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inquiry2-METHOXYACETOPHENONE CAS:4079-52-1 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic int
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inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
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inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
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inquiryLower price, sample is available,SDS test documents are available,large stock in warehouseAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:Fine chemical intermediates, used as the main raw material for the synthe
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inquiryEthanone,2-methoxy-1-phenyl- cas 4079-52-1Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express
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inquiryCompound sourcing ServicesAgency of testing serviceFactory audit serviceFounded in Dec. 1999, Nanjing Chemlin Chemical Industrial Co.,Ltd(CHEMLIN) has been covering the business scope from trading of chemicals to custom-synthesis & Manufacturing. Co
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inquiryFINETECH INDUSTRY LIMITED is a LONDON based CRO company providing drug discovery & development services to worldwide clients. FINETECH INDUSTRY LIMITED supplies the 2-METHOXYACETOPHENONE, CAS:4079-52-1 with the most competitive price and the best qua
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Debyesci is here who supplied several kinds of chemical products to global pharmaceutical, drug discovery, agrochemical and biotechnology industries for four yearsOur key scientific leadership team has gained experience in top research and developmen
1-phenyl-1,1,2-trimethoxyethane
methoxymethyl phenyl ketone
Conditions | Yield |
---|---|
With hydrogenchloride | 100% |
1-acetoxy-1-fluoro-1-phenyl-2-methoxyethane
methoxymethyl phenyl ketone
Conditions | Yield |
---|---|
With base | 100% |
methanol
acetophenone
A
iodoacetophenone
B
methoxymethyl phenyl ketone
Conditions | Yield |
---|---|
With ammonium iodide; Oxone for 2.3h; Reflux; | A 92% B 6% |
N-methoxy-N-methylbenzamide
chloromethyl methyl ether
methoxymethyl phenyl ketone
Conditions | Yield |
---|---|
With 4,4'-di-tert-butylbiphenyl; lithium In tetrahydrofuran; mineral oil at -78℃; for 2.5h; Inert atmosphere; Schlenk technique; | 91% |
Conditions | Yield |
---|---|
In(OSO2CF3)3 at 20℃; for 0.0333333h; | 90% |
With montmorillonite K-10 | 87% |
at 25℃; for 1h; Green chemistry; | 87% |
Conditions | Yield |
---|---|
With Ph[I(OH)OTf] 18-crown-6 complex monohydrate at -78 - 20℃; for 7h; | 87% |
With C6H6BF4IO*C12H24O6 In dichloromethane at -70 - 20℃; for 4.5h; Reagent/catalyst; Inert atmosphere; | 87% |
With iodosylbenzene; boron trifluoride diethyl etherate at -70 - 25℃; for 3.5h; Mechanism; var. silyl enol ethers; | 78% |
methoxydimethyl((1-phenylvinyl)oxy)silane
methoxymethyl phenyl ketone
Conditions | Yield |
---|---|
With [bis(acetoxy)iodo]benzene In dichloromethane at 25℃; Inert atmosphere; Schlenk technique; | 86% |
1-styrenyloxytrimethylsilane
methyl hypofluorite
methoxymethyl phenyl ketone
Conditions | Yield |
---|---|
In chloroform; acetonitrile at -40 - 20℃; | 85% |
Conditions | Yield |
---|---|
With 2-Picolinic acid; manganese(II) perchlorate hexahydrate; butanedial; dihydrogen peroxide; sodium acetate In acetonitrile at 0 - 20℃; for 1h; | 83% |
With chlorine-triphenylphosphine; dimethyl sulfoxide; triethylamine In dichloromethane at -78 - 20℃; for 3.25h; | 70% |
With bromopentacarbonylmanganese(I); N-methyl-N,N-di(2-pyridylmethyl)amine; acetone; sodium t-butanolate In toluene at 90℃; for 24h; Inert atmosphere; Schlenk technique; Darkness; | 35 %Chromat. |
Conditions | Yield |
---|---|
With tert.-butylhydroperoxide; tetra-(n-butyl)ammonium iodide; toluene-4-sulfonic acid hydrazide In water at 20℃; for 16h; Mechanism; Temperature; Reagent/catalyst; Schlenk technique; | 83% |
Conditions | Yield |
---|---|
With 2-Picolinic acid; manganese(II) perchlorate hexahydrate; butanedial; dihydrogen peroxide; sodium acetate In acetonitrile at 0 - 20℃; for 1h; | A 83% B n/a |
2-methoxyacetonitrile
phenylmagnesium chloride
methoxymethyl phenyl ketone
Conditions | Yield |
---|---|
Stage #1: 2-methoxyacetonitrile; phenylmagnesium chloride With copper(l) iodide In tetrahydrofuran for 0.5h; Reflux; Inert atmosphere; Stage #2: With sulfuric acid In tetrahydrofuran; water at 0 - 20℃; for 18h; Inert atmosphere; | 82% |
Stage #1: 2-methoxyacetonitrile; phenylmagnesium chloride With copper(l) iodide In tetrahydrofuran for 0.5h; Reflux; Stage #2: With sulfuric acid In tetrahydrofuran; water at 20℃; | 15% |
(methoxymethyl)triphenylphosphonium chloride
benzonitrile
methoxymethyl phenyl ketone
Conditions | Yield |
---|---|
Stage #1: (methoxymethyl)triphenylphosphonium chloride With phenyllithium In tetrahydrofuran at 0℃; for 0.166667h; Dehydrochlorination; Stage #2: benzonitrile In tetrahydrofuran at 20℃; for 2h; Alkylation; Stage #3: With water In tetrahydrofuran Hydrolysis; | 81% |
methanol
A
methoxymethyl phenyl ketone
B
2,2-dimethoxy-1-phenylethanone
C
methyl 2-methoxy-2-phenylacetate
Conditions | Yield |
---|---|
With perchloric acid; thallium(III) nitrate at 20℃; for 5h; | A 8% B 80% C 11% |
benzonitrile
(methoxymethyl)diphenylphosphine oxide
methoxymethyl phenyl ketone
Conditions | Yield |
---|---|
With phenyllithium In tetrahydrofuran Alkylation; | 80% |
Conditions | Yield |
---|---|
Stage #1: bromobenzene With iodine; magnesium In tetrahydrofuran at 40 - 70℃; for 3h; Inert atmosphere; Stage #2: 2-methoxyacetonitrile In tetrahydrofuran for 48h; Inert atmosphere; | 80% |
sodium methylate
1-chloroacetophenone
A
methoxymethyl phenyl ketone
B
1-phenyl-2-hydroxyethanone
Conditions | Yield |
---|---|
In methanol at 25℃; Kinetics; Concentration; | A 27.3% B 73.8% |
1-benzoyl-1,3-dimethoxyacetone
methoxymethyl phenyl ketone
Conditions | Yield |
---|---|
With hydrogenchloride In methanol at 50℃; for 20h; | 71% |
methanol
acetophenone
A
benzoic acid methyl ester
B
methoxymethyl phenyl ketone
C
2,2-dimethoxy-1-phenylethanone
D
benzeneacetic acid methyl ester
Conditions | Yield |
---|---|
With perchloric acid; thallium(III) nitrate at 20℃; for 5h; Product distribution; Mechanism; effect of the presence of HClO4; | A 2% B 8% C 2% D 71% |
3-(methoxymethyl)-3-phenyldioxetane
A
2-amino-1,9-dihydro-6H-purin-6-one
B
methoxymethyl phenyl ketone
Conditions | Yield |
---|---|
With 2',3',5'-triacetylguanosine In methanol at 0℃; for 36h; Further byproducts given; | A n/a B 70% C 12% D n/a |
sodium methylate
α-bromoacetophenone
A
methoxymethyl phenyl ketone
B
1-phenyl-2-hydroxyethanone
Conditions | Yield |
---|---|
In methanol at 25℃; Kinetics; Concentration; | A 36.3% B 67.2% |
ethyl 2-methoxyacetate
A
methoxymethyl phenyl ketone
B
1-hydroxy-2-methoxy-1,1-diphenylethane
Conditions | Yield |
---|---|
In diethyl ether at -78 - 20℃; | A 29% B 67% |
methanol
para-methylacetophenone
A
methoxymethyl phenyl ketone
B
methyl p-tolylacetate
Conditions | Yield |
---|---|
With [bis(acetoxy)iodo]benzene; hydrogen cation at 60℃; for 1h; oxidative rearrangement; | A 11% B 67% |
methanol
[bis(acetoxy)iodo]benzene
phenylacetylene
A
2-acetoxyacetophenone
B
methoxymethyl phenyl ketone
C
2-methoxy-1-phenylvinyl acetate
Conditions | Yield |
---|---|
at 70℃; for 12h; | A 66% B 13% C 6% |
Conditions | Yield |
---|---|
With iodosylbenzene; boron trifluoride diethyl etherate Product distribution; other α-metallo ketones; other alcohol; | 65% |
methanol
1-phenylbutan-1,3-dione
A
methoxymethyl phenyl ketone
B
benzeneacetic acid methyl ester
Conditions | Yield |
---|---|
With iodosylbenzene; boron trifluoride diethyl etherate for 8h; Mechanism; Ambient temperature; | A 63% B 24% |
With iodosylbenzene; boron trifluoride diethyl etherate for 8h; Ambient temperature; | A 63% B 24% |
styrene
methanol
A
methoxymethyl phenyl ketone
C
benzaldehyde
Conditions | Yield |
---|---|
With oxygen; magnesium oxide; 9-(2-mesityl)-10-methylacridinium perchlorate In ethyl acetate at 20℃; for 10h; Reagent/catalyst; Time; Solvent; Irradiation; Green chemistry; | A 6 %Spectr. B 63% C 8 %Spectr. |
morpholine
3-(methoxymethyl)-3-phenyldioxetane
A
methoxymethyl phenyl ketone
Conditions | Yield |
---|---|
In dichloromethane at 0℃; for 0.2h; | A 1% B 62% |
3-(methoxymethyl)-3-phenyldioxetane
A
methoxymethyl phenyl ketone
Conditions | Yield |
---|---|
With morpholine In dichloromethane at 0℃; for 0.2h; | A 1% B 62% |
methanol
acetophenone
A
methoxymethyl phenyl ketone
B
benzeneacetic acid methyl ester
Conditions | Yield |
---|---|
With [bis(acetoxy)iodo]benzene at 60℃; for 1h; | A 17% B 59% |
With [hydroxy(tosyloxy)]iodobenzene for 36h; Mechanism; Ambient temperature; var. p-substituted acetophenones, other reagents; | A 10% B 57% |
With [hydroxy(tosyloxy)]iodobenzene for 36h; Ambient temperature; | A 10% B 57% |
With [bis(acetoxy)iodo]benzene; sulfuric acid at 60℃; for 1h; | A 21% B 56% |
With [bis(acetoxy)iodo]benzene; hydrogen cation at 60℃; for 1h; oxidative rearrangement; | A 21% B 56% |
methoxymethyl phenyl ketone
(R)-Phenylglycinol
(R)-2,4-diphenyl-2-(methoxymethyl)-1,3-oxazolidine
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid In benzene for 72h; Heating; | 100% |
methoxymethyl phenyl ketone
allyltributylstanane
Conditions | Yield |
---|---|
With tin(ll) chloride In acetonitrile for 1h; | 100% |
5-iodoisatin
methoxymethyl phenyl ketone
Conditions | Yield |
---|---|
With hydrogenchloride; potassium hydroxide In ethanol for 72h; Heating; | 100% |
Conditions | Yield |
---|---|
Stage #1: methoxymethyl phenyl ketone; allylmagnesium bromide In tetrahydrofuran at 20℃; for 3h; Stage #2: With water; ammonium chloride In tetrahydrofuran | 100% |
In tetrahydrofuran at -78℃; Inert atmosphere; | 100% |
Stage #1: methoxymethyl phenyl ketone; allylmagnesium bromide In tetrahydrofuran at 20℃; for 3h; Stage #2: With water; ammonium chloride In tetrahydrofuran |
trimethylsilyl cyanide
methoxymethyl phenyl ketone
3-methoxy-2-phenyl-2-(trimethylsilyloxy)propionitrile
Conditions | Yield |
---|---|
indium(III) bromide In dichloromethane at 20℃; for 0.5h; | 99% |
With indium(III) bromide In dichloromethane at 20℃; for 0.5h; | 99% |
With zinc(II) iodide In dichloromethane for 24h; Ambient temperature; |
methoxymethyl phenyl ketone
(E)-cinnamyl(tributyl)tin
Conditions | Yield |
---|---|
With tin(ll) chloride In acetonitrile at 20℃; for 3h; | 99% |
4-bromo-trans-crotonic acid ethyl ester
methoxymethyl phenyl ketone
Conditions | Yield |
---|---|
With indium In tetrahydrofuran at 20℃; for 20h; | 99% |
Conditions | Yield |
---|---|
Stage #1: methoxymethyl phenyl ketone With lithium diisopropyl amide In tetrahydrofuran; hexane at -40℃; for 1h; Inert atmosphere; Schlenk technique; Stage #2: With indium(III) chloride In tetrahydrofuran; hexane at -40 - 25℃; for 1.5h; Inert atmosphere; Schlenk technique; Stage #3: benzaldehyde In tetrahydrofuran; hexane at 67℃; for 1h; Reagent/catalyst; Temperature; Aldol Addition; Inert atmosphere; Schlenk technique; | 99% |
2-aminopyridine
methoxymethyl phenyl ketone
3-Methoxy-2-phenylimidazo<1,2-a>pyridine
Conditions | Yield |
---|---|
With iodine In 1,2-dichloro-ethane at 100℃; for 0.5h; | 96% |
With copper(l) iodide; oxygen In 1,2-dichloro-ethane at 100℃; under 760.051 Torr; Sealed tube; | 71% |
With copper(l) iodide; oxygen In 1,2-dichloro-ethane at 100℃; for 16h; | 71% |
Conditions | Yield |
---|---|
With indium In tetrahydrofuran at 20℃; for 5h; | 95% |
Conditions | Yield |
---|---|
With indium In tetrahydrofuran; water at 20℃; for 16h; | 95% |
trimethylsilyl cyanide
methoxymethyl phenyl ketone
(R)-3-methoxy-2-phenyl-2-trimethylsilyloxypropanenitrile
Conditions | Yield |
---|---|
With tert-butyl methyl ether; Ru[t-leu]2[(S)-binap]; lithium phenolate at -40℃; for 2h; Inert atmosphere; optical yield given as %ee; enantioselective reaction; | 95% |
methoxymethyl phenyl ketone
Conditions | Yield |
---|---|
With [D]-sodium hydroxide; deuteromethanol; water-d2 for 21h; Reflux; | 95% |
Conditions | Yield |
---|---|
With potassium tert-butylate In N,N-dimethyl-formamide at 60℃; for 13h; Inert atmosphere; Schlenk technique; | 94% |
Conditions | Yield |
---|---|
With ammonium chloride; zinc In ethanol for 0.5h; Heating; | 93% |
With 2,6-bis[1-(2,6-dimethylphenylimino)ethyl]pyridine cobalt(II)dichloride; bis(pinacol)diborane; sodium t-butanolate In tetrahydrofuran; methanol at 65℃; for 24h; Schlenk technique; Inert atmosphere; | 30% |
Conditions | Yield |
---|---|
With sodium tetrahydroborate In methanol at 0 - 20℃; for 3.5h; | 92% |
With sodium tetrahydroborate In methanol at 0 - 20℃; Inert atmosphere; | 86% |
84% |
Conditions | Yield |
---|---|
With bromine for 1h; Heating; | 92% |
methoxymethyl phenyl ketone
tributyl(cyclohex-2-en-1-yl)stannane
Conditions | Yield |
---|---|
With tin(ll) chloride In acetonitrile at 20℃; for 3h; | 92% |
methoxymethyl phenyl ketone
isopropyl alcohol
(R)-2-methoxy-1-phenyl-ethanol
Conditions | Yield |
---|---|
With potassium tert-butylate In tert-butyl alcohol | 92% |
methoxymethyl phenyl ketone
methyl 2-oxo-2-phenylacetate
Conditions | Yield |
---|---|
With iodine; sodium carbonate In 1,2-dichloro-ethane at 60℃; for 3h; Time; | 92% |
Conditions | Yield |
---|---|
With hydrogenchloride; potassium hydroxide In ethanol for 72h; Heating; | 90% |
7-iodoisatin
methoxymethyl phenyl ketone
Conditions | Yield |
---|---|
With hydrogenchloride; potassium hydroxide In ethanol for 72h; Heating; | 90% |
Conditions | Yield |
---|---|
With indium In tetrahydrofuran Reformatsky-type reaction; Heating; | 90% |
Conditions | Yield |
---|---|
Stage #1: 2,3-dimethyl-buta-1,3-diene With dichloroindium hydride In tetrahydrofuran at 20℃; for 5h; Stage #2: methoxymethyl phenyl ketone With water In tetrahydrofuran at 20℃; for 14h; regioselective reaction; | 90% |
Conditions | Yield |
---|---|
With titanium(IV) tetrabutoxide; triethylsilyl chloride In dichloromethane at 20℃; | A n/a B 90% |
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