In water; acetonitrile for 1h; | 90% |
N-[(9H-fluoren-9-ylmethoxy)carbonyl]-L-alanine
Conditions | Yield |
---|---|
With potassium fluoride In tetrahydrofuran; methanol at 22℃; for 2h; | 86% |
N-[(9H-fluoren-9-ylmethoxy)carbonyl]-L-alanine
Conditions | Yield |
---|---|
With magnesium bromide ethyl etherate In dichloromethane at -20 - 22℃; for 3.5h; | 84% |
Nα-fluoren-9-ylmethoxycarbonyl-L-cysteine
N-[(9H-fluoren-9-ylmethoxy)carbonyl]-L-alanine
Conditions | Yield |
---|---|
With [4,4’-bis(1,1-dimethylethyl)-2,2’-bipyridine-N1,N1‘]bis [3,5-difluoro-2-[5-(trifluoromethyl)-2-pyridinyl-N]phenyl-C]iridium(III) hexafluorophosphate; triethyl phosphite In aq. phosphate buffer; acetonitrile at 20℃; for 0.5h; pH=6.5; Irradiation; | 84% |
methyl 2-(((9H-fluoren-9-yl)methoxy)carbonyl)aminopropanoate
N-[(9H-fluoren-9-ylmethoxy)carbonyl]-L-alanine
Conditions | Yield |
---|---|
With trimethyltin hydroxide In 1,2-dichloro-ethane at 80℃; for 5h; | 75% |
(2S)-N-<(fluoren-9-yl)methoxycarbonyl>alanine prop-2-enyl ester
N-[(9H-fluoren-9-ylmethoxy)carbonyl]-L-alanine
Conditions | Yield |
---|---|
With water; chlortris(triphenylphosphine)rhodium In ethanol for 1h; | 67% |
N-[(9H-fluoren-9-ylmethoxy)carbonyl]-L-alanine
Conditions | Yield |
---|---|
With trifluoroacetic acid In dichloromethane at 0℃; for 1.5h; | 61% |
A
L-alanin
B
N-[(9H-fluoren-9-ylmethoxy)carbonyl]-L-alanine
Conditions | Yield |
---|---|
With bis(tri-n-butyltin)oxide In chloroform at 61℃; for 60h; | A 40% B 18% |
N-[(9H-fluoren-9-ylmethoxy)carbonyl]-L-alanine
Conditions | Yield |
---|---|
With methanol In dichloromethane for 0.5h; Ambient temperature; Yield given; |
N-(9-fluorenylmethyloxycarbonyl)alanine 3,4,5-tris(octadecyloxy)benzyl ester
A
N-[(9H-fluoren-9-ylmethoxy)carbonyl]-L-alanine
B
5-(bromomethyl)-1,2,3-tris(octadecyloxy)benzene
Conditions | Yield |
---|---|
With hydrogen bromide In acetic acid |
N-(9-fluorenylmethyloxycarbonyl)alanine 3,4,5-tris(octadecyloxy)benzyl ester
A
N-[(9H-fluoren-9-ylmethoxy)carbonyl]-L-alanine
B
(3,4,5-trioctadecyloxyphenyl)methan-1-ol
Conditions | Yield |
---|---|
With hydrogenchloride In ethyl acetate at 20℃; |
N-[(9H-fluoren-9-ylmethoxy)carbonyl]-L-alanine
Conditions | Yield |
---|---|
With magnesium; acetic acid In methanol; N,N-dimethyl-formamide at 20℃; for 75h; |
N-[(9H-fluoren-9-ylmethoxy)carbonyl]-L-alanine
Conditions | Yield |
---|---|
With chymotrypsin In phosphate buffer for 16h; pH=8; |
N-[(9H-fluoren-9-ylmethoxy)carbonyl]-L-alanine
Conditions | Yield |
---|---|
With chymotrypsin In phosphate buffer for 16h; pH=8; |
Fmoc-Ala-MFE
A
N-[(9H-fluoren-9-ylmethoxy)carbonyl]-L-alanine
B
3-O-methylfluorescein
Conditions | Yield |
---|---|
With ethylenediaminetetraacetic acid; DL-dithiothreitol; cathepsin B In phosphate buffer at 37℃; pH=6.7; Enzyme kinetics; |
N-[(9H-fluoren-9-ylmethoxy)carbonyl]-L-alanine
N-(9-fluorenylmethoxycarbonyl)-L-alanyl fluoride
Conditions | Yield |
---|---|
With pyridine; trifluoro-[1,3,5]triazine In dichloromethane at 20℃; for 15h; | 100% |
With trifluoro-[1,3,5]triazine; triethylamine In dichloromethane at -40℃; for 2h; | 93% |
With pyridine; trifluoro-[1,3,5]triazine In dichloromethane for 4h; Ambient temperature; or in MeCN; | 85% |
N-[(9H-fluoren-9-ylmethoxy)carbonyl]-L-alanine
9H-fluoren-9-ylmethyl [(1S)-2-chloro-1-methyl-oxoethyl]carbamate
Conditions | Yield |
---|---|
With thionyl chloride In dichloromethane at 60℃; for 0.5h; Inert atmosphere; | 100% |
With thionyl chloride In dichloromethane for 0.5h; Reflux; | 98% |
With thionyl chloride In dichloromethane at 20℃; for 0.366667h; Sonication; | 96% |
N-[(9H-fluoren-9-ylmethoxy)carbonyl]-L-alanine
(S)-2-(N-fluorenylmethoxycarbonylamino)propanol
Conditions | Yield |
---|---|
Stage #1: N-[(9H-fluoren-9-ylmethoxy)carbonyl]-L-alanine With 4-methyl-morpholine In 1,2-dimethoxyethane at -15℃; for 1h; Stage #2: With sodium tetrahydroborate In 1,2-dimethoxyethane; water at -15℃; Further stages.; | 100% |
Stage #1: N-[(9H-fluoren-9-ylmethoxy)carbonyl]-L-alanine With isobutyl chloroformate In 1,2-dimethoxyethane at -15℃; for 0.0166667h; Acylation; Stage #2: With sodium tetrahydroborate In 1,2-dimethoxyethane at -15℃; for 0.00833333h; Reduction; | 91% |
Stage #1: N-[(9H-fluoren-9-ylmethoxy)carbonyl]-L-alanine With 2,4,6-tripropyl-1,3,5,2,4,6-trioxatriphosphinane-2,4,6-trioxide; N-ethyl-N,N-diisopropylamine In ethyl acetate at 0℃; for 0.166667h; Stage #2: With sodium tetrahydroborate In water; ethyl acetate at 0℃; for 0.416667h; | 88% |
N-[(9H-fluoren-9-ylmethoxy)carbonyl]-L-alanine
salvinorin B
Conditions | Yield |
---|---|
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 20℃; for 22h; | 100% |
With 4-methyl-morpholine; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate In dichloromethane at 50℃; for 24h; |
N-[(9H-fluoren-9-ylmethoxy)carbonyl]-L-alanine
Conditions | Yield |
---|---|
Stage #1: Fmoc-Ile-Wang resin With piperidine In N,N-dimethyl-formamide at 20℃; for 0.25h; Stage #2: N-[(9H-fluoren-9-ylmethoxy)carbonyl]-L-alanine With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine In dichloromethane; N,N-dimethyl-formamide at 20℃; for 3h; Stage #3: With piperidine In N,N-dimethyl-formamide at 20℃; for 0.25h; | 100% |
N-[(9H-fluoren-9-ylmethoxy)carbonyl]-L-alanine
N-Fmoc-D-Glu α-amide γ-tert-butyl ester
2-N-acetyl-1-β-O-allyl 4,6-O-isopropylidenemuramic acid
2-N-acetyl-1-β-O-allyl-muramoyl-L-alanyl-D-isoglutamine tert-butyl ester
Conditions | Yield |
---|---|
Multistep reaction.; | 100% |
(3,4-dimethoxy-phenethylamino)acetic acid allyl ester
N-[(9H-fluoren-9-ylmethoxy)carbonyl]-L-alanine
N-[(9H-fluorenyl-9-ylmethoxy)carbonyl]-L-alanyl-N-(3,4-dimethoxyphenethyl)glycine allyl ester
Conditions | Yield |
---|---|
Stage #1: N-[(9H-fluoren-9-ylmethoxy)carbonyl]-L-alanine With 4-methyl-morpholine; isobutyl chloroformate In N,N-dimethyl-formamide at 0℃; for 0.166667h; Stage #2: (3,4-dimethoxy-phenethylamino)acetic acid allyl ester In N,N-dimethyl-formamide at 20℃; | 100% |
N-[(9H-fluoren-9-ylmethoxy)carbonyl]-L-alanine
Conditions | Yield |
---|---|
With benzotriazol-1-ol; dicyclohexyl-carbodiimide In dichloromethane at 20℃; | 100% |
N-[(9H-fluoren-9-ylmethoxy)carbonyl]-L-alanine
Fmoc-Lys(tert-butoxycarbonyl)
N-(9-fluorenylmethoxycarbonyl)-D-alanine
H-(D)Ala-Ala-(D)-Ala-Lys(Boc)-(D)Ala-Lys(Boc)-OH
Conditions | Yield |
---|---|
Multistep reaction.; | 100% |
6-(tert-butoxycarbonylamino)hexanoic acid
Fmoc-Val-OH
N-[(9H-fluoren-9-ylmethoxy)carbonyl]-L-alanine
Boc-Ahx-Val-Ala-OH
Conditions | Yield |
---|---|
Multistep reaction.; | 100% |
N-Cbz-L-Phe
N-[(9H-fluoren-9-ylmethoxy)carbonyl]-L-alanine
O-benzyl-N-Fmoc-L-serine
Fmoc-Pro-OH
Fmoc-Ser(tBu)-OH
N-[(9H-fluoren-9-ylmethoxy)carbonyl]-L-methionine
Nα-FMOC-Nω-L-tosylarginine
N-(((9H-fluoren-9-yl)methoxy)carbonyl)-O-(tert-butyldimethylsilyl)-L-threonine
N-alpha-(9-fluorenylmethyloxycarbonyl)-L-aspartic acid beta-allyl ester
Z-Phe-Ala-Thr(TBS)-Met-Arg(Tos)-Tyr(Pen)-Pro-Ser(tBu)-Asp(OAll)-Ser(Bzl)-Asp(OtBu)-OH
Conditions | Yield |
---|---|
Stage #1: C42H37ClNO6Pol With morpholine Automated synthesizer; solid phase reaction; Stage #2: O-benzyl-N-Fmoc-L-serine With O‑(6‑chlorobezotriazol‑1‑yl)‑N,N,N,N‑tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; 6-chloro-1-hydroxybenzotriazole In 1-methyl-pyrrolidin-2-one Automated synthesizer; solid phase reaction; Stage #3: C29H31NO5; N-Cbz-L-Phe; N-[(9H-fluoren-9-ylmethoxy)carbonyl]-L-alanine; Fmoc-Pro-OH; Fmoc-Ser(tBu)-OH; N-[(9H-fluoren-9-ylmethoxy)carbonyl]-L-methionine; Nα-FMOC-Nω-L-tosylarginine; N-(((9H-fluoren-9-yl)methoxy)carbonyl)-O-(tert-butyldimethylsilyl)-L-threonine; N-alpha-(9-fluorenylmethyloxycarbonyl)-L-aspartic acid beta-allyl ester Further stages; | 100% |
N-(fluoren-9-ylmethoxycarbonyl)glycine
Fmoc-Leu-OH
N-[(9H-fluoren-9-ylmethoxy)carbonyl]-L-alanine
Fmoc-Ile-OH
3-[(S)-2-carboxy-2-(9H-fluoren-9-ylmethoxycarbonylamino)ethyl]indole-1-carboxylic acid tert-butyl ester
H2N-Gly-Trp(Boc)-Leu-Ala-Ala-Ile-Leu-Gly-OH
Conditions | Yield |
---|---|
Stage #1: N-(fluoren-9-ylmethoxycarbonyl)glycine With N-ethyl-N,N-diisopropylamine In dichloromethane for 3h; Automated synthesizer; solid phase reaction; Stage #2: With piperidine In N,N-dimethyl-formamide for 0.1h; Automated synthesizer; solid phase reaction; Stage #3: N-(fluoren-9-ylmethoxycarbonyl)glycine; Fmoc-Leu-OH; N-[(9H-fluoren-9-ylmethoxy)carbonyl]-L-alanine; Fmoc-Ile-OH; 3-[(S)-2-carboxy-2-(9H-fluoren-9-ylmethoxycarbonylamino)ethyl]indole-1-carboxylic acid tert-butyl ester Further stages; | 100% |
N-[(9H-fluoren-9-ylmethoxy)carbonyl]-L-alanine
(S)-(9H-fluoren-9-yl)methyl 1-(4-fluoro-2-(4-fluorophenylamino)phenylamino)-1-oxopropan-2-ylcarbamate
Conditions | Yield |
---|---|
Stage #1: N-[(9H-fluoren-9-ylmethoxy)carbonyl]-L-alanine With 4-methyl-morpholine; isobutyl chloroformate In dichloromethane at -10℃; for 0.5h; Stage #2: 5-fluoro-N1-(4-fluorophenyl)benzene-1,2-diamine In dichloromethane at -10℃; for 1h; | 100% |
Stage #1: N-[(9H-fluoren-9-ylmethoxy)carbonyl]-L-alanine With 4-methyl-morpholine; isobutyl chloroformate In dichloromethane at -10℃; for 0.5h; Stage #2: 5-fluoro-N1-(4-fluorophenyl)benzene-1,2-diamine In dichloromethane at -10℃; for 1h; |
N-[(9H-fluoren-9-ylmethoxy)carbonyl]-L-alanine
Fmoc-Pro-OH
trifluoroacetic acid
N-(9-fluorenylmethoxycarbonyl)-L-β-phenylselenocysteine
C2HF3O2*C17H24N4O3Se
Conditions | Yield |
---|---|
Stage #1: Fmoc-Pro-OH With ethyl cyanoglyoxylate-2-oxime; diisopropyl-carbodiimide In N,N-dimethyl-formamide at 20℃; for 1.5h; Stage #2: With piperidine In N,N-dimethyl-formamide at 20℃; for 0.2h; Stage #3: N-[(9H-fluoren-9-ylmethoxy)carbonyl]-L-alanine; trifluoroacetic acid; N-(9-fluorenylmethoxycarbonyl)-L-β-phenylselenocysteine Further stages; | 100% |
N-[(9H-fluoren-9-ylmethoxy)carbonyl]-L-alanine
Fmoc-Pro-OH
trifluoroacetic acid
N-(9-fluorenylmethoxycarbonyl)-L-β-phenylselenocysteine
C2HF3O2*C26H33N5O4Se2
Conditions | Yield |
---|---|
Stage #1: N-(9-fluorenylmethoxycarbonyl)-L-β-phenylselenocysteine With ethyl cyanoglyoxylate-2-oxime; diisopropyl-carbodiimide In N,N-dimethyl-formamide at 20℃; for 1.5h; Stage #2: With piperidine In N,N-dimethyl-formamide at 20℃; for 0.2h; Stage #3: N-[(9H-fluoren-9-ylmethoxy)carbonyl]-L-alanine; Fmoc-Pro-OH; trifluoroacetic acid; N-(9-fluorenylmethoxycarbonyl)-L-β-phenylselenocysteine Further stages; | 100% |
6-azido-2S-{[(9H-fluorenyl-9-ylmethoxy)carbonyl]amino}hexanoic acid
N-(fluoren-9-ylmethoxycarbonyl)glycine
N-[(9H-fluoren-9-ylmethoxy)carbonyl]-L-alanine
Fmoc-Pro-OH
Fmoc-Lys(tert-butoxycarbonyl)
N-α-Fmoc-N-ε-biotinyl-L-lysine
Conditions | Yield |
---|---|
Stage #1: Fmoc-gly-wang resin With piperidine In N,N-dimethyl-formamide for 0.333333h; SASRIN®-resin; Stage #2: Fmoc-Pro-OH With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide pH=8 - 9; SASRIN®-resin; Stage #3: 6-azido-2S-{[(9H-fluorenyl-9-ylmethoxy)carbonyl]amino}hexanoic acid; N-(fluoren-9-ylmethoxycarbonyl)glycine; N-[(9H-fluoren-9-ylmethoxy)carbonyl]-L-alanine; Fmoc-Lys(tert-butoxycarbonyl); N-α-Fmoc-N-ε-biotinyl-L-lysine Further stages; | 100% |
N-[(9H-fluoren-9-ylmethoxy)carbonyl]-L-alanine
1-methyl-1-phenylethyl 2,2,2-trichloroacetimidoate
Conditions | Yield |
---|---|
In dichloromethane at 20℃; for 16h; | 100% |
In dichloromethane at 10℃; for 1h; | 98% |
N-[(9H-fluoren-9-ylmethoxy)carbonyl]-L-alanine
Conditions | Yield |
---|---|
Stage #1: N-[(9H-fluoren-9-ylmethoxy)carbonyl]-L-alanine; HCl*H-Gln(Trt)-Ser(ψMe,M ePro)-Gly-Leu-Gly-Cys(Trt)-Asn(Trt)-Ser(tBu)-Phe-Arg(Pbf)-Tyr(tBu)-Okb, Kb=2,4-didocosyloxybenzyl With N-ethyl-N,N-diisopropylamine; 4-(4,6-dimethoxy-1,3,5-triazin-2-yl)-4-methylmorpholinium chloride In tetrahydrofuran; N,N-dimethyl-formamide at 20℃; for 0.5h; Stage #2: With piperidine; benzotriazol-1-ol; 1,8-diazabicyclo[5.4.0]undec-7-ene In tetrahydrofuran; N,N-dimethyl-formamide at 20℃; for 0.166667h; Stage #3: With hydrogenchloride In tetrahydrofuran; water; N,N-dimethyl-formamide pH=Ca. 6; | 100% |
N-[(9H-fluoren-9-ylmethoxy)carbonyl]-L-alanine
(S)-(-)-3-aminopiperidin-2-one
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate In N,N-dimethyl-formamide Inert atmosphere; | 100% |
N-(fluoren-9-ylmethoxycarbonyl)glycine
N-[(9H-fluoren-9-ylmethoxy)carbonyl]-L-alanine
acetic anhydride
Fmoc-Lys(tert-butoxycarbonyl)
Fmoc-His(Trt)-OH
3-[(S)-2-carboxy-2-(9H-fluoren-9-ylmethoxycarbonylamino)ethyl]indole-1-carboxylic acid tert-butyl ester
Conditions | Yield |
---|---|
Stage #1: 3-[(S)-2-carboxy-2-(9H-fluoren-9-ylmethoxycarbonylamino)ethyl]indole-1-carboxylic acid tert-butyl ester With benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 20℃; for 1h; Enzymatic reaction; Stage #2: With piperidine In N,N-dimethyl-formamide at 20℃; for 0.2h; Stage #3: N-(fluoren-9-ylmethoxycarbonyl)glycine; N-[(9H-fluoren-9-ylmethoxy)carbonyl]-L-alanine; acetic anhydride; Fmoc-Lys(tert-butoxycarbonyl); Fmoc-His(Trt)-OH; 3-[(S)-2-carboxy-2-(9H-fluoren-9-ylmethoxycarbonylamino)ethyl]indole-1-carboxylic acid tert-butyl ester; Nα-(9-fluorenylmethyloxycarbonyl)-Nγ-2,2,4,6,7-pentamethyldihydrobenzofuran-5-sulfonyl-L-arginine Further stages; | 100% |
Conditions | Yield |
---|---|
With benzotriazol-1-ol; diisopropyl-carbodiimide In dichloromethane at 20℃; for 5h; | 100% |
formaldehyd
N-[(9H-fluoren-9-ylmethoxy)carbonyl]-L-alanine
9H-fluoren-9-ylmethyl (S)-4-methyl-5-oxo-1,3-oxazolidine-3-carboxylate
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid In toluene for 2h; Reagent/catalyst; Temperature; Reflux; | 99% |
With toluene-4-sulfonic acid In acetonitrile at 120℃; for 0.0333333h; microwave irradiation; | 97% |
With toluene-4-sulfonic acid In toluene for 0.5h; Heating; | 96% |
N-[(9H-fluoren-9-ylmethoxy)carbonyl]-L-alanine
2,4-dichlorophenyl-4-bromomethyl-phenoxyacetate
(S)-2-(9H-Fluoren-9-ylmethoxycarbonylamino)-propionic acid 4-(2,4-dichloro-phenoxycarbonylmethoxy)-benzyl ester
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide for 3h; Ambient temperature; | 99% |
N-[(9H-fluoren-9-ylmethoxy)carbonyl]-L-alanine
Conditions | Yield |
---|---|
With diethyl cyanophosphonate; N-ethyl-N,N-diisopropylamine In dichloromethane at 20℃; Addition; Peptide-bond formation; | 99% |
N-[(9H-fluoren-9-ylmethoxy)carbonyl]-L-alanine
2-Nitrobenzenesulfonyl chloride
para-Chlorobenzyl alcohol
Conditions | Yield |
---|---|
Multistep reaction; | 99% |
N-[(9H-fluoren-9-ylmethoxy)carbonyl]-L-alanine
Fmoc-Pro-OH
(2S)-N-allyloxycarbonyl-L-proline
Conditions | Yield |
---|---|
Multistep reaction; | 99% |
(4R,2'S)-2-[1'-Alloc-Thr(propargyl)-pyrrolidin-2'-yl]-4-(3"-chloro-benzyl)-4,5-dihydro-oxazole-4-carboxylic acid methyl ester
N-[(9H-fluoren-9-ylmethoxy)carbonyl]-L-alanine
(4R,2'S)-2-[1'-Fmoc-Ala-Thr(propargyl)-pyrrolidin-2'-yl]-4-(3-chloro-benzyl)-4,5-dihydro-oxazole-4-carboxylic acid methyl ester
Conditions | Yield |
---|---|
Stage #1: (4R,2'S)-2-[1'-Alloc-Thr(propargyl)-pyrrolidin-2'-yl]-4-(3"-chloro-benzyl)-4,5-dihydro-oxazole-4-carboxylic acid methyl ester; N-[(9H-fluoren-9-ylmethoxy)carbonyl]-L-alanine With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 0 - 20℃; for 2h; Stage #2: (4R,2'S)-2-[1'-Alloc-Thr(propargyl)-pyrrolidin-2'-yl]-4-(3"-chloro-benzyl)-4,5-dihydro-oxazole-4-carboxylic acid methyl ester With 1,4-diaza-bicyclo[2.2.2]octane; tetrakis(triphenylphosphine) palladium(0) In dichloromethane at 20℃; for 0.333333h; | 99% |
N-[(9H-fluoren-9-ylmethoxy)carbonyl]-L-alanine
3β-hydroxy-pregn-4-en-20-one
C39H47NO5
Conditions | Yield |
---|---|
With dmap; dicyclohexyl-carbodiimide In dichloromethane Inert atmosphere; | 99% |
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