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inquiryAbout Product Details SCYLLO-INOSITOL Basic information Product Name: SCYLLO-INOSITOL Synonyms: COCOSITOL;Inositol, scyllo-;QUERCINITOL;SCYLLITO;SCYLLITOL;SCYLLO-INOSITOL;Scyllito
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superior quality Appearance:?White Crystalline Solid Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:1kg/bag, 1kg/drum or 25kg/drum or as per your request. Application:scyllo-Inositol, acyclohexanehexol derivative
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myo-inositol
Conditions | Yield |
---|---|
With water; trifluoroacetic acid at 20℃; for 1h; | 94% |
With trifluoroacetic acid for 2h; | |
With trifluoroacetic acid In water |
1-O-benzoyl-scyllo-inositol
myo-inositol
Conditions | Yield |
---|---|
With sodium methylate In methanol for 3h; Hydrolysis; Heating; | 88% |
myo-inositol
Conditions | Yield |
---|---|
Stage #1: 1-O-allyl-2,5-di-O-benzyl-scyllo-inositol With methanol; 10percent Pd/C for 6h; Heating; Stage #2: With hydrogenchloride at 80℃; Stage #3: With hydrogen; 10percent Pd/C In methanol; water for 12h; Further stages.; | 85% |
Penta-O-acetyl-myo-inosose
myo-inositol
Conditions | Yield |
---|---|
With sodium tetrahydroborate In methanol for 0.5h; Ambient temperature; | 78% |
Conditions | Yield |
---|---|
With ethanol; nickel at 125℃; under 95616 Torr; Hydrogenation; |
1,2:4,5-Dianhydro-epi-inositol
A
neo-inositol
B
myo-inositol
chiro-inositol
Conditions | Yield |
---|---|
With sulfuric acid for 3h; Heating; | A 15 % Spectr. B 5 % Spectr. C 80 % Spectr. |
1,2:4,5-Dianhydro-muco-inosit
A
D-myo-inositol
B
muco-inositol
C
myo-inositol
chiro-inositol
Conditions | Yield |
---|---|
With sulfuric acid for 3h; Heating; | A 0.5 % Spectr. B 80 % Spectr. C 0.5 % Spectr. D 19 % Spectr. |
Conditions | Yield |
---|---|
nickel In water for 24h; Heating; Yield given; | |
Stage #1: D-myo-inositol; lyo Acetobactor Species In water at 28℃; under 1018.63 Torr; for 120h; pH=~ 4 - 7; Enzymatic reaction; Industry scale; Stage #2: With sodium hydroxide In water at 120 - 125℃; for 0.166667h; pH=12 - 13; Product distribution / selectivity; Industry scale; |
Conditions | Yield |
---|---|
With sodium amalgam; acetic acid Trennung von dem Stereoisomeren ueber das Hexaacetyl-Derivat; | |
With water; platinum Hydrogenation; |
myo-inositol
Conditions | Yield |
---|---|
With hydrogen; palladium dihydroxide In methanol at 20℃; for 24h; | 18.4 mg |
(+)-(1S,2R,3R,4S)-1,4-diacetoxy-2,3-dibromocyclohex-5-ene
myo-inositol
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1.1: 80 percent / sodium / tetrahydrofuran / 13 h / 0 - 20 °C 2.1: 71 percent / aq. H2O2; trifluoroacetic anhydride; Na2CO3 / CH2Cl2 / 3 h / 20 °C 3.1: 96 percent / PPTS / acetone / 16 h / 20 °C 4.1: sodium / 24 h / 90 °C 4.2: 60 percent / aq. HCl / tetrahydrofuran / 20 °C 5.1: methanol / 10percent Pd/C / 6 h / Heating 5.2: aq. HCl / 80 °C 5.3: 85 percent / H2 / 10percent Pd/C / methanol; H2O / 12 h View Scheme |
(1R,2S,3S,4R)-1,4-di-O-benzylconduritol B
myo-inositol
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1.1: 71 percent / aq. H2O2; trifluoroacetic anhydride; Na2CO3 / CH2Cl2 / 3 h / 20 °C 2.1: 96 percent / PPTS / acetone / 16 h / 20 °C 3.1: sodium / 24 h / 90 °C 3.2: 60 percent / aq. HCl / tetrahydrofuran / 20 °C 4.1: methanol / 10percent Pd/C / 6 h / Heating 4.2: aq. HCl / 80 °C 4.3: 85 percent / H2 / 10percent Pd/C / methanol; H2O / 12 h View Scheme |
2,3-anhydro-1,4-di-O-benzyl-myo-inositol
myo-inositol
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: 96 percent / PPTS / acetone / 16 h / 20 °C 2.1: sodium / 24 h / 90 °C 2.2: 60 percent / aq. HCl / tetrahydrofuran / 20 °C 3.1: methanol / 10percent Pd/C / 6 h / Heating 3.2: aq. HCl / 80 °C 3.3: 85 percent / H2 / 10percent Pd/C / methanol; H2O / 12 h View Scheme |
myo-inositol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: sodium / 24 h / 90 °C 1.2: 60 percent / aq. HCl / tetrahydrofuran / 20 °C 2.1: methanol / 10percent Pd/C / 6 h / Heating 2.2: aq. HCl / 80 °C 2.3: 85 percent / H2 / 10percent Pd/C / methanol; H2O / 12 h View Scheme |
myo-inositol
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1.1: 1.99 g / Me2SO; oxalyl chloride / CH2Cl2 / 1 h / -78 °C 2.1: 99 percent / sodium borohydride / methanol; tetrahydrofuran / 0.5 h / 20 °C 3.1: MeONa / methanol / 12 h / Heating 3.2: 98 percent / pyridine / 24 h / 20 °C 4.1: 98 percent / iso-butylamine / methanol / 12 h / Heating 5.1: 94 percent / trifluoroacetic acid; water / 1 h / 20 °C View Scheme |
myo-inositol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 98 percent / iso-butylamine / methanol / 12 h / Heating 2: 94 percent / trifluoroacetic acid; water / 1 h / 20 °C View Scheme |
myo-inositol
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: MeONa / methanol / 12 h / Heating 1.2: 98 percent / pyridine / 24 h / 20 °C 2.1: 98 percent / iso-butylamine / methanol / 12 h / Heating 3.1: 94 percent / trifluoroacetic acid; water / 1 h / 20 °C View Scheme |
myo-inositol
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1.1: 99 percent / sodium borohydride / methanol; tetrahydrofuran / 0.5 h / 20 °C 2.1: MeONa / methanol / 12 h / Heating 2.2: 98 percent / pyridine / 24 h / 20 °C 3.1: 98 percent / iso-butylamine / methanol / 12 h / Heating 4.1: 94 percent / trifluoroacetic acid; water / 1 h / 20 °C View Scheme |
myo-inositol
Conditions | Yield |
---|---|
Multi-step reaction with 6 steps 1.1: 2.01 g / iso-butylamine / methanol / 12 h / Heating 2.1: 1.99 g / Me2SO; oxalyl chloride / CH2Cl2 / 1 h / -78 °C 3.1: 99 percent / sodium borohydride / methanol; tetrahydrofuran / 0.5 h / 20 °C 4.1: MeONa / methanol / 12 h / Heating 4.2: 98 percent / pyridine / 24 h / 20 °C 5.1: 98 percent / iso-butylamine / methanol / 12 h / Heating 6.1: 94 percent / trifluoroacetic acid; water / 1 h / 20 °C View Scheme |
methyl 2,3,4-tri-O-benzyl-D-glucopyranoside
myo-inositol
Conditions | Yield |
---|---|
Multi-step reaction with 6 steps 1: N,N-dicyclohexylcarbodiimide; trifluoroacetic acid; pyridine / dimethylsulfoxide; benzene / 24 h / 20 °C 2: Et3N; 4-(dimethylamino)pyridine / 1,2-dichloro-ethane / 3 h / Heating 3: PdCl2 / dioxane; H2O / 3 h / 60 °C 4: NaBH4 / methanol / 0.5 h / 0 °C 5: NaOH / methanol / 12 h / 20 °C 6: 18.4 mg / H2 / Pd(OH)2/C / methanol / 24 h / 20 °C View Scheme | |
Multi-step reaction with 6 steps 1: N,N-dicyclohexylcarbodiimide; trifluoroacetic acid; pyridine / dimethylsulfoxide; benzene / 24 h / 20 °C 2: Et3N; 4-(dimethylamino)pyridine / 1,2-dichloro-ethane / 3 h / Heating 3: PdCl2 / dioxane; H2O / 3 h / 60 °C 4: NaBH4 / methanol / 0.5 h / 0 °C 5: NaOH / methanol / 12 h / 20 °C 6: 18.4 mg / H2 / Pd(OH)2/C / methanol / 24 h / 20 °C View Scheme |
methyl 6-aldehydo-2,3,4-tri-O-benzyl-α-D-glucopyranoside
myo-inositol
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1: Et3N; 4-(dimethylamino)pyridine / 1,2-dichloro-ethane / 3 h / Heating 2: PdCl2 / dioxane; H2O / 3 h / 60 °C 3: NaBH4 / methanol / 0.5 h / 0 °C 4: NaOH / methanol / 12 h / 20 °C 5: 18.4 mg / H2 / Pd(OH)2/C / methanol / 24 h / 20 °C View Scheme | |
Multi-step reaction with 5 steps 1: Et3N; 4-(dimethylamino)pyridine / 1,2-dichloro-ethane / 3 h / Heating 2: PdCl2 / dioxane; H2O / 3 h / 60 °C 3: NaBH4 / methanol / 0.5 h / 0 °C 4: NaOH / methanol / 12 h / 20 °C 5: 18.4 mg / H2 / Pd(OH)2/C / methanol / 24 h / 20 °C View Scheme |
(1R,2S,3S,4R,5S)-3,4,5-tribenzyloxy-2-hydroxy-6-oxocyclohexyl acetate
myo-inositol
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: NaBH4 / methanol / 0.5 h / 0 °C 2: NaOH / methanol / 12 h / 20 °C 3: 18.4 mg / H2 / Pd(OH)2/C / methanol / 24 h / 20 °C View Scheme |
(E)-methyl 6-O-acetyl-2,3,4-tri-O-benzyl-α-D-gluco-hex-5-enopyranoside
myo-inositol
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: PdCl2 / dioxane; H2O / 3 h / 60 °C 2: NaBH4 / methanol / 0.5 h / 0 °C 3: NaOH / methanol / 12 h / 20 °C 4: 18.4 mg / H2 / Pd(OH)2/C / methanol / 24 h / 20 °C View Scheme |
(Z)-methyl 6-O-acetyl-2,3,4-tri-O-benzyl-α-D-gluco-hex-5-enopyranoside
myo-inositol
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: PdCl2 / dioxane; H2O / 3 h / 60 °C 2: NaBH4 / methanol / 0.5 h / 0 °C 3: NaOH / methanol / 12 h / 20 °C 4: 18.4 mg / H2 / Pd(OH)2/C / methanol / 24 h / 20 °C View Scheme |
D-1-O-acetyl-3,4,5-tri-O-benzyl-scyllo-inositol
myo-inositol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: NaOH / methanol / 12 h / 20 °C 2: 18.4 mg / H2 / Pd(OH)2/C / methanol / 24 h / 20 °C View Scheme |
methanol
sodium tetrahydroborate
A
Trimethyl borate
B
myo-inositol
Conditions | Yield |
---|---|
With sulfuric acid with concd. H2SO4; | |
With H2SO4; scyllomyo-inosose with concd. H2SO4; |
myo-inositol
Conditions | Yield |
---|---|
With sulfuric acid; water at 36 - 43℃; for 5h; pH=2 - 3.5; Industry scale; | |
With hydrogenchloride; water at 85 - 95℃; Product distribution / selectivity; |
D-myo-inositol
A
1L-chiro-inositol
B
neo-inositol
C
myo-inositol
Conditions | Yield |
---|---|
nickel In water at 95 - 100℃; Product distribution / selectivity; |
Conditions | Yield |
---|---|
With cellobiase In aq. buffer at 40℃; for 20h; pH=7.0; Enzymatic reaction; |
Conditions | Yield |
---|---|
for 1h; Reflux; | 89% |
Conditions | Yield |
---|---|
In water for 1h; Reflux; | 89% |
myo-inositol
4-methylphenylboronic acid
tetra(n-butyl)ammonium hydroxide
Conditions | Yield |
---|---|
In water for 1h; Reflux; | 89% |
Conditions | Yield |
---|---|
for 1h; Reflux; | 87% |
Conditions | Yield |
---|---|
for 1h; Reflux; | 86% |
Conditions | Yield |
---|---|
In water for 1h; Reflux; | 86% |
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid In N,N-dimethyl-formamide at 100℃; for 22h; Inert atmosphere; | 84% |
Conditions | Yield |
---|---|
In water for 1h; Reflux; | 84% |
In water for 1h; Reflux; | 84% |
Conditions | Yield |
---|---|
for 1h; Reflux; | 82% |
myo-inositol
n-octanoic acid chloride
1,2,3,4,5,6-all-trans-Hexakis(octanoyloxy)cyclohexane
Conditions | Yield |
---|---|
With trifluoroacetic acid for 2h; Ambient temperature; | 74% |
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid In toluene Inert atmosphere; Reflux; | 71% |
myo-inositol
Dibenzyl N,N-diisopropylphosphoramidite
Conditions | Yield |
---|---|
Stage #1: myo-inositol; Dibenzyl N,N-diisopropylphosphoramidite With 1H-tetrazole In N,N-dimethyl-formamide; acetonitrile at 20℃; for 24h; Stage #2: With dihydrogen peroxide In water; N,N-dimethyl-formamide; acetonitrile at 0 - 20℃; for 12h; pH=7; Aqueous sodium phosphate buffer; | 55% |
Stage #1: myo-inositol; Dibenzyl N,N-diisopropylphosphoramidite With N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 20℃; for 24h; phosphorylation; Stage #2: With dihydrogen peroxide In phosphate buffer at 20℃; pH=7; Oxidation; | 44% |
myo-inositol
N,N-diethyl-1,5-dihydro-3H-2,4,3-benzodioxaphosphepin-3-amine
Conditions | Yield |
---|---|
Stage #1: myo-inositol; N,N-diethyl-1,5-dihydro-3H-2,4,3-benzodioxaphosphepin-3-amine With 1H-tetrazole In dichloromethane at 20℃; Stage #2: With 3-chloro-benzenecarboperoxoic acid In dichloromethane at 20℃; for 1h; Further stages.; | 40% |
Conditions | Yield |
---|---|
Stage #1: myo-inositol; benzyl bromide With tetrabutylammomium bromide; di(n-butyl)tin oxide; N-ethyl-N,N-diisopropylamine In neat (no solvent) at 90℃; for 2.5h; Stage #2: With tetrabutylammomium bromide; di(n-butyl)tin oxide; N-ethyl-N,N-diisopropylamine In neat (no solvent) at 90℃; for 6.5h; regioselective reaction; | 40% |
Conditions | Yield |
---|---|
Stage #1: C29H41ClN2O2; myo-inositol With pyridine In dichloromethane for 24h; Reflux; Inert atmosphere; Stage #2: In dichloromethane at 60℃; for 12h; Sealed flask; Large scale reaction; | 19.6% |
myo-inositol
Conditions | Yield |
---|---|
With hydrogenchloride; acetic acid at 160℃; isoinositol; | |
With hydrogenchloride; acetic acid at 160℃; pseudoinositol; |
Conditions | Yield |
---|---|
With zinc(II) chloride scyllitol hexaacetate; |
Nonanoyl chloride
myo-inositol
1,2,3,4,5,6-all-trans-Hexakis(nonanoyloxy)cyclohexane
Conditions | Yield |
---|---|
In trifluoroacetic acid Ambient temperature; |
2-(pentylthio)acetic acid
myo-inositol
Pentylsulfanyl-acetic acid 2,3,4,5,6-pentakis-(2-pentylsulfanyl-acetoxy)-cyclohexyl ester
Conditions | Yield |
---|---|
With trifluoroacetic acid for 18h; Ambient temperature; |
5-Chlorovaleroyl chloride
myo-inositol
5-Chloro-pentanoic acid 2,3,4,5,6-pentakis-(5-chloro-pentanoyloxy)-cyclohexyl ester
Conditions | Yield |
---|---|
In trifluoroacetic acid Ambient temperature; |
5-bromovaleroyl chloride
myo-inositol
5-Bromo-pentanoic acid 2,3,4,5,6-pentakis-(5-bromo-pentanoyloxy)-cyclohexyl ester
Conditions | Yield |
---|---|
In trifluoroacetic acid Ambient temperature; |
6-bromohexanoyl chloride
myo-inositol
6-Bromo-hexanoic acid 2,3,4,5,6-pentakis-(6-bromo-hexanoyloxy)-cyclohexyl ester
Conditions | Yield |
---|---|
In trifluoroacetic acid Ambient temperature; |
3-Butyloxypropanoic acid
myo-inositol
3-Butoxy-propionic acid 2,3,4,5,6-pentakis-(3-butoxy-propionyloxy)-cyclohexyl ester
Conditions | Yield |
---|---|
With trifluoroacetic acid for 18h; Ambient temperature; |
3-(butylthio)propionic acid
myo-inositol
3-Butylsulfanyl-propionic acid 2,3,4,5,6-pentakis-(3-butylsulfanyl-propionyloxy)-cyclohexyl ester
Conditions | Yield |
---|---|
With trifluoroacetic acid for 18h; Ambient temperature; |
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