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Cas:455-38-9
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inquiry3-Fluorobenzoic acidProduct name: 3-Fluorobenzoic acidCAS: 455-38-9Structural formula:Quality specification:Appearance: White powderContent: 98.0%(HPLC)minMelting point: 122-124℃Appearance:White powder Storage:Sealed and preserved Package:200/Kilogra
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inquiryhigh quality Appearance:white powder Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea Port:shanghai
3-Fluorobenzoic acid Product name: 3-Fluorobenzoic acid CAS: 455-38-9 Structural formula: Quality specification: Appearance: White powder Content: 98.0%(HPLC)min Melting point: 122-124℃ Our Server 1. Competitive offers with standa
Cas:455-38-9
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inquiryTIANFUCHEM--455-38-9--3-Fluorobenzoic acid factory price Our company was built in 2009 with an ISO certificate.In the past 10 years, we have grown up as a famous fine chemicals supplier in China And we had established stable business re
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inquiryProduct Description Product website: http://www.finerchem.com Product Name 3-Fluorobenzoic acid CAS No. 455-38-9
Cas:455-38-9
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inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
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inquiryName: 3-Fluorobenzoic acid Synonyms: 3-fluorobenzoate CAS:455-38-9 MF: C7H4FO2 Appearance: white powder Storage:Store in cool and dry place, away from sun light. Package: 25kgs/drum Application:Organic Synthesis Transportation:By sea or b
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Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
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inquiryCompany Introduction 1. Established in 2005, with two independent business divisions: Fine chemicals division; Pharmaceutical division. 2. Main product: Optical brightener Textile auxiliary Dye stuff Pigments
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Min.Order:1 Gram
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The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
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inquiryMassive Chemical is certified with ISO9001 and ISO14001 manufacturer for this product. We will offer all documents as requirement for the materials which includes, Certificate of Analysis, Material Safety Data Sheet, and Method of Analysis and
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inquirySuperior quality, moderate price & quick delivery. Appearance:off white crystalline powder Storage:In Room Temperature Package:25kg/drum, or as per your request. Application:For medicine , pesticide intermediates Transportation: as per your
Product name: 3-Fluorobenzoic Acid CAS No.: 455-38-9 Molecule Formula:C7H4FO2 Molecule Weight:139.10 Purity: 99.0% Package: 25kg/drum Description:White powder Manufacture Standards:Enterprise Standard TESTING ITEMS
Cas:455-38-9
Min.Order:1 Kilogram
Negotiable
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inquiry3-Fluorobenzoic acid Chemical Properties Melting point 122-124 °C (lit.) Boiling point 226.1°C (rough estimate) density 1.474 storage temp. Refrigerator solubility 1.5g/l pka 3.86(at 25℃) form Powder color White
Cas:455-38-9
Min.Order:1 Gram
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inquiryConditions | Yield |
---|---|
With potassium ferrate(VI) In neat (no solvent) for 2h; Milling; | 98.9% |
With oxygen; copper(II) acetate monohydrate; cobalt(II) diacetate tetrahydrate In water at 70℃; under 760.051 Torr; for 12h; | 98% |
With oxygen; Langlois reagent In acetonitrile at 25℃; under 760.051 Torr; for 12h; Irradiation; Green chemistry; | 95% |
Conditions | Yield |
---|---|
With oxygen; pyridinium chlorochromate In water at 120℃; under 45004.5 Torr; for 2h; | 95% |
With copper(l) iodide; oxygen; nitric acid at 160℃; under 11251.1 - 18751.9 Torr; for 4.7h; Autoclave; | 84.7% |
With cerium(III) chloride; 1,1,1-trichloroethanol; oxygen In acetonitrile at 60℃; Irradiation; | 83% |
Conditions | Yield |
---|---|
With pyridine hydrogenfluoride; sodium nitrite 1.) O deg C, 20 min, 2.) 80 deg C, 1 h; | 95% |
With hydrogen fluoride; sodium nitrite | |
Ueberfuehrung in die Diazoaminoverbindung und Zersetzung mit rauchender Fluorwasserstoffsaeure; | |
With pyridine; hydrogen fluoride; sodium nitrite 1.) room temperature, 2.) 0 deg C, 3.) 80 deg C; Yield given. Multistep reaction; | |
Stage #1: meta-aminobenzoic acid With sodium nitrite at 70℃; for 1.5h; Schiemann Aromatic Fluorination; Stage #2: With hydrogen fluoride; boric acid Stage #3: In toluene at 110℃; |
Conditions | Yield |
---|---|
With dichloro(1,5-cyclooctadiene)ruthenium(II); C30H30N3P2(1+)*Cl(1-); potassium hydroxide In toluene at 120℃; for 24h; Inert atmosphere; Schlenk technique; | 94% |
With lithium hydroxide monohydrate; oxygen In water at 25℃; for 12h; | 93% |
With picoline; tert.-butylhydroperoxide; chlorophyllin coppered trisodium salt In water at 80℃; for 15h; Temperature; chemoselective reaction; | 93% |
3-fluorobenzoic acid
Conditions | Yield |
---|---|
With palladium diacetate; sodium hydride In N,N-dimethyl acetamide at 60℃; for 3h; Inert atmosphere; | 94% |
With palladium diacetate; sodium hydride In N,N-dimethyl acetamide at 50℃; for 5h; Inert atmosphere; | 94% |
3-fluorobenzoic acid
Conditions | Yield |
---|---|
With water; tetra-(n-butyl)ammonium iodide at 80℃; for 15h; Reagent/catalyst; | 91% |
With zinc diacetate; water; tetra-(n-butyl)ammonium iodide at 80℃; for 24h; | 90% |
With tetra-(n-butyl)ammonium iodide; acetic acid In water at 80℃; for 15h; Reagent/catalyst; | 84% |
1-(3-fluorophenyl)ethane-1,2-diol
3-fluorobenzoic acid
Conditions | Yield |
---|---|
With tert.-butylhydroperoxide; potassium tert-butylate In water at 80℃; for 8h; | 87% |
Conditions | Yield |
---|---|
With manganese; bis(triphenylphosphine)nickel(II) chloride; 2.9-dimethyl-1,10-phenanthroline In N,N-dimethyl-formamide at 20℃; under 760.051 Torr; for 20h; Schlenk technique; Inert atmosphere; Glovebox; | 87% |
Conditions | Yield |
---|---|
With acetic acid; silver carbonate In dimethyl sulfoxide at 120℃; for 16h; regioselective reaction; | 86% |
With [Au(1,3-bis(2,6-diisopropylphenyl)-4,5-dihydroimidazol-2-ylidene)(O2CAd)] In toluene at 120℃; regioselective reaction; |
methanol
3-fluorobromobenzene
carbon monoxide
A
3-fluorobenzoic acid
B
methyl 3-fluorobenzoate
Conditions | Yield |
---|---|
With tert-Amyl alcohol; sodium hydride; cobalt(II) acetate In tetrahydrofuran at 40℃; under 760 Torr; for 7h; Irradiation; | A 8% B 85% |
2,4-dimethylthiosemicarbazide
3-fluorobenzoyl chloride
A
3-fluorobenzoic acid
B
5-(3-fluorophenyl)-2,4-dihydro-2,4-dimethyl-3H-1,2,4-triazole-3-thione
Conditions | Yield |
---|---|
With sodium hydroxide In water; toluene at 50 - 84℃; for 1.75h; Kinetics; Temperature; Large scale; | A n/a B 85% |
Conditions | Yield |
---|---|
With 1-hydroxy-pyrrolidine-2,5-dione; oxygen; nitric acid at 90℃; under 1500.15 - 6000.6 Torr; for 30h; Autoclave; Green chemistry; | 84.13% |
Conditions | Yield |
---|---|
Stage #1: 1-ethynyl-3-fluoro-benzene With tert.-butylhydroperoxide; iron(III) chloride hexahydrate; sodium hydroxide In water at 80℃; for 10h; Stage #2: With hydrogenchloride In water at 20℃; | 83% |
With hydroxylamine hydrochloride; iodine In dimethyl sulfoxide at 100℃; for 8h; | 60% |
Conditions | Yield |
---|---|
With formic acid; 1,3-bis-(diphenylphosphino)propane; nickel(II) acetate tetrahydrate; acetic anhydride In tetrahydrofuran at 100℃; for 24h; Schlenk technique; Inert atmosphere; Sealed tube; | 81% |
1-Fluoro-3-iodobenzene
lithium formate monohydrate
3-fluorobenzoic acid
Conditions | Yield |
---|---|
With bis(1,5-cyclooctadiene)nickel(0); formic acid; 1,3-bis-(diphenylphosphino)propane; acetic anhydride In tetrahydrofuran at 100℃; for 24h; Schlenk technique; Inert atmosphere; | 81% |
Conditions | Yield |
---|---|
With niobium(V) oxide; water In neat (no solvent) for 24h; Reflux; Inert atmosphere; | 80% |
With hydrogenchloride In 1,4-dioxane at 90℃; for 3h; Rate constant; |
Conditions | Yield |
---|---|
Stage #1: 2-(3-fluorophenyl)-5,5-dimethyl-1,3,2-dioxaborinane; carbon dioxide With [Ni(N,N'-bis[2,6-bis(diphenylmethyl)-4-methylphenyl]imidazole-2-ylidene)(allyl)Cl]; potassium tert-butylate In toluene at 100℃; under 760.051 Torr; for 15h; Schlenk technique; Inert atmosphere; Stage #2: With hydrogenchloride In water; ethyl acetate; toluene at 20℃; | 78% |
diethoxyphosphoryl-acetic acid ethyl ester
3-Fluorobenzaldehyde
A
3-fluorobenzoic acid
B
3-(3-Fluorophenyl)acrylic acid ethyl ester
Conditions | Yield |
---|---|
Stage #1: diethoxyphosphoryl-acetic acid ethyl ester; 3-Fluorobenzaldehyde With potassium carbonate for 6h; Horner-Wadsworth-Emmons olefination; Neat (no solvent); high-speed ball milling; Stage #2: With Oxone for 12h; Neat (no solvent); high-speed ball milling; optical yield given as %de; diastereoselective reaction; | A n/a B 77% |
Conditions | Yield |
---|---|
Stage #1: 3-fluorophenol With fluorosulfonyl fluoride; sodium hydride In N,N-dimethyl-formamide for 0.5h; Stage #2: carbon dioxide With manganese; bis(triphenylphosphine)nickel(II) chloride; 2.9-dimethyl-1,10-phenanthroline In N,N-dimethyl-formamide at 20℃; under 760.051 Torr; for 20h; Schlenk technique; Inert atmosphere; Glovebox; | 73% |
Conditions | Yield |
---|---|
With manganese; 2,9-dibutyl-4,7-dimethyl-1,10-phenanthroline; tetraethylammonium iodide; lithium acetate; cobalt(II) bromide In N,N-dimethyl acetamide at 100℃; under 760.051 Torr; for 12h; Inert atmosphere; Schlenk technique; | 71% |
Stage #1: 3-chlorofluorobenzene With bis(cyclopentadienyl)titanium dichloride; butyl magnesium bromide In tetrahydrofuran at 40℃; for 6h; Inert atmosphere; Schlenk technique; Stage #2: carbon dioxide In tetrahydrofuran at 20℃; for 2h; Inert atmosphere; Schlenk technique; | 60% |
Conditions | Yield |
---|---|
With iron(III) chloride; cerium(III) chloride; tetrabutyl-ammonium chloride; oxygen In acetonitrile at 20℃; under 760.051 Torr; for 24h; Schlenk technique; Irradiation; | 71% |
Conditions | Yield |
---|---|
With copper(l) iodide; hydroxylamine hydrochloride; oxygen In dimethyl sulfoxide at 100℃; for 10h; | 65% |
With hydroxylamine hydrochloride; iodine In dimethyl sulfoxide at 100℃; for 5h; | 64% |
With sodium hydroxide; potassium chloride; potassium hexacyanoferrate(III) In methanol; water at 30℃; Kinetics; further temperature; |
Conditions | Yield |
---|---|
With manganese; 2.9-dimethyl-1,10-phenanthroline; lithium acetate; cobalt(II) bromide In N,N-dimethyl acetamide at 20℃; under 760.051 Torr; for 12h; Inert atmosphere; Schlenk technique; | 64% |
4-bromo-2-chloro-5-fluorobenzoic acid
A
3-fluorobenzoic acid
B
2-chloro-5-fluoro-benzoic acid
Conditions | Yield |
---|---|
With triethanolamine; C33H21IrN3O9S3(3-) In water for 6h; Alkaline conditions; Inert atmosphere; Irradiation; | A 60% B n/a |
Conditions | Yield |
---|---|
With picoline; tert.-butylhydroperoxide; chlorophyllin coppered trisodium salt In water at 60℃; for 12h; Temperature; chemoselective reaction; | A 35% B 56% |
Conditions | Yield |
---|---|
With copper(l) iodide; N,N,N,N,-tetramethylethylenediamine; diethylzinc In N,N-dimethyl acetamide at 70℃; under 760.051 Torr; | 55% |
Stage #1: 1-Fluoro-3-iodobenzene With copper In tetrahydrofuran at 25℃; for 0.5h; Stage #2: carbon dioxide In tetrahydrofuran for 24h; | 31% |
Stage #1: carbon dioxide; 1-Fluoro-3-iodobenzene With tert.-butyl lithium In pentane at -70℃; Inert atmosphere; Stage #2: With sulfuric acid; water In pentane at 20℃; Inert atmosphere; | 17% |
Conditions | Yield |
---|---|
With ethanol In water at 85℃; for 50h; von Richter Aromatic Carboxylation; Ionic liquid; | 52% |
carbon dioxide
3-fluorophenyl 4-methylbenzenesulfonate
3-fluorobenzoic acid
Conditions | Yield |
---|---|
With manganese; (2,2'-bipyridine)nickel(II) dibromide In N,N-dimethyl-formamide at 60℃; under 760.051 Torr; | 51% |
3-fluorobenzoic acid
Conditions | Yield |
---|---|
With fluorine In FC-72 at -85℃; for 0.583333h; | 24% |
3-fluorobromobenzene
carbon monoxide
A
3-fluorobenzoic acid
B
methyl 3-fluorobenzoate
Conditions | Yield |
---|---|
With methanol; tert-Amyl alcohol; sodium hydride; cobalt(II) acetate In tetrahydrofuran at 40℃; under 760 Torr; for 7h; Irradiation; | A 8% B 8% |
Conditions | Yield |
---|---|
Stage #1: 3-fluorobenzoic acid With N,N-dimethyl-formamide In dichloromethane at 0℃; for 0.0833333h; Stage #2: With oxalyl dichloride In dichloromethane at 20℃; for 12h; | 100% |
With thionyl chloride Heating; | 87% |
With phosphorus pentachloride |
3-fluorobenzoic acid
Conditions | Yield |
---|---|
With 6-chloro-3-((dimethylamino)(dimethyliminio)methyl)-1H-benzo[d][1,2,3]triazol-3-ium-1-olatehexafluorophosphate(V); N-ethyl-N,N-diisopropylamine In dichloromethane; N,N-dimethyl-formamide at 20℃; for 2.25h; | 100% |
Conditions | Yield |
---|---|
With C30H54N6Ru(2+)*2BF4(1-); potassium perfluoro-tert-butoxide; potassium carbonate at 140℃; for 24h; Glovebox; Inert atmosphere; | 99% |
Conditions | Yield |
---|---|
Stage #1: 3-fluorobenzoic acid With N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate In N,N-dimethyl-formamide at 0℃; Stage #2: L-leucine ethyl ester hydrochloride In N,N-dimethyl-formamide at 0 - 20℃; | 99% |
Conditions | Yield |
---|---|
With borane-ammonia complex In 5,5-dimethyl-1,3-cyclohexadiene for 6h; Reflux; | 99% |
3-fluorobenzoic acid
Conditions | Yield |
---|---|
With caesium carbonate In dichloromethane at 20℃; for 16h; Inert atmosphere; Schlenk technique; | 99% |
Conditions | Yield |
---|---|
With sulfated zirconia at 130℃; for 1h; Catalytic behavior; Temperature; Time; Microwave irradiation; | 98.5% |
bis(dimethylphenylphosphine)tris(pentafluorothiophenolato)osmium(III)
3-fluorobenzoic acid
Conditions | Yield |
---|---|
In acetone (air); shaking (room temp., 48 h); solvent removal (vac.), washing (EtOH), crystn. (acetone-EtOH); elem. anal.; | 98% |
3-fluorobenzoic acid
N-biphenyl-4-yl-3-oxo-3-piperazin-1-yl-propionamide hydrochloride
N-biphenyl-4-yl-3-[4-(3-fluoro-benzoyl)-piperazin-1-yl]-3-oxo-propionamide
Conditions | Yield |
---|---|
With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 10 - 20℃; | 98% |
3-fluorobenzoic acid
Conditions | Yield |
---|---|
With [2,2]bipyridinyl; oxygen; palladium diacetate In tetrahydrofuran at 60℃; under 760.051 Torr; for 12h; Schlenk technique; Molecular sieve; | 98% |
Cyclohexyl isocyanide
3-fluorobenzoic acid
4-[2,2-bis(trimethylsilyl)ethenyl]benzaldehyde
Conditions | Yield |
---|---|
In water at 20℃; for 1.5h; Passerini Condensation; | 98% |
Conditions | Yield |
---|---|
With sulfuric acid; nitric acid | 97% |
With sulfuric acid; nitric acid; phosphorus pentoxide at 0℃; for 3h; | 95% |
With sulfuric acid; nitric acid at 0 - 20℃; for 1h; | 93% |
Conditions | Yield |
---|---|
With potassium carbonate In dimethyl sulfoxide at 60℃; for 3h; | 97% |
3-fluorobenzoic acid
Conditions | Yield |
---|---|
With 2,4,6-tripropyl-1,3,5,2,4,6-trioxatriphosphinane-2,4,6-trioxide; triethylamine In ethyl acetate for 1h; | 97% |
3-fluorobenzoic acid
Conditions | Yield |
---|---|
With 2,4,6-tripropyl-1,3,5,2,4,6-trioxatriphosphinane-2,4,6-trioxide; triethylamine In ethyl acetate at 20℃; for 1.16667h; | 96% |
3-fluorobenzoic acid
N-isocyaniminotriphenylphosphorane
dimethylglyoxal
3-[5-(3-fluorophenyl)-1,3,4-oxadiazol-2-yl]-3-hydroxybutan-2-one
Conditions | Yield |
---|---|
In water at 20 - 26℃; for 12h; Green chemistry; | 95% |
In dichloromethane at 20℃; for 12.25h; tandem Passerini/intramolecular aza-Wittig reaction; | 90% |
ethyl 2,3,4-tri-O-benzyl-1-thio-α-D-glucopyranoside
3-fluorobenzoic acid
Conditions | Yield |
---|---|
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 20℃; for 18h; | 95% |
Conditions | Yield |
---|---|
With silver carbonate; palladium dichloride In dimethyl sulfoxide; N,N-dimethyl-formamide at 80℃; for 7h; | 95% |
3-fluorobenzoic acid
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate In N,N-dimethyl-formamide at 20℃; for 1h; | 95% |
Conditions | Yield |
---|---|
With di-isopropyl azodicarboxylate; triphenylphosphine In tetrahydrofuran at 0 - 20℃; for 48h; Schlenk technique; Inert atmosphere; | 95% |
With di-isopropyl azodicarboxylate; triphenylphosphine In tetrahydrofuran at 0 - 20℃; for 24h; |
3-fluorobenzoic acid
Conditions | Yield |
---|---|
With caesium carbonate In dichloromethane at 20℃; for 16h; Inert atmosphere; Schlenk technique; | 95% |
3-fluorobenzoic acid
Conditions | Yield |
---|---|
With O‑(6‑chlorobezotriazol‑1‑yl)‑N,N,N,N‑tetramethyluronium hexafluorophosphate; triethylamine In ethyl acetate at 70℃; for 1h; | 94.15% |
Conditions | Yield |
---|---|
With oxygen; lithium hydroxide In water at 20℃; for 14h; Sonication; | 94% |
3-fluorobenzoic acid
Conditions | Yield |
---|---|
With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 20℃; for 22h; | 94% |
1,2,3-Benzotriazole
3-fluorobenzoic acid
1-(3-fluorobenzoyl)benzotriazole
Conditions | Yield |
---|---|
With thionyl chloride In dichloromethane for 2h; Inert atmosphere; | 93% |
With thionyl chloride In dichloromethane at 20℃; | 80% |
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