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Qingdao Beluga Import and Export Co., LTD

Beluga chemical professional supply 4-Amino-3,5-dichlorophenacylbromide Why choose Beluga chemical 1. Beluga Chemical has a professional RESEARCH and development team and strong technical force to ensure technical support and research capabilitie

4-Amino-3,5-dichlorophenacylbromide

Cas:37148-47-3

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

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Zibo Dorne chemical technology co. LTD

Product Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,

4-Amino-3,5-dichloro-alpha-bromoacetophenone High quality/Best price/In stock

Cas:37148-47-3

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

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Dayang Chem (Hangzhou) Co.,Ltd.

Dayangchem's R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantities

4-AMINO-3,5-DICHLOROPHENACYLBROMIDE

Cas:37148-47-3

Min.Order:1 Kilogram

FOB Price: $3.0

Type:Lab/Research institutions

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Hebei Mojin Biotechnology Co.,Ltd

Company information: Hebei Mojin Biotechnology Co., Ltd, Our company is a professional in chemical raw materials and chemical reagents research and development production enterprises. Our business covers more than 30 countries, most of the big custo

4-Amino-3, 5-Dichlorophenacylbromide CAS 37148-47-3

Cas:37148-47-3

Min.Order:1 Kilogram

FOB Price: $8.0 / 10.0

Type:Trading Company

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Shaanxi New nine Material Technology Co., Ltd.

Our Advantage: 1. Rich experience We specialize in this filed for many years, our APIs exported to all over the world and and we established long friendly relations of cooperation with our clients. 2. Great quality,purity and favorable Good quali

4-Amino-3 5-Dichlorophenacylbromide

Cas:37148-47-3

Min.Order:1 Kilogram

FOB Price: $10.0

Type:Trading Company

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Zibo Hangyu Biotechnology Development Co., Ltd

Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi

Factory supply 4-Amino-3,5-dichlorophenacylbromide

Cas:37148-47-3

Min.Order:10 Gram

Negotiable

Type:Lab/Research institutions

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Shandong Hanjiang Chemical Co., Ltd.

Hello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by email in time prod

4-Amino-3,5-dichloro-alpha-bromoacetophenone

Cas:37148-47-3

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

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Wuhan Fortuna Chemical Co.,Ltd

4-Amino-3,5-dichloro-alpha-bromoacetophenone Cas 37148-47-3 Company profile Wuhan Fortuna Chemical Co.,Ltd established in 2006, is a big integrative chemical enterprise being engaged in Pharmaceutical & its intermediates, Food/Feed additives

4-Amino-3,5-dichloro-alpha-bromoacetophenone Cas 37148-47-3

Cas:37148-47-3

Min.Order:10 Kilogram

FOB Price: $10.0

Type:Trading Company

inquiry

Xi'an Xszo Chem Co., Ltd.

1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience 2. Free samples will be provided,ensure specifications and quality are right for customer 3. Customers will receive the most professional techn

Large Stock 99.0% 4-Amino-3,5-dichloro-alpha-bromoacetophenone 37148-47-3 Producer

Cas:37148-47-3

Min.Order:1 Gram

FOB Price: $0.1

Type:Manufacturers

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Ality Chemical Corporation

The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi

Factory Supply Ethanone,1-(4-amino-3,5-dichlorophenyl)-2-bromo-

Cas:37148-47-3

Min.Order:1

Negotiable

Type:Other

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Hubei DiBo chemical co., LTD

Name: 4-Amino-3,5-Dichloro-A-Bromo-Acetophenone CAS no. : 37148-47-3 Molecular formula: C8H6BrCl2NO Molecular weight:282.9493 Product Quality 12 years of chemical raw materials Mature operation of the industry System stability Data storage

4-Amino-3,5-Dichloro-A-Bromo-Acetophenone /CAS :37148-47-3/raw material/high-quality

Cas:37148-47-3

Min.Order:25 Kilogram

FOB Price: $1.0 / 2.0

Type:Other

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Hebei Nengqian Chemical Import and Export Co., LTD

Our Advantage Rich Experience Our products are sold all over Europe,North&South America, Sino-East, Asia and pacific area as well as Africa,we establish long term. Quality service Company cooperates with research institutes. We strictly con

CAS 37148-47-3 4-Amino-3, 5-Dichlorophenacylbromide

Cas:37148-47-3

Min.Order:1 Kilogram

FOB Price: $1.0 / 10.0

Type:Trading Company

inquiry

Zhuozhou Wenxi import and Export Co., Ltd

WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et

Pharmaceutical Grade CAS 37148-47-3 with competitive price

Cas:37148-47-3

Min.Order:1 Kilogram

FOB Price: $139.0 / 210.0

Type:Trading Company

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Hebei yanxi chemical co.,LTD.

hebei yanxi chemical co., LTD who registered capital of 10 million yuan, nearly to $2 million, we have a pharmaceutical raw materials factory production of pharmaceutical raw materials, and a reagent r&d center, and we do research and developmen

4-Amino-3,5-dichlorophenacylbromide CAS NO.37148-47-3

Cas:37148-47-3

Min.Order:20 Kilogram

FOB Price: $10.0 / 100.0

Type:Trading Company

inquiry

Wuhan Han Sheng New Material Technology Co.,Ltd

Our advantages: 1.Wuhan Han Sheng New Material Technology Co.,Ltd is a professional raw powder factory in China founded in 2022, all powders are factory directly supplying. 2.Our products have exported to Germany, Norway, Poland, Finland, Spain, UK

4-Amino-3,5-dichloro-alpha-bromoacetophenone 37148-47-3 In Bulk Supply

Cas:37148-47-3

Min.Order:1 Kilogram

Negotiable

Type:Trading Company

inquiry

Hebei Sankai Chemical Technology Co., Ltd

1. Product advantages ♦ High purity, all above 98.5%, no impurities after dissolution ♦ We will test each batch to ensure quality ♦ OEM and private brand services designed for free ♦ Various cap colors available ♦ W

4-Amino-3,5-dichloro-alpha-bromoacetophenone CAS:37148-47-3

Cas:37148-47-3

Min.Order:1 Metric Ton

FOB Price: $380.0 / 590.0

Type:Trading Company

inquiry

Shanghai Upbio Tech Co.,Ltd

1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized

Ethanone,1-(4-amino-3,5-dichlorophenyl)-2-bromo- 37148-47-3

Cas:37148-47-3

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Changchun Artel lmport and Export trade company

Minimum Order Qty. 10 Gram Supply Ability 500 Kilograms/Month Storage store in cool, dry, ventilated place 20℃ Delivery Time 3 business days after payment Payment Term TT,western union,Paypal,MoneyGram Package 10g,20g,50g,100g,500g,1KGS,5KGS,10KGS,25

4-Amino-3,5-dichlorophenacylbromide supplier in China 37148-47-3

Cas:37148-47-3

Min.Order:10 Gram

Negotiable

Type:Trading Company

inquiry

Shanghai Terui OP New Material Technology Co., Ltd.

We generally use secure shipping methods that do not require you to do any customs clearance. Free shipping to your address without worrying about any customs issues. We have a professional customs clearance team to 100% guarantee the safe delivery o

4-Amino-3, 5-Dichloro-Alpha-Bromoacetophenone CAS 37148-47-3 with Good Price

Cas:37148-47-3

Min.Order:1 Kilogram

Negotiable

Type:Trading Company

inquiry

Shanxi Ankesi Biotechnology Co., Ltd

Our Advantage 1. Rich experience We specialize in this filed for many years, our APIs exported to all over the world and and we established long friendly relations of cooperation with our clients. 2. Great quality,purity and favorable Good qual

4-Amino-3, 5-Dichlorophenacylbromide CAS 37148-47-3 AKS

Cas:37148-47-3

Min.Order:1 Kilogram

Negotiable

Type:Trading Company

inquiry

Wuhan Wonda Pharm Limited

1.high quality: quality is life. quality is the most important element for all goods. we have a lab doing research in wuhan china. hplc and nmr is available if needed. 2.reasonable price: we provide high quality products with competi

intermediates 4-Amino-3,5-dichlorophenacylbromide CAS 37148-47-3 with factory price

Cas:37148-47-3

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Hubei Jiutian Bio-medical Technology Co., Ltd

1,we produce and sell good chemicals around the world. 2,our success rate is about 95%. this means, if customer order is accepted, the probability that the customer will obtain the ordered substances, is 95%. 3,our staff consists of highly qualifie

4-Amino-3,5-dichloro-alp ha-bromoacetophenone CAS 37148-47-3

Cas:37148-47-3

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Hebei Quanhe Biotechnology Co. LTD

1. Timely and efficient service to ensure communication with customers 2. Produce products of different specifications and sizes according to your requirements. 3. Quality procedures and standards recognized by SGS. Advanced plant equipment ensures

4-Amino-3,5-dichlorophenacylbromide

Cas:37148-47-3

Min.Order:1 Kilogram

FOB Price: $30.0 / 50.0

Type:Lab/Research institutions

inquiry

Hangzhou Keyingchem Co.,Ltd

Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det

4-Amino-3,5-dichlorophenacylbromide

Cas:37148-47-3

Min.Order:0 Metric Ton

Negotiable

Type:Lab/Research institutions

inquiry

Hefei Zhaobo Technology Co., Ltd.

4-Amino-3,5-dichloro-alpha-bromoacetophenone CAS 37148-47-3 Purity: 99% Min Application: Intermediates Appearance: Powder Package: Bag Delivery: 3-5days Our Advantage & Service 1.Top quality: Using high quality material and establish

4-Amino-3,5-dichloro-alpha-bromoacetophenone CAS 37148-47-3

Cas:37148-47-3

Min.Order:1 Kilogram

FOB Price: $10.0 / 50.0

Type:Trading Company

inquiry

Saiwante (shanghai) New Material Technology Co., Ltd.

Appearance/Colour:Yellow solid Vapor Pressure:1.71E-06mmHg at 25°C Melting Point:142-145 °C Refractive Index:1.643 Boiling Point:396.4 °C at 760 mmHg PKA:-2.21±0.10(Predicted) Flash Point:193.6 °C PSA:43.0900

the best price 37148-47-3 4-Amino-3,5-dichlorophenacylbromide

Cas:37148-47-3

Min.Order:1 Gram

FOB Price: $5.0

Type:Trading Company

inquiry

SHENGZHIKAI TECHNOLOGY INDUSTRY CO., LTD

Company Profile SHENGZHIKAI TECHNOLOGY INDUSTRY CO., LTD is a high-tech enterprise dedicated to the fields of fine chemical products.The scope of products covers pharmaceutical intermediates, plant extracts, chemical reagent, animal p

High Purity 4-Amino-3,5-dichloro-alpha-bromoacetophenone CAS 37148-47-3

Cas:37148-47-3

Min.Order:1 Kilogram

FOB Price: $8.0 / 10.0

Type:Trading Company

inquiry

SHANGHAI SYSTEAM BIOCHEM CO., LTD

We are one of a few suppliers that can offer custom synthesis service of this product We are specialized in custom synthesis, chemical/pharmaceutical/ pesticides outsourcing and contract research. We are committed to prov

1-(4-Amino-3,5-dichlorophenyl)-2-bromoethanone

Cas:37148-47-3

Min.Order:100 Gram

FOB Price: $100.0 / 2000.0

Type:Lab/Research institutions

inquiry

Henan Tianfu Chemical Co., Ltd.

Our company was built in 2009 with an ISO certificate.In the past 5 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so on.O

4-Amino-3,5-dichloro-alpha-bromoacetophenone

Cas:37148-47-3

Min.Order:1 Kilogram

FOB Price: $20.0

Type:Lab/Research institutions

inquiry

Xiamen Jenny Chemical Technology Co., Ltd.

GMP standard, high purity, competitive price, in stock 1. Quick Response: within 6 hours after receiving your email. 2. Quality Guarantee: All products are strictly tested by our QC, confirmed by QA, and approved by a third-party lab in China, USA,

4-Amino-3,5-dichlorophenacylbromide

Cas:37148-47-3

Min.Order:1 Milligram

Negotiable

Type:Trading Company

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Synthetic route

1-(4-amino-3,5-dichlorophenyl)-1-ethanone
37148-48-4

1-(4-amino-3,5-dichlorophenyl)-1-ethanone

1-(4-amino-3,5-dichlorophenyl)-2-bromoethan-1-one
37148-47-3

1-(4-amino-3,5-dichlorophenyl)-2-bromoethan-1-one

Conditions
ConditionsYield
With bromine at 20℃; for 3h;95.2%
Stage #1: 1-(4-amino-3,5-dichlorophenyl)-1-ethanone With bromine In chloroform for 0.5h; Reflux; Inert atmosphere;
Stage #2: With triethylamine; phosphonic acid diethyl ester In tetrahydrofuran at 0 - 20℃; for 0.166667h; Inert atmosphere;
89%
Stage #1: 1-(4-amino-3,5-dichlorophenyl)-1-ethanone With bromine In tetrahydrofuran; chloroform for 0.416667h; Reflux;
Stage #2: With diethyl phosphite; triethylamine In tetrahydrofuran at 20℃; for 0.166667h;
89%
2,6-Dichloroaniline
608-31-1

2,6-Dichloroaniline

1-(4-amino-3,5-dichlorophenyl)-2-bromoethan-1-one
37148-47-3

1-(4-amino-3,5-dichlorophenyl)-2-bromoethan-1-one

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: iron(III) chloride / chloroform / 6 h / 0 - 20 °C
2: bromine / 3 h / 20 °C
View Scheme
4-Aminoacetophenone
99-92-3

4-Aminoacetophenone

1-(4-amino-3,5-dichlorophenyl)-2-bromoethan-1-one
37148-47-3

1-(4-amino-3,5-dichlorophenyl)-2-bromoethan-1-one

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: N-chloro-succinimide / acetonitrile / 4.5 h / 20 °C
2: copper(ll) bromide / ethyl acetate; chloroform; ethanol / 2 h / Reflux
View Scheme
1,1,1,3,3,3-hexadeuterio-2-(trideuteriomethyl)propan-2-amine
6045-08-5

1,1,1,3,3,3-hexadeuterio-2-(trideuteriomethyl)propan-2-amine

1-(4-amino-3,5-dichlorophenyl)-2-bromoethan-1-one
37148-47-3

1-(4-amino-3,5-dichlorophenyl)-2-bromoethan-1-one

4-amino-α-D9-tert-butylamine-3,5-dichloroacetophenone hydrochloride

4-amino-α-D9-tert-butylamine-3,5-dichloroacetophenone hydrochloride

Conditions
ConditionsYield
In acetonitrile at 20℃; for 6h; Solvent;96%
With N-ethyl-N,N-diisopropylamine In chloroform for 3h; Reflux;72%
1-(4-amino-3,5-dichlorophenyl)-2-bromoethan-1-one
37148-47-3

1-(4-amino-3,5-dichlorophenyl)-2-bromoethan-1-one

2-Amino-2-methyl-1-propanol
124-68-5

2-Amino-2-methyl-1-propanol

1-(4-amino-3,5-dichlorophenyl)-2-(1-hydroxy-2-methylpropan-2-ylamino)ethanone

1-(4-amino-3,5-dichlorophenyl)-2-(1-hydroxy-2-methylpropan-2-ylamino)ethanone

Conditions
ConditionsYield
In chloroform at 20℃; for 2h;91%
N-Methyl-2-amino-2-methyl-1-propanol
27646-80-6

N-Methyl-2-amino-2-methyl-1-propanol

1-(4-amino-3,5-dichlorophenyl)-2-bromoethan-1-one
37148-47-3

1-(4-amino-3,5-dichlorophenyl)-2-bromoethan-1-one

2-(4-amino-3,5-dichlorophenyl)-4,5,5-trimethylmorpholin-2-ol
1242652-49-8

2-(4-amino-3,5-dichlorophenyl)-4,5,5-trimethylmorpholin-2-ol

Conditions
ConditionsYield
In chloroform at 20℃; for 2h;91%
1-(4-amino-3,5-dichlorophenyl)-2-bromoethan-1-one
37148-47-3

1-(4-amino-3,5-dichlorophenyl)-2-bromoethan-1-one

3-aminoterephthalic acid
10312-55-7

3-aminoterephthalic acid

2-aminoterephthalic acid bis-[2-(4-amino-3,5-dichlorophenyl)-2-oxo-ethyl] ester

2-aminoterephthalic acid bis-[2-(4-amino-3,5-dichlorophenyl)-2-oxo-ethyl] ester

Conditions
ConditionsYield
With potassium carbonate In N,N-dimethyl-formamide for 1h;90%
thioanthranilic acid
32187-15-8

thioanthranilic acid

1-(4-amino-3,5-dichlorophenyl)-2-bromoethan-1-one
37148-47-3

1-(4-amino-3,5-dichlorophenyl)-2-bromoethan-1-one

S-[2-(4-amino-3,5-dichlorophenyl)-2-oxoethyl]-2-aminobenzenecarbothioate

S-[2-(4-amino-3,5-dichlorophenyl)-2-oxoethyl]-2-aminobenzenecarbothioate

Conditions
ConditionsYield
With triethylamine In N,N-dimethyl-formamide at 20℃; for 1h;90%
1-(4-amino-3,5-dichlorophenyl)-2-bromoethan-1-one
37148-47-3

1-(4-amino-3,5-dichlorophenyl)-2-bromoethan-1-one

sodium diformamide
18197-26-7

sodium diformamide

C10H8Cl2N2O3

C10H8Cl2N2O3

Conditions
ConditionsYield
In acetonitrile at 70℃; for 2h;88.1%
1-(4-amino-3,5-dichlorophenyl)-2-bromoethan-1-one
37148-47-3

1-(4-amino-3,5-dichlorophenyl)-2-bromoethan-1-one

2-amino-benzene-1,4-dicarboxylic acid,4-methyl ester
85743-02-8

2-amino-benzene-1,4-dicarboxylic acid,4-methyl ester

1-[2-(4-amino-3,5-dichlorophenyl)-2-oxoethyl]-4-methyl-2-aminoterephthalate

1-[2-(4-amino-3,5-dichlorophenyl)-2-oxoethyl]-4-methyl-2-aminoterephthalate

Conditions
ConditionsYield
With sodium hydrogencarbonate In N,N-dimethyl-formamide at 20℃;82%
acetylguanidine
5699-40-1

acetylguanidine

1-(4-amino-3,5-dichlorophenyl)-2-bromoethan-1-one
37148-47-3

1-(4-amino-3,5-dichlorophenyl)-2-bromoethan-1-one

N-(4-(4-amino-3,5-dichlorophenyl)-1H-imidazol-2-yl)acetamide

N-(4-(4-amino-3,5-dichlorophenyl)-1H-imidazol-2-yl)acetamide

Conditions
ConditionsYield
In acetonitrile at 100℃; for 3h;81%
In acetonitrile at 100℃; for 3h;81%
1-(4-amino-3,5-dichlorophenyl)-2-bromoethan-1-one
37148-47-3

1-(4-amino-3,5-dichlorophenyl)-2-bromoethan-1-one

isopropylamine
75-31-0

isopropylamine

1-(4-amino-3,5-dichloro)-2-isopropylaminoethanone

1-(4-amino-3,5-dichloro)-2-isopropylaminoethanone

Conditions
ConditionsYield
at 20℃; for 6h;80.2%
1-(4-amino-3,5-dichlorophenyl)-2-bromoethan-1-one
37148-47-3

1-(4-amino-3,5-dichlorophenyl)-2-bromoethan-1-one

d7-isopropylamine

d7-isopropylamine

D7-1-(4-amino-3,5-dichloro)-2-isopropylaminoethanone

D7-1-(4-amino-3,5-dichloro)-2-isopropylaminoethanone

Conditions
ConditionsYield
for 3h; Reflux;79.5%
1-(4-amino-3,5-dichlorophenyl)-2-bromoethan-1-one
37148-47-3

1-(4-amino-3,5-dichlorophenyl)-2-bromoethan-1-one

anthranilic acid
118-92-3

anthranilic acid

2-Amino-benzoic acid 2-(4-amino-3,5-dichloro-phenyl)-2-oxo-ethyl ester

2-Amino-benzoic acid 2-(4-amino-3,5-dichloro-phenyl)-2-oxo-ethyl ester

Conditions
ConditionsYield
With sodium hydrogencarbonate In N,N-dimethyl-formamide 1.) 90 - 100 deg C, 2.) 25 - 28 deg C, 1 h;79%
1-(4-amino-3,5-dichlorophenyl)-2-bromoethan-1-one
37148-47-3

1-(4-amino-3,5-dichlorophenyl)-2-bromoethan-1-one

thiourea
17356-08-0

thiourea

4-(4-amino-3,5-dichlorophenyl)thiazol-2-amine

4-(4-amino-3,5-dichlorophenyl)thiazol-2-amine

Conditions
ConditionsYield
In water at 20℃; for 2h;76%
In water at 20℃; for 2h;76%
1-(4-amino-3,5-dichlorophenyl)-2-bromoethan-1-one
37148-47-3

1-(4-amino-3,5-dichlorophenyl)-2-bromoethan-1-one

2-mercapto-6-methylpyrimidin-4(3H)-one
56-04-2

2-mercapto-6-methylpyrimidin-4(3H)-one

2-((2-(4-amino-3,5-dichlorophenyl)-2-oxoethyl)thio)-6-methylpyrimidin-4(3H)-one

2-((2-(4-amino-3,5-dichlorophenyl)-2-oxoethyl)thio)-6-methylpyrimidin-4(3H)-one

Conditions
ConditionsYield
Stage #1: 2-mercapto-6-methylpyrimidin-4(3H)-one With potassium hydroxide In methanol at 22 - 25℃; under 760.014 Torr; for 0.25h; Inert atmosphere;
Stage #2: 1-(4-amino-3,5-dichlorophenyl)-2-bromoethan-1-one In methanol at 22 - 25℃; under 760.014 Torr; for 12h; Inert atmosphere;
71%
3-aminophthalic acid
5434-20-8

3-aminophthalic acid

1-(4-amino-3,5-dichlorophenyl)-2-bromoethan-1-one
37148-47-3

1-(4-amino-3,5-dichlorophenyl)-2-bromoethan-1-one

C24H17Cl4N3O6

C24H17Cl4N3O6

Conditions
ConditionsYield
With triethylamine In N,N-dimethyl-formamide at 20℃; for 2h;68%
1-(4-amino-3,5-dichlorophenyl)-2-bromoethan-1-one
37148-47-3

1-(4-amino-3,5-dichlorophenyl)-2-bromoethan-1-one

2-mercaptopyrimidin-4(3H)-one
141-90-2

2-mercaptopyrimidin-4(3H)-one

2-((2-(4-amino-3,5-dichlorophenyl)-2-oxoethyl)thio)-pyrimidin-4(3H)-one

2-((2-(4-amino-3,5-dichlorophenyl)-2-oxoethyl)thio)-pyrimidin-4(3H)-one

Conditions
ConditionsYield
Stage #1: 2-mercaptopyrimidin-4(3H)-one With potassium hydroxide In methanol at 22 - 25℃; under 760.014 Torr; for 0.25h; Inert atmosphere;
Stage #2: 1-(4-amino-3,5-dichlorophenyl)-2-bromoethan-1-one In methanol at 22 - 25℃; under 760.014 Torr; for 12h; Inert atmosphere;
68%
1,1,1,3,3,3-hexadeuterio-2-(trideuteriomethyl)propan-2-amine
6045-08-5

1,1,1,3,3,3-hexadeuterio-2-(trideuteriomethyl)propan-2-amine

1-(4-amino-3,5-dichlorophenyl)-2-bromoethan-1-one
37148-47-3

1-(4-amino-3,5-dichlorophenyl)-2-bromoethan-1-one

clenbuterol-D9

clenbuterol-D9

Conditions
ConditionsYield
Stage #1: 1,1,1,3,3,3-hexadeuterio-2-(trideuteriomethyl)propan-2-amine; 1-(4-amino-3,5-dichlorophenyl)-2-bromoethan-1-one With tetrabutylammomium bromide In dichloromethane at 30℃; for 5h;
Stage #2: With sodium tetrahydroborate In dichloromethane at 20℃; for 5h;
57.8%
monoethyl phthalate
2306-33-4

monoethyl phthalate

1-(4-amino-3,5-dichlorophenyl)-2-bromoethan-1-one
37148-47-3

1-(4-amino-3,5-dichlorophenyl)-2-bromoethan-1-one

o-phthalic acid 1-[2-(4-amino-3,5-dichlorophenyl)-2-oxoethyl] ester 2-ethyl ester

o-phthalic acid 1-[2-(4-amino-3,5-dichlorophenyl)-2-oxoethyl] ester 2-ethyl ester

Conditions
ConditionsYield
With triethylamine In acetone for 0.5h; Heating;52%
1-(4-amino-3,5-dichlorophenyl)-2-bromoethan-1-one
37148-47-3

1-(4-amino-3,5-dichlorophenyl)-2-bromoethan-1-one

cyanoacetic acid
372-09-8

cyanoacetic acid

C11H8Cl2N2O3
1078715-64-6

C11H8Cl2N2O3

Conditions
ConditionsYield
With 1,8-diazabicyclo[5.4.0]undec-7-ene In N,N-dimethyl-formamide at 0℃; for 5h;51%
(2,3-dihydrobenzo[1,4]dioxin-2-ylmethyl)amine
4442-59-5

(2,3-dihydrobenzo[1,4]dioxin-2-ylmethyl)amine

1-(4-amino-3,5-dichlorophenyl)-2-bromoethan-1-one
37148-47-3

1-(4-amino-3,5-dichlorophenyl)-2-bromoethan-1-one

1-(4-amino-3,5-dichlorophenyl)-2-(1,4-benzodioxan-2-methylamino)etanone hydrochloride

1-(4-amino-3,5-dichlorophenyl)-2-(1,4-benzodioxan-2-methylamino)etanone hydrochloride

Conditions
ConditionsYield
In methanol for 6h; Heating;50%
hydrogen ethyl malonate
1071-46-1

hydrogen ethyl malonate

1-(4-amino-3,5-dichlorophenyl)-2-bromoethan-1-one
37148-47-3

1-(4-amino-3,5-dichlorophenyl)-2-bromoethan-1-one

C13H13Cl2NO5
1078715-65-7

C13H13Cl2NO5

Conditions
ConditionsYield
With sodium hydroxide In N,N-dimethyl-formamide at 0℃; for 1h;43%
<(β,β,β,β',β',β'-D6)isopropyl>amine
55432-59-2

<(β,β,β,β',β',β'-D6)isopropyl>amine

1-(4-amino-3,5-dichlorophenyl)-2-bromoethan-1-one
37148-47-3

1-(4-amino-3,5-dichlorophenyl)-2-bromoethan-1-one

(d6)-1-(4-amino-3,5-dichlorophenyl)-2-(isopropylamino)ethan-1-one

(d6)-1-(4-amino-3,5-dichlorophenyl)-2-(isopropylamino)ethan-1-one

Conditions
ConditionsYield
In chloroform at 63℃; for 5h; Sealed tube;37.4%
1-(4-amino-3,5-dichlorophenyl)-2-bromoethan-1-one
37148-47-3

1-(4-amino-3,5-dichlorophenyl)-2-bromoethan-1-one

tert-butylamine
75-64-9

tert-butylamine

clenbuterol
37148-27-9

clenbuterol

Conditions
ConditionsYield
Stage #1: 1-(4-amino-3,5-dichlorophenyl)-2-bromoethan-1-one; tert-butylamine In tetrahydrofuran; ethanol at 0 - 20℃; for 4h; Inert atmosphere;
Stage #2: With potassium borohydride In tetrahydrofuran; ethanol for 2h; Cooling with ice;
Stage #3: With methanol In tetrahydrofuran; ethanol at 20℃; for 16h;
35%
morpholine
110-91-8

morpholine

1-(4-amino-3,5-dichlorophenyl)-2-bromoethan-1-one
37148-47-3

1-(4-amino-3,5-dichlorophenyl)-2-bromoethan-1-one

1-(4-amino-3,5-dichloro-phenyl)-2-morpholin-4-yl-ethanol
37163-03-4

1-(4-amino-3,5-dichloro-phenyl)-2-morpholin-4-yl-ethanol

Conditions
ConditionsYield
(i), (ii) NaBH4; Multistep reaction;
1,1,1,3,3,3-hexadeuterio-2-(trideuteriomethyl)propan-2-amine
6045-08-5

1,1,1,3,3,3-hexadeuterio-2-(trideuteriomethyl)propan-2-amine

1-(4-amino-3,5-dichlorophenyl)-2-bromoethan-1-one
37148-47-3

1-(4-amino-3,5-dichlorophenyl)-2-bromoethan-1-one

4-amino-α-D9-tert-butylamino-3,5-dichloroacetophenone

4-amino-α-D9-tert-butylamino-3,5-dichloroacetophenone

Conditions
ConditionsYield
In chloroform for 2h; Heating;
1-(4-amino-3,5-dichlorophenyl)-2-bromoethan-1-one
37148-47-3

1-(4-amino-3,5-dichlorophenyl)-2-bromoethan-1-one

3-(4-amino-3,5-dichlorobenzoyl)-4-hydroxyisochromen-1-one

3-(4-amino-3,5-dichlorobenzoyl)-4-hydroxyisochromen-1-one

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 52 percent / triethylamine / acetone / 0.5 h / Heating
2: 82 percent / KOH / 1-methyl-pyrrolidin-2-one / 2 h / 45 °C
View Scheme
1-(4-amino-3,5-dichlorophenyl)-2-bromoethan-1-one
37148-47-3

1-(4-amino-3,5-dichlorophenyl)-2-bromoethan-1-one

4-amino-3,5-dichloro-α-(1,4-benzodioxan-2-methylaminomethyl)benzenemethanol hydrochloride

4-amino-3,5-dichloro-α-(1,4-benzodioxan-2-methylaminomethyl)benzenemethanol hydrochloride

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 50 percent / methanol / 6 h / Heating
2: 58 percent / sodium borohydride / methanol; H2O / 1.) 0 deg C; 2.) rt, 1 h
View Scheme
(R)-1-methyl-3-(4-aminocarbonylphenyl)propylamine

(R)-1-methyl-3-(4-aminocarbonylphenyl)propylamine

1-(4-amino-3,5-dichlorophenyl)-2-bromoethan-1-one
37148-47-3

1-(4-amino-3,5-dichlorophenyl)-2-bromoethan-1-one

p-[(R)-3-[bis-[(RS)-4-amino-3,5-dichloro-β-hydroxyphenethyl]amino]butyl]benzamide

p-[(R)-3-[bis-[(RS)-4-amino-3,5-dichloro-β-hydroxyphenethyl]amino]butyl]benzamide

Conditions
ConditionsYield
With sodium borohydrid; ammonia In methanol; chloroform; water
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