bulk production ProName: 4-Chloro-4'-fluorobutyrophenone CasNo: 3874-54-2 Molecular Formula: C10H10ClFO Appearance: white powder Application: Chemical,Pharmacetical,OLED intermedia... DeliveryTime: in stock, deliver aga
Cas:3874-54-2
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inquiryWelcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our
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inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
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inquiryAs a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem’s R&D center offer custom synthesis according to the contract research and development services for t
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inquiryProduct Description Product website: http://www.finerchem.com Product Name 4-Chloro-4'-fluorobutyrophenone CAS No. 3874-54-2
Cas:3874-54-2
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inquiryOur advantages: 1, High quality with competitive price: 1) Standard:BP/USP/EP/Enterprise standard 2) All Purity≥99% 3) We are manufacturer and can provide high quality products with factory price. 2, Fast and safe delivery 1) Parcel can
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inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
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inquiry1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized
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inquiry4-Chloro-4'-fluorobutyrophenone CAS:3874-54-2 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high qualit
Cas:3874-54-2
Min.Order:1 Gram
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inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
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inquiryAdvantage : LIDE PHARMACEUTICALS LTD. is a mid-small manufacturing-type enterprise, engaged in pharmaceutical intermediates of R&D, custom-made and production, and also involving trading chemicals for export. We have established the R&
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inquiryCompany information: Hebei Mojin Biotechnology Co., Ltd, Our company is a professional in chemical raw materials and chemical reagents research and development production enterprises. Our business covers more than 30 countries, most of the big cust
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
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inquiryBest quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia
Appearance: light yellow liquid Storage:Store in a cool,dry place and keep away from direct strong light Package:As customer request Application:Used for research and industrial manufacture. Transportation:Common products:Sea/Ai
Cas:3874-54-2
Min.Order:100 Metric Ton
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inquiryCompany Introduction 1. Established in 2005, with two independent business divisions: Fine chemicals division; Pharmaceutical division. 2. Main product: Optical brightener Textile auxiliary Dye stuff Pigments
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Min.Order:1 Gram
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Type:Lab/Research institutions
inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
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inquiryOur Advantage: 1. Rich experience We specialize in this filed for many years, our APIs exported to all over the world and and we established long friendly relations of cooperation with our clients. 2. Great quality,purity and favorable Good quali
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inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
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inquiryEstablished in 2010, located in Hangzhou Qinglan science park, lingruichem is a technical company mainly focus on the Custom synthesis, manufacturing, sales of chemicals to various industries. In our R&D centre, we have a staff of skilled and experie
Superior quality, moderate price & quick delivery. Appearance:colourless or light yellow liquid Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:25kg/drum, or as per your request. Application:Used for APIs Tra
Cas:3874-54-2
Min.Order:1 Kilogram
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Type:Trading Company
inquiryProduct name: 4-Chloro-4’-Fluoro Butyrophenone CAS No.:3874-54-2 Molecule Formula:C10H10ClFO Molecule Weight:200.63 Purity: 99% Package: 25kg/drum Description:Yellow or light yellow liquid Manufacture Standards:Enterprise Standard
Cas:3874-54-2
Min.Order:1 Kilogram
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Type:Lab/Research institutions
inquiryOur company was built in 2009 with an ISO certificate. In the past 5 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so o
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Min.Order:1 Kilogram
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Type:Lab/Research institutions
inquiryHangzhou Huarong Pharm Co., Ltd. established since 2009 , has been always focusing on supplying products and services to our clients in the field of small molecule drug. Huarong Pharm has built platforms for the research, development and manufac
Cas:3874-54-2
Min.Order:1 Gram
FOB Price: $1.0 / 2.0
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inquiryProduct Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
Cas:3874-54-2
Min.Order:1 Gram
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inquirySynonyms: GAMMA-CHLORO-4-FLUOROBUTYROPHENONE;GAMMA-CHLORO-P-FLUOROBUTYROPHENONE;G-CHLORO-P-FLUOROBUTYROPHENONE;AKOS BBS-00006481;4-CHLORO-1-(4-FLUOROPHENYL)-1-BUTANONE;4-CHLORO-1-(4-FLUOROPHENYL)-1-OXOBUTANE;4-CHLORO-4'-FLUOROBUTYROPHENONE;4-CH
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Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryZhenyu biotech exported this product to many countries and regions at best price. if you are looking for the material's manufacturer or supplier in china, zhenyu biotech is your best choice. pls contact with us freely for getting detailed
Cas:3874-54-2
Min.Order:1 Kilogram
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inquiryMelting point 5-6 ° C Boiling point: 130-132 ° C (0.97513 mmHg) Density: 1.22 g / ml at 25 ° C (lit.) Refractive index n 20 / D 1.5255 (lit.) Flash point > 230 ° F Appearance:Slightly yellow-greenish clear oil Storage:Sealed in
Cas:3874-54-2
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryZhejiang Jiuzhou Chem Co., Ltd is a national high-and new-tech enterprise specialized in the research, manufacturing of APIs and intermediates. Our company has passed the ISO9001 quality system and established an image as a provider of high qua
Cas:3874-54-2
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inquiryfluorobenzene
4-Chlorobutanoyl chloride
4-(4-fluorophenyl)-4-oxo-n-butyl chloride
Conditions | Yield |
---|---|
With aluminum (III) chloride In dichloromethane at 20℃; for 4h; Time; | 90% |
With aluminium trichloride In carbon disulfide at 20℃; for 2h; | 73.2% |
With aluminium trichloride |
4-chloro-1-(4-fluorophenyl)-1,1-(ethylenedioxy)butane
4-(4-fluorophenyl)-4-oxo-n-butyl chloride
Conditions | Yield |
---|---|
In(OSO2CF3)3 In acetone at 100℃; for 0.0833333h; microwave irradiation; | 89% |
4-flourophenylmagnesium bromide
4-Chlorobutanoyl chloride
4-(4-fluorophenyl)-4-oxo-n-butyl chloride
Conditions | Yield |
---|---|
Stage #1: 4-Chlorobutanoyl chloride With 1-methyl-pyrrolidin-2-one In toluene at 0℃; for 0.5h; Stage #2: 4-flourophenylmagnesium bromide In tetrahydrofuran; toluene at -10 - 0℃; for 4.25h; chemoselective reaction; | 88% |
1-(4-chlorobut-1-yn-1-yl)-4-fluorobenzene
4-(4-fluorophenyl)-4-oxo-n-butyl chloride
Conditions | Yield |
---|---|
With iron(III) chloride; water; silver(I) triflimide In 1,4-dioxane for 18h; regioselective reaction; | 85% |
With water; bis(trifluoromethanesulfonyl)amide In 1,4-dioxane at 100℃; | 85% |
With water In 1,4-dioxane at 80 - 120℃; regioselective reaction; | 85% |
1-(4-fluorophenyl)cyclobutan-1-ol
4-(4-fluorophenyl)-4-oxo-n-butyl chloride
Conditions | Yield |
---|---|
With manganese(II) triflate; tetrabutylammonium acetate; acetic acid; magnesium chloride In acetonitrile at 25℃; for 3.5h; Inert atmosphere; Electrochemical reaction; Sealed tube; | 84% |
With 1,10-Phenanthroline; tert-butylhypochlorite; silver trifluoromethanesulfonate In acetonitrile at 20℃; for 6h; Inert atmosphere; Schlenk technique; regioselective reaction; | 81% |
4-chlorobutyraldehyde
1-Bromo-4-fluorobenzene
4-(4-fluorophenyl)-4-oxo-n-butyl chloride
Conditions | Yield |
---|---|
With Quinuclidine; 4,4'-di-tert-butyl-2,2'-bipyridine nickel(II) bromide; [Ir(C6H2F2-C5H3NCF3)2(4,4′-di-tert-butyl-2,2′-dipyridyl)]; potassium carbonate In 1,4-dioxane at 20℃; for 20h; Inert atmosphere; Sealed tube; Irradiation; | 77% |
With palladium diacetate; 9,10-phenanthrenequinone; potassium hydrogencarbonate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene In acetone at 20℃; for 24h; Reagent/catalyst; Irradiation; | 71% |
1-iodo-3-chloro-propane
4-fluoroboronic acid
molybdenum hexacarbonyl
4-(4-fluorophenyl)-4-oxo-n-butyl chloride
Conditions | Yield |
---|---|
Stage #1: 1-iodo-3-chloro-propane; 4-fluoroboronic acid With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In water; benzene at 20℃; for 24h; Suzuki-Miyaura Coupling; Inert atmosphere; Irradiation; Stage #2: molybdenum hexacarbonyl With 1,8-diazabicyclo[5.4.0]undec-7-ene In acetonitrile at 70℃; Suzuki-Miyaura Coupling; Inert atmosphere; | 68% |
1-ethynyl-4-fluorobenzene
3-chloropropionyl peroxide
4-(4-fluorophenyl)-4-oxo-n-butyl chloride
Conditions | Yield |
---|---|
With iron(III) trifluoromethanesulfonate; trifluorormethanesulfonic acid In tetrahydrofuran at 70 - 80℃; for 12.25h; Inert atmosphere; Schlenk technique; | 60% |
3-chloro-4'-fluoropropiophenone
diethyl 4-chloromethyl-1,4-dihydro-2,6-dimethylpyridine-3,5-dicarboxylate
4-(4-fluorophenyl)-4-oxo-n-butyl chloride
Conditions | Yield |
---|---|
With manganese; di-tert-butyl peroxide; α,α,α-trifluorotoluene at 100℃; for 48h; Inert atmosphere; | 51% |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: iodine; magnesium / tetrahydrofuran / Inert atmosphere; Reflux; Sealed tube 1.2: 0 - 20 °C / Inert atmosphere; Sealed tube 2.1: acetic acid; manganese(II) triflate; magnesium chloride; tetrabutylammonium acetate / acetonitrile / 3.5 h / 25 °C / Inert atmosphere; Electrochemical reaction; Sealed tube View Scheme |
para-thiocresol
4-(4-fluorophenyl)-4-oxo-n-butyl chloride
1-(4-fluorophenyl)-4-(p-tolylthio)butan-1-one
Conditions | Yield |
---|---|
100% | |
With triethylamine In tetrahydrofuran for 16h; Ambient temperature; | 99% |
N-methoxylamine hydrochloride
4-(4-fluorophenyl)-4-oxo-n-butyl chloride
4-chloro-1-(4-fluorophenyl)butan-1-one O-methyl oxime
Conditions | Yield |
---|---|
With pyridine at 20℃; | 100% |
Conditions | Yield |
---|---|
With sodium hydroxide In water at 60℃; for 5h; | 100% |
Conditions | Yield |
---|---|
With triethylamine In tetrahydrofuran | 99% |
With triethylamine In tetrahydrofuran | 99% |
Conditions | Yield |
---|---|
With triethylamine In tetrahydrofuran | 99% |
ethylene glycol
4-(4-fluorophenyl)-4-oxo-n-butyl chloride
4-chloro-1-(4-fluorophenyl)-1,1-(ethylenedioxy)butane
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid In water; toluene for 16h; Inert atmosphere; Reflux; | 98% |
With toluene-4-sulfonic acid In benzene for 18h; Heating; | 93% |
With toluene-4-sulfonic acid In benzene for 15h; Heating; | 90% |
Conditions | Yield |
---|---|
With sodium hydrogencarbonate; sodium iodide In acetonitrile for 22h; Reflux; | 96% |
4-(4-fluorophenyl)-4-oxo-n-butyl chloride
(+/-)-4-chloro-1-(4-fluorophenyl)butan-1-ol
Conditions | Yield |
---|---|
With sodium tetrahydroborate In ethanol at 0℃; for 7h; | 95% |
With sodium tetrahydroborate In ethanol at 0 - 20℃; for 3h; | 94% |
With sodium tetrahydroborate In ethanol at 0 - 20℃; for 12h; | 93% |
4-(4-fluorophenyl)-4-oxo-n-butyl chloride
1-iodo-3-(p-fluorophenylcarbonyl)propane
Conditions | Yield |
---|---|
With sodium iodide In butanone for 3h; Heating; | 95% |
With sodium iodide In acetone for 24h; Reflux; | 92% |
With sodium iodide In acetone for 16h; Reflux; | 77% |
In sodium iodide; butanone | |
With sodium iodide In [(2)H6]acetone for 8h; Reflux; |
4-(4-fluorophenyl)-4-oxo-n-butyl chloride
4-(n-butyl)fluorobenzene
Conditions | Yield |
---|---|
With nickel In tetrahydrofuran for 15h; Heating; | 95% |
4-(4-fluorophenyl)-4-oxo-n-butyl chloride
C10H10FN3O
Conditions | Yield |
---|---|
With sodium azide In N,N-dimethyl-formamide | 95% |
With sodium azide; potassium iodide In N,N-dimethyl-formamide at 90℃; |
4-(4-fluorophenyl)-4-oxo-n-butyl chloride
(S)-2-methylpropane-2-sulfinamide
(S,E)-N-(4-chloro-1-(4-fluorophenyl)butylidene)-2-methylpropane-2-sulfinamide
Conditions | Yield |
---|---|
With titanium (IV) ethoxide In tetrahydrofuran at 65℃; for 48h; Inert atmosphere; | 94% |
4-(4-fluorophenyl)-4-oxo-n-butyl chloride
Conditions | Yield |
---|---|
Stage #1: 4-(4-fluorophenyl)-4-oxo-n-butyl chloride With C32H33FeN3O2Si; 4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane In toluene at -40 - 20℃; for 2h; Schlenk technique; Glovebox; Stage #2: With potassium carbonate In methanol; toluene at 20℃; for 12h; Schlenk technique; Glovebox; enantioselective reaction; | 94% |
4-(4-fluorophenyl)-4-oxo-n-butyl chloride
1-Phenyl-1,3,8-triaza-spiro[4.5]decan-4-one
spiperone
Conditions | Yield |
---|---|
With diisopropylamine In N,N-dimethyl-formamide at 80℃; for 17h; Inert atmosphere; | 93% |
With triethylamine; potassium iodide In acetonitrile for 20h; Heating; | 74% |
With triethylamine; potassium iodide In acetonitrile for 20h; Inert atmosphere; Reflux; | 63% |
4-(4-fluorophenyl)-4-oxo-n-butyl chloride
potassium thioacetate
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide at 0 - 20℃; for 10h; Inert atmosphere; | 92% |
4-(4-fluorophenyl)-4-oxo-n-butyl chloride
(1R)-(+)-4-chloro-1-(4-fluorophenyl)butan-1-ol
Conditions | Yield |
---|---|
With B-chlorodiisopinocampheylborane In diethyl ether at -25℃; for 16h; | 90% |
With C22H27Cl2CoN3O; sodium triethylborohydride; 4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane In tetrahydrofuran at 20℃; for 2h; Inert atmosphere; enantioselective reaction; | 87% |
Stage #1: 4-(4-fluorophenyl)-4-oxo-n-butyl chloride With Triethoxysilane; (S,E)-(+)-2,6-diisopropyl-N-(2-((2-(4-phenyl-4,5-dihydrooxazol-2-yl)phenyl)amino)benzylidene)aniline; sodium triethylborohydride; cobalt(II) chloride In tetrahydrofuran; dichloromethane at 20℃; for 15h; Schlenk technique; Inert atmosphere; Stage #2: With potassium carbonate In tetrahydrofuran; methanol; dichloromethane at 20℃; for 2h; Schlenk technique; Inert atmosphere; enantioselective reaction; | 75% |
Multi-step reaction with 2 steps 1: 81 percent / NaBH4 / methanol / 4 °C View Scheme | |
With B-chlorodiisopinocampheylborane In tetrahydrofuran; diethyl ether; 2,2'-iminobis[ethanol] at 25℃; |
4-(4-fluorophenyl)-4-oxo-n-butyl chloride
(1S)-(-)-4-chloro-1-(4-fluorophenyl)butan-1-ol
Conditions | Yield |
---|---|
With (-)-diisopinocamphenylborane chloride In diethyl ether at -25℃; for 16h; | 90% |
Multi-step reaction with 2 steps 1: 81 percent / NaBH4 / methanol / 4 °C View Scheme | |
With (-)-diisopinocamphenylborane chloride In tetrahydrofuran; diethyl ether; 2,2'-iminobis[ethanol] at 25℃; |
4-fluorobenzylic alcohol
4-(4-fluorophenyl)-4-oxo-n-butyl chloride
cyclopropyl-[4-(4-fluoro-benzyloxy)-phenyl]-methanone
Conditions | Yield |
---|---|
With tetrabutylammomium bromide; sodium hydride In tetrahydrofuran at 30℃; for 18h; | 90% |
4-(4-fluorophenyl)-4-oxo-n-butyl chloride
Conditions | Yield |
---|---|
Stage #1: 4-(4-fluorophenyl)-4-oxo-n-butyl chloride With (S)-2,2',6,6'-tetramethoxy-4,4'-bis(diphenylphosphino)-3,3'-bipyridine; phenylsilane; copper(II) acetate monohydrate In toluene at -20 - 20℃; for 48h; Stage #2: With hydrogenchloride In water; toluene Reagent/catalyst; enantioselective reaction; | 90% |
Conditions | Yield |
---|---|
With methyllithium lithium bromide In tetrahydrofuran; diethyl ether at -78℃; for 0.0833333h; Inert atmosphere; | 90% |
Conditions | Yield |
---|---|
With potassium carbonate In dimethyl sulfoxide at 140℃; | 90% |
4-(4-fluorophenyl)-4-oxo-n-butyl chloride
1-(4-chlorobutyl)-4-fluorobenzene
Conditions | Yield |
---|---|
With triethylsilane; trifluoroacetic acid at 0℃; for 2h; | 89% |
With hydrogen; palladium on activated charcoal In ethanol | |
With hydrogenchloride; mercury dichloride; zinc In toluene for 5h; Reflux; | |
With triethylsilane In trifluoroacetic acid |
4-(4-fluorophenyl)-4-oxo-n-butyl chloride
4-flourophenylmagnesium bromide
δ-Hydroxy-δ-bis(p-fluorophenyl)butyl chloride
Conditions | Yield |
---|---|
In diethyl ether Heating; | 88.4% |
4-hydroxy-4-phenylpiperidin
4-(4-fluorophenyl)-4-oxo-n-butyl chloride
1-(4-fluorophenyl)-4-(4-hydroxy-4-phenylpiperidin-1-yl)butan-1-one
Conditions | Yield |
---|---|
With sodium hydrogencarbonate; potassium iodide In toluene for 24h; Reflux; | 88% |
With potassium iodate; potassium carbonate In toluene Inert atmosphere; | 27% |
With toluene; potassium iodide |
4-(4-chlorophenyl)-4-hydroxypiperidine
4-(4-fluorophenyl)-4-oxo-n-butyl chloride
haloperidol
Conditions | Yield |
---|---|
With potassium carbonate; potassium iodide In acetonitrile at 75℃; for 24h; Temperature; | 88% |
With potassium iodide In toluene for 45h; Reflux; | 85% |
With potassium iodide In toluene at 130℃; for 45h; Sealed tube; | 79% |
1-(4-chlorophenyl)-1,4-diazepane
4-(4-fluorophenyl)-4-oxo-n-butyl chloride
Conditions | Yield |
---|---|
With potassium carbonate; potassium iodide In 1,2-dimethoxyethane for 18h; Heating; | 87% |
[bis(acetoxy)iodo]benzene
4-(4-fluorophenyl)-4-oxo-n-butyl chloride
C12H12ClFO3
Conditions | Yield |
---|---|
With tetrabutylammomium bromide; potassium hydroxide In 1,4-dioxane at 20℃; for 1h; | 87% |
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