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Cas:4097-88-5
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Type:Manufacturers
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Changzhou Extraordinary Pharmatech co., LTD. As a leading chemical manufacturer and supplier in China.DAS authentication is passed.We can provide the popular precursor chemicals, we have our own strong R & D team, have our own laboratories and fa
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Min.Order:1 Gram
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Min.Order:1 Gram
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FINETECH INDUSTRY LIMITED is a LONDON based CRO company providing drug discovery & development services to worldwide clients. FINETECH INDUSTRY LIMITED supplies the N-Methyl-2,2'-diaminodiethylamine, CAS:4097-88-5 with the most competitive price and
N-METHYL-2,2'-DIAMINODIETHYLAMINE, 98%, 4097-88-5 Appearance:liquid Storage:dry and ventilated place Package:suitable for shipping Application:N-METHYL-2,2'-DIAMINODIETHYLAMINE, 98%, 4097-88-5 Transportation:common shipping Port:shanghai
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inquiryintermediateAppearance:liquid Storage:Normal temperature Package:1kg/25kg/customized Application:intermediate Transportation:By Ship/Air
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inquiryN-methyliminodiacetonitrile
A
1-methyl-piperazine
B
1,5-diamino-3-azamethylpentane
Conditions | Yield |
---|---|
With hydrogen In methanol at 120 - 600℃; under 15001.5 Torr; Temperature; Solvent; Reagent/catalyst; | A 92.4% B 6.8% |
N1-(2-aminoethyl)-N1-methylethane-1,2-diamine trihydrochloride
1,5-diamino-3-azamethylpentane
Conditions | Yield |
---|---|
With sodium methylate In methanol at 0 - 5℃; for 3h; Large scale; | 88% |
N,N di(dimethyl-2,5 pyrolido-2 ethyl), N methylamine
1,5-diamino-3-azamethylpentane
Conditions | Yield |
---|---|
With potassium carbonate In ethanol at 80℃; for 96h; Heating; | 26% |
N,N'-(3-methyl-3-aza-pentanediyl)-bis-benzenesulfonamide
1,5-diamino-3-azamethylpentane
Conditions | Yield |
---|---|
With sulfuric acid |
Conditions | Yield |
---|---|
(i) phthalimide , (ii) aq. HCl; Multistep reaction; |
phthalimide
N-Methyldiethanolamine
A
1,5-diamino-3-azamethylpentane
B
N-(2-hydroxyethyl)-N-methylethylenediamine
Conditions | Yield |
---|---|
With hydrogenchloride; water 1.) 100 deg C, 4 h; 2.) 90 deg C, 50 h; Yield given. Multistep reaction; | |
With hydrogenchloride; water 1.) 100 deg C, 4 h; 2.) 90 deg C, 50 h; Multistep reaction; |
mechlorethamine hydrochloride
A
1-methyl-piperazine
B
1,5-diamino-3-azamethylpentane
Conditions | Yield |
---|---|
With ammonia; sodium carbonate In water-d2 Title compound not separated from byproducts; |
1,5-diamino-3-azamethylpentane
Tert-butyl isocyanate
bis[(N'-tert-butylureido)-N-ethyl]-N-methylamine
Conditions | Yield |
---|---|
In tetrahydrofuran at 20℃; | 96.2% |
4,7-dichloroquinoline
1,5-diamino-3-azamethylpentane
N1-(2-aminoethyl)-N2-(7-chloroquinolin-4-yl)-N1-methylethane-1,2-diamine
Conditions | Yield |
---|---|
In neat (no solvent) at 125℃; for 2h; | 95% |
at 90 - 135℃; for 4h; | 92% |
at 70℃; | 57% |
In neat (no solvent) at 90℃; Inert atmosphere; | 57% |
With potassium phosphate; palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl In 1,4-dioxane at 90℃; for 17h; Inert atmosphere; | 1.39 g |
Conditions | Yield |
---|---|
at 20℃; Cooling with ice; | 94% |
1,5-diamino-3-azamethylpentane
Conditions | Yield |
---|---|
In water at 20℃; Solvent; Temperature; | 92.9% |
Conditions | Yield |
---|---|
Stage #1: 2,6-Pyridinedicarboxaldehyde; 1,5-diamino-3-azamethylpentane With sodium tetrahydroborate In ethanol at 20℃; for 2h; Stage #2: With hydrogenchloride; water In 1,4-dioxane | 92% |
1,5-diamino-3-azamethylpentane
2,7-naphthalenedicarboxaldehyde
Conditions | Yield |
---|---|
In acetonitrile at 20℃; for 96h; | 92% |
Conditions | Yield |
---|---|
In chloroform for 2h; Heating; | 90% |
ethanol
1,5-diamino-3-azamethylpentane
3,3'-bis(2-hydroxybenzaldehyde)
Conditions | Yield |
---|---|
In ethanol to EtOH soln. 3,3'-(3-oxapentane-1,5-diyldioxy)bis(2-hydroxybenzaldehyde) 1,5-diamino-3-azamethylpentane in EtOH was added dropwise and refluxedfor 15 min, GdCl3*6H2O in EtOH was added and refluxed for 2 h; soln. was evapd. to dryness, residue was treated with EtOH, filtered, and dried in vacuo; elem. anal.; | 90% |
Conditions | Yield |
---|---|
In ethanol for 12h; Inert atmosphere; | 90% |
Conditions | Yield |
---|---|
With triethylamine In tetrahydrofuran Inert atmosphere; Schlenk technique; | 90% |
1-chloro-7-methoxy-4-nitro-10H-acridin-9-one
1,5-diamino-3-azamethylpentane
Conditions | Yield |
---|---|
With triethylamine In dimethyl sulfoxide at 80℃; for 3h; | 88% |
1,5-diamino-3-azamethylpentane
di-tert-butyl dicarbonate
tert-butyl (2-((2-aminoethyl)(methyl)amino)ethyl)carbamate
Conditions | Yield |
---|---|
With dmap In chloroform at 20℃; for 16h; | 88% |
In tetrahydrofuran at 0 - 20℃; for 20.5h; | 46% |
In dichloromethane at 0 - 20℃; for 3h; | 30% |
7-chloro-4-bromo-quinoline
1,5-diamino-3-azamethylpentane
N2-(7-Chloro-4-quinolinyl)-N1-[2-[(7-chloro-4-quinolinyl)amino]ethyl]-N1-methyl-1,2-ethanediamine
Conditions | Yield |
---|---|
With potassium phosphate; palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl In 1,4-dioxane at 90℃; for 18h; Inert atmosphere; | 88% |
With potassium phosphate; palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl In 1,4-dioxane; water at 120℃; for 16h; Inert atmosphere; Sealed tube; | 43% |
1,5-diamino-3-azamethylpentane
p-toluenesulfonyl chloride
N,N'-((methylazanediyl)bis(ethane-2,1-diyl))bis(4-methylbenzenesulfonamide)
Conditions | Yield |
---|---|
With sodium hydroxide In diethyl ether at 40℃; for 3h; | 87% |
fac-[CoCl3(1,4,7-triazacyclononane)]
1,5-diamino-3-azamethylpentane
Conditions | Yield |
---|---|
With HClO4 In isopropyl alcohol 50°C, 8h; chromy. (Sephadex-C-25, HClO4); evapn.; addn. of ethanol or propanol; pptn.; elem. anal.; | 87% |
1,5-diamino-3-azamethylpentane
1-chloro-4-nitro-9,10-dihydro-9-acridinone
Conditions | Yield |
---|---|
With triethylamine In dimethyl sulfoxide at 80℃; for 3h; | 86% |
Conditions | Yield |
---|---|
In ethyl acetate at 0℃; for 2h; Inert atmosphere; | 86% |
With triethylamine In chloroform at 0℃; for 1h; | 70% |
1,5-diamino-3-azamethylpentane
1-nitro-9-oxo-9,10-dihydroacridine-4-carbonyl fluoride
Conditions | Yield |
---|---|
With pyridine In N,N-dimethyl-formamide for 4h; | 86% |
1,5-diamino-3-azamethylpentane
{2-[2-(2-acetylamino-thiazol-4-yl)-acetylamino]-thiazol-4-yl}-acetic acid 2,5-dioxo-pyrrolidin-1-yl ester
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide at 20℃; for 4h; | 85% |
Conditions | Yield |
---|---|
With sodium hydroxide In dichloromethane at 0℃; for 3h; | 85% |
With sodium hydroxide In dichloromethane; water at 0℃; for 5h; Solvent; Temperature; |
6-methyl-2-oxo-1-[3-(trifluoromethyl)phenyl]-1,2-dihydropyridine-3-carboxylic acid
1,5-diamino-3-azamethylpentane
C33H31F6N5O4
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine; HATU In N,N-dimethyl-formamide at 20℃; for 3h; | 84% |
With N-ethyl-N,N-diisopropylamine; HATU In N,N-dimethyl-formamide at 20℃; for 3h; | 84% |
1,5-diamino-3-azamethylpentane
4-chloro-7-trifluoromethyl quinoline
N1-methyl-N1-(2-((7-trifluoromethyl)quinolin-4-yl)aminoethyl)propane-1,3-diamine
Conditions | Yield |
---|---|
In neat (no solvent) at 140℃; for 2h; | 83% |
1,5-diamino-3-azamethylpentane
2-(2,6-dioxotetrahydro-2H-pyran-3-yl)-1H-benzo[f]isoindole-1,3(2H)-dione
2-(3-(1,3-dioxo-1H-benzo[f]isoindol-2(3H)-yl)-2,6-dioxopiperidin-1-yl)-N-(2-(3-(1,3-dioxo-1H-benzo[f]isoindol-2(3H)-yl)-2,6-dioxopiperidin-1-yl)ethyl)-N-methylethanamine hydrochloride
Conditions | Yield |
---|---|
Stage #1: 1,5-diamino-3-azamethylpentane; 2-(2,6-dioxotetrahydro-2H-pyran-3-yl)-1H-benzo[f]isoindole-1,3(2H)-dione In N,N-dimethyl-formamide at 20℃; for 48h; Stage #2: With hydrogenchloride In water pH=1; Stage #3: With acetic anhydride; acetyl chloride for 48h; Reflux; | 81% |
Conditions | Yield |
---|---|
In ethanol for 13h; Reflux; Inert atmosphere; | 81% |
Conditions | Yield |
---|---|
In water a soln. of Ni salt added dropwise to a soln. of amine, a soln. of KSeCNadded slowly, kepted in desicator over CaCl2; crysts. separated, washed (chilled water), dried (CaCl2); elem. anal., TGA; | 80% |
Conditions | Yield |
---|---|
In water aq. soln. of KSeCN was added to aq. soln. of Cd(ClO4)*6H2O with stirringfor 10 min, ligand was added slowly, stirred for 30 min; filtered, kept in CaCl2 desiccator for a few ds; elem. anal.; | 80% |
Conditions | Yield |
---|---|
With sodium hydroxide In dichloromethane at 0 - 25℃; for 12h; | 80% |
4,7-dichloroquinoline
1,5-diamino-3-azamethylpentane
N2-(7-Chloro-4-quinolinyl)-N1-[2-[(7-chloro-4-quinolinyl)amino]ethyl]-N1-methyl-1,2-ethanediamine
Conditions | Yield |
---|---|
In neat (no solvent) at 90℃; Inert atmosphere; | 79.3% |
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