We are manufacturer of this product. If you are looking for the material's manufacturer or supplier in China, Ality Group is your best choice. Specifications of our 5-Propyl-1,3-benzenediol CAS 500-49-2: Items
Cas:500-49-2
Min.Order:1 Gram
FOB Price: $2.0 / 3.0
Type:Other
inquiry5-Propyl-1,3-benzenediol Basic information Product Name: 5-Propyl-1,3-benzenediol 5-Propyl-1,3-benzenediol;Divarinol;1,3-Benzenediol, 5-propyl- CAS: 500-49-2 MF: C9H12O2 MW: 152.19 EINECS: Product Categories: Mol File: 500-49-2
Cas:500-49-2
Min.Order:1 Kilogram
FOB Price: $0.01 / 0.02
Type:Lab/Research institutions
inquiryUnique advantages Guaranteed purity High quality & competitive price Quality control Fast feedback Prompt shipment Appearance:Off-white to yellow or Khaki powder Storage:cool dry place Package:1kg/foil bag;25kg/drum Application:pharmaceutic
Cas:500-49-2
Min.Order:1 Kilogram
Negotiable
Type:Trading Company
inquiryOur main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
Cas:500-49-2
Min.Order:5 Kiloliter
FOB Price: $1.2 / 5.0
Type:Manufacturers
inquiryOur company was built in 2009 with an ISO certificate.In the past 5 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so on.O
Cas:500-49-2
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryOur advantages: 1. High quality and competitive price: 1) Standard: BP/USP/EP/ enterprise standard 2) All purity ≥99% 3) We are manufacturers and can provide high quality products at factory prices. 2. Fast and safe delivery 1) The package c
Cas:500-49-2
Min.Order:1 Kilogram
FOB Price: $5.0 / 10.0
Type:Trading Company
inquiryAppearance:Light yellow to off-white solid Storage:Keep in a cool, dry and airtight place Package:25kg/drum Application:Intermediate of organic synthesis Transportation:Express/Sea/Air Port:Any port in China
Cas:500-49-2
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiry1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized
Cas:500-49-2
Min.Order:1 Kilogram
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Type:Lab/Research institutions
inquiryOur Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We
Cas:500-49-2
Min.Order:10 Kilogram
Negotiable
Type:Trading Company
inquiry5-Propyl-1,3-benzenediol CAS:500-49-2 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic in
Cas:500-49-2
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
Cas:500-49-2
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryOur company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At present,
Cas:500-49-2
Min.Order:1 Gram
FOB Price: $90.0
Type:Trading Company
inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
Cas:500-49-2
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
Cas:500-49-2
Min.Order:0 Metric Ton
Negotiable
Type:Lab/Research institutions
inquiry5-propylbenzene-1,3-diol CAS 500-49-2 Description Purity: 99% Min Application: Intermediates Appearance: Powder Package: Bag Delivery: 3-5days Our Advantage & Service 1.Top quality: Using high quality material and establishing a st
Cas:500-49-2
Min.Order:1 Kilogram
FOB Price: $10.0 / 50.0
Type:Trading Company
inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:500-49-2
Min.Order:10 Gram
FOB Price: $100.0
Type:Lab/Research institutions
inquiryWe are one of a few suppliers that can offer custom synthesis service of this product We are specialized in custom synthesis, chemical/pharmaceutical/ pesticides outsourcing and contract research. We are committed to prov
Cas:500-49-2
Min.Order:100 Gram
FOB Price: $100.0 / 2000.0
Type:Lab/Research institutions
inquiryEstablished in May 2015, TaiChem Ltd. is initially invested by a British research and development company and started by PhDs back from aboard. The company is registered in China Medical City (CMC), Taizhou, Jiangsu Province, and the production site
Cas:500-49-2
Min.Order:10 Gram
Negotiable
Type:Lab/Research institutions
inquiryWhy is SINOWAY: 1) Specialized in pharmaceutical and healthcare industrial for 34 years. 2) ISO 9001:2015 & SGS audited supplier . 3) Accept various payment terms : T.T 30-60 days. 4) We have warehouse in USA with quickly shipment . 5) We c
Cas:500-49-2
Min.Order:1 Kilogram
Negotiable
Type:Trading Company
inquiryProduct name: 5-Propylbenzene-1,3-Diol CAS No.:500-49-2 Molecule Formula:C9H12O2 Molecule Weight:152.19 Purity: 99.0% Package: 25kg/drum Description:White crystalline powder Manufacture Standards:Enterprise Standard TESTING ITEMS
Cas:500-49-2
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryOur Advantages A. International Top level TechnologyOur company owned biomedicine experts are famous at home and abroad with rich experience in research and development in the field of efficient chiral functional molecules research and development an
Cas:500-49-2
Min.Order:0
Negotiable
Type:Trading Company
inquiryfactory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B
Cas:500-49-2
Min.Order:1 Kilogram
FOB Price: $18.0 / 20.0
Type:Trading Company
inquiry1.High Quality: Quality is life. Quality is the most important element for all goods. We have a lab doing research in Wuhan China and produce sarms in bulk quantity. We have 8 years experience making all kinds of sarms. And all our old customers thr
Cas:500-49-2
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryProduct Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
Cas:500-49-2
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryZhenyu biotech exported this product to many countries and regions at best price. if you are looking for the material's manufacturer or supplier in china, zhenyu biotech is your best choice. pls contact with us freely for getting detailed
Cas:500-49-2
Min.Order:1 Kilogram
FOB Price: $2.0
Type:Lab/Research institutions
inquiryShandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W
Cas:500-49-2
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiry1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer
Cas:500-49-2
Min.Order:1 Metric Ton
FOB Price: $1.5
Type:Trading Company
inquiryGOLDEN PHARMA CO.,LIMITED.is a professional pharmaceutical company,our team have more than 20years expereince in pharmaceutical production and sales. we are a professional technical enterprise specializing in the R & D, production,QA regulation
We are a Union of chemistry in China, consists of chemists,engineers, laboratories,factories in China. We organize surplus capacity of R&D and production as well as custom synthesis for chemical products and chemical business project. We are supp
Cas:500-49-2
Min.Order:1 Metric Ton
FOB Price: $1.0
Type:Trading Company
inquiryStock products, own laboratory Package:Grams, Kilograms Application:For R&D Transportation:According to customer request Port:Shanghai
Cas:500-49-2
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiry1,3-dimethoxy-5-propylbenzene
5-propyl-1,3-benzenediol
Conditions | Yield |
---|---|
With hydrogen bromide; acetic acid In water at 125℃; for 3h; Inert atmosphere; | 99% |
With hydrogen iodide; acetic anhydride for 1h; Heating; | 90% |
With hydrogen bromide; acetic acid for 3h; Heating; | 70% |
Conditions | Yield |
---|---|
With hydrogen iodide |
Conditions | Yield |
---|---|
With potassium hydroxide | |
With hydrogen iodide | |
Multi-step reaction with 2 steps 1: natrium carbonate 2: hydriodic acid View Scheme | |
Multi-step reaction with 2 steps 1: natrium carbonate 2: alkalies View Scheme | |
Multi-step reaction with 2 steps 1: alkali 2: hydriodic acid View Scheme |
Conditions | Yield |
---|---|
With water | |
With alkalies |
2-Bromo-3-hydroxy-5-propyl-cyclohex-2-enone
5-propyl-1,3-benzenediol
Conditions | Yield |
---|---|
With acetic acid |
2,4-dihydroxy-6-propylbenzoic acid ethyl ester
5-propyl-1,3-benzenediol
Conditions | Yield |
---|---|
With sodium hydroxide In water Heating; |
3-allylresorcinol
5-propyl-1,3-benzenediol
Conditions | Yield |
---|---|
With triphenyl phosphite; hydrogen In chloroform at 25℃; Rate constant; Mechanism; |
1,3-dimethoxy-5-propylbenzene
hydrogen iodide
5-propyl-1,3-benzenediol
divaricatic acid
A
5-propyl-1,3-benzenediol
B
carbon dioxide
C
2-hydroxy-4-methoxy-6-propylbenzoic acid
2-hydroxy-4-methoxy-6-propylbenzoic acid
hydrogen iodide
A
5-propyl-1,3-benzenediol
B
carbon dioxide
C
methyl iodide
divaricatic acid
hydrogen iodide
A
5-propyl-1,3-benzenediol
B
carbon dioxide
C
methyl iodide
2-hydroxy-4-(2-hydroxy-4-methoxy-6-pentyl-benzoyloxy)-6-propyl-benzoic acid
A
5-propyl-1,3-benzenediol
B
2-hydroxy-4-methoxy-6-pentylbenzoic acid
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1: Et3N / tetrahydrofuran / 1 h / 0 - 20 °C 2: 62 percent / Li, naphthalene / tetrahydrofuran / 2 h / -30 - 0 °C 3: 69 percent / Et3N / tetrahydrofuran / 1.08 h / 0 °C 4: 60 percent / NaI, Zn / 1,2-dimethoxy-ethane / 8 h / Heating 5: 70 percent / 45percent HBr, glacial AcOH / 3 h / Heating View Scheme |
1-(3,5-dimethoxyphenyl)propan-2-ol
5-propyl-1,3-benzenediol
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 69 percent / Et3N / tetrahydrofuran / 1.08 h / 0 °C 2: 60 percent / NaI, Zn / 1,2-dimethoxy-ethane / 8 h / Heating 3: 70 percent / 45percent HBr, glacial AcOH / 3 h / Heating View Scheme |
3,5-dimethoxybenzyl trimethylsilyl ether
5-propyl-1,3-benzenediol
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: 62 percent / Li, naphthalene / tetrahydrofuran / 2 h / -30 - 0 °C 2: 69 percent / Et3N / tetrahydrofuran / 1.08 h / 0 °C 3: 60 percent / NaI, Zn / 1,2-dimethoxy-ethane / 8 h / Heating 4: 70 percent / 45percent HBr, glacial AcOH / 3 h / Heating View Scheme |
Methanesulfonic acid 2-(3,5-dimethoxy-phenyl)-1-methyl-ethyl ester
5-propyl-1,3-benzenediol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 60 percent / NaI, Zn / 1,2-dimethoxy-ethane / 8 h / Heating 2: 70 percent / 45percent HBr, glacial AcOH / 3 h / Heating View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 1.) Mg; MeI / diethyl ether / 1.) 3 h, reflux; 2.) 1 h, reflux 2: hydrogen, conc. H2SO4 / 10percent Pd-C / ethyl acetate / 4 h / 2942.03 Torr / Ambient temperature 3: NaI, ClSiMe3 / acetonitrile / 36 h / Heating View Scheme | |
Multi-step reaction with 3 steps 1: diethyl ether / 1 h / 0 °C 2: hydrogen; palladium 10% on activated carbon; sulfuric acid / ethanol / 4 h / 3040.2 Torr 3: boron tribromide / dichloromethane / 2 h / -15 - 20 °C / Inert atmosphere View Scheme | |
Multi-step reaction with 3 steps 1.1: n-butyllithium / hexane; tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere 1.2: 0 - 20 °C / Inert atmosphere 2.1: 5%-palladium/activated carbon; hydrogen / ethyl acetate / 2 h 3.1: acetic acid; hydrogen bromide / water / 3 h / 125 °C / Inert atmosphere View Scheme |
1-(3,5-dimethoxy-phenyl)-propan-1-ol
5-propyl-1,3-benzenediol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: hydrogen, conc. H2SO4 / 10percent Pd-C / ethyl acetate / 4 h / 2942.03 Torr / Ambient temperature 2: NaI, ClSiMe3 / acetonitrile / 36 h / Heating View Scheme | |
Multi-step reaction with 2 steps 1: hydrogen; palladium 10% on activated carbon; sulfuric acid / ethanol / 4 h / 3040.2 Torr 2: boron tribromide / dichloromethane / 2 h / -15 - 20 °C / Inert atmosphere View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1: 89 percent / (COCl)2 / benzene / 2 h, room t., 1 h, reflux 2: 70 percent / NaOAc, H2 / 10percent Pd-C / 2427.2 Torr / 1h, then 60 degC, overnight 3: 1.) Mg; MeI / diethyl ether / 1.) 3 h, reflux; 2.) 1 h, reflux 4: hydrogen, conc. H2SO4 / 10percent Pd-C / ethyl acetate / 4 h / 2942.03 Torr / Ambient temperature 5: NaI, ClSiMe3 / acetonitrile / 36 h / Heating View Scheme | |
Multi-step reaction with 8 steps 4: 28.8 g / fluoroboric acid, sodium nitrite / H2O 5: 7.6 g / warming, distillation 6: 1.) lithium / 1.) ether, 2 h 7: Cu-quinoline 8: boron tribromide, pyridine hydrochloride / CH2Cl2 / 24 h / -78 °C View Scheme | |
Multi-step reaction with 7 steps 4: 28.8 g / fluoroboric acid, sodium nitrite / H2O 5: 7.6 g / warming, distillation 6: 63.5 percent / lithium chips / diethyl ether / 0.5 h 7: boron tribromide, pyridine hydrochloride / CH2Cl2 / 24 h / -78 °C View Scheme | |
Multi-step reaction with 3 steps 1: 85 percent / diethyl ether / 1.) from -78 deg C to 0 deg C , 1.5 h, 2.) RT, 18 h 2: 1.) H2N4*H2O, 2.) KOH / 1.) EtOH, reflux, 6 h, 2.) 230 deg C, 0.5 h 3: 90 percent / Ac2O, HI / 1 h / Heating View Scheme | |
Multi-step reaction with 6 steps 1: thionyl chloride; N,N-dimethyl-formamide / toluene / 6 h / 100 °C 2: triethylamine / dichloromethane / 0 °C 3: 2-methyltetrahydrofuran / 5 h / 0 °C 4: hydrazine hydrate / ethanol / 6 h / Reflux 5: potassium hydroxide / 0.5 h / 230 °C 6: pyridine hydrochloride / 4 h / 200 °C View Scheme |
3,5-dimethoxybenzoyl chloride
5-propyl-1,3-benzenediol
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: 70 percent / NaOAc, H2 / 10percent Pd-C / 2427.2 Torr / 1h, then 60 degC, overnight 2: 1.) Mg; MeI / diethyl ether / 1.) 3 h, reflux; 2.) 1 h, reflux 3: hydrogen, conc. H2SO4 / 10percent Pd-C / ethyl acetate / 4 h / 2942.03 Torr / Ambient temperature 4: NaI, ClSiMe3 / acetonitrile / 36 h / Heating View Scheme | |
Multi-step reaction with 7 steps 3: 28.8 g / fluoroboric acid, sodium nitrite / H2O 4: 7.6 g / warming, distillation 5: 1.) lithium / 1.) ether, 2 h 6: Cu-quinoline 7: boron tribromide, pyridine hydrochloride / CH2Cl2 / 24 h / -78 °C View Scheme | |
Multi-step reaction with 6 steps 3: 28.8 g / fluoroboric acid, sodium nitrite / H2O 4: 7.6 g / warming, distillation 5: 63.5 percent / lithium chips / diethyl ether / 0.5 h 6: boron tribromide, pyridine hydrochloride / CH2Cl2 / 24 h / -78 °C View Scheme | |
Multi-step reaction with 5 steps 1: triethylamine / dichloromethane / 0 °C 2: 2-methyltetrahydrofuran / 5 h / 0 °C 3: hydrazine hydrate / ethanol / 6 h / Reflux 4: potassium hydroxide / 0.5 h / 230 °C 5: pyridine hydrochloride / 4 h / 200 °C View Scheme |
ethyl 3,5-dimethoxybenzoate
5-propyl-1,3-benzenediol
Conditions | Yield |
---|---|
Multi-step reaction with 12 steps 1: 78 percent / hydrazine hydrate / 2 h / Heating 2: 63 percent / sodium nitrite, hydrochloric acid (2M), acetic acid (glacial) / H2O / 1 h / -10 °C 3: 93 percent / toluene / 2.5 h / Heating 4: 8.7 g / sodium hydroxide (20percent) / 60 °C 8: 28.8 g / fluoroboric acid, sodium nitrite / H2O 9: 7.6 g / warming, distillation 10: 1.) lithium / 1.) ether, 2 h 11: Cu-quinoline 12: boron tribromide, pyridine hydrochloride / CH2Cl2 / 24 h / -78 °C View Scheme | |
Multi-step reaction with 11 steps 1: 78 percent / hydrazine hydrate / 2 h / Heating 2: 63 percent / sodium nitrite, hydrochloric acid (2M), acetic acid (glacial) / H2O / 1 h / -10 °C 3: 93 percent / toluene / 2.5 h / Heating 4: 8.7 g / sodium hydroxide (20percent) / 60 °C 8: 28.8 g / fluoroboric acid, sodium nitrite / H2O 9: 7.6 g / warming, distillation 10: 63.5 percent / lithium chips / diethyl ether / 0.5 h 11: boron tribromide, pyridine hydrochloride / CH2Cl2 / 24 h / -78 °C View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 9 steps 1: 84 percent / sodium hydroxide / heating 5: 28.8 g / fluoroboric acid, sodium nitrite / H2O 6: 7.6 g / warming, distillation 7: 1.) lithium / 1.) ether, 2 h 8: Cu-quinoline 9: boron tribromide, pyridine hydrochloride / CH2Cl2 / 24 h / -78 °C View Scheme | |
Multi-step reaction with 8 steps 1: 84 percent / sodium hydroxide / heating 5: 28.8 g / fluoroboric acid, sodium nitrite / H2O 6: 7.6 g / warming, distillation 7: 63.5 percent / lithium chips / diethyl ether / 0.5 h 8: boron tribromide, pyridine hydrochloride / CH2Cl2 / 24 h / -78 °C View Scheme |
3,5-dimethoxybenzamide
5-propyl-1,3-benzenediol
Conditions | Yield |
---|---|
Multi-step reaction with 6 steps 2: 28.8 g / fluoroboric acid, sodium nitrite / H2O 3: 7.6 g / warming, distillation 4: 1.) lithium / 1.) ether, 2 h 5: Cu-quinoline 6: boron tribromide, pyridine hydrochloride / CH2Cl2 / 24 h / -78 °C View Scheme | |
Multi-step reaction with 5 steps 2: 28.8 g / fluoroboric acid, sodium nitrite / H2O 3: 7.6 g / warming, distillation 4: 63.5 percent / lithium chips / diethyl ether / 0.5 h 5: boron tribromide, pyridine hydrochloride / CH2Cl2 / 24 h / -78 °C View Scheme |
2,4-dimethoxy-6-propylbenzoic acid
5-propyl-1,3-benzenediol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: Cu-quinoline 2: boron tribromide, pyridine hydrochloride / CH2Cl2 / 24 h / -78 °C View Scheme |
azido(3,5-dimethoxyphenyl)methanone
5-propyl-1,3-benzenediol
Conditions | Yield |
---|---|
Multi-step reaction with 10 steps 1: 93 percent / toluene / 2.5 h / Heating 2: 8.7 g / sodium hydroxide (20percent) / 60 °C 6: 28.8 g / fluoroboric acid, sodium nitrite / H2O 7: 7.6 g / warming, distillation 8: 1.) lithium / 1.) ether, 2 h 9: Cu-quinoline 10: boron tribromide, pyridine hydrochloride / CH2Cl2 / 24 h / -78 °C View Scheme | |
Multi-step reaction with 9 steps 1: 93 percent / toluene / 2.5 h / Heating 2: 8.7 g / sodium hydroxide (20percent) / 60 °C 6: 28.8 g / fluoroboric acid, sodium nitrite / H2O 7: 7.6 g / warming, distillation 8: 63.5 percent / lithium chips / diethyl ether / 0.5 h 9: boron tribromide, pyridine hydrochloride / CH2Cl2 / 24 h / -78 °C View Scheme |
3,5-dimethoxy-benzoic acid hydrazide
5-propyl-1,3-benzenediol
Conditions | Yield |
---|---|
Multi-step reaction with 11 steps 1: 63 percent / sodium nitrite, hydrochloric acid (2M), acetic acid (glacial) / H2O / 1 h / -10 °C 2: 93 percent / toluene / 2.5 h / Heating 3: 8.7 g / sodium hydroxide (20percent) / 60 °C 7: 28.8 g / fluoroboric acid, sodium nitrite / H2O 8: 7.6 g / warming, distillation 9: 1.) lithium / 1.) ether, 2 h 10: Cu-quinoline 11: boron tribromide, pyridine hydrochloride / CH2Cl2 / 24 h / -78 °C View Scheme | |
Multi-step reaction with 10 steps 1: 63 percent / sodium nitrite, hydrochloric acid (2M), acetic acid (glacial) / H2O / 1 h / -10 °C 2: 93 percent / toluene / 2.5 h / Heating 3: 8.7 g / sodium hydroxide (20percent) / 60 °C 7: 28.8 g / fluoroboric acid, sodium nitrite / H2O 8: 7.6 g / warming, distillation 9: 63.5 percent / lithium chips / diethyl ether / 0.5 h 10: boron tribromide, pyridine hydrochloride / CH2Cl2 / 24 h / -78 °C View Scheme |
3,5-dimethoxyfluorobenzene
5-propyl-1,3-benzenediol
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 1.) lithium / 1.) ether, 2 h 2: Cu-quinoline 3: boron tribromide, pyridine hydrochloride / CH2Cl2 / 24 h / -78 °C View Scheme | |
Multi-step reaction with 2 steps 1: 63.5 percent / lithium chips / diethyl ether / 0.5 h 2: boron tribromide, pyridine hydrochloride / CH2Cl2 / 24 h / -78 °C View Scheme |
5-propyl-1,3-benzenediol
Conditions | Yield |
---|---|
Stage #1: 5-propyl-1,3-benzenediol With bromine In dichloromethane at -50℃; for 0.5h; Stage #2: With sodium thiosulfate In dichloromethane; water at 0℃; Temperature; | 82% |
Conditions | Yield |
---|---|
With triethylamine In acetonitrile at 70℃; for 8h; | 69% |
diethyl 2-acetylglutarate
5-propyl-1,3-benzenediol
3-(5-hydroxy-4-methyl-2-oxo-7-propyl-2H-chromen-3-yl)-propionic acid ethyl ester
Conditions | Yield |
---|---|
With trichlorophosphate | 61% |
5-propyl-1,3-benzenediol
4-benzyloxy-2-hydroxy-6-pentylbenzoic acid
Conditions | Yield |
---|---|
With dicyclohexyl-carbodiimide In toluene for 47h; Ambient temperature; | 58% |
Conditions | Yield |
---|---|
With boron trifluoride diethyl etherate In dichloromethane for 0.116667h; Flow reactor; | A 56% B 30% |
Conditions | Yield |
---|---|
With dicyclohexyl-carbodiimide In toluene for 120h; Ambient temperature; | A 38% B 13% |
5-propyl-1,3-benzenediol
(-)-trans-Isopiperitenol
Conditions | Yield |
---|---|
With aluminum oxide; boron trifluoride diethyl etherate In dichloromethane for 0.00277778h; Inert atmosphere; Reflux; | A 37% B 12% C 18% |
5-propyl-1,3-benzenediol
(S)-cis-Verbenol
Propyl-delta(8)-tetrahydrocannabiol
Conditions | Yield |
---|---|
With trifluorormethanesulfonic acid In dichloromethane at 0 - 20℃; for 3h; | 20% |
hydrogen cyanide
5-propyl-1,3-benzenediol
2,4-dihydroxy-6-propylbenzaldehyde
Conditions | Yield |
---|---|
With diethyl ether durch Erhitzen des Reaktionsprodukts mit Wasser; |
5-propyl-1,3-benzenediol
Conditions | Yield |
---|---|
With bromine; acetic acid |
Conditions | Yield |
---|---|
With sodium acetate at 85℃; | |
With pyridine Acetylation; |
5-propyl-1,3-benzenediol
ethyl 4-methyl-2-cyclohexanone-1-carboxylate
1-hydroxy-9-methyl-3-propyl-7,8,9,10-tetrahydro-benzo[c]chromen-6-one
Conditions | Yield |
---|---|
With trichlorophosphate; benzene |
5-propyl-1,3-benzenediol
Conditions | Yield |
---|---|
With trichlorophosphate; benzene |
5-propyl-1,3-benzenediol
2,4-dihydroxy-6-propylbenzaldehyde
Conditions | Yield |
---|---|
With hydrogenchloride; diethyl ether durch Erhitzen des Reaktionsprodukts mit Wasser; |
5-propyl-1,3-benzenediol
pulegone
trichlorophosphate
benzene
5-propyl-1,3-benzenediol
trichlorophosphate
benzene
1-hydroxy-9-methyl-3-propyl-7,8,9,10-tetrahydro-benzo[c]chromen-6-one
hydrogenchloride
diethyl ether
5-propyl-1,3-benzenediol
2,4-dihydroxy-6-propylbenzaldehyde
Conditions | Yield |
---|---|
Kochen des Reaktionsprodukts mit Wasser; |
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