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Hefei TNJ chemical industry co.,ltd

1,ISO Certificate 2,Factory price 3,Free sample and Fast delivery Appearance:Colorless transparent liquid Storage:All products should be stored at a dry and ventilated location away from fire and other dangerous goods, and should avoid direct sunl

N-Methyldiethanolamine,CAS 105-59-9

Cas:105-59-9

Min.Order:1 Metric Ton

FOB Price: $1.0

Type:Trading Company

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Ality Chemical Corporation

The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi

Factory Supply 2,2'-methyliminodiethanol

Cas:105-59-9

Min.Order:1

Negotiable

Type:Other

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Xi'an Xszo Chem Co., Ltd.

1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s

High Quality 99% Ethanol,2,2'-(methylimino)bis- 105-59-9 ISO Manufacturer

Cas:105-59-9

Min.Order:1 Gram

FOB Price: $0.1

Type:Manufacturers

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Chemwill Asia Co., Ltd.

Chemwill Asia co.,Ltd is one of the leading manufacturer in CHINA. Product quality, process, price and service N-Methyldiethanolamine 105-59-9 Factory MDEA PRICE IN STOCK 2,2'-(Methylimino)diethanol COA CAS 105-59-9 CAS 105-59-9 highly q

N-Methyldiethanolamine 105-59-9 Factory MDEA PRICE IN STOCK 2,2'-(Methylimino)diethanol COA CAS 105-59-9

Cas:105-59-9

Min.Order:5 Kiloliter

FOB Price: $3.5 / 5.0

Type:Manufacturers

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Henan Tianfu Chemical Co., Ltd.

good quality competitive price small-quantity accepted Product name: N-Methyldiethanolamine CAS number: 105-59-9 PH: 11.5 at 100 g/l at 20 °C (68 °F) Melting point: -21 °C (-6 °F) Boiling point

N-Methyldiethanolamine with good qulity

Cas:105-59-9

Min.Order:100 Gram

Negotiable

Type:Lab/Research institutions

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Hebei Nengqian Chemical Import and Export Co., LTD

Our advantages: 1. All inquiries will be replied within 12 hours. 2. Dedication to quality, supply & service. 3. Strictly on selecting raw materials. 4. Reasonable & competitive price, fast lead time. 5. Sample is available for your eva

N-Methyldiethanolamine

Cas:105-59-9

Min.Order:1 Gram

FOB Price: $1000.0 / 1300.0

Type:Trading Company

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Wuhan Han Sheng New Material Technology Co.,Ltd

Our Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We

N-Methyl Diethanolamine/MDEA 105-59-9

Cas:105-59-9

Min.Order:10 Kilogram

Negotiable

Type:Trading Company

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Henan Sinotech Import&Export Corporation

Item Name Quality Index Best quality Appearance Colorless or yellowish sticky liquid without suspended substance Density (20℃) g

N-Methyldiethanolamine MDEA

Cas:105-59-9

Min.Order:5 Metric Ton

FOB Price: $1.0 / 2.0

Type:Other

inquiry

Hangzhou Sartort Biopharma Co., Ltd

Appearance:Clear colorless to light yellow liquid Storage:Store below +30°C. Package:200kg/Drum Application:N-Methyldiethanolamine is a reagent used for protection of boronic acids as N-methyl-O,O-diethanolamine esters. Transportation:Express/Sea/

N-Methyldiethanolamine with high quality

Cas:105-59-9

Min.Order:1 Kilogram

FOB Price: $1.0

Type:Lab/Research institutions

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Shanghai Upbio Tech Co.,Ltd

1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized

Ethanol,2,2'-(methylimino)bis- 105-59-9

Cas:105-59-9

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Xi'an Faithful Biotech Co., Ltd.

We are the manufacturers and suppliers of API in China, and warehouse in Germany and USA of California, which can quickly and safely deliver to your address 1.High quality and competitive price. 2.Free sample for your evaluation. 3.Promptly delivery

Shanghai Minstar Chemical Co., Ltd

N-Methyldiethanolamine Basic information Product Name: N-Methyldiethanolamine Synonyms: N,N-BIS(2-HYDROXYETHYL)METHYLAMINE;N-METHYL-2,2'-IMINODIETHANOL;N-METHYL-2,2-IMINOBIS(ETHANOL);N-METHYLDIETHANOLAMINE;N-METHYL-N-(2-HYDROXYETHYL)-2-AMI

N-Methyldiethanolamine

Cas:105-59-9

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Baoji Guokang Healthchem co.,ltd

Our company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At prese

Glucosamine AMINO ACIDS

Cas:105-59-9

Min.Order:1 Kilogram

FOB Price: $4.0 / 5.0

Type:Trading Company

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Qingdao Beluga Import and Export Co., LTD

N-Methyldiethanolamine CAS:105-59-9 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic inte

N-Methyldiethanolamine CAS:105-59-9

Cas:105-59-9

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Shandong Hanjiang Chemical Co., Ltd.

Hello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai

Ethanol,2,2'-(methylimino)bis-

Cas:105-59-9

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Henan Wentao Chemical Product Co., Ltd.

Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

Ethanol,2,2'-(methylimino)bis-

Cas:105-59-9

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Triumph International Development Limilted

Triumph has the complete production of G- KG - MT service chain,we can make the new technology into productivity quickly in the research and development of new products. Main Service 1.Own made fine chemical products 2.Out sourcing and quality c

N-Methyldiethanolamine

Cas:105-59-9

Min.Order:100 Metric Ton

Negotiable

Type:Lab/Research institutions

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Qingdao Jinlida trading Co.,Ltd

Full experience of large numbers containers loading in Chinese sea port Fast shipment by reputed shipping line Packing with pallet as buyer's special request Best service after shipment with e mail Cargoes together with container sales serv

N-Methyldiethanolamine

Cas:105-59-9

Min.Order:1 Metric Ton

Negotiable

Type:Trading Company

inquiry

Hangzhou Keyingchem Co.,Ltd

Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det

N-Methyl Diethanolamine

Cas:105-59-9

Min.Order:0 Metric Ton

Negotiable

Type:Lab/Research institutions

inquiry

Hangzhou J&H Chemical Co., Ltd.

J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

Ethanol,2,2'-(methylimino)bis-

Cas:105-59-9

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Shanghai Massive Chemical Technology Co., Ltd.

Massive Chemical is certified with ISO9001 and ISO14001 manufacturer for this product. We will offer all documents as requirement for the materials which includes, Certificate of Analysis, Material Safety Data Sheet, and Method of Analysis and

N-Methyldiethanolamine

Cas:105-59-9

Min.Order:1 Gram

FOB Price: $1.0

Type:Lab/Research institutions

inquiry

Zibo Hangyu Biotechnology Development Co., Ltd

Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi

High quality N-Methyldiethanolamine

Cas:105-59-9

Min.Order:10 Gram

FOB Price: $100.0

Type:Lab/Research institutions

inquiry

SHANGHAI SYSTEAM BIOCHEM CO., LTD

We are one of a few suppliers that can offer custom synthesis service of this product We are specialized in custom synthesis, chemical/pharmaceutical/ pesticides outsourcing and contract research. We are committed to prov

N-Methyl Diethanolamine

Cas:105-59-9

Min.Order:100 Gram

FOB Price: $100.0 / 2000.0

Type:Lab/Research institutions

inquiry

HANGZHOU YUNUO CHEMICAL CO.,LTD

Superior quality, moderate price & quick delivery. Appearance:colourless liquid Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:25kg/drum, or as per your request. Application:Used as Pharmaceutical Intermediat

Ethanol,2,2'-(methylimino)bis-

Cas:105-59-9

Min.Order:1 Kilogram

Negotiable

Type:Trading Company

inquiry

TaiChem Taizhou Limited

Established in May 2015, TaiChem Ltd. is initially invested by a British research and development company and started by PhDs back from aboard. The company is registered in China Medical City (CMC), Taizhou, Jiangsu Province, and the production site

Diethanolmethylamine

Cas:105-59-9

Min.Order:10 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Hebei Kunsui Technology Co., Ltd.

1. A strong scientific research team . 2. Stable quality (with a complete scientific research center and testing center to ensure the quality stability of each batch of products). 3. Rich export experience (with practical experience in exporting to m

Organic N-Methyldiethanolamine Powder CAS 105-59-9

Cas:105-59-9

Min.Order:1 Kilogram

FOB Price: $8.2 / 8.8

Type:Trading Company

inquiry

Siwei Development Group Ltd.

Product name: N-Methyl Diethanolamine CAS No.: 105-59-9 Molecule Formula:C5H13NO2 Molecule Weight:119.16 Purity: 99.0% Package: 200kg/drum Description:Colorless or light yellow viscous liquid Manufacture Standards:Enterprise Standard

Lower Price N-Methyl Diethanolamine on stock

Cas:105-59-9

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Zibo Dorne chemical technology co. LTD

Product Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,

Jiangsu Qianyu Molecular Technology Co., LTD.

Our Advantages A. International Top level TechnologyOur company owned biomedicine experts are famous at home and abroad with rich experience in research and development in the field of efficient chiral functional molecules research and development an

Buy Top Purity Diethanolmethylamine

Cas:105-59-9

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Xiamen Jenny Chemical Technology Co., Ltd.

GMP standard, high purity, competitive price, in stock 1. Quick Response: within 6 hours after receiving your email. 2. Quality Guarantee: All products are strictly tested by our QC, confirmed by QA, and approved by a third-party lab in China, USA,

N-Methyldiethanolamine

Cas:105-59-9

Min.Order:1 Milligram

Negotiable

Type:Trading Company

inquiry

Synthetic route

formaldehyd
50-00-0

formaldehyd

2,2'-iminobis[ethanol]
111-42-2

2,2'-iminobis[ethanol]

N-Methyldiethanolamine
105-59-9

N-Methyldiethanolamine

Conditions
ConditionsYield
With hydrogen In methanol at 125℃; under 10501.1 Torr; for 4h; Autoclave;92%
und Hydrierung des Reaktionspodukts an Raney-Nickel bei 85grad/175 at;
oxirane
75-21-8

oxirane

methylamine
74-89-5

methylamine

A

(2-hydroxyethyl)(methyl)amine
109-83-1

(2-hydroxyethyl)(methyl)amine

B

N-Methyldiethanolamine
105-59-9

N-Methyldiethanolamine

C

2,2'-((1-hydroxypropan-2-yl)azanediyl)bis(ethan-1-ol)
68998-54-9

2,2'-((1-hydroxypropan-2-yl)azanediyl)bis(ethan-1-ol)

Conditions
ConditionsYield
water at 62.84 - 71.84℃; under 7500.75 Torr; for 0.2h; Heating / reflux;A 16.7%
B 83.3%
C n/a
at 66.84 - 76.84℃; under 9000.9 Torr; for 0.116667h; Heating / reflux;A 63.5%
B 36.4%
C 0.02%
water at 61.54 - 63.34℃; under 7500.75 Torr; for 0.2h; Heating / reflux;
at 66.34℃; under 9000.9 Torr; for 0.116667h; Heating / reflux;
formaldehyd
50-00-0

formaldehyd

formaldehyde cyano hydride

formaldehyde cyano hydride

A

2-(N,N-dimethylamino)ethanol
108-01-0

2-(N,N-dimethylamino)ethanol

B

N-Methyldiethanolamine
105-59-9

N-Methyldiethanolamine

Conditions
ConditionsYield
With methanol; nickel at 95 - 100℃; under 514855 Torr;
triethanolamine
102-71-6

triethanolamine

A

2-(N,N-dimethylamino)ethanol
108-01-0

2-(N,N-dimethylamino)ethanol

B

N-Methyldiethanolamine
105-59-9

N-Methyldiethanolamine

Conditions
ConditionsYield
With hydrogen; palladium/alumina at 290℃; for 5h; Product distribution; various temp., time, catalysts;
With hydrogen; Pt/Al2O3 at 320℃; for 5h;
(2-hydroxyethyl)(methyl)amine
109-83-1

(2-hydroxyethyl)(methyl)amine

3-oxa-1,5-dichloropentane
111-44-4

3-oxa-1,5-dichloropentane

A

N-Methyldiethanolamine
105-59-9

N-Methyldiethanolamine

B

3,9-dimethyl-6-oxa-3,9-diaza-undecane-1,11-diol
115188-50-6

3,9-dimethyl-6-oxa-3,9-diaza-undecane-1,11-diol

Conditions
ConditionsYield
With sodium carbonate In toluene for 48h; Heating;A 14%
B 37%
(2-hydroxyethyl)(methyl)amine
109-83-1

(2-hydroxyethyl)(methyl)amine

2-chloro-ethanol
107-07-3

2-chloro-ethanol

N-Methyldiethanolamine
105-59-9

N-Methyldiethanolamine

Conditions
ConditionsYield
With water at 120℃;
mechlorethamine hydrochloride
55-86-7

mechlorethamine hydrochloride

A

N-Methyldiethanolamine
105-59-9

N-Methyldiethanolamine

B

bis-(2-hydroxy-ethyl)-{2-[(2-hydroxy-ethyl)-methyl-amino]-ethyl}-methyl-ammonium; chloride
111068-26-9

bis-(2-hydroxy-ethyl)-{2-[(2-hydroxy-ethyl)-methyl-amino]-ethyl}-methyl-ammonium; chloride

Conditions
ConditionsYield
With sodium hydroxide; sodium carbonate In water-d2 for 24h; Title compound not separated from byproducts;
N-methyldiethanolamine phenylboronic ester
65796-77-2

N-methyldiethanolamine phenylboronic ester

A

N-Methyldiethanolamine
105-59-9

N-Methyldiethanolamine

B

phenylboronic acid
98-80-6

phenylboronic acid

Conditions
ConditionsYield
With water In 1,4-dioxane; water Kinetics; byproducts: (HOCH2CH2)2NMe; hydrolysis in water/dioxane mixts. of different concns.;
oxirane
75-21-8

oxirane

methylamine
74-89-5

methylamine

N-Methyldiethanolamine
105-59-9

N-Methyldiethanolamine

2-(oxazolidin-3-yl)ethanol
20073-50-1

2-(oxazolidin-3-yl)ethanol

N-Methyldiethanolamine
105-59-9

N-Methyldiethanolamine

Conditions
ConditionsYield
With formic acid; water
With formic acid; water
4-(2-hydroxy-ethyl)-morpholin-2-one
5038-12-0

4-(2-hydroxy-ethyl)-morpholin-2-one

N-Methyldiethanolamine
105-59-9

N-Methyldiethanolamine

Conditions
ConditionsYield
With potassium hydroxide
formaldehyd
50-00-0

formaldehyd

formate of bis-<2-hydroxy-ethyl>-amine

formate of bis-<2-hydroxy-ethyl>-amine

N-Methyldiethanolamine
105-59-9

N-Methyldiethanolamine

Conditions
ConditionsYield
at 100 - 110℃;
formaldehyd
50-00-0

formaldehyd

hydrochloride of bis-<2-hydroxy-ethyl>-amine

hydrochloride of bis-<2-hydroxy-ethyl>-amine

N-Methyldiethanolamine
105-59-9

N-Methyldiethanolamine

Conditions
ConditionsYield
at 160 - 165℃;
nitrogen mustard
51-75-2

nitrogen mustard

NaHCO3

NaHCO3

N-Methyldiethanolamine
105-59-9

N-Methyldiethanolamine

methylamine
74-89-5

methylamine

2-chloro-ethanol
107-07-3

2-chloro-ethanol

N-Methyldiethanolamine
105-59-9

N-Methyldiethanolamine

Conditions
ConditionsYield
at 100℃;
formaldehyd
50-00-0

formaldehyd

formic acid
64-18-6

formic acid

2,2'-iminobis[ethanol]
111-42-2

2,2'-iminobis[ethanol]

N-Methyldiethanolamine
105-59-9

N-Methyldiethanolamine

Conditions
ConditionsYield
With water zuletzt auf dem Dampfbad;
GLUTATHIONE
70-18-8

GLUTATHIONE

nitrogen mustard
51-75-2

nitrogen mustard

A

N-Methyldiethanolamine
105-59-9

N-Methyldiethanolamine

B

(S)-2-Amino-4-((R)-1-(carboxymethyl-carbamoyl)-2-{2-[(2-hydroxy-ethyl)-methyl-amino]-ethylsulfanyl}-ethylcarbamoyl)-butyric acid

(S)-2-Amino-4-((R)-1-(carboxymethyl-carbamoyl)-2-{2-[(2-hydroxy-ethyl)-methyl-amino]-ethylsulfanyl}-ethylcarbamoyl)-butyric acid

C

(S)-2-Amino-4-[(R)-2-[2-({2-[(R)-2-((S)-4-amino-4-carboxy-butyrylamino)-2-(carboxymethyl-carbamoyl)-ethylsulfanyl]-ethyl}-methyl-amino)-ethylsulfanyl]-1-(carboxymethyl-carbamoyl)-ethylcarbamoyl]-butyric acid
124605-74-9

(S)-2-Amino-4-[(R)-2-[2-({2-[(R)-2-((S)-4-amino-4-carboxy-butyrylamino)-2-(carboxymethyl-carbamoyl)-ethylsulfanyl]-ethyl}-methyl-amino)-ethylsulfanyl]-1-(carboxymethyl-carbamoyl)-ethylcarbamoyl]-butyric acid

Conditions
ConditionsYield
In water-d2 at 30℃; for 3.06667h; Mechanism; 0.06 M phosphate, pH 7.0, NMR characterization;
Ethoxy-bis(2-hydroxyethyl)methylammonium
92336-62-4

Ethoxy-bis(2-hydroxyethyl)methylammonium

N-Methyldiethanolamine
105-59-9

N-Methyldiethanolamine

Conditions
ConditionsYield
(i) AgCl, (ii) H2, Pd-C; Multistep reaction;
methanol
67-56-1

methanol

formaldehyd
50-00-0

formaldehyd

glycolonitrile
107-16-4

glycolonitrile

cobalt

cobalt

A

2-(N,N-dimethylamino)ethanol
108-01-0

2-(N,N-dimethylamino)ethanol

B

N-Methyldiethanolamine
105-59-9

N-Methyldiethanolamine

Conditions
ConditionsYield
at 90 - 110℃; under 514855 Torr; Hydrogenation;
methanol
67-56-1

methanol

formaldehyd
50-00-0

formaldehyd

glycolonitrile
107-16-4

glycolonitrile

nickel

nickel

A

2-(N,N-dimethylamino)ethanol
108-01-0

2-(N,N-dimethylamino)ethanol

B

N-Methyldiethanolamine
105-59-9

N-Methyldiethanolamine

Conditions
ConditionsYield
at 90 - 110℃; under 514855 Torr; Hydrogenation;
water
7732-18-5

water

nitrogen mustard
51-75-2

nitrogen mustard

A

N-Methyldiethanolamine
105-59-9

N-Methyldiethanolamine

B

2‐[(2-chloroethyl)(methyl)amino]ethanol
51822-57-2

2‐[(2-chloroethyl)(methyl)amino]ethanol

C

1.4-dimethyl-1.4-bis-<2-chloro-ethyl>-piperazinium dichloride

1.4-dimethyl-1.4-bis-<2-chloro-ethyl>-piperazinium dichloride

Conditions
ConditionsYield
wandelt sich bei Raumtemperatur nach mehreren Tagen;
water
7732-18-5

water

mechlorethamine hydrochloride
55-86-7

mechlorethamine hydrochloride

NaHCO3

NaHCO3

A

N-Methyldiethanolamine
105-59-9

N-Methyldiethanolamine

B

N-methyl-N.N'.N'-tris-<2-hydroxy-ethyl>-ethylenediamine-N'-methochloride

N-methyl-N.N'.N'-tris-<2-hydroxy-ethyl>-ethylenediamine-N'-methochloride

C

1.4-dimethyl-1.4-bis-<2-chloro-ethyl>-piperazinium dichloride

1.4-dimethyl-1.4-bis-<2-chloro-ethyl>-piperazinium dichloride

D

1.4-dimethyl-1.4-bis-<2-hydroxy-ethyl>-piperazinium dichloride

1.4-dimethyl-1.4-bis-<2-hydroxy-ethyl>-piperazinium dichloride

tertamethylammonium iodide
75-58-1

tertamethylammonium iodide

2,2'-iminobis[ethanol]
111-42-2

2,2'-iminobis[ethanol]

A

N-Methyldiethanolamine
105-59-9

N-Methyldiethanolamine

B

trimethylamine
75-50-3

trimethylamine

Conditions
ConditionsYield
at 154℃; Rate constant;
oxirane
75-21-8

oxirane

methylamine
74-89-5

methylamine

A

(2-hydroxyethyl)(methyl)amine
109-83-1

(2-hydroxyethyl)(methyl)amine

B

N-Methyldiethanolamine
105-59-9

N-Methyldiethanolamine

Conditions
ConditionsYield
unter starker Kuehlung;
N-Methyldiethanolamine
105-59-9

N-Methyldiethanolamine

(5-chloropyridin-2-yl)boronic acid
652148-91-9

(5-chloropyridin-2-yl)boronic acid

2-(5-chloro-pyridin-2-yl)-6-methyl-[1,3,6,2]dioxazaborocane

2-(5-chloro-pyridin-2-yl)-6-methyl-[1,3,6,2]dioxazaborocane

Conditions
ConditionsYield
With magnesium sulfate In dichloromethane at 20℃; for 18h;100%
N-Methyldiethanolamine
105-59-9

N-Methyldiethanolamine

(6-chloropyridin-2-yl)boronic acid

(6-chloropyridin-2-yl)boronic acid

2-(6-chloro-pyridin-2-yl)-6-methyl-[1,3,6,2]dioxazaborocane

2-(6-chloro-pyridin-2-yl)-6-methyl-[1,3,6,2]dioxazaborocane

Conditions
ConditionsYield
With magnesium sulfate In dichloromethane at 20℃; for 18h;100%
N-Methyldiethanolamine
105-59-9

N-Methyldiethanolamine

tetramethoxygermanium

tetramethoxygermanium

4,12-dimethyl-1,7,9,15-tetraoxa-4,12-diaza-8-germaspiro[7.7]pentadecane

4,12-dimethyl-1,7,9,15-tetraoxa-4,12-diaza-8-germaspiro[7.7]pentadecane

Conditions
ConditionsYield
In benzene under Ar atm. mixt. MeN(CH2CH2OH)2, Ge(OMe)4, and benzene was refluxed for 2 h; volatiles were removedin vacuo; elem. anal.;100%
bis(dimethylamino)dimethylgermane
14103-74-3

bis(dimethylamino)dimethylgermane

N-Methyldiethanolamine
105-59-9

N-Methyldiethanolamine

2,2,6-trimethyl-1,3-dioxa-6-aza-2-germacyclooctane
722458-51-7

2,2,6-trimethyl-1,3-dioxa-6-aza-2-germacyclooctane

Conditions
ConditionsYield
In toluene byproducts: HNMe2; under Ar, stirring at 70 °C for 10 h; volatiles were removed in vac., elem. anal.;100%
N-Methyldiethanolamine
105-59-9

N-Methyldiethanolamine

(2-{[(trifluoromethyl)sulfonyl]oxy}phenyl)boronic acid
1437769-74-8

(2-{[(trifluoromethyl)sulfonyl]oxy}phenyl)boronic acid

2-(6-methyl-1,3,6,2-dioxazaborocan-2-yl)phenyl trifluoromethanesulfonate

2-(6-methyl-1,3,6,2-dioxazaborocan-2-yl)phenyl trifluoromethanesulfonate

Conditions
ConditionsYield
In dichloromethane at 20℃;100%
1-Chlorohexane
544-10-5

1-Chlorohexane

N-Methyldiethanolamine
105-59-9

N-Methyldiethanolamine

C11H26NO2(1+)*Cl(1-)

C11H26NO2(1+)*Cl(1-)

Conditions
ConditionsYield
With sodium iodide In acetonitrile for 96h; Reflux;100%
N-Methyldiethanolamine
105-59-9

N-Methyldiethanolamine

1,3-dibromoazulen-2-ylboronic acid

1,3-dibromoazulen-2-ylboronic acid

1,3-dibromoazulen-2-ylboronic acid N-methyldiethanolamine ester

1,3-dibromoazulen-2-ylboronic acid N-methyldiethanolamine ester

Conditions
ConditionsYield
In tetrahydrofuran at 20℃; for 3h; Inert atmosphere; Molecular sieve;100%
N-Methyldiethanolamine
105-59-9

N-Methyldiethanolamine

((1R,2S,3R,4R)-3-(methoxycarbonyl)bicyclo[2.2.1]hept-5-en-2-yl)boronic acid

((1R,2S,3R,4R)-3-(methoxycarbonyl)bicyclo[2.2.1]hept-5-en-2-yl)boronic acid

methyl (1R,2R,3S,4R)-3-(4-methyltetrahydro-2H-4l4,8l4-[1,3,2]oxazaborolo[2,3-b][1,3,2]oxazaborol-8-yl)bicyclo[2.2.1]hept-5-ene-2-carboxylate

methyl (1R,2R,3S,4R)-3-(4-methyltetrahydro-2H-4l4,8l4-[1,3,2]oxazaborolo[2,3-b][1,3,2]oxazaborol-8-yl)bicyclo[2.2.1]hept-5-ene-2-carboxylate

Conditions
ConditionsYield
In benzene at 100℃; for 4h; Molecular sieve;100%
N-Methyldiethanolamine
105-59-9

N-Methyldiethanolamine

2-oxo-propionic acid
127-17-3

2-oxo-propionic acid

PA-NMDEA salt

PA-NMDEA salt

Conditions
ConditionsYield
In acetone at 35 - 45℃;100%
Indole-3-pyruvic acid
392-12-1

Indole-3-pyruvic acid

N-Methyldiethanolamine
105-59-9

N-Methyldiethanolamine

I-3-PA-NMDEA

I-3-PA-NMDEA

Conditions
ConditionsYield
In acetone at 40℃;100%
N-Methyldiethanolamine
105-59-9

N-Methyldiethanolamine

niobium (V) ethoxide
3236-82-6

niobium (V) ethoxide

[Nb(mdea)(OEt)3]

[Nb(mdea)(OEt)3]

Conditions
ConditionsYield
In toluene at 20℃; for 3h; Inert atmosphere; Schlenk technique; Glovebox;100%
N-Methyldiethanolamine
105-59-9

N-Methyldiethanolamine

methyl iodide
74-88-4

methyl iodide

di(methoxyethyl)dimethylammonium iodide
863031-19-0

di(methoxyethyl)dimethylammonium iodide

Conditions
ConditionsYield
Stage #1: N-Methyldiethanolamine With sodium hydride In tetrahydrofuran at 25 - 40℃; for 0.5h;
Stage #2: methyl iodide at 40℃; for 7h;
99.2%
dichloro-acetic acid
79-43-6

dichloro-acetic acid

N-Methyldiethanolamine
105-59-9

N-Methyldiethanolamine

N-methyldiethanolamine dichloroacetate

N-methyldiethanolamine dichloroacetate

Conditions
ConditionsYield
In methanol at 20℃; for 24h;99%
at 20℃; for 12h; Cooling with ice;98%
N-Methyldiethanolamine
105-59-9

N-Methyldiethanolamine

4-methyl-morpholine
109-02-4

4-methyl-morpholine

Conditions
ConditionsYield
Stage #1: N-Methyldiethanolamine With sulfuric acid at 60 - 170℃; for 7.5h;
Stage #2: at 60 - 70℃; for 0.5h; Temperature; Reagent/catalyst; Time;
98.4%
With hydrogenchloride at 160℃; im Rohr; Uebersaettigen mit Alkalilauge und Destillieren mit Wasserdampf;
With sulfuric acid at 160℃; Uebersaettigen mit Alkalilauge und Destillieren mit Wasserdampf;
With aluminum oxide; silica gel at 400℃;
With rare-earth based solid catalyst at 200℃; Temperature;
N-Methyldiethanolamine
105-59-9

N-Methyldiethanolamine

nitrogen mustard
51-75-2

nitrogen mustard

Conditions
ConditionsYield
With thionyl chloride In dichloromethane at 0 - 20℃; for 2h; Inert atmosphere; Schlenk technique;98%
With thionyl chloride; benzene zuletzt bei Siedetemperatur;
With thionyl chloride; chloroform zuletzt bei Siedetemperatur;
N-Methyldiethanolamine
105-59-9

N-Methyldiethanolamine

(6-bromopyridin-2-yl)boronic acid
440680-34-2

(6-bromopyridin-2-yl)boronic acid

2-(6-bromopyridin-2-yl)-6-methyl[1,3,6,2]dioxazaborocane

2-(6-bromopyridin-2-yl)-6-methyl[1,3,6,2]dioxazaborocane

Conditions
ConditionsYield
With magnesium sulfate In dichloromethane at 20℃; for 18h;98%
3,5-Di-tert-butylcatechol
1020-31-1

3,5-Di-tert-butylcatechol

N-Methyldiethanolamine
105-59-9

N-Methyldiethanolamine

tetrapropyloxygermane
128426-02-8

tetrapropyloxygermane

((CH3)3C)2C6H2O2Ge(OCH2CH2)2NCH3
134576-38-8

((CH3)3C)2C6H2O2Ge(OCH2CH2)2NCH3

Conditions
ConditionsYield
In benzene byproducts: CH3CH2CH2OH; refluxing a mixt. of tetrapropoxygermane, corresponding α-diol and diethanolamine in benzene (2-4 h), cooling, crystn.; filtration, washing (benzene, ether), drying (vac.); evapn. of the filtrate (vac.) down to half bulk, isolation of a further amt. of the product; elem. anal.;98%
N-Methyldiethanolamine
105-59-9

N-Methyldiethanolamine

2-(4-chloro-phenylsulfonyl)acetic acid
3405-89-8

2-(4-chloro-phenylsulfonyl)acetic acid

N,N-bis(2-hydroxyethyl)-N-methylammonium 2-(4-chlorophenylsulfonyl)acetate
1448165-12-5

N,N-bis(2-hydroxyethyl)-N-methylammonium 2-(4-chlorophenylsulfonyl)acetate

Conditions
ConditionsYield
98%
at 25℃;95%
titanium(IV) tetraethanolate

titanium(IV) tetraethanolate

N-Methyldiethanolamine
105-59-9

N-Methyldiethanolamine

C9H21NO4Ti

C9H21NO4Ti

Conditions
ConditionsYield
In tetrahydrofuran at 40℃; Inert atmosphere;98%
N-Methyldiethanolamine
105-59-9

N-Methyldiethanolamine

chloro(propylthio)acetylene
66566-80-1

chloro(propylthio)acetylene

3-(2-Hydroxy-ethyl)-3-methyl-2-[1-propylsulfanyl-meth-(E)-ylidene]-oxazolidin-3-ium; chloride
97427-21-9

3-(2-Hydroxy-ethyl)-3-methyl-2-[1-propylsulfanyl-meth-(E)-ylidene]-oxazolidin-3-ium; chloride

Conditions
ConditionsYield
In diethyl ether at 20℃; for 3h;97%
N-Methyldiethanolamine
105-59-9

N-Methyldiethanolamine

m-nitrobenzene boronic acid
13331-27-6

m-nitrobenzene boronic acid

(N-B)-Perhydro-2-(3-nitrophenyl)-6-methyl-1,3-dioxa-6-aza-2-boracine

(N-B)-Perhydro-2-(3-nitrophenyl)-6-methyl-1,3-dioxa-6-aza-2-boracine

Conditions
ConditionsYield
In toluene at 100℃; for 1h;97%
N-Methyldiethanolamine
105-59-9

N-Methyldiethanolamine

1-Bromodocosane
6938-66-5

1-Bromodocosane

Br(1-)*C27H58NO2(1+)
125343-56-8

Br(1-)*C27H58NO2(1+)

Conditions
ConditionsYield
In toluene; acetonitrile at 100℃; for 24h;97%
N-Methyldiethanolamine
105-59-9

N-Methyldiethanolamine

N-methyl-N-2-hydroxyethyl-2-aminoethanol-N-oxide
58567-81-0

N-methyl-N-2-hydroxyethyl-2-aminoethanol-N-oxide

Conditions
ConditionsYield
With dihydrogen peroxide96%
With dihydrogen peroxide
N-Methyldiethanolamine
105-59-9

N-Methyldiethanolamine

mechlorethamine hydrochloride
55-86-7

mechlorethamine hydrochloride

Conditions
ConditionsYield
With thionyl chloride In chloroform at 20℃; for 2h;96%
With thionyl chloride In dichloromethane at 0 - 20℃; for 24h;92%
With thionyl chloride In dichloromethane at 20℃; for 48h; Cooling with ice;85%
N-Methyldiethanolamine
105-59-9

N-Methyldiethanolamine

4,4'-(1,1,1,3,3,3-hexafluoroisopropylidene)diphthalic anhydride
1107-00-2

4,4'-(1,1,1,3,3,3-hexafluoroisopropylidene)diphthalic anhydride

di(4-isocyanatophenyl)methane
101-68-8

di(4-isocyanatophenyl)methane

polymer, product of diol-diisocyanate condensation followed by polycondensation with dianhydride and heating; monomer(s): 4,4\-methylenebis(phenyl isocyanate); N-methyldiethanolamine; 4,4\-(hexafluoroisopropylidene)bis(phthalic anhydride)

polymer, product of diol-diisocyanate condensation followed by polycondensation with dianhydride and heating; monomer(s): 4,4\-methylenebis(phenyl isocyanate); N-methyldiethanolamine; 4,4\-(hexafluoroisopropylidene)bis(phthalic anhydride)

Conditions
ConditionsYield
Stage #1: N-Methyldiethanolamine; di(4-isocyanatophenyl)methane In N,N-dimethyl-formamide at 20℃; for 1h;
Stage #2: 4,4'-(1,1,1,3,3,3-hexafluoroisopropylidene)diphthalic anhydride In N,N-dimethyl-formamide at 60 - 80℃;
Stage #3: for 15h; Heating; vacuum;
96%
N-Methyldiethanolamine
105-59-9

N-Methyldiethanolamine

lead(II) oxide

lead(II) oxide

lead(II) N-methyldiethanolaminate
880645-65-8

lead(II) N-methyldiethanolaminate

Conditions
ConditionsYield
In toluene byproducts: H2O; under N2, 2 equiv. of N-compd., reflux in dry toluene with removing of water (with a mol. sieve) for ca. 4 h; volatiles were removed in vac., solid was recrystd. from hot toluene on slow cooling to -22 °C, elem. anal.;96%
N-Methyldiethanolamine
105-59-9

N-Methyldiethanolamine

4-nitrophenylboronic acid
24067-17-2

4-nitrophenylboronic acid

C11H15BN2O4
133468-62-9

C11H15BN2O4

Conditions
ConditionsYield
In toluene at 100℃; for 1h;96%
N-Methyldiethanolamine
105-59-9

N-Methyldiethanolamine

propargyl bromide
106-96-7

propargyl bromide

N,N-bis(2-hydroxyethyl)-N-methylprop-2-yn-1-aminium bromide

N,N-bis(2-hydroxyethyl)-N-methylprop-2-yn-1-aminium bromide

Conditions
ConditionsYield
In N,N-dimethyl-formamide at 20℃;95%
With potassium hydroxide
In N,N-dimethyl-formamide at 20℃; for 24h;
n-dodecanoyl chloride
112-16-3

n-dodecanoyl chloride

N-Methyldiethanolamine
105-59-9

N-Methyldiethanolamine

bis<2-(dodecyloxycarbonyl)ethyl>methylamine hydrochloride
79898-78-5

bis<2-(dodecyloxycarbonyl)ethyl>methylamine hydrochloride

Conditions
ConditionsYield
In N,N-dimethyl-formamide95%
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