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Zhuozhou Wenxi import and Export Co., Ltd

WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et

Wholesale price CAS 3585-33-9 with best price

Cas:3585-33-9

Min.Order:1 Kilogram

FOB Price: $139.0 / 210.0

Type:Trading Company

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Dayang Chem (Hangzhou) Co.,Ltd.

As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem’s R&D center offer custom synthesis according to the contract research and development services for the fine chemicals, ph

Lithium dimethylamide

Cas:3585-33-9

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Shanghai Upbio Tech Co.,Ltd

1.In No Less 10 years exporting experience. you can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specializ

Methanamine, N-methyl-,lithium salt (9CI)

Cas:3585-33-9

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

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Henan Wentao Chemical Product Co., Ltd.

Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

Methanamine, N-methyl-,lithium salt (9CI)

Cas:3585-33-9

Min.Order:0

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HANGZHOU YUNUO CHEMICAL CO.,LTD

superior quality moderate price & quick delivery Appearance:powder Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:1kg/bag, 1kg/drum or 25kg/drum or as per your request. Application:Used to make other chemic

Lithium dimethylamide

Cas:3585-33-9

Min.Order:1 Kilogram

Negotiable

Type:Trading Company

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Ality Chemical Corporation

The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi

Factory Supply Lithium dimethylamide

Cas:3585-33-9

Min.Order:0 Metric Ton

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Type:Other

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Shanghai Minstar Chemical Co., Ltd

Product Name: LITHIUM DIMETHYLAMIDE Synonyms: LITHIUM DIMETHYLAMIDE;LITHIUM DIMETHYLAMIDE, 5 WT. % SUSPENSIO N IN HEXANES;Lithiumdimethylamide,95%;Methanamine, N-methyl-, lithium salt;lithium dimethylamide preparation;(Dimethylamino) lithium;Di

Lithium dimethylamide 3585-33-9 C2H6LiN

Cas:3585-33-9

Min.Order:1 Gram

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TAIZHOU ZHENYU BIOTECHNOLOGY CO., LTD

Zhenyu biotech exported this product to many countries and regions at best price. if you are looking for the material's manufacturer or supplier in china, zhenyu biotech is your best choice. pls contact with us freely for getting detailed

LITHIUM DIMETHYLAMIDE

Cas:3585-33-9

Min.Order:1 Kilogram

FOB Price: $2.0

Type:Lab/Research institutions

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Antimex Chemical Limied

Ansciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali

LithiuM diMethylaMide

Cas:3585-33-9

Min.Order:0

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ZHEJIANG JIUZHOU CHEM CO.,LTD

factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin

LITHIUM DIMETHYLAMIDE

Cas:3585-33-9

Min.Order:0

Negotiable

Type:Trading Company

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Hangzhou Share Chemical Co., Ltd

At Share Chemical Company, we scrupulously abide by our policy of “Excellent Quality at a Reasonable Price”. We strive to satisfy all of our customers by providing the finest quality products supported by the finest in customer servi

LithiuM diMethylaMide, 10% w/v in h

Cas:3585-33-9

Min.Order:1 Gram

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Type:Other

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Shanghai united Scientific Co.,Ltd.

United Scientific Company Located in Shanghai of China , is a competitive player in the global specialty and fine chemical market. Fenghua has both the expertise and flexibility to produce a wide range of chemicals. Focusing on developing the innovat

Methanamine, N-methyl-,lithium salt (9CI)

Cas:3585-33-9

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Strem Chemicals, Inc.

1.High Quality Specialty Chemicals2.Expertise and Experience in Manufacturing High Purity, High Quality Chemicals3.Long Term Focus in Inorganics, Organometallics and Metals4.ISO 9001 CertifiedAppearance:off-white pwdr.

Lithium dimethylamide, 95%

Cas:3585-33-9

Min.Order:0

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Type:Other

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Finetech Industry Limited

FINETECH INDUSTRY LIMITED is a LONDON based CRO company providing drug discovery & development services to worldwide clients. FINETECH INDUSTRY LIMITED supplies the LITHIUM DIMETHYLAMIDE, CAS:3585-33-9 with the most competitive price and the best qua

LITHIUM DIMETHYLAMIDE

Cas:3585-33-9

Min.Order:0

Negotiable

Type:Trading Company

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Debye Scientific

Debyesci is here who supplied several kinds of chemical products to global pharmaceutical, drug discovery, agrochemical and biotechnology industries for four yearsOur key scientific leadership team has gained experience in top research and developmen

Lithiumdimethylamide

Cas:3585-33-9

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Chemical Co.Ltd

Manufacturer,strong R&D,professional team Storage:Store in a cool, dry place. Store in a tightly closed container. Package:according to your requirement Application:ZhiShang Chemical is owned by ZhiShang Group, is a professional new-type chemicals en

Methanamine, N-methyl-,lithium salt (9CI)

Cas:3585-33-9

Min.Order:0

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Sigma-Aldrich Chemie GmbH

Package:10, 50 g in glass bottle Application:Lithium dimethylamide is used as a reagent in the synthesis of boron-nitrogen heterocycles and 2,2 diborabiphenyl. It is a deprotecting agent which is employed in demethylation of bis(imino)pyrid...

Lithium dimethylamide

Cas:3585-33-9

Min.Order:0

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Synthetic route

trityllithium
733-90-4

trityllithium

dimethyl amine
124-40-3

dimethyl amine

A

triphenylmethane
519-73-3

triphenylmethane

B

lithium dimethylamide
3585-33-9

lithium dimethylamide

Conditions
ConditionsYield
In tetrahydrofuran at 30℃; Equilibrium constant;
1-cyclopentenyllithium
67788-09-4

1-cyclopentenyllithium

3,4-dimethoxy-3-cyclobutene-1,2-dione
5222-73-1

3,4-dimethoxy-3-cyclobutene-1,2-dione

C5H10LiN

C5H10LiN

A

lithium dimethylamide
3585-33-9

lithium dimethylamide

(3aS,5aR,8aS)-3a-Hydroxy-2,3-dimethoxy-4-methylene-4,5,5a,6,7,8-hexahydro-3aH-cyclopenta[c]pentalen-1-one

(3aS,5aR,8aS)-3a-Hydroxy-2,3-dimethoxy-4-methylene-4,5,5a,6,7,8-hexahydro-3aH-cyclopenta[c]pentalen-1-one

(3aS,3bR,6aS,7aR)-7a-Dimethylaminomethyl-3a-hydroxy-2,3-dimethoxy-3a,3b,4,5,6,6a,7,7a-octahydro-cyclopenta[a]pentalen-1-one

(3aS,3bR,6aS,7aR)-7a-Dimethylaminomethyl-3a-hydroxy-2,3-dimethoxy-3a,3b,4,5,6,6a,7,7a-octahydro-cyclopenta[a]pentalen-1-one

(3aS,3bR,6aR,7aR)-7a-Dimethylaminomethyl-3a-hydroxy-2,3-dimethoxy-3a,3b,4,5,6,6a,7,7a-octahydro-cyclopenta[a]pentalen-1-one

(3aS,3bR,6aR,7aR)-7a-Dimethylaminomethyl-3a-hydroxy-2,3-dimethoxy-3a,3b,4,5,6,6a,7,7a-octahydro-cyclopenta[a]pentalen-1-one

Conditions
ConditionsYield
Mechanism; other squarates, other alkenyllithium compounds, other 2-lithioallylamines, multistep reaction, 1.) THF, pentane, 1 h, 2.) THF, pentane, -78 deg C -> room temperature;
dimethyl amine
124-40-3

dimethyl amine

lithium dimethylamide
3585-33-9

lithium dimethylamide

Conditions
ConditionsYield
With n-butyllithium
With n-hexyllithium In tetrahydrofuran; hexane at 10℃;
With n-butyllithium In hexane for 1h; Cooling with ice;
n-hexyllithium
21369-64-2

n-hexyllithium

dimethyl amine
124-40-3

dimethyl amine

lithium dimethylamide
3585-33-9

lithium dimethylamide

Conditions
ConditionsYield
In tetrahydrofuran; hexane at 10℃;
Mo(NMe2)6Li2(THF)2

Mo(NMe2)6Li2(THF)2

lithium dimethylamide
3585-33-9

lithium dimethylamide

Conditions
ConditionsYield
In not given dissocn. in soln.;
Mo(NMe2)6Li2(THF)2

Mo(NMe2)6Li2(THF)2

A

lithium dimethylamide
3585-33-9

lithium dimethylamide

B

tetrakis(dimethylamido)molybdenum(IV)
100207-68-9

tetrakis(dimethylamido)molybdenum(IV)

Conditions
ConditionsYield
In benzene
In toluene
N,N-dimethylammonium chloride
506-59-2

N,N-dimethylammonium chloride

lithium dimethylamide
3585-33-9

lithium dimethylamide

Conditions
ConditionsYield
With n-butyllithium In tetrahydrofuran at -78 - 20℃; for 14h; Inert atmosphere;
n-butyllithium
109-72-8, 29786-93-4

n-butyllithium

dimethyl amine
124-40-3

dimethyl amine

lithium dimethylamide
3585-33-9

lithium dimethylamide

Conditions
ConditionsYield
In hexane; toluene at -20 - -15℃;
bis(dimethylamino)chlorocarbenium trifluoroacetate

bis(dimethylamino)chlorocarbenium trifluoroacetate

lithium dimethylamide
3585-33-9

lithium dimethylamide

hexamethylguanidinium trifluoroacetate

hexamethylguanidinium trifluoroacetate

Conditions
ConditionsYield
In acetonitrile at 20℃; for 5h;99.2%
bis(dimethylamino)chlorocarbenium trifluoroacetate

bis(dimethylamino)chlorocarbenium trifluoroacetate

lithium dimethylamide
3585-33-9

lithium dimethylamide

hexamethylguanidinium trifluoroacetate

hexamethylguanidinium trifluoroacetate

Conditions
ConditionsYield
In acetonitrile99.2%
lithium dimethylamide
3585-33-9

lithium dimethylamide

diphenyltin(IV) dichloride
1135-99-5

diphenyltin(IV) dichloride

bis(dimethylamido)diphenyltin(IV)
1087-64-5

bis(dimethylamido)diphenyltin(IV)

Conditions
ConditionsYield
In benzene under inert conditions, 1 equiv. of Sn-compd was added to an ice-cooled suspension of 2.2 equiv. of LiNMe2 in benzene, stirring at room temp. for 2 d; mixt. was filtered, volatiles were removed in vac.;99%
In not given
(p-Me2NC6H4)2SnCl2
56541-98-1

(p-Me2NC6H4)2SnCl2

lithium dimethylamide
3585-33-9

lithium dimethylamide

(p-Me2NC6H4)2Sn(NMe2)2
880475-50-3

(p-Me2NC6H4)2Sn(NMe2)2

Conditions
ConditionsYield
In benzene under inert conditions, 1 equiv. of Sn-compd was added to an ice-cooled suspension of 2.2 equiv. of LiNMe2 in benzene, stirring at room temp. for 2 d; mixt. was filtered, volatiles were removed in vac.;99%
lithium dimethylamide
3585-33-9

lithium dimethylamide

di(p-tolyl)tin dichloride
32538-29-7

di(p-tolyl)tin dichloride

(p-MeC6H4)2Sn(NMe2)2
952516-08-4

(p-MeC6H4)2Sn(NMe2)2

Conditions
ConditionsYield
In benzene under inert conditions, 1 equiv. of Sn-compd was added to an ice-cooled suspension of 2.2 equiv. of LiNMe2 in benzene, stirring at room temp. for 2 d; mixt. was filtered, volatiles were removed in vac.;99%
dichloro[bis(p-methoxyphenyl)]stannane
56541-97-0

dichloro[bis(p-methoxyphenyl)]stannane

lithium dimethylamide
3585-33-9

lithium dimethylamide

(p-MeOC6H4)2Sn(NMe2)2
952516-06-2

(p-MeOC6H4)2Sn(NMe2)2

Conditions
ConditionsYield
In benzene under inert conditions, 1 equiv. of Sn-compd was added to an ice-cooled suspension of 2.2 equiv. of LiNMe2 in benzene, stirring at room temp. for 2 d; mixt. was filtered, volatiles were removed in vac.;99%
lithium dimethylamide
3585-33-9

lithium dimethylamide

bis(4-fluorophenyl)tin dichloride
17236-61-2

bis(4-fluorophenyl)tin dichloride

(p-FC6H4)2Sn(NMe2)2
952516-10-8

(p-FC6H4)2Sn(NMe2)2

Conditions
ConditionsYield
In benzene under inert conditions, 1 equiv. of Sn-compd was added to an ice-cooled suspension of 2.2 equiv. of LiNMe2 in benzene, stirring at room temp. for 2 d; mixt. was filtered, volatiles were removed in vac.;99%
di(4-trifluoromethylphenyl)tindichloride
77459-83-7

di(4-trifluoromethylphenyl)tindichloride

lithium dimethylamide
3585-33-9

lithium dimethylamide

(p-CF3C6H4)2Sn(NMe2)2
952516-13-1

(p-CF3C6H4)2Sn(NMe2)2

Conditions
ConditionsYield
In benzene under inert conditions, 1 equiv. of Sn-compd was added to an ice-cooled suspension of 2.2 equiv. of LiNMe2 in benzene, stirring at room temp. for 2 d; mixt. was filtered, volatiles were removed in vac.;99%
(C5(CH3)5)TaCl2(C6H5C)2
75522-28-0

(C5(CH3)5)TaCl2(C6H5C)2

lithium dimethylamide
3585-33-9

lithium dimethylamide

A

(C5(CH3)5)Ta(C6H5CCC6H5)(N(CH3)2)Cl

(C5(CH3)5)Ta(C6H5CCC6H5)(N(CH3)2)Cl

B

(C5(CH3)5)Ta(C6H5CCC6H5)(N(CH3)2)2

(C5(CH3)5)Ta(C6H5CCC6H5)(N(CH3)2)2

Conditions
ConditionsYield
In toluene under N2; addn. of 2 equiv LiNMe2 to the soln. of the Ta-complex in toluene, mixt. stirred (room temp., 8 h); filtered (Celite), filtrate concd., layered with hexane, crystn. (24 h), elem. anal.;A 98.7%
B 0%
Hexamethylcyclotrisiloxane
541-05-9

Hexamethylcyclotrisiloxane

lithium dimethylamide
3585-33-9

lithium dimethylamide

lithium (dimethylamino)dimethylsilanolate

lithium (dimethylamino)dimethylsilanolate

Conditions
ConditionsYield
In tetrahydrofuran for 4h;98%
Salen((t)Bu)AlCl
182315-48-6

Salen((t)Bu)AlCl

lithium dimethylamide
3585-33-9

lithium dimethylamide

((CH3)2N)Al((CH2NCHC6H2(C(CH3)3)2O)2)
182315-57-7

((CH3)2N)Al((CH2NCHC6H2(C(CH3)3)2O)2)

Conditions
ConditionsYield
In toluene stirring (35°C, 24 h); filtering, evapn. (reduced pressure); elem. anal.;98%
quinuclidine dichlorogallane adduct

quinuclidine dichlorogallane adduct

lithium dimethylamide
3585-33-9

lithium dimethylamide

[HGa(NMe2)2]2
676995-07-6

[HGa(NMe2)2]2

Conditions
ConditionsYield
In diethyl ether byproducts: LiCl, quinuclidine; under N2; to a stirred slurry of Li-contg. compd. (81.5 mmol) in Et2O at-78°C was added dropwise a soln. of Ga-contg. compd. (40.7 mmol) in Et2O; the mixt. was allowed to warm to room temp. and stirred for 17 h; volatiles were removed under vac.; pentane was added and the resulting slurry was filtered to sep. LiCl and a filtrate; the filtrate was concd. and stored at -20°C overnight; elem. anal.;97%
lithium dimethylamide
3585-33-9

lithium dimethylamide

1-Chlor-N,N,N',N'-tetramethylformamidinium-trifluormethansulfonat
105142-17-4

1-Chlor-N,N,N',N'-tetramethylformamidinium-trifluormethansulfonat

N,N,N',N',N'',N''-hexamethylguanidinium triflate

N,N,N',N',N'',N''-hexamethylguanidinium triflate

Conditions
ConditionsYield
In acetonitrile at 20℃; for 12h;96.7%
lithium dimethylamide
3585-33-9

lithium dimethylamide

1-Chlor-N,N,N',N'-tetramethylformamidinium-trifluormethansulfonat
105142-17-4

1-Chlor-N,N,N',N'-tetramethylformamidinium-trifluormethansulfonat

hexamethyl guanidinium trifluoromethane sulfonate

hexamethyl guanidinium trifluoromethane sulfonate

Conditions
ConditionsYield
In diethyl ether; acetonitrile96.7%
bis(dimethylamino)chlorocarbenium tosylate

bis(dimethylamino)chlorocarbenium tosylate

lithium dimethylamide
3585-33-9

lithium dimethylamide

hexamethylguanidinium tosylate

hexamethylguanidinium tosylate

Conditions
ConditionsYield
In acetonitrile at 20℃; for 5h;96.6%
bis(dimethylamino)chlorocarbenium tosylate

bis(dimethylamino)chlorocarbenium tosylate

lithium dimethylamide
3585-33-9

lithium dimethylamide

hexamethylguanidinium tosylate

hexamethylguanidinium tosylate

Conditions
ConditionsYield
In acetonitrile96.6%
pentacarbonyl(1,4-diethoxy-4-methylpentynylidene)chromium

pentacarbonyl(1,4-diethoxy-4-methylpentynylidene)chromium

lithium dimethylamide
3585-33-9

lithium dimethylamide

A

pentacarbonyl{(2E)-3-(dimethylamino)-1,4-diethoxy-4-methylpentenylidene}chromium

pentacarbonyl{(2E)-3-(dimethylamino)-1,4-diethoxy-4-methylpentenylidene}chromium

B

pentacarbonyl{3-(dimethylamino)-4-ethoxy-4-methyl-1,2-pentadienylidene}chromium

pentacarbonyl{3-(dimethylamino)-4-ethoxy-4-methyl-1,2-pentadienylidene}chromium

Conditions
ConditionsYield
In diethyl ether addn. of the Li-amide in Et2O to the Cr-complex in Et2O under N2 at 20°C, stirred for 30 min; evapd. (vac.), chromy.;A 0%
B 96%
tetrahydrofuran
109-99-9

tetrahydrofuran

lithium dimethylamide
3585-33-9

lithium dimethylamide

zirconium(IV) chloride
10026-11-6

zirconium(IV) chloride

2Li(1+)*6C2H6N(1-)*Zr(4+)*2C4H8O

2Li(1+)*6C2H6N(1-)*Zr(4+)*2C4H8O

Conditions
ConditionsYield
With lithium chloride In toluene at 20℃; for 12h; Inert atmosphere;96%
2,4-dicarba-closo-heptaborane
20693-69-0

2,4-dicarba-closo-heptaborane

lithium dimethylamide
3585-33-9

lithium dimethylamide

2,4-dicarba-nido-hexaborate(8)(1-)
39394-97-3

2,4-dicarba-nido-hexaborate(8)(1-)

Conditions
ConditionsYield
In acetonitrile N2-atmosphere, condensing C2B5H7 to Li-compd. in NMR-tube (vac., -195°C), warming (room temp.), shaking, standing (2 min), cooling (-195°C), addn. of MeCN, warming (ambient temp.), standing (room temp., 2 months); not isolated; (11)B-NMR;95%
Cp*TiCl3
12129-06-5

Cp*TiCl3

lithium dimethylamide
3585-33-9

lithium dimethylamide

mono(pentamethylcyclopentadienyl)tris(dimethylamido)titanium(IV)

mono(pentamethylcyclopentadienyl)tris(dimethylamido)titanium(IV)

Conditions
ConditionsYield
In hexane suspn. of Ti-complex and LiNMe2 is stirred in hexane (under Ar) for 15 h; filtn., concn. the volume, cooling to -40°C for 24 h, elem. anal.;95%
1,2-Mo2Br2(CH2SiMe3)4
75059-90-4

1,2-Mo2Br2(CH2SiMe3)4

lithium dimethylamide
3585-33-9

lithium dimethylamide

A

1,2-bis(dimethylamido)tetrakis(trimethylsilylmethyl)dimolybdenum(Mo-Mo)

1,2-bis(dimethylamido)tetrakis(trimethylsilylmethyl)dimolybdenum(Mo-Mo)

B

1,1-bis(dimethylamido)tetrakis(trimethylsilylmethyl)dimolybdenum(Mo-Mo)
75059-94-8

1,1-bis(dimethylamido)tetrakis(trimethylsilylmethyl)dimolybdenum(Mo-Mo)

Conditions
ConditionsYield
In hexane byproducts: LiCl; react. at -50°C, then warming to 0°C over 2 h; filtration, solvent stripped, products are not sepd., detected by NMR, elem. anal.;A 5%
B 95%
In hexane byproducts: LiBr; filtration, removal of solvent in vac.;
[Zr(η5-C5Me4SiMeH-η1-NBu-t)Cl2]
570401-34-2

[Zr(η5-C5Me4SiMeH-η1-NBu-t)Cl2]

lithium dimethylamide
3585-33-9

lithium dimethylamide

[Zr(η5-C5Me4SiMeH-η1-NBu-t)(NMe2)2]
570401-37-5

[Zr(η5-C5Me4SiMeH-η1-NBu-t)(NMe2)2]

Conditions
ConditionsYield
In toluene toluene was added at -78°C to a mixt. of compounds, warmed to room temp., stirred for 21 h (Ar); solvent was removed under reduced pressure, extd. with hexane, filtered,evapd.; elem. anal.;95%
[(tert-butylcalix[4]arene methyl ether)chlorotitanium(IV)] toluene

[(tert-butylcalix[4]arene methyl ether)chlorotitanium(IV)] toluene

lithium dimethylamide
3585-33-9

lithium dimethylamide

[(tert-butylcalix[4]arene methyl ether)(dimethylamido)titanium(IV)]
850538-56-6

[(tert-butylcalix[4]arene methyl ether)(dimethylamido)titanium(IV)]

Conditions
ConditionsYield
In toluene N2, to a soln. of 1.15 equiv. of Li compd. added at room temp. a soln., of Ti compd., stirred for 12 h; filtered (Celite), volatiles removed (vac.), suspnd. (hexane), ppt. collected, dried (vac.); elem. anal.;95%
TaCl(dimethylamide)3(1,1-dimethyl-2-(trimethylsilyl)hydrazide)

TaCl(dimethylamide)3(1,1-dimethyl-2-(trimethylsilyl)hydrazide)

lithium dimethylamide
3585-33-9

lithium dimethylamide

Ta(dimethylamide)4(1,1-dimethyl-2-(trimethylsilyl)hydrazide)
1233220-56-8

Ta(dimethylamide)4(1,1-dimethyl-2-(trimethylsilyl)hydrazide)

Conditions
ConditionsYield
In pentane byproducts: LiCl; addn. of LiN(CH3)2 to Ta complex in pentane at -30°C, slow warming to room temp., stirring for 24 h; filtration, extn. with pentane, concn., storage at -30°C, isolation of solid;95%
bis(dimethylamino)chlorocarbenium thiocyanate

bis(dimethylamino)chlorocarbenium thiocyanate

lithium dimethylamide
3585-33-9

lithium dimethylamide

1,1,2,2,3,3-Hexamethylguanidiniumthiocyanat
68897-49-4

1,1,2,2,3,3-Hexamethylguanidiniumthiocyanat

Conditions
ConditionsYield
In acetonitrile at 20℃; for 5h;94.8%
bis(dimethylamino)chlorocarbenium thiocyanate

bis(dimethylamino)chlorocarbenium thiocyanate

lithium dimethylamide
3585-33-9

lithium dimethylamide

hexamethylguanidinium thiocyanate

hexamethylguanidinium thiocyanate

Conditions
ConditionsYield
In acetonitrile94.8%
aluminium trichloride
7446-70-0

aluminium trichloride

lithium dimethylamide
3585-33-9

lithium dimethylamide

tris(benzyl)aluminum
14994-03-7

tris(benzyl)aluminum

[(C6H5CH2)2AlN(CH3)2]2

[(C6H5CH2)2AlN(CH3)2]2

Conditions
ConditionsYield
In toluene byproducts: LiCl; inert atmosphere; treatment of Al(CH2Ph)3 with AlCl3, suspending in PhMe, addn. of LiNMe2 at 25°C, stirring for 12 h; removal of volatiles, extn. into PhMe, filtration, evapn.;94%
Diethylcyanamide
617-83-4

Diethylcyanamide

lithium dimethylamide
3585-33-9

lithium dimethylamide

zinc(II) chloride
7646-85-7

zinc(II) chloride

lithium hexamethyldisilazane
4039-32-1

lithium hexamethyldisilazane

[zinc(μ-1,1-dimethyl-3,3-diethylguanidine)(N(SiMe3)2)]2
1000163-77-8

[zinc(μ-1,1-dimethyl-3,3-diethylguanidine)(N(SiMe3)2)]2

Conditions
ConditionsYield
In diethyl ether byproducts: LiCl; (Ar); Li-dialkylamide dissolved in ether; equimolar cyanamide added dropwise; stirred for 30 min; equimolar LiN(SiMe3)2 and ZnCl2 added; stirredfor 24 h; centrifuged; soln. concd.; cooled to -35°C; elem. anal.;94%
(η(5)-indenyl)trichlorotitanium
84365-55-9

(η(5)-indenyl)trichlorotitanium

lithium dimethylamide
3585-33-9

lithium dimethylamide

[Ti(η5-Ind)(NMe2)Cl2]

[Ti(η5-Ind)(NMe2)Cl2]

Conditions
ConditionsYield
In toluene to stirred suspn. of Ti-complex in toluene at -80°C was added dropwise suspn. of LiNMe2 in toluene, warmed to room temp., stirred overnight under Ar; solvent was evapd. to dryness, washed with hexane, extd. with toluene, cooled to -20°C; elem. anal.;93%
1,3-dimethyl-2-chloroimidazolidinium nitrate

1,3-dimethyl-2-chloroimidazolidinium nitrate

lithium dimethylamide
3585-33-9

lithium dimethylamide

1,3-dimethyl-2-dimethylaminoimidazolidinium nitrate

1,3-dimethyl-2-dimethylaminoimidazolidinium nitrate

Conditions
ConditionsYield
In acetonitrile at 20℃; for 5h;92.2%

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