CAS No.40064-34-4,4,4-Piperidinediol hydrochloride Suppliers

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Synthetic route

: piperidin-4-one; hydrochloride sesquiethylate

: 40064-34-4
4-piperidone monohydrochloride monohydrate

Conditions

Conditions	Yield
With hydrogenchloride; water

: 40064-34-4
4-piperidone monohydrochloride monohydrate

: 6092-80-4
phenoxyamine hydrochloride

: 49540-52-5
1,2,3,4-tetrahydro[1]benzofuro[3,2-c]pyridine hydrochloride

Conditions

Conditions	Yield
With hydrogenchloride In isopropyl alcohol	100%

: 40064-34-4
4-piperidone monohydrochloride monohydrate

: 149-73-5
trimethyl orthoformate

: 77542-16-6
4,4-dimethoxypiperidine monohydrochloride

Conditions

Conditions	Yield
With toluene-4-sulfonic acid In methanol at 20℃; for 22h;	100%

: 40064-34-4
4-piperidone monohydrochloride monohydrate

: 76-83-5
trityl chloride

: 112257-60-0
1-triphenylmethyl-4-piperidone

Conditions

Conditions	Yield
With triethylamine In N-methyl-acetamide; water	98.3%
With triethylamine In N,N-dimethyl-formamide at 60℃; for 5h;	70.2%

: 24424-99-5
di-tert-butyl dicarbonate

: 40064-34-4
4-piperidone monohydrochloride monohydrate

: 79099-07-3
N-tert-butyloxycarbonylpiperidin-4-one

Conditions

Conditions	Yield
With sodium hydroxide In 1,4-dioxane; water for 12h; Cooling with ice;	94%
With sodium hydroxide In 1,4-dioxane	92.5%
With triethylamine In dichloromethane; ethyl acetate	86%

: 40064-34-4
4-piperidone monohydrochloride monohydrate

: 497-19-8
sodium carbonate

: 1514-96-1
4-chloro-2-(trifluoromethyl)pyrimidine

: 1-[2-(Trifluoromethyl)-4-pyrimidinyl]-4-piperidone

Conditions

Conditions	Yield
In dichloromethane	92%

: 61380-07-2
2-(thiophen-2-yl)ethyl methanesulfonate

: 40064-34-4
4-piperidone monohydrochloride monohydrate

: 92065-14-0
N-[2-(2-thienyl)ethyl]-4-piperidinone

Conditions

Conditions	Yield
Stage #1: 4-piperidone monohydrochloride monohydrate With N-benzyl-N,N,N-triethylammonium chloride; potassium carbonate In acetonitrile at 60℃; for 1h; Stage #2: 2-(thiophen-2-yl)ethyl methanesulfonate In acetonitrile at 80℃; for 24h; Reagent/catalyst;	90%

: 51417-51-7
7-bromo-1H-indole

: 40064-34-4
4-piperidone monohydrochloride monohydrate

: 312631-09-7
7-bromo-3-piperidin-4-yl-1H-indole

Conditions

Conditions	Yield
	89%

: 2219-51-4
[1,1,2,2-(2)H4]ethane-1,2-diol

: 40064-34-4
4-piperidone monohydrochloride monohydrate

: 84376-17-0
2,2,3,3-tetradeutero-1,4-dioxa-8-azaspiro<4,5>decane

Conditions

Conditions	Yield
In benzene for 48h; Heating;	88%

: C16H15FO2

: 40064-34-4
4-piperidone monohydrochloride monohydrate

: 1-[2′-(2-fluoroethyl)-2-methylbiphenyl-4-carbonyl]-piperidin-4-one

Conditions

Conditions	Yield
Stage #1: C16H15FO2 With 4-methyl-morpholine; 1-[(1-(cyano-2-ethoxy-2-oxoethylidenaminooxy)dimethylamino-morpholino)]-uronium hexafluorophosphate In N,N-dimethyl-formamide for 0.166667h; Cooling with ice; Stage #2: 4-piperidone monohydrochloride monohydrate In N,N-dimethyl-formamide at 0 - 20℃;	88%

: 5825-45-6
1-amino-1,2,3,4-tetrahydroquinoline

: 40064-34-4
4-piperidone monohydrochloride monohydrate

: 5,6,8,9,10,11-hexahydro-4H-pyrido[3',4':4,5]pyrrolo[3,2,1-ij]quinoline

Conditions

Conditions	Yield
With hydrogenchloride	85%

: 5825-45-6
1-amino-1,2,3,4-tetrahydroquinoline

: 40064-34-4
4-piperidone monohydrochloride monohydrate

: 5,6,8,9,10,11-hexahydro-4H-pyrido[3',4':4,5]pyrrolo[3,2,1-ij]quinoline; hydrochloride

Conditions

Conditions	Yield
With hydrogenchloride In ethanol for 3h; Reflux;	85%

: 20667-05-4
2-methyl-1,2-pentanediol

: 40064-34-4
4-piperidone monohydrochloride monohydrate

: 4-piperidone 2-propylpropyleneacetal

Conditions

Conditions	Yield
With p-toluenesulfonic acid monohydrate In toluene	84%

: 448-19-1
4-fluoro-2-methoxy-1-nitrobenzene

: 40064-34-4
4-piperidone monohydrochloride monohydrate

: 761440-64-6
1-(3-methoxy-4 nitrophenyl)piperidin-4-one

Conditions

Conditions	Yield
With N-ethyl-N,N-diisopropylamine In acetonitrile at 80℃; Inert atmosphere;	84%

: 1006-94-6
5-methoxylindole

: 40064-34-4
4-piperidone monohydrochloride monohydrate

: 52157-82-1
4-(5-methoxy-1H-indol-3-yl)piperidine

Conditions

Conditions	Yield
	83%

: 40064-34-4
4-piperidone monohydrochloride monohydrate

: 41840-28-2
S-tert-butoxycarbonyl-4,6-dimethyl-2-mercaptopyrimidine

: 79099-07-3
N-tert-butyloxycarbonylpiperidin-4-one

Conditions

Conditions	Yield
With triethylamine In 1,4-dioxane; water for 6h; Ambient temperature;	81.3%

: 5-(bromomethyl)-2-(2-nitrophenyl)benzo[d]oxazole

: 40064-34-4
4-piperidone monohydrochloride monohydrate

: 1-((2-(2-nitrophenyl)benzo[d]oxazol-5-yl)methyl)piperidin-4-one

Conditions

Conditions	Yield
With acetic anhydride; potassium carbonate In acetonitrile at 20℃; for 5h;	81.2%

: 19335-11-6
1H-indazol-5-ylamine

: 40064-34-4
4-piperidone monohydrochloride monohydrate

: 144-55-8
sodium hydrogencarbonate

: 611-19-8
1-chloro-2-(chloromethyl)benzene

: N-[1-(2-Chlorobenzyl)-4-piperidyl]-N-(1H-5 indazolyl)amine

Conditions

Conditions	Yield
With potassium carbonate; acetic acid In methanol; acetonitrile	80%

: 19335-11-6
1H-indazol-5-ylamine

: 40064-34-4
4-piperidone monohydrochloride monohydrate

: 144-55-8
sodium hydrogencarbonate

: 352-11-4
1-chloromethyl-4-fluorobenzene

: N-[1-(4-Fluorobenzyl)-4-piperidyl]-N-(1H-5-indazolyl)amine

Conditions

Conditions	Yield
With potassium carbonate; acetic acid In methanol; acetonitrile	79%

: 19335-11-6
1H-indazol-5-ylamine

: 40064-34-4
4-piperidone monohydrochloride monohydrate

: 144-55-8
sodium hydrogencarbonate

: 620-20-2
1-Chloro-3-chloromethyl-benzene

: N-[1-(3-Chlorobenzyl)-4-piperidyl]-N-(1H-5-indazolyl)amine

Conditions

Conditions	Yield
With potassium carbonate In methanol; acetonitrile	79%

: 19335-11-6
1H-indazol-5-ylamine

: 40064-34-4
4-piperidone monohydrochloride monohydrate

: 144-55-8
sodium hydrogencarbonate

: 104-83-6
1-Chloro-4-(chloromethyl)benzene

: N-[1-(4-Chlorobenzyl)-4-piperidyl]-N-(1H-5-indazolyl)amine

Conditions

Conditions	Yield
With potassium carbonate; acetic acid In methanol; acetonitrile	79%

: 23468-31-7
6-chloropiperonyl chloride

: 19335-11-6
1H-indazol-5-ylamine

: 40064-34-4
4-piperidone monohydrochloride monohydrate

: 144-55-8
sodium hydrogencarbonate

: N-{1-[(6-Chloro-1,3-benzodioxol-5-yl)methyl]-4-piperidyl}-N-(1H-5-indazolyl)amine

Conditions

Conditions	Yield
With potassium carbonate; acetic acid In methanol; acetonitrile	78%

: 40064-34-4
4-piperidone monohydrochloride monohydrate

: 87-42-3
6-chloro-7H-purine

: 1-(purin-6-yl)piperidin-4-one

Conditions

Conditions	Yield
With triethylamine In N,N-dimethyl-formamide at 50℃; for 2h;	77%

: 19335-11-6
1H-indazol-5-ylamine

: 40064-34-4
4-piperidone monohydrochloride monohydrate

: 144-55-8
sodium hydrogencarbonate

: 104-82-5
4-Methylbenzyl chloride

: N-(1H-5-Indazolyl)-N-[1-(4-methylbenzyl)-4-piperidyl]amine

Conditions

Conditions	Yield
With potassium carbonate; acetic acid In methanol; acetonitrile	76%

: 50709-33-6
2-bromophenylhydrazine hydrochloride

: 40064-34-4
4-piperidone monohydrochloride monohydrate

: 1059630-11-3
6-bromo-2,3,4,5-tetrahydro-1H-pyrido[4,3-b]indole hydrochloric acid salt

Conditions

Conditions	Yield
With hydrogenchloride In ethanol for 6h; Reflux; Inert atmosphere;	76%

: 40064-34-4
4-piperidone monohydrochloride monohydrate

: 5451-40-1
2,6-dichloro-7H-purine

: 1-(2-chloropurin-6-yl)piperidin-4-one

Conditions

Conditions	Yield
With triethylamine In isopropyl alcohol at 60℃; for 2h;	76%

: 19335-11-6
1H-indazol-5-ylamine

: 40064-34-4
4-piperidone monohydrochloride monohydrate

: 144-55-8
sodium hydrogencarbonate

: 836-42-0
4-benzyloxybenzyl chloride

: N-{1-[4-(Benzyloxy)benzyl]-4-piperidyl}-N-(1H-5-indazolyl)amine

Conditions

Conditions	Yield
With potassium carbonate; acetic acid In methanol; acetonitrile	75%

: 19335-11-6
1H-indazol-5-ylamine

: 40064-34-4
4-piperidone monohydrochloride monohydrate

: 144-55-8
sodium hydrogencarbonate

: 824-94-2
p-methoxybenzyl chloride

: N-(1H-5-Indazolyl)-N-[1-(4-methoxybenzyl)-4-piperidyl]amine

Conditions

Conditions	Yield
With potassium carbonate; acetic acid In methanol; acetonitrile	74%

: 948-65-2
2-phenyl-indole

: 40064-34-4
4-piperidone monohydrochloride monohydrate

: 221109-25-7
2-phenyl-3-(1,2,3,6-tetrahydropyridin-4-yl)-1H-indole

Conditions

Conditions	Yield
With phosphoric acid In acetic acid; ethyl acetate	73%

: 92259-86-4
1-amino-2,3-dihydroindole hydrochloride

: 40064-34-4
4-piperidone monohydrochloride monohydrate

: 313666-86-3
4,5,7,8,9,10-hexahydropyrido[4,3-b]pyrrolo[3,2,1-hi]indole

Conditions

Conditions	Yield
In isopropyl alcohol for 4h; Reflux;	73%

: 40064-34-4
4-piperidone monohydrochloride monohydrate

: 72482-64-5
2,4-difluorobenzoyl chloride

: 4-(2,4-difluorobenzoyl)piperidinone

Conditions

Conditions	Yield
With triethylamine In dichloromethane	71%

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