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Cas:3610-36-4
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Min.Order:1 Kilogram
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Min.Order:1 Kilogram
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Cas:3610-36-4
Min.Order:1 Gram
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inquiry3-(2-Aminoethyl)-6-methoxyindole CAS:3610-36-4 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality o
Cas:3610-36-4
Min.Order:1 Gram
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inquirysuperior quality moderate price & quick delivery Appearance:off-white to beige crystalline powder Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:1kg/bag, 1kg/drum or 25kg/drum or as per your request. Applic
Cas:3610-36-4
Min.Order:1 Kilogram
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Min.Order:10 Gram
Negotiable
Type:Lab/Research institutions
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Cas:3610-36-4
Min.Order:1 Gram
Negotiable
Type:Other
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Min.Order:1 Kilogram
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Min.Order:1 Gram
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Type:Lab/Research institutions
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Cas:3610-36-4
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inquiryLower price, sample is available,SDS test documents are available,large stock in warehouseAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:Fine chemical intermediates, used as the main raw material for the synthe
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Cas:3610-36-4
Min.Order:100 Gram
Negotiable
Type:Lab/Research institutions
inquiryAcmec is a leading manufacturer and supplier of biochemical reagents and life science products. We have over 40,000 items in stock (real-time inventory) and offer discounted prices to registered members of the online store ( www.acmec.com.cn ) Appea
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Min.Order:1 bottle
Negotiable
Type:Lab/Research institutions
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Ansciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali
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Cas:3610-36-4
Min.Order:0
Negotiable
Type:Trading Company
inquiry2-(2-Aminoethyl)-5-methoxyindole cas 3610-36-4Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express
Cas:3610-36-4
Min.Order:0
Negotiable
Type:Other
inquiryR & D enterprises have their own stock in stockAppearance:To be subject to the object Package:5g Application:pharmaceutical intermediates Transportation:Air Port:Shanghai;Guangzhou
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Cas:3610-36-4
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiry2-carboxyethyl-3-(2-phthalimidoethyl)-6-methoxyindole
2-(6-methoxy-1H-indol-3-yl)ethanamine
Conditions | Yield |
---|---|
Stage #1: 2-carboxyethyl-3-(2-phthalimidoethyl)-6-methoxyindole With potassium hydroxide In water for 3h; Heating; Stage #2: With hydrogenchloride In water for 10h; Heating; | 90% |
2-(6-methoxy-1H-indol-3-yl)ethanamine
Conditions | Yield |
---|---|
Stage #1: C25H42N2O3Si With trifluoroacetic acid In dichloromethane at 20℃; for 1h; Inert atmosphere; Stage #2: With cesium fluoride In tetrahydrofuran; methanol; toluene at 20℃; for 6h; Inert atmosphere; | 58% |
2-(6-methoxy-1H-indol-3-yl)acetonitrile
2-(6-methoxy-1H-indol-3-yl)ethanamine
Conditions | Yield |
---|---|
With methanol; ammonia; nickel under 73550.8 Torr; Hydrogenation; | |
With lithium aluminium tetrahydride; diethyl ether | |
With ethanol; sodium |
2-(6-methoxy-1H-indol-3-yl)-2-oxo-acetamide
2-(6-methoxy-1H-indol-3-yl)ethanamine
Conditions | Yield |
---|---|
With tetrahydrofuran; lithium aluminium tetrahydride |
6-methoxytryptamine-2-carboxylic acid
2-(6-methoxy-1H-indol-3-yl)ethanamine
Conditions | Yield |
---|---|
With hydrogenchloride |
6-methoxy-3-(2-nitroethyl)-1H-indole
2-(6-methoxy-1H-indol-3-yl)ethanamine
Conditions | Yield |
---|---|
With hydrogen; palladium on activated charcoal In ethanol under 2585.7 Torr; for 12h; |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 27 percent / tert-butylcatechol / xylene / 3 h / Heating 2: H2 / 10 percent Pd/C / ethanol / 12 h / 2585.7 Torr View Scheme | |
Multi-step reaction with 2 steps 1: methyl magnesium iodide; diethyl ether / Behandeln des Reaktionsgemisches mit Chloracetonitril 2: sodium; ethanol View Scheme | |
Multi-step reaction with 3 steps 1: acetic acid; dioxane 2: dimethyl sulfate; acetic acid; THF / Erwaermen des Reaktionsprodukts in H2O mit KCN 3: Raney nickel; NH3; methanol / 73550.8 Torr / Hydrogenation View Scheme | |
Multi-step reaction with 3 steps 1: diethyl ether 2: concentrated aqueous NH3 3: LiAlH4; THF View Scheme | |
Multi-step reaction with 2 steps 1.1: trichlorophosphate / 0.5 h / 0 °C / Inert atmosphere; Schlenk technique 1.2: 2 h / 20 °C / Inert atmosphere; Schlenk technique 2.1: ammonium acetate / 2 h / 115 °C / Inert atmosphere; Schlenk technique 2.2: 3 h / 0 - 65 °C / Inert atmosphere; Schlenk technique View Scheme |
6-methoxy-3-((trimethyl-14-azaneyl)methyl)-1H-indole iodide
2-(6-methoxy-1H-indol-3-yl)ethanamine
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 2: LiAlH4; diethyl ether View Scheme |
1-(6-methoxy-1H-indol-3-yl)-N,N-dimethylmethanamine
2-(6-methoxy-1H-indol-3-yl)ethanamine
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: dimethyl sulfate; acetic acid; THF / Erwaermen des Reaktionsprodukts in H2O mit KCN 2: Raney nickel; NH3; methanol / 73550.8 Torr / Hydrogenation View Scheme |
7-methoxy-2,3,4,9-tetrahydro-1H-pyrido<3,4-b>indol-1-one
2-(6-methoxy-1H-indol-3-yl)ethanamine
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: aq.-ethanolic KOH 2: aqueous HCl View Scheme |
(6-methoxy-1H-indol-3-yl)(oxo)acetyl chloride
2-(6-methoxy-1H-indol-3-yl)ethanamine
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: concentrated aqueous NH3 2: LiAlH4; THF View Scheme |
2,β-Dinitro-4-methoxy-styrol
2-(6-methoxy-1H-indol-3-yl)ethanamine
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: ethyl acetate; palladium/charcoal; ethanol / Hydrogenation.Reagens 4: Essigsaeure 2: diethyl ether 3: concentrated aqueous NH3 4: LiAlH4; THF View Scheme |
6-methoxy-3-(2-nitrovinyl)indole
2-(6-methoxy-1H-indol-3-yl)ethanamine
Conditions | Yield |
---|---|
With lithium aluminium tetrahydride In tetrahydrofuran at 20℃; |
6-methoxylindole
1-dimethylamino-2-nitroethene
2-(6-methoxy-1H-indol-3-yl)ethanamine
Conditions | Yield |
---|---|
Stage #1: 6-methoxylindole; 1-dimethylamino-2-nitroethene In dichloromethane; trifluoroacetic acid at 20℃; for 2h; Stage #2: With lithium aluminium tetrahydride In tetrahydrofuran at -78℃; |
6-methoxy-1H-indole-3-carbaldehyde
nitromethane
2-(6-methoxy-1H-indol-3-yl)ethanamine
Conditions | Yield |
---|---|
Stage #1: 6-methoxy-1H-indole-3-carbaldehyde; nitromethane With ammonium acetate at 115℃; for 2h; Henry Nitro Aldol Condensation; Inert atmosphere; Schlenk technique; Stage #2: With lithium aluminium tetrahydride In tetrahydrofuran at 0 - 65℃; for 3h; Inert atmosphere; Schlenk technique; | 270 mg |
4-chlorobenzaldehyde
2-(6-methoxy-1H-indol-3-yl)ethanamine
C18H17ClN2O
Conditions | Yield |
---|---|
With sodium sulfate In dichloromethane at 23℃; for 3h; Inert atmosphere; Sealed tube; | 100% |
With sodium sulfate In dichloromethane at 23℃; for 3h; Inert atmosphere; |
Conditions | Yield |
---|---|
With sodium sulfate In dichloromethane at 23℃; for 3h; Inert atmosphere; Sealed tube; | 100% |
4-formylbenzonitrile-α-d1
2-(6-methoxy-1H-indol-3-yl)ethanamine
Conditions | Yield |
---|---|
With sodium sulfate In dichloromethane at 23℃; for 3h; Inert atmosphere; Sealed tube; | 100% |
Glyoxilic acid
2-(6-methoxy-1H-indol-3-yl)ethanamine
7-methoxy-2,3,4,9-tetrahydro-1H-β-carboline-1-carboxylic acid
Conditions | Yield |
---|---|
With potassium carbonate In water; ethyl acetate at 20℃; for 24h; pH=5; Pictet-Spengler Synthesis; | 99% |
With potassium hydroxide In water at 20℃; for 12h; pH=3 - 4; Pictet-Spengler reaction; | |
With NaOAc buffer In ethyl acetate for 48h; pH=4.5; |
2-(6-methoxy-1H-indol-3-yl)ethanamine
Trifluoroacetaldehyde ethyl hemiacetal
7-methoxy-1-trifluoromethyl-1,2,3,4-tetrahydro-9H-pyrido<3,4-b>indole
Conditions | Yield |
---|---|
at 110 - 120℃; for 5h; | 98.4% |
With hydrogenchloride In methanol at 20℃; Pictet-Spengler cyclisation; |
1,1-dimethoxyethane
2-(6-methoxy-1H-indol-3-yl)ethanamine
7-methoxy-1-methyl-2,3,4,9-tetrahydro-1H-pyrido[3,4-b]indole hydrochloride
Conditions | Yield |
---|---|
Stage #1: 1,1-dimethoxyethane; 2-(6-methoxy-1H-indol-3-yl)ethanamine With trifluoroacetic acid In 1,2-dichloro-ethane at 110℃; for 0.05h; Pictet-Spengler Synthesis; Sealed tube; Microwave irradiation; Stage #2: With hydrogenchloride In ethyl acetate at 20℃; | 98% |
Conditions | Yield |
---|---|
With (S)-N-benzyl-2-(3-(3,5-bis(trifluoromethyl)phenyl)thioureido)-N,3-dimethylbutanamide; benzoic acid In toluene at 23℃; for 24h; Pictet-Spengler Synthesis; Inert atmosphere; Sealed tube; enantioselective reaction; | 98% |
3-pyridinecarboxaldehyde
trifluoroacetic acid
2-(6-methoxy-1H-indol-3-yl)ethanamine
Conditions | Yield |
---|---|
In 1,2-dichloro-ethane at 110℃; for 0.0833333h; Pictet-Spengler Synthesis; Sealed tube; Microwave irradiation; | 97% |
di-tert-butyl dicarbonate
2-(6-methoxy-1H-indol-3-yl)ethanamine
C16H22N2O3
Conditions | Yield |
---|---|
With triethylamine In tetrahydrofuran at 20℃; for 12h; | 96% |
Conditions | Yield |
---|---|
Stage #1: benzaldehyde; 2-(6-methoxy-1H-indol-3-yl)ethanamine With trifluoroacetic acid In 1,2-dichloro-ethane at 110℃; for 0.183333h; Pictet-Spengler Synthesis; Sealed tube; Microwave irradiation; Stage #2: With hydrogenchloride In ethyl acetate at 20℃; | 95% |
4-chlorobenzaldehyde
2-(6-methoxy-1H-indol-3-yl)ethanamine
(R)-1-(4-chlorophenyl)-7-methoxy-2,3,4,9-tetrahydro-1H-pyrido[3,4-b]indole
Conditions | Yield |
---|---|
With 1,1'-(2S,2'S)-1,1'-(4,10-dimethyl-1,4,7,10-tetraazacyclododecane-1,7-diyl)bis(3-methyl-1-oxobutane-2,1-diyl)bis(3-(3,5-bis(trifluoromethyl)phenyl)thiourea); 4-methoxybenzoic acid In toluene at 20℃; for 72h; Pictet-Spengler Synthesis; enantioselective reaction; | 93% |
With (S)-N-benzyl-2-(3-(3,5-bis(trifluoromethyl)phenyl)thioureido)-N,3-dimethylbutanamide; benzoic acid In toluene at 23℃; for 66h; Pictet-Spengler cyclisation; Inert atmosphere; optical yield given as %ee; enantioselective reaction; | 78% |
3,4,5-trimethoxybenzoylformic acid
2-(6-methoxy-1H-indol-3-yl)ethanamine
Conditions | Yield |
---|---|
With 1,1'-carbonyldiimidazole | 93% |
acetaldehyde
2-(6-methoxy-1H-indol-3-yl)ethanamine
tetrahydroharmine
Conditions | Yield |
---|---|
With hydrogenchloride In water at 40℃; for 6h; Pictet-Spengler Synthesis; | 92% |
With sulfuric acid In water at 110℃; for 0.333333h; | 63% |
With sulfuric acid | |
Stage #1: 2-(6-methoxy-1H-indol-3-yl)ethanamine With hydrogenchloride In water at 30℃; Stage #2: acetaldehyde In water for 10h; | |
With acetic acid for 8h; Reflux; |
isobutyraldehyde
2-(6-methoxy-1H-indol-3-yl)ethanamine
(R)-1-isopropyl-7-methoxy-2,3,4,9-tetrahydro-1H-pyrido[3,4-b]indole
Conditions | Yield |
---|---|
With (S)-N-benzyl-2-(3-(3,5-bis(trifluoromethyl)phenyl)thioureido)-N,3-dimethylbutanamide In toluene at 23℃; for 88h; Pictet-Spengler cyclisation; Inert atmosphere; optical yield given as %ee; enantioselective reaction; | 90% |
Conditions | Yield |
---|---|
With 1,1'-(2S,2'S)-1,1'-(4,10-dimethyl-1,4,7,10-tetraazacyclododecane-1,7-diyl)bis(3-methyl-1-oxobutane-2,1-diyl)bis(3-(3,5-bis(trifluoromethyl)phenyl)thiourea); 4-methoxybenzoic acid In toluene at 20℃; for 72h; Pictet-Spengler Synthesis; enantioselective reaction; | 89% |
Conditions | Yield |
---|---|
With magnesium sulfate In acetonitrile for 1h; Strecker reaction; | 87% |
m-bromobenzoic aldehyde
2-(6-methoxy-1H-indol-3-yl)ethanamine
(R)-1-(3-bromophenyl)-7-methoxy-2,3,4,9-tetrahydro-1H-pyrido[3,4-b]indole
Conditions | Yield |
---|---|
With (S)-N-benzyl-2-(3-(3,5-bis(trifluoromethyl)phenyl)thioureido)-N,3-dimethylbutanamide; benzoic acid In toluene at 23℃; for 19h; Pictet-Spengler cyclisation; Inert atmosphere; optical yield given as %ee; enantioselective reaction; | 87% |
With 1,1'-(2S,2'S)-1,1'-(4,10-dimethyl-1,4,7,10-tetraazacyclododecane-1,7-diyl)bis(3-methyl-1-oxobutane-2,1-diyl)bis(3-(3,5-bis(trifluoromethyl)phenyl)thiourea); 4-methoxybenzoic acid In toluene at 20℃; for 72h; Pictet-Spengler Synthesis; enantioselective reaction; | 84% |
benzaldehyde
2-(6-methoxy-1H-indol-3-yl)ethanamine
7-methoxy-1-phenyl-2,3,4,9-tetrahydro-1H-β-carboline
Conditions | Yield |
---|---|
With 2,4,6-tripropyl-1,3,5,2,4,6-trioxatriphosphinane-2,4,6-trioxide In ethyl acetate at 110℃; for 0.166667h; Microwave irradiation; Sealed tube; | 87% |
Conditions | Yield |
---|---|
With magnesium sulfate In acetonitrile diastereoselective reaction; | 87% |
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 20 - 30℃; for 2h; Inert atmosphere; | 87% |
acetic anhydride
2-(6-methoxy-1H-indol-3-yl)ethanamine
N-(2-(6-methoxy-1H-indol-3-yl)ethyl)acetamide
Conditions | Yield |
---|---|
With TEA In tetrahydrofuran for 6h; Ambient temperature; | 86% |
2-Ethylbutyraldehyde
2-(6-methoxy-1H-indol-3-yl)ethanamine
(R)-7-methoxy-1-(pentan-3-yl)-2,3,4,9-tetrahydro-1H-pyrido[3,4-b]indole
Conditions | Yield |
---|---|
With (S)-N-benzyl-2-(3-(3,5-bis(trifluoromethyl)phenyl)thioureido)-N,3-dimethylbutanamide In toluene at 23℃; for 120h; Pictet-Spengler cyclisation; Inert atmosphere; optical yield given as %ee; enantioselective reaction; | 84% |
4-bromo-benzaldehyde
2-(6-methoxy-1H-indol-3-yl)ethanamine
(R)-1-(4-bromophenyl)-7-methoxy-2,3,4,9-tetrahydro-1H-pyrido[3,4-b]indole
Conditions | Yield |
---|---|
With 1,1'-(2S,2'S)-1,1'-(4,10-dimethyl-1,4,7,10-tetraazacyclododecane-1,7-diyl)bis(3-methyl-1-oxobutane-2,1-diyl)bis(3-(3,5-bis(trifluoromethyl)phenyl)thiourea); 4-methoxybenzoic acid In toluene at 20℃; for 72h; Pictet-Spengler Synthesis; enantioselective reaction; | 84% |
With (S)-N-benzyl-2-(3-(3,5-bis(trifluoromethyl)phenyl)thioureido)-N,3-dimethylbutanamide; benzoic acid In toluene at 23℃; for 74h; Pictet-Spengler cyclisation; Inert atmosphere; optical yield given as %ee; enantioselective reaction; | 79% |
2-(isocyanatomethyl)-1,3-dioxolane
2-(6-methoxy-1H-indol-3-yl)ethanamine
9-methoxy-5,6,11,11b-tetrahydro-1H-imidazo[1',5':1,2]pyrido[3,4-b]indol-3(2H)-one
Conditions | Yield |
---|---|
Stage #1: 2-(isocyanatomethyl)-1,3-dioxolane; 2-(6-methoxy-1H-indol-3-yl)ethanamine In tetrahydrofuran at 20℃; for 7h; Pictet-Spengler Synthesis; Inert atmosphere; Stage #2: With hydrogenchloride In methanol; water at 55℃; for 4h; Pictet-Spengler Synthesis; Inert atmosphere; | 84% |
N-(4-carboxybenzyl)-1-(3-chlorophenyl)-N-methylmethanaminium chloride
2-(6-methoxy-1H-indol-3-yl)ethanamine
4-{[(3-chlorobenzyl)(methyl)amino]methyl}-N-[2-(6-methoxy-1H-indol-3-yl)ethyl]benzamide
Conditions | Yield |
---|---|
With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; triethylamine In N,N-dimethyl-formamide at 20℃; | 82% |
Conditions | Yield |
---|---|
Stage #1: isobutyraldehyde; 2-(6-methoxy-1H-indol-3-yl)ethanamine With trifluoroacetic acid In 1,2-dichloro-ethane at 110℃; for 0.05h; Pictet-Spengler Synthesis; Sealed tube; Microwave irradiation; Stage #2: With hydrogenchloride In ethyl acetate at 20℃; | 82% |
isobutyraldehyde
trifluoroacetic acid
2-(6-methoxy-1H-indol-3-yl)ethanamine
Conditions | Yield |
---|---|
In 1,2-dichloro-ethane at 110℃; for 0.05h; Pictet-Spengler Synthesis; Sealed tube; Microwave irradiation; | 82% |
4-fluorobenzaldehyde
2-(6-methoxy-1H-indol-3-yl)ethanamine
(R)-1-(4-fluorophenyl)-7-methoxy-2,3,4,9-tetrahydro-1H-pyrido[3,4-b]indole
Conditions | Yield |
---|---|
With (S)-N-benzyl-2-(3-(3,5-bis(trifluoromethyl)phenyl)thioureido)-N,3-dimethylbutanamide; benzoic acid In toluene at 23℃; for 70h; Pictet-Spengler cyclisation; Inert atmosphere; optical yield given as %ee; enantioselective reaction; | 81% |
2-(6-methoxy-1H-indol-3-yl)ethanamine
(+)-peganumine A
Conditions | Yield |
---|---|
With (R)-2,6-bis(3,5-difluoro-4-(trifluoromethyl)phenyl)-4H-dinaphtho[2,1-d:1',2'-f][1,3,2]dithiazepine 3,3,5,5-tetraoxide In toluene at 60℃; Catalytic behavior; Solvent; Temperature; Pictet-Spengler Synthesis; Inert atmosphere; Schlenk technique; Molecular sieve; Sealed tube; enantioselective reaction; | 81% |
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