Dayangchem's R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantities
Cas:52-86-8
Min.Order:1 Kilogram
FOB Price: $3.0
Type:Lab/Research institutions
inquiryWe can provide GMP validation service that complies with SFDA, FDA, WHO and EU EMPA.Excellent registration team could help us easlily to register our products in different countries.If you and your customer are interested in some products or need C
Cas:52-86-8
Min.Order:1 Gram
Negotiable
Type:Manufacturers
inquirygood quality Appearance:white powder Storage:cold storage Package:meet the demand of customer Application:diagnostic reagent Transportation:by sea or by air Port:Shanghai, Qingdao Port
The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s
Cas:52-86-8
Min.Order:1 Gram
FOB Price: $0.1
Type:Manufacturers
inquiryShanghai Seasonsgreen Chemical is a high-tech research and development, production, sale and custom synthesis set in one high-tech chemical products enterprises. Our sales and marketing division is located in Shanghai, serving international pharmaceu
Cas:52-86-8
Min.Order:1 Kilogram
FOB Price: $1.0
Type:Manufacturers
inquiryOur main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
Name: Haloperidol Synonyms: haloperidol; haloperidol; haloperidol; 1-(4-fluorophenyl) -4-[4-(4-chlorophenyl) -4-hydroxy-1-piperidinyl]-1-butanone; iohexol impurity J; haloperidol; haloperidol; haloperidol; methanol test standard (halop
Cas:52-86-8
Min.Order:25 Kilogram
FOB Price: $1.0 / 2.0
Type:Other
inquiryWith our good experience, we offer detailed technical support and advice to assist customers. We communicate closely with customers to establish their quality requirements. Consistent Quality Our plant has strict quality control in each manufacturin
WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
Cas:52-86-8
Min.Order:10 Gram
FOB Price: $146.0 / 176.0
Type:Trading Company
inquiryAdvantage : LIDE PHARMACEUTICALS LTD. is a mid-small manufacturing-type enterprise, engaged in pharmaceutical intermediates of R&D, custom-made and production, and also involving trading chemicals for export. We have established the R&
Cas:52-86-8
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiryProduct Name: Haloperidol Synonyms: 1-(3-p-Fluorobenzoylpropyl)-4-p-chlorophenyl-4-hydroxypiperidine;1-Butanone, 4-[4-(4-chlorophenyl)-4-hydroxy-1-piperidinyl]-1-(4-fluorophenyl)-;1-butanone,4-(4-(4
Advantages: Hubei XinRunde Chemical Co., Ltd is a renowned pharmaceutical manufacturer. We can offer high quality products at competitive price in quick delivery with 100% custom pass guaranteed. Never stop striving to offer our best s
Cas:52-86-8
Min.Order:10 Gram
Negotiable
Type:Other
inquiry1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized
Cas:52-86-8
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryHaloperidol CAS: 52-86-8 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic intermediates,
Cas:52-86-8
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
Cas:52-86-8
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiryWe have overseas warehouses in California, New Laredo Mexico, Vancouver Canada, Amsterdam Netherlands, and Melbourne Australia. Overseas warehouses can provide some of the best-selling products. We look forward to the cooperation of local powerful
Cas:52-86-8
Min.Order:1 Kilogram
Negotiable
Type:Trading Company
inquiryOur Services 1. New Molecules R&D 2. Own test center HPLC NMR GC LC-MS 3. API and Intermediates from China reputed manufacturers 4. Documents support COA MOA MSDS DMF open part Our advantages 1. Government awarded company. Top 100 enter
Our advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We have s
Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
Haloperidol CAS 52-86-8 Purity: 99% Min Application: Intermediates Appearance: Powder Package: Bag Delivery: 3-5days Our Advantage & Service 1.Top quality: Using high quality material and establishing a strict quality control system,
Cas:52-86-8
Min.Order:1 Kilogram
FOB Price: $10.0 / 50.0
Type:Trading Company
inquiryOur Strengths 1.Place of Origin China with Super quality by reasonable price. 2.Fast delivery by safe express way to all the country. 3.Has a number of highly qualified engineers and experts to provide guidance for reagents. 4.When you meet problems
Cas:52-86-8
Min.Order:1 Kilogram
FOB Price: $10.0 / 20.0
Type:Trading Company
inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:52-86-8
Min.Order:10 Gram
FOB Price: $100.0
Type:Lab/Research institutions
inquiryHaloperidolAppearance:white powder Storage:Keep away of light, cool place Package:according to customers' requirements Application:pharmaceutical intermediates Transportation:By air(EMS or EUB or FedEx or TNT ect...) or by sea(FOB or CIF or CNF ect..
superior quality Appearance:White Crystalline Powder Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:1kg/bag, 1kg/drum or 25kg/drum or as per your request. Application:Antidyskinetic; antipsychotic Transportation:
Established in May 2015, TaiChem Ltd. is initially invested by a British research and development company and started by PhDs back from aboard. The company is registered in China Medical City (CMC), Taizhou, Jiangsu Province, and the production site
1. Product advantages ♦ High purity, all above 98.5%, no impurities after the dissolution ♦ We will test each batch to ensure quality ♦ OEM and private brand services designed for free ♦ Various cap colors available &diam
Cas:52-86-8
Min.Order:1 Kilogram
FOB Price: $7.0 / 10.0
Type:Trading Company
inquiryOur Advantages A. International Top level TechnologyOur company owned biomedicine experts are famous at home and abroad with rich experience in research and development in the field of efficient chiral functional molecules research and development an
4-(4-chlorophenyl)-1-<4-(4-nitrophenyl)-4-oxobutyl>-4-piperidinol
haloperidol
Conditions | Yield |
---|---|
With tetrabutyl ammonium fluoride In dimethyl sulfoxide at 160℃; for 0.166667h; Inert atmosphere; Microwave irradiation; Anhydrous conditions; | 99% |
With hydrogen fluoride; potassium oxalate; potassium carbonate; [2.2.2]cryptande | 65% |
With hydrogen fluoride; potassium oxalate; potassium carbonate; [2.2.2]cryptande In dimethyl sulfoxide at 160℃; for 0.333333h; | 60% |
4-(4-chlorophenyl)-4-hydroxypiperidine
4-(4-fluorophenyl)-4-oxo-n-butyl chloride
haloperidol
Conditions | Yield |
---|---|
With potassium carbonate; potassium iodide In acetonitrile at 75℃; for 24h; Temperature; | 88% |
With potassium iodide In toluene for 45h; Reflux; | 85% |
With potassium iodide In toluene at 130℃; for 45h; Sealed tube; | 79% |
4-<4-(4-chlorophenyl)-4-hydroxypiperidino>-1,1-ethylenedioxy-1-(4-fluorophenyl)butane
haloperidol
Conditions | Yield |
---|---|
With hydrogenchloride In methanol for 6h; Heating; | 65% |
With hydrogenchloride In methanol for 2h; Heating; | 65% |
4-fluorophenyl trifluoromethanesulfonate
haloperidol
Conditions | Yield |
---|---|
With 2,2,6,6-tetramethyl-piperidine; bis(1,5-cyclooctadiene)nickel (0); acetone; [2-((diphenylphospino)methyl)-2-methyl-1,3-propanediyl]bis[diphenylphosphine] In toluene at 130℃; for 20h; Inert atmosphere; | 37% |
Chlorohaloperidol
haloperidol
Conditions | Yield |
---|---|
With hydrogen fluoride; tetra(n-butyl)ammonium hydroxide |
4-(4-chlorophenyl)-4-hydroxypiperidine
haloperidol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 78 percent / acetic acid; NaCNBH3 / methanol / 30 h / 20 °C 2: 65 percent / conc. HCl / methanol / 2 h / Heating View Scheme | |
Multi-step reaction with 2 steps 1: K2CO3, KI / dimethylformamide / 17.5 h / 100 °C 2: 65 percent / conc. HCl / methanol / 6 h / Heating View Scheme | |
Multi-step reaction with 2 steps 1: potassium iodide / toluene / 48 h / Reflux; Inert atmosphere 2: bis(1,5-cyclooctadiene)nickel (0); [2-((diphenylphospino)methyl)-2-methyl-1,3-propanediyl]bis[diphenylphosphine]; acetone; 2,2,6,6-tetramethyl-piperidine / toluene / 20 h / 130 °C / Inert atmosphere View Scheme |
methyl 3-(4-fluorobenzoyl)-propionate
haloperidol
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: 83 percent / p-TsOH / benzene / 20 h / Heating 2: 93 percent / DIBAL-H / CH2Cl2; tetrahydrofuran / 1 h / -78 °C 3: 78 percent / acetic acid; NaCNBH3 / methanol / 30 h / 20 °C 4: 65 percent / conc. HCl / methanol / 2 h / Heating View Scheme |
3-[2-(4-fluorophenyl)-[1,3]dioxolan-2-yl]propionaldehyde
haloperidol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 78 percent / acetic acid; NaCNBH3 / methanol / 30 h / 20 °C 2: 65 percent / conc. HCl / methanol / 2 h / Heating View Scheme |
3-[2-(4-fluorophenyl)-[1,3]dioxolan-2-yl]propionic acid methyl ester
haloperidol
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 93 percent / DIBAL-H / CH2Cl2; tetrahydrofuran / 1 h / -78 °C 2: 78 percent / acetic acid; NaCNBH3 / methanol / 30 h / 20 °C 3: 65 percent / conc. HCl / methanol / 2 h / Heating View Scheme |
(4-aminophenyl)(cyclopropyl)methanone
haloperidol
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: 1) HBF4, NaNO2, 2) Cu, NaNO2 / 1) H2O, 30 min, 2) H2O, 1 h 2: 75 percent / conc. HCl / methanol / 0.5 h / 120 °C 3: 31 percent / KI / toluene / 100 - 110 °C 4: 60 percent / HF, potassium carbonate, potassium oxalate, kryptofix 222 / dimethylsulfoxide / 0.33 h / 160 °C View Scheme |
1-(4-acetylaminophenyl)-4-chloro-1-butanone
haloperidol
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1: 90 percent / 4 M NaOH / ethanol / 2 h / Heating 2: 1) HBF4, NaNO2, 2) Cu, NaNO2 / 1) H2O, 30 min, 2) H2O, 1 h 3: 75 percent / conc. HCl / methanol / 0.5 h / 120 °C 4: 31 percent / KI / toluene / 100 - 110 °C 5: 60 percent / HF, potassium carbonate, potassium oxalate, kryptofix 222 / dimethylsulfoxide / 0.33 h / 160 °C View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 6 steps 1: 20 percent / AlCl3 / CS2 / room temperature, 30 min; 60 deg C, 2 h 2: 90 percent / 4 M NaOH / ethanol / 2 h / Heating 3: 1) HBF4, NaNO2, 2) Cu, NaNO2 / 1) H2O, 30 min, 2) H2O, 1 h 4: 75 percent / conc. HCl / methanol / 0.5 h / 120 °C 5: 31 percent / KI / toluene / 100 - 110 °C 6: 60 percent / HF, potassium carbonate, potassium oxalate, kryptofix 222 / dimethylsulfoxide / 0.33 h / 160 °C View Scheme |
cyclopropyl(4-nitrophenyl)methanone
haloperidol
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 75 percent / conc. HCl / methanol / 0.5 h / 120 °C 2: 31 percent / KI / toluene / 100 - 110 °C 3: 60 percent / HF, potassium carbonate, potassium oxalate, kryptofix 222 / dimethylsulfoxide / 0.33 h / 160 °C View Scheme |
4-chloro-4'-nitrobutyrophenone
haloperidol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 31 percent / KI / toluene / 100 - 110 °C 2: 60 percent / HF, potassium carbonate, potassium oxalate, kryptofix 222 / dimethylsulfoxide / 0.33 h / 160 °C View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: p-toluenesulfonic acid / benzene / 12 h / Heating 2: K2CO3, KI / dimethylformamide / 17.5 h / 100 °C 3: 65 percent / conc. HCl / methanol / 6 h / Heating View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: K2CO3, KI / dimethylformamide / 17.5 h / 100 °C 2: 65 percent / conc. HCl / methanol / 6 h / Heating View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: AlCl3 2: toluene View Scheme |
4-Brom-4-(4-chlor-phenyl)-piperidin
haloperidol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: NaOH-solution; water 2: toluene View Scheme |
reduced haloperidol
haloperidol
Conditions | Yield |
---|---|
With manganese dioxide In chloroform |
1-(4-chlorobut-1-yn-1-yl)-4-fluorobenzene
haloperidol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: iron(III) chloride; water; silver(I) triflimide / 1,4-dioxane / 18 h 2: potassium iodide / toluene / 25 h / 125 °C View Scheme | |
Multi-step reaction with 2 steps 1: bis(trifluoromethanesulfonyl)amide; water / 1,4-dioxane / 100 °C 2: potassium iodide; sodium hydrogencarbonate / toluene / 100 °C View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: iodine; magnesium / tetrahydrofuran / 4 h / 60 - 70 °C / Inert atmosphere 1.2: 6 h / 30 °C / Inert atmosphere 1.3: 3 h / 60 °C / Inert atmosphere 2.1: hydrogen; palladium on activated charcoal / water / 24 h / 25 °C / 750.08 Torr 3.1: potassium carbonate; potassium iodide / acetonitrile / 24 h / 75 °C View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: iodine; magnesium / tetrahydrofuran / 4 h / 60 - 70 °C / Inert atmosphere 1.2: 6 h / 30 °C / Inert atmosphere 1.3: 3 h / 60 °C / Inert atmosphere 2.1: hydrogen; palladium on activated charcoal / water / 24 h / 25 °C / 750.08 Torr 3.1: potassium carbonate; potassium iodide / acetonitrile / 24 h / 75 °C View Scheme |
N-benzyl-4-(4-chlorophenyl)-4-hydroxypiperidin
haloperidol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: hydrogen; palladium on activated charcoal / water / 24 h / 25 °C / 750.08 Torr 2: potassium carbonate; potassium iodide / acetonitrile / 24 h / 75 °C View Scheme |
haloperidol
Conditions | Yield |
---|---|
With tris(pentafluorophenyl)borate; water-d2 In toluene at 100℃; for 12h; Inert atmosphere; regioselective reaction; | 97% |
With [(N,N′-bis(2,6-diisopropylphenyl)-2,3-butanediimine)Ni(μ−H)]2; deuterium at -196 - 80℃; under 760.051 Torr; for 24h; Reagent/catalyst; Sealed tube; | 32 mg |
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In dichloromethane for 24h; Inert atmosphere; | 96.7% |
haloperidol
Conditions | Yield |
---|---|
With perfluoro-cis-2-n-butyl-3-n-propyloxaziridine; HCFC-225ca,cb In dichloromethane at -60℃; for 0.333333h; | 96% |
In CaH2; dichloromethane | 71% |
haloperidol
Conditions | Yield |
---|---|
With bis(η3-allyl-μ-chloropalladium(II)); 1-deuteriodiphenylmethanol; 3-(2,6-dibenzhydryl-4-methylphenyl)-4,5-dimethyl-1-(2,4,6-trimethylbenzyl)imidazolium chloride; caesium carbonate In toluene at 90℃; for 16h; Inert atmosphere; | 94% |
Conditions | Yield |
---|---|
In methanol; chloroform at 20℃; for 0.75h; | 93% |
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide for 5h; Heating; | 92% |
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide for 5h; Heating; | 92% |
Conditions | Yield |
---|---|
With C17H24N5Ru(1+)*F6P(1-); potassium acetate; potassium carbonate In 1-methyl-pyrrolidin-2-one at 35℃; for 48h; Inert atmosphere; | 92% |
haloperidol
3-trifluoromethylaniline
1-(4-fluorophenyl)-4-(4-hydroxy-4-(4-((3-(trifluoromethyl)phenyl)amino)phenyl)piperidin-1-yl)butan-1-one
Conditions | Yield |
---|---|
With Pd-PEPPSI-(2,6-(3-pentyl)pentylphenyl-2H-imidazol-2-ylidene)Cl-o-picoline; caesium carbonate In 1,2-dimethoxyethane at 45℃; for 24h; Buchwald-Hartwig Coupling; Inert atmosphere; Glovebox; | 91% |
haloperidol
reduced haloperidol
Conditions | Yield |
---|---|
With sodium tetrahydroborate In methanol at 20℃; for 1.33333h; | 90% |
With sodium tetrahydroborate In ethanol at 0 - 20℃; | 90% |
With human liver dihydrodiol dehydrogenase 1; NADPH In phosphate buffer at 25℃; pH=6.0; Enzyme kinetics; Further Variations:; Reagents; |
Conditions | Yield |
---|---|
Stage #1: haloperidol With copper diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl In tetrahydrofuran for 0.0833333h; Inert atmosphere; Stage #2: 1,2-propanediene With (dimethoxy)methylsilane In tetrahydrofuran at 20℃; for 12h; Inert atmosphere; | 90% |
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide for 3h; Ambient temperature; | 89% |
Conditions | Yield |
---|---|
In methanol; chloroform at 20℃; for 0.75h; | 89% |
haloperidol
Conditions | Yield |
---|---|
With [(N,N’-bis(1R,2R,3R,5S)-(−)-isopinocampheyl-1,2-ethanediimine-radical)NiI(μ2-H)]2; deuterium at -196 - 80℃; under 760.051 Torr; for 24h; Reagent/catalyst; Sealed tube; | 89% |
Conditions | Yield |
---|---|
With trifluoroborane diethyl ether In methanol; hexane; dichloromethane; ethyl acetate | 88% |
haloperidol
Conditions | Yield |
---|---|
Stage #1: haloperidol With C40H55Cl5N3Pd In toluene at 0℃; for 0.0833333h; Negishi Coupling; Inert atmosphere; Cooling with ice; Stage #2: 1-ethylpropylzinc bromide In tetrahydrofuran; toluene at 23℃; for 16h; Inert atmosphere; | 88% |
Conditions | Yield |
---|---|
In tetrahydrofuran for 2h; Solvent; Temperature; Inert atmosphere; Reflux; | 88% |
haloperidol
Conditions | Yield |
---|---|
With C37H40MnN2O2P2(1+)*Br(1-); sodium t-butanolate In isopropyl alcohol; toluene at 50℃; for 6h; Inert atmosphere; Schlenk technique; enantioselective reaction; | 85% |
haloperidol
B
4-<4-hydroxy-4-(4-aminophenyl)piperidinyl>-1-(4-fluorophenyl)butanone
Conditions | Yield |
---|---|
With C46H71Cl3N2Pd; ammonia; sodium t-butanolate In 1,4-dioxane at 80℃; for 2h; Inert atmosphere; Schlenk technique; | A n/a B 84% |
haloperidol
4-(4-chlorophenyl)-1-<4-(4-fluorophenyl)-4-oxobutyl>-1,2,3,6-tetrahydopyridine
Conditions | Yield |
---|---|
With hydrogenchloride; acetic acid for 24h; Reflux; Inert atmosphere; | 84% |
haloperidol
Conditions | Yield |
---|---|
Stage #1: N-tert-butyldimethylsilyl-S-fluoromethyl-S-(2-pyridyl)sulfoximine With potassium hexamethylsilazane In tetrahydrofuran at -78℃; for 0.5h; Inert atmosphere; Stage #2: haloperidol In tetrahydrofuran at -78℃; for 3h; Inert atmosphere; stereoselective reaction; | 82% |
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide for 3h; Heating; | 80% |
haloperidol
2-(aminooxy)-N,N-diethylethanamine dihydrochloride
Conditions | Yield |
---|---|
With pyridine In ethanol for 32h; Heating; | 76.9% |
Conditions | Yield |
---|---|
With sodium amide for 1h; Heating; | 75% |
haloperidol
4-(4'-chlorophenyl)-1-(4'-(4-fluorophenyl)butyl)piperidin-4-ol
Conditions | Yield |
---|---|
With [(C6H6)(PCy3)(CO)RuH]+*BF4−; hydrogen; phenol In 1,4-dioxane; isopropyl alcohol under 1520.1 Torr; for 12h; Inert atmosphere; Glovebox; Schlenk technique; chemoselective reaction; | 68% |
haloperidol
Conditions | Yield |
---|---|
With pyridine In ethanol for 32h; Heating; | 67.7% |
3-(tert-butyloxycarbonylamino)propionic acid
haloperidol
C29H36ClFN2O5
Conditions | Yield |
---|---|
Stage #1: 3-(tert-butyloxycarbonylamino)propionic acid; haloperidol With dmap In dichloromethane for 0.5h; Cooling with ice; Stage #2: With dicyclohexyl-carbodiimide In dichloromethane at 20℃; for 25h; Cooling with ice; | 64.6% |
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