Products

Refine

Country

Business Type

Certificate

Display

Dayang Chem (Hangzhou) Co.,Ltd.

Dayangchem's R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantities

2',4',6'-Trihydroxyacetophenone monohydrate Manufacturer/High quality/Best price/In stock

Cas:480-66-0

Min.Order:1 Kilogram

FOB Price: $3.0

Type:Lab/Research institutions

inquiry

Simagchem Corporation

Welcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our

High quality 2,4,6-Trihydroxyacetophenone supplier in China

Cas:480-66-0

Min.Order:0 Metric Ton

Negotiable

Type:Manufacturers

inquiry

Henan Allgreen Chemical Co.,Ltd

2',4',6'-Trihydroxyacetophenone monohydrate Basic information Product Name: 2',4',6'-Trihydroxyacetophenone monohydrate Synonyms: 1-(2,4,6-T

480-66-02',4',6'-Trihydroxyacetophenone monohydrate

Cas:480-66-0

Min.Order:1 Kilogram

Negotiable

Type:Manufacturers

inquiry

Chemwill Asia Co., Ltd.

Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block

Phloroacetophenone

Cas:480-66-0

Min.Order:5 Kiloliter

FOB Price: $1.2 / 5.0

Type:Manufacturers

inquiry

Henan Tianfu Chemical Co., Ltd.

Our company was built in 2009 with an ISO certificate.In the past 5 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so on.O

1-(2,4,6-TRIHYDROXYPHENYL)-ETHANONE

Cas:480-66-0

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Zhuozhou Wenxi import and Export Co., Ltd

WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et

New production CAS 480-66-0 with best quality

Cas:480-66-0

Min.Order:1 Kilogram

FOB Price: $139.0 / 210.0

Type:Trading Company

inquiry

Wuhan Han Sheng New Material Technology Co.,Ltd

Our Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We

High quality 2',4',6'-Trihydroxyacetophenone monohydrate CAS NO.480-66-0

Cas:480-66-0

Min.Order:10 Kilogram

Negotiable

Type:Trading Company

inquiry

Hebei Sankai Chemical Technology Co., Ltd

1. Product advantages ♦ High purity, all above 98.5%, no impurities after dissolution ♦ We will test each batch to ensure quality ♦ OEM and private brand services designed for free ♦ Various cap colors available ♦ W

2',4',6'-Trihydroxyacetophenone monohydrate CAS:480-66-0

Cas:480-66-0

Min.Order:1 Kilogram

FOB Price: $290.0 / 590.0

Type:Trading Company

inquiry

Henan Sinotech Import&Export Corporation

Product name 2',4',6'-Trihydroxyacetophenone monohydrate CAS NO. 480-66-0 Molecular formula C8H8O4.H2O

2',4',6'-Trihydroxyacetophenone monohydrate

Cas:480-66-0

Min.Order:5 Metric Ton

FOB Price: $1.0 / 2.0

Type:Other

inquiry

Shanghai Upbio Tech Co.,Ltd

1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized

2',4',6'-Trihydroxyacetophenone monohydrate 480-66-0

Cas:480-66-0

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Baoji Guokang Healthchem co.,ltd

Our company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At prese

2',4',6'-Trihydroxyacetophenone monohydrate

Cas:480-66-0

Min.Order:1 Kilogram

FOB Price: $100.0 / 120.0

Type:Trading Company

inquiry

Qingdao Beluga Import and Export Co., LTD

2',4',6'-Trihydroxyacetophenone monohydrate CAS:480-66-0 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, speciali

2',4',6'-Trihydroxyacetophenone monohydrate CAS:480-66-0

Cas:480-66-0

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Shandong Hanjiang Chemical Co., Ltd.

Hello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai

2',4',6'-Trihydroxyacetophenone monohydrate

Cas:480-66-0

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Henan Wentao Chemical Product Co., Ltd.

Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

2',4',6'-Trihydroxyacetophenone monohydrate

Cas:480-66-0

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Xiamen Hisunny Chemical Co.,Ltd

Best quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia

2,4,6-Trihydroxylacetophenone

Cas:480-66-0

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Afine Chemicals Limited

Company Introduction 1. Established in 2005, with two independent business divisions: Fine chemicals division; Pharmaceutical division. 2. Main product: Optical brightener Textile auxiliary Dye stuff Pigments

2',4',6'-TRIHYDROXYACETOPHENONE MONOHYDRATE

Cas:480-66-0

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Hangzhou J&H Chemical Co., Ltd.

J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

2,4,6-Trihydroxylacetophenone

Cas:480-66-0

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Ality Chemical Corporation

The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi

Factory Supply 2',4',6'-Trihydroxyacetophenone monohydrate

Cas:480-66-0

Min.Order:0 Metric Ton

Negotiable

Type:Other

inquiry

Zibo Hangyu Biotechnology Development Co., Ltd

Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi

High quality 2',4',6'-Trihydroxyacetophenone monohydrate

Cas:480-66-0

Min.Order:10 Gram

FOB Price: $100.0

Type:Lab/Research institutions

inquiry

SHANGHAI SYSTEAM BIOCHEM CO., LTD

We are one of a few suppliers that can offer custom synthesis service of this product We are specialized in custom synthesis, chemical/pharmaceutical/ pesticides outsourcing and contract research. We are committed to prov

High quality 2',4',6'-Trihydroxyacetophenone monohydrate CAS NO.480-66-0

Cas:480-66-0

Min.Order:100 Gram

FOB Price: $100.0 / 2000.0

Type:Lab/Research institutions

inquiry

HANGZHOU YUNUO CHEMICAL CO.,LTD

Superior quality, moderate price & quick delivery. Appearance:Light Brown Solid Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:as per your request Application:Induced choleresis in rats is mediated through mu

2',4',6'-Trihydroxyacetophenone monohydrate

Cas:480-66-0

Min.Order:100 Gram

Negotiable

Type:Trading Company

inquiry

Zibo Dorne chemical technology co. LTD

Product Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,

2',4',6'-Trihydroxyacetophenone monohydrate

Cas:480-66-0

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Jiangsu Qianyu Molecular Technology Co., LTD.

Our Advantages A. International Top level TechnologyOur company owned biomedicine experts are famous at home and abroad with rich experience in research and development in the field of efficient chiral functional molecules research and development an

Best Offer2',4',6'-Trihydroxyacetophenone monohydrate

Cas:480-66-0

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Xiamen Jenny Chemical Technology Co., Ltd.

GMP standard, high purity, competitive price, in stock 1. Quick Response: within 6 hours after receiving your email. 2. Quality Guarantee: All products are strictly tested by our QC, confirmed by QA, and approved by a third-party lab in China, USA,

2',4',6'-Trihydroxyacetophenonemonohydrate

Cas:480-66-0

Min.Order:1 Milligram

Negotiable

Type:Trading Company

inquiry

Shanghai Minstar Chemical Co., Ltd

2',4',6'-Trihydroxyacetophenone monohydrate Chemical Properties Melting point 219-221 °C(lit.) Boiling point 257.07°C (rough estimate) density 1.3037 (rough estimate) refractive index 1.5090 (estimate) storage temp

2',4',6'-Trihydroxyacetophenone monohydrate

Cas:480-66-0

Min.Order:1 Gram

FOB Price: $66.0

Type:Lab/Research institutions

inquiry

EAST CHEMSOURCES LIMITED

factory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B

High quality 2',4',6'-Trihydroxyacetophenone monohydrate CAS NO.480-66-0

Cas:480-66-0

Min.Order:1 Kilogram

FOB Price: $18.0 / 20.0

Type:Trading Company

inquiry

Shandong Mopai Biotechnology Co., LTD

Shandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W

High quality 2',4',6'-Trihydroxyacetophenone monohydrate CAS NO.480-66-0

Cas:480-66-0

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

KAISA GROUP INC

1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer

High quality 2',4',6'-Trihydroxyacetophenone monohydrate CAS NO.480-66-0

Cas:480-66-0

Min.Order:1 Metric Ton

FOB Price: $1.5

Type:Trading Company

inquiry

Hangzhou Zhongqi chem Co.,Ltd.

Located in Hangzhou National Hi-Tech Industrial Development Zone, zhongqichem is a technical company mainly focus on the Custom synthesis, manufacturing, sales of chemicals to various industries. Benefiting from the outstanding customer service and h

2',4',6'-Trihydroxyacetophenone monohydrate

Cas:480-66-0

Min.Order:0

Negotiable

Type:Other

inquiry

Hubei Langyou International Trading Co., Ltd

1.Good capacity; 2.Safe deliver 3. High quality with best price Appearance:White Powder Storage:Dry and cool place Package:100g/ bag, 2 kg/ bag, 25kg/ carton or as required Application:For Pharmaceutical Intermediates Transportation:By DHL, TNT

2',4',6'-Trihydroxyacetophenone monohydrate

Cas:480-66-0

Min.Order:10 Gram

Negotiable

Type:Other

inquiry

Synthetic route

3,5-dihydroxyphenol
108-73-6

3,5-dihydroxyphenol

acetonitrile
75-05-8

acetonitrile

2,4,6-trihydroxyacetophenone
480-66-0

2,4,6-trihydroxyacetophenone

Conditions
ConditionsYield
Stage #1: 3,5-dihydroxyphenol; acetonitrile With hydrogenchloride; zinc(II) chloride In di-isopropyl ether at 0℃;
Stage #2: With water for 2h; Reflux;
96.2%
Stage #1: 3,5-dihydroxyphenol; acetonitrile With hydrogenchloride; zinc(II) chloride In diethyl ether at -20℃; for 2h;
Stage #2: With water for 2h; Reflux;
80%
With hydrogenchloride; zinc(II) chloride In diethyl ether for 6h; Cooling with ice;80.7%
1-(2,4,6-tris((tert-butyldimethylsilyl)oxy)phenyl)ethan-1-one
265975-36-8

1-(2,4,6-tris((tert-butyldimethylsilyl)oxy)phenyl)ethan-1-one

2,4,6-trihydroxyacetophenone
480-66-0

2,4,6-trihydroxyacetophenone

Conditions
ConditionsYield
With N,N,N',N'-tetramethylguanidine In acetonitrile at 50℃; for 1h;92%
3,5-dihydroxyphenol
108-73-6

3,5-dihydroxyphenol

acetic acid butyl ester
123-86-4

acetic acid butyl ester

2,4,6-trihydroxyacetophenone
480-66-0

2,4,6-trihydroxyacetophenone

Conditions
ConditionsYield
With 4-chlorophenylethylamine; copper(I) bromide at 5℃; for 35h; Temperature; Reflux;92%
3,5-dihydroxyphenol
108-73-6

3,5-dihydroxyphenol

acetic anhydride
108-24-7

acetic anhydride

2,4,6-trihydroxyacetophenone
480-66-0

2,4,6-trihydroxyacetophenone

Conditions
ConditionsYield
With boron trifluoride diethyl etherate In ethyl acetate at 40℃; for 10h;90%
With boron trifluoride diethyl etherate In ethyl acetate at 40℃; for 10h;90%
With boron trifluoride diethyl etherate at 20℃; for 15h; Inert atmosphere;88%
2-(1-iminoethyl)phenyl-1,3,5-triol hydrochloride

2-(1-iminoethyl)phenyl-1,3,5-triol hydrochloride

2,4,6-trihydroxyacetophenone
480-66-0

2,4,6-trihydroxyacetophenone

Conditions
ConditionsYield
With water Heating;90%
With water for 3h; Reflux;20%
With water for 3h; Reflux;20%
With water for 1.5h; Heating;
In water for 2h; Reflux;
1-{4-[(tert-butyldimethylsilyl)oxy]-2,6-dihydroxyphenyl}ethan-1-one
139140-13-9

1-{4-[(tert-butyldimethylsilyl)oxy]-2,6-dihydroxyphenyl}ethan-1-one

2,4,6-trihydroxyacetophenone
480-66-0

2,4,6-trihydroxyacetophenone

Conditions
ConditionsYield
With KF-Al2O3 (basic) In acetonitrile for 18h; Ambient temperature;86%
1-[2,4,6-tris(acetyloxy)phenyl]ethanone
144152-27-2

1-[2,4,6-tris(acetyloxy)phenyl]ethanone

2,4,6-trihydroxyacetophenone
480-66-0

2,4,6-trihydroxyacetophenone

Conditions
ConditionsYield
With water; sodium acetate In ethanol for 5h; Reflux;86%
3,5-dihydroxyphenol
108-73-6

3,5-dihydroxyphenol

acetyl chloride
75-36-5

acetyl chloride

2,4,6-trihydroxyacetophenone
480-66-0

2,4,6-trihydroxyacetophenone

Conditions
ConditionsYield
With carbon disulfide; aluminum (III) chloride In nitrobenzene at 20 - 50℃; for 1h;85.7%
Stage #1: 3,5-dihydroxyphenol With aluminum (III) chloride In dichloromethane; nitrobenzene at 0℃; Inert atmosphere;
Stage #2: acetyl chloride In dichloromethane; nitrobenzene at 0 - 90℃; for 4h; Inert atmosphere;
85%
Stage #1: 3,5-dihydroxyphenol With aluminum (III) chloride In nitrobenzene; 1,2-dichloro-ethane at 0℃; for 0.166667h; Friedel-Crafts Acylation; Inert atmosphere;
Stage #2: acetyl chloride In nitrobenzene; 1,2-dichloro-ethane for 5h; Friedel-Crafts Acylation; Inert atmosphere;
82.5%
3,5-dihydroxyphenol
108-73-6

3,5-dihydroxyphenol

acetic acid
64-19-7

acetic acid

2,4,6-trihydroxyacetophenone
480-66-0

2,4,6-trihydroxyacetophenone

Conditions
ConditionsYield
With zinc(II) chloride at 140 - 145℃; for 2h; Friedel Crafts acylation;80%
With boron trifluoride
1-[2,4-bis(benzyloxy)-6-hydroxyphenyl]ethanone
18065-05-9

1-[2,4-bis(benzyloxy)-6-hydroxyphenyl]ethanone

2,4,6-trihydroxyacetophenone
480-66-0

2,4,6-trihydroxyacetophenone

Conditions
ConditionsYield
With triethylammonium formate; palladium on activated charcoal for 2h; Ambient temperature;75%
3,5-dihydroxyphenol
108-73-6

3,5-dihydroxyphenol

acetic anhydride
108-24-7

acetic anhydride

A

2,4-diacetylphloroglucinol
2161-86-6

2,4-diacetylphloroglucinol

B

2,4,6-trihydroxyacetophenone
480-66-0

2,4,6-trihydroxyacetophenone

Conditions
ConditionsYield
With zinc(II) chloride at 145 - 150℃; for 0.25h;A 25%
B 50%
3,5-dihydroxyphenol
108-73-6

3,5-dihydroxyphenol

benzene-1,4-diyl diacetate
1205-91-0

benzene-1,4-diyl diacetate

A

2,4,6-trihydroxyacetophenone
480-66-0

2,4,6-trihydroxyacetophenone

B

2,5-Dihydroxyacetophenone
490-78-8

2,5-Dihydroxyacetophenone

Conditions
ConditionsYield
With boron trifluoride diethyl etherate In benzene for 0.5h; cross Fries reaction; microwave irradiation;A 35%
B 40%
acetylacetone
123-54-6

acetylacetone

malonic acid dimethyl ester
108-59-8

malonic acid dimethyl ester

A

2,4,6-trihydroxyacetophenone
480-66-0

2,4,6-trihydroxyacetophenone

B

methyl orsellinate
3187-58-4

methyl orsellinate

Conditions
ConditionsYield
With n-butyllithium; sodium hydride In tetrahydrofuran; hexane for 48h; Heating;A 30%
B 8%
3,5-dihydroxyphenol
108-73-6

3,5-dihydroxyphenol

Phenyl acetate
122-79-2

Phenyl acetate

2,4,6-trihydroxyacetophenone
480-66-0

2,4,6-trihydroxyacetophenone

Conditions
ConditionsYield
With boron trifluoride diethyl etherate In benzene for 3h; crossover Friess rearrangement; Heating;30%
3,5-dihydroxyphenol
108-73-6

3,5-dihydroxyphenol

A

4-methyl-5,7-dihydroxycoumarin
2107-76-8

4-methyl-5,7-dihydroxycoumarin

B

2,4,6-trihydroxyacetophenone
480-66-0

2,4,6-trihydroxyacetophenone

Conditions
ConditionsYield
With aluminium trichloride; nitrobenzene; acetyl chloride Erhitzen des Reaktionsprodukts mit wss. Salzsaeure;
2,4-diacetylphloroglucinol
2161-86-6

2,4-diacetylphloroglucinol

2,4,6-trihydroxyacetophenone
480-66-0

2,4,6-trihydroxyacetophenone

Conditions
ConditionsYield
With sodium hydroxide at 25℃;
With sodium methylate In methanol
1,3,5-triacetyl-2,4,6-trihydroxybenzene
2161-87-7

1,3,5-triacetyl-2,4,6-trihydroxybenzene

2,4,6-trihydroxyacetophenone
480-66-0

2,4,6-trihydroxyacetophenone

Conditions
ConditionsYield
With sodium hydroxide at 25℃;
Multi-step reaction with 2 steps
1: diluted NaOH-solution
2: diluted NaOH-solution / 25 °C
View Scheme
3-(3-ethoxycarbonyl-2,4,6-trihydroxy-phenyl)-3-oxo-propionic acid ethyl ester

3-(3-ethoxycarbonyl-2,4,6-trihydroxy-phenyl)-3-oxo-propionic acid ethyl ester

2,4,6-trihydroxyacetophenone
480-66-0

2,4,6-trihydroxyacetophenone

Conditions
ConditionsYield
With water at 160 - 170℃;
2-(5,7-dihydroxy-4-methylene-4H-chromen-2-yl)-phloroglucinol

2-(5,7-dihydroxy-4-methylene-4H-chromen-2-yl)-phloroglucinol

furan-2,3,5(4H)-trione pyridine (1:1)

furan-2,3,5(4H)-trione pyridine (1:1)

2,4,6-trihydroxyacetophenone
480-66-0

2,4,6-trihydroxyacetophenone

3,5-dihydroxyphenol
108-73-6

3,5-dihydroxyphenol

acetyl chloride
75-36-5

acetyl chloride

A

4-methyl-5,7-dihydroxycoumarin
2107-76-8

4-methyl-5,7-dihydroxycoumarin

B

2,4,6-trihydroxyacetophenone
480-66-0

2,4,6-trihydroxyacetophenone

Conditions
ConditionsYield
With aluminium trichloride; nitrobenzene Erhitzen des Reaktionsprodukts mit wss.HCl;
methyl 3,5,7-trioxooctanoate
23066-87-7

methyl 3,5,7-trioxooctanoate

2,4,6-trihydroxyacetophenone
480-66-0

2,4,6-trihydroxyacetophenone

Conditions
ConditionsYield
With potassium hydroxide
2-hydroxy-4,6-dimethoxyacetophenone
90-24-4

2-hydroxy-4,6-dimethoxyacetophenone

A

2,4,6-trihydroxyacetophenone
480-66-0

2,4,6-trihydroxyacetophenone

B

4,6-dihydroxy-2-methoxyacetophenone
3602-54-8

4,6-dihydroxy-2-methoxyacetophenone

Conditions
ConditionsYield
With aluminium trichloride In chlorobenzene for 1h; Heating;A 1.6 g
B 2.0 g
3,5-dihydroxyphenol
108-73-6

3,5-dihydroxyphenol

acetic acid
64-19-7

acetic acid

A

2,4-diacetylphloroglucinol
2161-86-6

2,4-diacetylphloroglucinol

B

2,4,6-trihydroxyacetophenone
480-66-0

2,4,6-trihydroxyacetophenone

Conditions
ConditionsYield
With boron trifluoride diethyl etherate at 100℃; for 2h;
1-(2,4,6-trimethoxyphenyl)ethanone
832-58-6

1-(2,4,6-trimethoxyphenyl)ethanone

A

2-hydroxy-4,6-dimethoxyacetophenone
90-24-4

2-hydroxy-4,6-dimethoxyacetophenone

B

2,4,6-trihydroxyacetophenone
480-66-0

2,4,6-trihydroxyacetophenone

C

2,6-dihydroxy-4-methoxy-acetophenone
7507-89-3

2,6-dihydroxy-4-methoxy-acetophenone

D

4,6-dihydroxy-2-methoxyacetophenone
3602-54-8

4,6-dihydroxy-2-methoxyacetophenone

Conditions
ConditionsYield
With aluminium trichloride In chlorobenzeneA n/a
B n/a
C n/a
D 29 % Chromat.
1-(2,4,6-trimethoxyphenyl)ethanone
832-58-6

1-(2,4,6-trimethoxyphenyl)ethanone

2,4,6-trihydroxyacetophenone
480-66-0

2,4,6-trihydroxyacetophenone

Conditions
ConditionsYield
With pyridine hydrochloride
2-hydroxy-4,6-dimethoxyacetophenone
90-24-4

2-hydroxy-4,6-dimethoxyacetophenone

2,4,6-trihydroxyacetophenone
480-66-0

2,4,6-trihydroxyacetophenone

Conditions
ConditionsYield
With In methanol; water
hydrogenchloride
7647-01-0

hydrogenchloride

3,5-dihydroxyphenol
108-73-6

3,5-dihydroxyphenol

diethyl ether
60-29-7

diethyl ether

acetonitrile
75-05-8

acetonitrile

2,4,6-trihydroxyacetophenone
480-66-0

2,4,6-trihydroxyacetophenone

Conditions
ConditionsYield
nachfolgend Kochen des Reaktionsproduktes mit Wasser;
3,5-dihydroxyphenol
108-73-6

3,5-dihydroxyphenol

Resorcinol diacetate
108-58-7

Resorcinol diacetate

sulfuric acid
7664-93-9

sulfuric acid

A

2',4'-dihydroxy-4-acetophenone
89-84-9

2',4'-dihydroxy-4-acetophenone

B

2,4-diacetylphloroglucinol
2161-86-6

2,4-diacetylphloroglucinol

C

2,4,6-trihydroxyacetophenone
480-66-0

2,4,6-trihydroxyacetophenone

1-<2.4.6-trihydroxy-phenyl>-ethanone-(1)-imine sulfate

1-<2.4.6-trihydroxy-phenyl>-ethanone-(1)-imine sulfate

2,4,6-trihydroxyacetophenone
480-66-0

2,4,6-trihydroxyacetophenone

Conditions
ConditionsYield
With water
2,4,6-trihydroxyacetophenone
480-66-0

2,4,6-trihydroxyacetophenone

dimethyl sulfate
77-78-1

dimethyl sulfate

2-hydroxy-4,6-dimethoxyacetophenone
90-24-4

2-hydroxy-4,6-dimethoxyacetophenone

Conditions
ConditionsYield
With potassium carbonate In acetone Inert atmosphere;100%
With potassium carbonate In acetone for 3h; Reflux;100%
With potassium carbonate In acetone at 66℃; for 2h; Inert atmosphere;100%
Dimethoxymethane
109-87-5

Dimethoxymethane

2,4,6-trihydroxyacetophenone
480-66-0

2,4,6-trihydroxyacetophenone

2'-hydroxy-4',6'-bis(methoxymethoxy)acetophenone
65490-09-7

2'-hydroxy-4',6'-bis(methoxymethoxy)acetophenone

Conditions
ConditionsYield
Stage #1: Dimethoxymethane With acetyl chloride; zinc dibromide In dichloromethane at 20 - 30℃; for 3.5h;
Stage #2: 2,4,6-trihydroxyacetophenone With N-ethyl-N,N-diisopropylamine In dichloromethane at 5 - 10℃;
100%
Stage #1: Dimethoxymethane With acetyl chloride; zinc dibromide at 20℃; for 2h; Inert atmosphere;
Stage #2: 2,4,6-trihydroxyacetophenone With diisopropylamine In dichloromethane for 3h; Inert atmosphere; Cooling with ice; regioselective reaction;
50%
Stage #1: Dimethoxymethane With acetyl chloride; zinc dibromide In dichloromethane at 20℃; for 3.5h;
Stage #2: 2,4,6-trihydroxyacetophenone With N-ethyl-N,N-diisopropylamine In dichloromethane at 5℃;
2,4,6-trihydroxyacetophenone
480-66-0

2,4,6-trihydroxyacetophenone

tert-butyldimethylsilyl chloride
18162-48-6

tert-butyldimethylsilyl chloride

1-{4-[(tert-butyldimethylsilyl)oxy]-2,6-dihydroxyphenyl}ethan-1-one
139140-13-9

1-{4-[(tert-butyldimethylsilyl)oxy]-2,6-dihydroxyphenyl}ethan-1-one

Conditions
ConditionsYield
Stage #1: 2,4,6-trihydroxyacetophenone; tert-butyldimethylsilyl chloride With 1H-imidazole In N,N-dimethyl-formamide at 20℃; for 1h; Inert atmosphere;
Stage #2: With pyridinium p-toluenesulfonate In methanol for 4h; Inert atmosphere; Reflux;
99%
2,4,6-trihydroxyacetophenone
480-66-0

2,4,6-trihydroxyacetophenone

acetic anhydride
108-24-7

acetic anhydride

3-Acetyl-5,7-bis(acetyloxy)-2-methyl-4H-1-benzopyran-4-one
1162-81-8

3-Acetyl-5,7-bis(acetyloxy)-2-methyl-4H-1-benzopyran-4-one

Conditions
ConditionsYield
With sodium acetate for 9h; Heating;98%
With sodium acetate
With sodium acetate for 10h; Heating;11.8 g
With sodium acetate for 10h; Heating / reflux;
With sodium acetate for 10h; Heating / reflux;
dimedone
3471-13-4

dimedone

2,4,6-trihydroxyacetophenone
480-66-0

2,4,6-trihydroxyacetophenone

isobutyraldehyde
78-84-2

isobutyraldehyde

2-(1-(3-acetyl-2,4,6-trihydroxy-5-(1-(2-hydroxy-4,4-dimethyl-6-oxocyclohex-1-enyl)-2-methylpropyl)phenyl)-2-methylpropyl)-3-hydroxy-5,5-dimethylcyclohex-2-enone
1224866-14-1

2-(1-(3-acetyl-2,4,6-trihydroxy-5-(1-(2-hydroxy-4,4-dimethyl-6-oxocyclohex-1-enyl)-2-methylpropyl)phenyl)-2-methylpropyl)-3-hydroxy-5,5-dimethylcyclohex-2-enone

Conditions
ConditionsYield
Stage #1: dimedone; isobutyraldehyde With piperidine In dichloromethane at 20℃; for 0.25h; Mannich reaction;
Stage #2: With hydrogenchloride; ammonium chloride In water
Stage #3: 2,4,6-trihydroxyacetophenone With sodium hydride In tetrahydrofuran at 20℃; for 3h; Friedel Crafts alkylation;
96%
2,4,6-trihydroxyacetophenone
480-66-0

2,4,6-trihydroxyacetophenone

acetic anhydride
108-24-7

acetic anhydride

acetic acid 5-acetoxy-2-acetyl-3-hydroxyphenyl ester
17820-33-6

acetic acid 5-acetoxy-2-acetyl-3-hydroxyphenyl ester

Conditions
ConditionsYield
With pyridine; dmap at 60℃; for 3h;95%
With pyridine; dmap at 60℃; for 3h;95%
With pyridine for 5h; Ambient temperature;38%
With pyridine
2,4,6-trihydroxyacetophenone
480-66-0

2,4,6-trihydroxyacetophenone

chloromethyl methyl ether
107-30-2

chloromethyl methyl ether

2,4,6-tri-MOM phloracetophenone
36804-11-2

2,4,6-tri-MOM phloracetophenone

Conditions
ConditionsYield
With sodium hydride In N,N-dimethyl-formamide at 0 - 20℃; for 0.75h;95%
With sodium hydride In N,N-dimethyl-formamide at 85℃; for 4h; Temperature;95%
Stage #1: 2,4,6-trihydroxyacetophenone With sodium hydride In N,N-dimethyl-formamide; mineral oil at 0℃; for 0.0833333h; Inert atmosphere;
Stage #2: chloromethyl methyl ether In N,N-dimethyl-formamide; mineral oil at 0 - 20℃; for 0.75h; Inert atmosphere;
83%
2,4,6-trihydroxyacetophenone
480-66-0

2,4,6-trihydroxyacetophenone

tert-butyldimethylsilyl chloride
18162-48-6

tert-butyldimethylsilyl chloride

1-(2,4,6-tris((tert-butyldimethylsilyl)oxy)phenyl)ethan-1-one
265975-36-8

1-(2,4,6-tris((tert-butyldimethylsilyl)oxy)phenyl)ethan-1-one

Conditions
ConditionsYield
With 1,8-diazabicyclo[5.4.0]undec-7-ene In dichloromethane at 20℃; silylation;95%
With sodium hydride In tetrahydrofuran; mineral oil at 0℃; for 3h;91%
2,4,6-trihydroxyacetophenone
480-66-0

2,4,6-trihydroxyacetophenone

benzyl bromide
100-39-0

benzyl bromide

1-[2,4-bis(benzyloxy)-6-hydroxyphenyl]ethanone
18065-05-9

1-[2,4-bis(benzyloxy)-6-hydroxyphenyl]ethanone

Conditions
ConditionsYield
With potassium carbonate In N,N-dimethyl-formamide at 20℃; for 6h;95%
With potassium carbonate In N,N-dimethyl-formamide94%
With potassium carbonate In acetonitrile for 3h; Reflux;91%
2,4,6-trihydroxyacetophenone
480-66-0

2,4,6-trihydroxyacetophenone

3,5-dihydroxyphenol
108-73-6

3,5-dihydroxyphenol

Conditions
ConditionsYield
With tin(IV) chloride In 1,2-dichloro-ethane Heating;95%
2,4,6-trihydroxyacetophenone
480-66-0

2,4,6-trihydroxyacetophenone

acetyl chloride
75-36-5

acetyl chloride

3-acetyl-5,7-dihydroxy-2-methyl-chromen-4-one
1022-78-2

3-acetyl-5,7-dihydroxy-2-methyl-chromen-4-one

Conditions
ConditionsYield
Stage #1: 2,4,6-trihydroxyacetophenone With potassium carbonate In tetrahydrofuran at 20 - 50℃; for 1h;
Stage #2: acetyl chloride In tetrahydrofuran for 4h; Heating / reflux;
Stage #3: With hydrogenchloride In tetrahydrofuran; water
95%
With 1,8-diazabicyclo[5.4.0]undec-7-ene In pyridine at 80 - 90℃; for 7h;51%
bromethyl methyl ether
13057-17-5

bromethyl methyl ether

2,4,6-trihydroxyacetophenone
480-66-0

2,4,6-trihydroxyacetophenone

2,4,6-tri-MOM phloracetophenone
36804-11-2

2,4,6-tri-MOM phloracetophenone

Conditions
ConditionsYield
With sodium hydride In tetrahydrofuran; mineral oil at 0℃; for 3h;95%
2,4,6-trihydroxyacetophenone
480-66-0

2,4,6-trihydroxyacetophenone

2-hydroxy-4,6-dimethoxyacetophenone
90-24-4

2-hydroxy-4,6-dimethoxyacetophenone

Conditions
ConditionsYield
With potassium carbonate; dimethyl sulfate In acetone94.4%
With dimethylsulfide; potassium carbonate In acetone at 20℃;
2,4,6-trihydroxyacetophenone
480-66-0

2,4,6-trihydroxyacetophenone

chloromethyl methyl ether
107-30-2

chloromethyl methyl ether

2'-hydroxy-4',6'-bis(methoxymethoxy)acetophenone
65490-09-7

2'-hydroxy-4',6'-bis(methoxymethoxy)acetophenone

Conditions
ConditionsYield
Stage #1: 2,4,6-trihydroxyacetophenone With N-ethyl-N,N-diisopropylamine In dichloromethane at 0℃; Inert atmosphere;
Stage #2: chloromethyl methyl ether In dichloromethane at 0 - 20℃;
94%
With N-ethyl-N,N-diisopropylamine In dichloromethane at 0 - 20℃; for 0.25h; Inert atmosphere;94%
With potassium carbonate In acetone Reflux;90%
2,4,6-trihydroxyacetophenone
480-66-0

2,4,6-trihydroxyacetophenone

tert-butyldimethylsilyl chloride
18162-48-6

tert-butyldimethylsilyl chloride

1-(2,4-bis((tert-butyldimethylsilyl)oxy)-6-hydroxyphenyl)-2-ethan-1-one
108956-90-7

1-(2,4-bis((tert-butyldimethylsilyl)oxy)-6-hydroxyphenyl)-2-ethan-1-one

Conditions
ConditionsYield
With 1H-imidazole In N,N-dimethyl-formamide for 0.5h;94%
With 1H-imidazole In N,N-dimethyl-formamide for 2h;92%
With triethylamine In dichloromethane at 20℃; for 1.5h; Inert atmosphere;83%
2,4,6-trihydroxyacetophenone
480-66-0

2,4,6-trihydroxyacetophenone

p-toluenesulfonyl chloride
98-59-9

p-toluenesulfonyl chloride

4-acetyl-5-hydroxy-1,3-phenylene bis(4-methylbenzenesulfonate)
68097-14-3

4-acetyl-5-hydroxy-1,3-phenylene bis(4-methylbenzenesulfonate)

Conditions
ConditionsYield
With potassium carbonate In acetone Inert atmosphere; Reflux;94%
With potassium carbonate In acetone for 5h; Reflux;
chloro-trimethyl-silane
75-77-4

chloro-trimethyl-silane

2,4,6-trihydroxyacetophenone
480-66-0

2,4,6-trihydroxyacetophenone

2,4,6-tris(trimethylsilyloxy)acetophenone

2,4,6-tris(trimethylsilyloxy)acetophenone

Conditions
ConditionsYield
With triethylamine In diethyl ether at 7℃; Heating;93%
Farnesal
502-67-0

Farnesal

2,4,6-trihydroxyacetophenone
480-66-0

2,4,6-trihydroxyacetophenone

C38H52O4

C38H52O4

Conditions
ConditionsYield
With ethylenediamine diacetic acid In dichloromethane at 20℃; for 10h;93%
2,4,6-trihydroxyacetophenone
480-66-0

2,4,6-trihydroxyacetophenone

triisopropylsilyl trifluoromethanesulfonate
80522-42-5

triisopropylsilyl trifluoromethanesulfonate

1-(2-hydroxy-4,6-diisopropylsilyloxyphenyl)ethanone
1198596-15-4

1-(2-hydroxy-4,6-diisopropylsilyloxyphenyl)ethanone

Conditions
ConditionsYield
Stage #1: 2,4,6-trihydroxyacetophenone With triethylamine In dichloromethane; water at -78 - 20℃; Inert atmosphere;
Stage #2: triisopropylsilyl trifluoromethanesulfonate In dichloromethane; water at -78℃; for 1h; Inert atmosphere;
93%
2,4,6-trihydroxyacetophenone
480-66-0

2,4,6-trihydroxyacetophenone

acetic anhydride
108-24-7

acetic anhydride

2,4-diacetylphloroglucinol
2161-86-6

2,4-diacetylphloroglucinol

Conditions
ConditionsYield
With boron trifluoride diethyl etherate; acetic acid for 21h; Heating;92%
With boron trifluoride diethyl etherate at 20℃; for 24h; Acetylation;90%
Stage #1: 2,4,6-trihydroxyacetophenone; acetic anhydride With boron trifluoride diethyl etherate In acetic acid Marchand reaction; Reflux;
Stage #2: With sodium hydroxide In methanol for 5h;
Stage #3: With hydrogenchloride In methanol; water
2,4,6-trihydroxyacetophenone
480-66-0

2,4,6-trihydroxyacetophenone

o-chlorobenzoyl chloride
609-65-4

o-chlorobenzoyl chloride

2',4',6'-tris(2-chlorobenzoyloxy)acetophenone
920006-70-8

2',4',6'-tris(2-chlorobenzoyloxy)acetophenone

Conditions
ConditionsYield
With pyridine; dmap at 20℃; for 3h;92%
2,4,6-trihydroxyacetophenone
480-66-0

2,4,6-trihydroxyacetophenone

methyl trifluoromethanesulfonate
333-27-7

methyl trifluoromethanesulfonate

2-hydroxy-4,6-dimethoxyacetophenone
90-24-4

2-hydroxy-4,6-dimethoxyacetophenone

Conditions
ConditionsYield
With potassium carbonate In acetone at 0 - 70℃; for 10h;92%
With potassium carbonate In acetone for 3h; Reflux;88%
2-iodo-propane
75-30-9

2-iodo-propane

2,4,6-trihydroxyacetophenone
480-66-0

2,4,6-trihydroxyacetophenone

1-(2-hydroxy-4,6-diisopropoxyphenyl)ethanone
93344-48-0

1-(2-hydroxy-4,6-diisopropoxyphenyl)ethanone

Conditions
ConditionsYield
With potassium carbonate In N,N-dimethyl-formamide at 60℃; for 10h; Inert atmosphere;92%
2,4,6-trihydroxyacetophenone
480-66-0

2,4,6-trihydroxyacetophenone

ethyl phloroglucinol
94632-41-4

ethyl phloroglucinol

Conditions
ConditionsYield
With hydrogenchloride; sodium cyanoborohydride In methanol; water for 12h;91%
With amalgamated zinc; ethanol; acetic acid weiteres Reagens: wss. HCl;
With hydrogenchloride; sodium cyanoborohydride In methanol for 24h;100 % Spectr.
With dimethylamine borane In tetrahydrofuran for 24h; Heating;
2,4,6-trihydroxyacetophenone
480-66-0

2,4,6-trihydroxyacetophenone

N,N-dimethyl-formamide
68-12-2, 33513-42-7

N,N-dimethyl-formamide

3'-formyl-2',4',6'-trihydroxyacetophenone
62018-55-7

3'-formyl-2',4',6'-trihydroxyacetophenone

Conditions
ConditionsYield
Stage #1: 2,4,6-trihydroxyacetophenone; N,N-dimethyl-formamide With trichlorophosphate In ethyl acetate at 20℃; for 1h; Vilsmeier-Haack Formylation;
Stage #2: In water; ethyl acetate
91%
With trichlorophosphate at 20℃;70%
With trichlorophosphate In ethyl acetate at 20℃; for 1h; Vilsmeier-Haack Formylation; Cooling with ice;64.7%
With trichlorophosphate In ethyl acetate at 20℃; for 0.5h; Vilsmeier-Haack formylation;
bromethyl methyl ether
13057-17-5

bromethyl methyl ether

2,4,6-trihydroxyacetophenone
480-66-0

2,4,6-trihydroxyacetophenone

2'-hydroxy-4',6'-bis(methoxymethoxy)acetophenone
65490-09-7

2'-hydroxy-4',6'-bis(methoxymethoxy)acetophenone

Conditions
ConditionsYield
With N-ethyl-N,N-diisopropylamine In dichloromethane at 0 - 20℃; for 5h; Inert atmosphere;91%
Stage #1: bromethyl methyl ether; 2,4,6-trihydroxyacetophenone With N-ethyl-N,N-diisopropylamine In dichloromethane for 0.333333h; Cooling with ice;
Stage #2: bromethyl methyl ether In dichloromethane for 12.3h;
75.5%
With N-ethyl-N,N-diisopropylamine In dichloromethane at 3℃; for 3h; Inert atmosphere;74.5%
With potassium carbonate In acetone for 3h; Heating;68%
With potassium carbonate In acetone for 3h; Reflux;68%
2,4,6-trihydroxyacetophenone
480-66-0

2,4,6-trihydroxyacetophenone

isobutyryl chloride
79-30-1

isobutyryl chloride

1-(3-acetyl-2,4,6-trihydroxyphenyl)-2-methylpropan-1-one

1-(3-acetyl-2,4,6-trihydroxyphenyl)-2-methylpropan-1-one

Conditions
ConditionsYield
With silica sulphuric acid In neat (no solvent) at 60℃; Friedel-Crafts Acylation; Green chemistry;91%
With methanesulfonic acid; acetic acid In neat (no solvent) at 80℃; for 0.25h; Temperature; Friedel-Crafts Acylation; Inert atmosphere;

Hot Products

Post buying leads

About|Contact|Cas|Product Name|Molecular|Country|Encyclopedia

Message|New Cas|MSDS|Service|Advertisement|CAS DataBase|Article Data|Manufacturers | Chemical Catalog

©2008 LookChem.com,License: ICP

NO.:Zhejiang16009103

complaints:service@lookchem.com Desktop View