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Cas:3916-44-7
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inquiry4-HYDROXY-4'-NITROBIPHENYL CAS:3916-44-7 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality or
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inquiryProduct Detail Minimum Order Qty. 10 Gram
Cas:3916-44-7
Min.Order:10 Gram
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inquiry4-Hydroxy-4'-nitrobiphenyl CAS: 3916-44-7 Specification Item Standard Identification A.H-NMR:Comply with the structure B.LC-MS:Comply with the structure C.The
Cas:3916-44-7
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Cas:3916-44-7
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inquiryProduct Name: 4-HYDROXY-4'-NITROBIPHENYL Synonyms: 4'-Nitro[1,1'-biphenyl]-4-ol;TIMTEC-BB SBB008411;4-HYDROXY-4'-NITROBIPHENYL;4'-NITRO-4-BIPHENY
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para-nitrophenyl bromide
4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenol
4-(4-nitrophenyl)phenol
Conditions | Yield |
---|---|
With sodium phosphate; palladium on activated charcoal In water; isopropyl alcohol at 20℃; for 8h; Suzuki-Miyaura cross-coupling; | 95% |
With tetrakis(triphenylphosphine) palladium(0); sodium carbonate In tetrahydrofuran; water; toluene at 80℃; for 5h; Suzuki Coupling; Inert atmosphere; |
Conditions | Yield |
---|---|
With potassium carbonate In ethanol; water at 20℃; for 1h; Suzuki-Miyaura Coupling; | 95% |
Conditions | Yield |
---|---|
Stage #1: 4-(benzoyloxy)-4'-nitrobiphenyl With potassium carbonate In ethanol; water at 80℃; for 24h; Stage #2: With hydrogenchloride; water In ethanol | 72% |
With potassium hydroxide |
p-nitrobenzene iodide
1,4-Phenyldiboronic acid
A
4-(4-nitrophenyl)phenol
B
p,p-dinitro-p-terphenyl
Conditions | Yield |
---|---|
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In 1,2-dimethoxyethane at 80℃; for 16h; | A 20% B 66% |
Conditions | Yield |
---|---|
With tetrakis(triphenylphosphine) palladium(0); sodium carbonate In tetrahydrofuran; water; toluene at 80℃; for 5h; Suzuki Coupling; Inert atmosphere; | 62.7% |
(4-Nitrophenyl)acetylene
2-(trimethylsiloxy)cyclohexa-1,3-diene
4-(4-nitrophenyl)phenol
Conditions | Yield |
---|---|
Stage #1: (4-Nitrophenyl)acetylene; 2-(trimethylsiloxy)cyclohexa-1,3-diene at 140℃; for 2h; Diels-Alder reaction; Stage #2: With potassium carbonate In methanol for 0.166667h; Further stages.; | 40% |
Conditions | Yield |
---|---|
With hydrogenchloride Diazotization.nachf. Behandeln mit verd. Schwefelsaeure und Zersetzen des Diazoniumsulfats mit Wasserdampf; | |
Stage #1: With sulfuric acid; sodium nitrite In water at 0℃; for 0.666667h; Diazotization; Stage #2: 4-amino-4'-nitrobiphenyl With water for 3h; Hydrolysis; Heating; |
Conditions | Yield |
---|---|
With hydrogen bromide; acetic acid at 120℃; |
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: pyridine / 0.5 h / 20 °C 2: acetic acid; nitric acid / 80 - 90 °C 3: potassium hydroxide / ethanol; water / Reflux View Scheme | |
Multi-step reaction with 4 steps 1: triethylamine / tetrahydrofuran / 24 h / 0 - 20 °C 2: acetic acid; nitric acid / tetrahydrofuran / 0.5 h / 85 - 90 °C 3: potassium hydroxide / ethanol; water / 0.5 h / Reflux 4: hydrogenchloride / water View Scheme | |
Multi-step reaction with 3 steps 1: triethylamine / dichloromethane 2: sodium nitrite; acetic acid; nitric acid 3: potassium hydroxide; water / ethanol View Scheme |
4-(4-nitrophenyl)phenol
Conditions | Yield |
---|---|
With hydrogenchloride In water |
Conditions | Yield |
---|---|
With palladium diacetate; potassium carbonate In N,N-dimethyl-formamide Suzuki-Miyaura Coupling; |
Conditions | Yield |
---|---|
With tetrakis(triphenylphosphine) palladium(0); sodium carbonate In tetrahydrofuran; water; toluene at 80℃; for 5h; Suzuki Coupling; Inert atmosphere; |
Conditions | Yield |
---|---|
With triethylamine at 20℃; for 1.5h; | 100% |
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 80℃; for 2h; | 99% |
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 90℃; for 7h; | 95% |
Conditions | Yield |
---|---|
With hydrogen; palladium on activated charcoal In ethanol | 94% |
With hydrogen; palladium on activated charcoal In ethyl acetate at 20℃; under 1861.73 Torr; for 18h; | 93% |
Zinin reduction; |
Conditions | Yield |
---|---|
With sodium hydride In N,N-dimethyl-formamide at 20℃; | 93% |
Conditions | Yield |
---|---|
With sodium hydroxide In N,N-dimethyl-formamide for 36h; Heating; | 93% |
Conditions | Yield |
---|---|
With potassium carbonate In acetone for 48h; Heating / reflux; | 89% |
Conditions | Yield |
---|---|
Stage #1: 4-(4-nitrophenyl)phenol With sodium hydride In N,N-dimethyl-formamide at 20℃; for 0.25h; Stage #2: N,N-Dimethylthiocarbamoyl chloride In N,N-dimethyl-formamide at 60℃; for 1.25h; | 81% |
Conditions | Yield |
---|---|
With potassium carbonate In acetone at 65℃; for 48h; | 73% |
4-(4-nitrophenyl)phenol
n-hexadecanoyl chloride
4'-nitrobiphenyl-4-yl palmitoylsulfamate
Conditions | Yield |
---|---|
Stage #1: 4-(4-nitrophenyl)phenol With formic acid; isocyanate de chlorosulfonyle In N,N-dimethyl acetamide at 0 - 20℃; for 3.16667h; Inert atmosphere; Stage #2: n-hexadecanoyl chloride With dmap; triethylamine In dichloromethane; N,N-dimethyl-formamide at 0 - 20℃; Inert atmosphere; | 65% |
4-(4-nitrophenyl)phenol
3-quinuclidinol
3-[(4'-nitro-1,1'-biphenyl-4-yl)oxy]quinuclidine
Conditions | Yield |
---|---|
With di-isopropyl azodicarboxylate; triphenylphosphine In tetrahydrofuran at 20℃; for 48h; | 62% |
With di-isopropyl azodicarboxylate; triphenylphosphine In tetrahydrofuran at 20℃; for 48h; | 62% |
With di-isopropyl azodicarboxylate; triphenylphosphine In tetrahydrofuran at 20℃; for 48h; | 62% |
With di-isopropyl azodicarboxylate; triphenylphosphine In tetrahydrofuran at 20℃; for 48h; | 62% |
With di-isopropyl azodicarboxylate; triphenylphosphine In tetrahydrofuran at 20℃; for 48h; | 62% |
Conditions | Yield |
---|---|
With potassium carbonate In acetone at 65℃; for 48h; | 62% |
4-(4-nitrophenyl)phenol
4-nitrobiphenyl-4'-ferrocenyl benzoate
Conditions | Yield |
---|---|
With 4-dimethylaminopyridine; dicyclohexylcarbodiimide In dichloromethane under dry N2, stirring at room temp. for 72 h; soln. was filtered, solvent was removed, residue was chromd., ppt. was recrystd. from MeOH-CH2Cl2; elem. anal.; | 59% |
4-(4-nitrophenyl)phenol
chloroacetic acid ethyl ester
ethyl 4'-nitrobiphenyl-4-yloxyacetate
Conditions | Yield |
---|---|
With potassium carbonate; sodium iodide In acetone for 2h; Heating; | 44% |
Conditions | Yield |
---|---|
With sodium hydroxide In ethanol at 60℃; for 20h; | 40% |
4-(4-nitrophenyl)phenol
hexamethylenetetramine
A
4-hydroxy-4'-nitro-1,1'-biphenyl-3-carbaldehyde
Conditions | Yield |
---|---|
With trifluoroacetic acid at 125℃; for 72h; Duff Aldehyde Synthesis; Inert atmosphere; Sealed tube; | A 30% B 33% |
4-(4-nitrophenyl)phenol
2.6-Dinitro-4-(4-nitro-phenyl)-phenol
Conditions | Yield |
---|---|
With nitric acid; acetic acid | |
Multi-step reaction with 2 steps 1: glacial acetic acid; sodium nitrite 2: bei der Nitrierung View Scheme |
4-(4-nitrophenyl)phenol
3.4'-dinitro-4-oxy-diphenyl
Conditions | Yield |
---|---|
With acetic acid; sodium nitrite |
4-(4-nitrophenyl)phenol
3-bromo-4'-nitro-biphenyl-4-ol
Conditions | Yield |
---|---|
With chloroform; bromine |
4-(4-nitrophenyl)phenol
acetic acid-(4'-nitro-biphenyl-4-yl ester)
4-(4-nitrophenyl)phenol
Conditions | Yield |
---|---|
With chloroform; bromine |
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