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Hebei Nengqian Chemical Import and Export Co., LTD

Our Advantage Rich Experience Our products are sold all over Europe,North&South America, Sino-East, Asia and pacific area as well as Africa,we establish long term. Quality service Company cooperates with research institutes. We strictly con

548-35-6 TRUXENE

Cas:548-35-6

Min.Order:1 Kilogram

FOB Price: $15.0 / 50.0

Type:Trading Company

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Zhuozhou Wenxi import and Export Co., Ltd

WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et

Pharmaceutical Grade CAS 548-35-6 with competitive price

Cas:548-35-6

Min.Order:1 Kilogram

FOB Price: $139.0 / 210.0

Type:Trading Company

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Shijiazhuang Sdyano Fine Chemical Co., Ltd

1. Best prices with satisfied quality; 2. It's clients' right to choose the package's Courier (EMS, DHL, FedEx, UPS); 3.It's clients' right to choose the packing way for his produccts from many recent effective packing ways;

TRUXENE

Cas:548-35-6

Min.Order:0 Metric Ton

Negotiable

Type:Trading Company

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Shanghai Upbio Tech Co.,Ltd

1.In No Less 10 years exporting experience. you can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specializ

5H-Tribenzo[a,f,k]trindene,10,15-dihydro-

Cas:548-35-6

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Hangzhou J&H Chemical Co., Ltd.

J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

5H-Tribenzo[a,f,k]trindene,10,15-dihydro-

Cas:548-35-6

Min.Order:0

Negotiable

Type:Lab/Research institutions

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TAIZHOU ZHENYU BIOTECHNOLOGY CO., LTD

Zhenyu biotech exported this product to many countries and regions at best price. if you are looking for the material's manufacturer or supplier in china, zhenyu biotech is your best choice. pls contact with us freely for getting detailed

TRUXENE

Cas:548-35-6

Min.Order:1 Kilogram

FOB Price: $2.0

Type:Lab/Research institutions

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Kono Chem Co.,Ltd

high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou

10,15-dihydro-5H-tribenzo[a,f,k]triindene

Cas:548-35-6

Min.Order:0

Negotiable

Type:Other

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Henan Allgreen Chemical Co.,Ltd

high quality Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea

Truxene

Cas:548-35-6

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Hebei Sankai Chemical Technology Co., Ltd

1. Product advantages? High purity, all above 98.5%, no impurities after dissolution? We will test each batch to ensure quality? OEM and private brand services designed for free? Various cap colors available? We can also provide MT1 peptide powder2.

TRUXENE

Cas:548-35-6

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Antimex Chemical Limied

TruxeneAppearance:detailed in specifications Storage:Keep away of light, cool place Package:25kg/drum;200kg/drum Application:An important raw material and intermediate used in Organic Synthesis, Pharmaceuticals Transportation:Sea/air/courier

Truxene

Cas:548-35-6

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Hangzhou Fandachem Co.,Ltd

5H-Tribenzo[a,f,k]trindene,10,15-dihydro- cas 548-35-6Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express

5H-Tribenzo[a,f,k]trindene,10,15-dihydro- cas 548-35-6

Cas:548-35-6

Min.Order:0

Negotiable

Type:Other

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ZHEJIANG JIUZHOU CHEM CO.,LTD

factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin

TRUXENE

Cas:548-35-6

Min.Order:0

Negotiable

Type:Trading Company

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Jilin haofei import and export trade Co.,Ltd

Price, service, company and transport advantage: 1. Best service, place of origin China, high quality, and reasonable price. 2. It's customers' right to choose the package (EMS, DHL, FEDEX, UPS). 3. It's customers' right

Truxene CAS NO.548-35-6

Cas:548-35-6

Min.Order:0

Negotiable

Type:Trading Company

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XinChem Corporation

We have our own research and development center, provide reliable quality products for you. Appearance:white powder Storage:Store in dry and cool place. Application:Pharmaceutical intermediates

the lowest price Truxene 98% supplier

Cas:548-35-6

Min.Order:0 Metric Ton

Negotiable

Type:Other

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Nanjing Chemlin Chemical Co., Ltd.

Compound sourcing ServicesAgency of testing serviceFactory audit serviceFounded in Dec. 1999, Nanjing Chemlin Chemical Industrial Co.,Ltd(CHEMLIN) has been covering the business scope from trading of chemicals to custom-synthesis & Manufacturing. Co

548-35-6

Cas:548-35-6

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Cerametek Materials（ShenZhen）Co., Ltd.

sub/micron to mesh powders (near/spheres, whiskers, flake, fiber, porous) and grain/ball, thin/ thick metal / alloys pieces / parts, thin and thick (particle) film materials /target, and custom-made crystals, substrates/parts. In the industries and a

10,15-Dihydro-5H-tribenzo[a,f,k]triindene

Cas:548-35-6

Min.Order:0

Negotiable

Type:Other

inquiry

Novo nordisk inc

5H-Tribenzo[a,f,k]trindene,10,15-dihydro- 548-35-6 Storage:as prescribe by the manaufacturer Package:pack as requested

5H-Tribenzo[a,f,k]trindene,10,15-dihydro-

Cas:548-35-6

Min.Order:60 Kilogram

Negotiable

Type:Trading Company

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View More

Synthetic route

inden-1-one
83-33-0

inden-1-one

truxene
548-35-6

truxene

Conditions
ConditionsYield
With hydrogenchloride; acetic acid In water at 100℃; for 16h;100%
With hydrogenchloride; acetic acid at 100℃; for 16h;98%
With hydrogenchloride; acetic acid In water at 120℃; for 10h;90%
truxenone
4430-15-3

truxenone

truxene
548-35-6

truxene

Conditions
ConditionsYield
With hydrazine hydrate In diethylene glycol at 180℃; for 24h; Temperature; Wolff-Kishner Reduction;85%
With acetic anhydride; zinc
3-(methylthio)indene
90474-54-7

3-(methylthio)indene

methyl iodide
74-88-4

methyl iodide

truxene
548-35-6

truxene

Conditions
ConditionsYield
In dichloromethane for 12h; Heating;66%
inden-1-one
83-33-0

inden-1-one

2-indanone
615-13-4

2-indanone

A

truxene
548-35-6

truxene

B

isotruxene
17509-71-6

isotruxene

Conditions
ConditionsYield
With hydrogenchloride; acetic acid at 100℃; for 12h;A 15%
B 61%
...Expand
3-Phenylpropionic acid
501-52-0

3-Phenylpropionic acid

truxene
548-35-6

truxene

Conditions
ConditionsYield
Stage #1: 3-Phenylpropionic acid at 60 - 65℃; for 1h; Inert atmosphere;
Stage #2: With water at 160℃; for 3h; Inert atmosphere;		57%
With PPA at 60 - 170℃;50%
With polyphosphoric acid at 60 - 160℃; for 3h; Inert atmosphere;49%
inden-1-one
83-33-0

inden-1-one

A

truxene
548-35-6

truxene

B

2-(2,3-dihydro-1H-inden-1-ylidene)-2,3-dihydro-1H-inden-1-one
17563-12-1

2-(2,3-dihydro-1H-inden-1-ylidene)-2,3-dihydro-1H-inden-1-one

Conditions
ConditionsYield
η-benzene-η-pentamethylcyclopentadienylrhodium(III) tetrafluoroborate at 200℃; for 5h; aldol condensation;A 54%
B 42%
Methyl fluorosulfonate
421-20-5

Methyl fluorosulfonate

3-(methylthio)indene
90474-54-7

3-(methylthio)indene

A

truxene
548-35-6

truxene

B

trimethylsulfonium fluorosulfonate

trimethylsulfonium fluorosulfonate

C

2-(3-Indenyl)-3-(methylthio)inden

2-(3-Indenyl)-3-(methylthio)inden

Conditions
ConditionsYield
In tetrachloromethane at -30℃; for 1h;A 4%
B n/a
C 26%
...Expand
3,4-Diphenyl-2,5-thiophendimethanol
87694-43-7

3,4-Diphenyl-2,5-thiophendimethanol

A

truxene
548-35-6

truxene

B

5,7-Dihydrodiindeno<2,1-b:1',2'-d>thiophen
7099-34-5

5,7-Dihydrodiindeno<2,1-b:1',2'-d>thiophen

Conditions
ConditionsYield
With PPA In xylene for 3h; Ambient temperature;A n/a
B 11%
4b,4c,9b,9c-tetrahydro-cyclobuta[1,2-a;3,4-a']diindene-5,10-dione
17062-22-5, 21899-40-1, 28289-76-1

4b,4c,9b,9c-tetrahydro-cyclobuta[1,2-a;3,4-a']diindene-5,10-dione

truxene
548-35-6

truxene

Conditions
ConditionsYield
With phosphorus; hydrogen iodide at 180℃;
Multi-step reaction with 2 steps
1: bei der Destillation
View Scheme
2,3-dihydro-3'H-[1,2']biindenyliden-1'-one
5706-06-9

2,3-dihydro-3'H-[1,2']biindenyliden-1'-one

truxene
548-35-6

truxene

Conditions
ConditionsYield
With sulfuric acid
With phosphorus pentaoxide
inden-1-one
83-33-0

inden-1-one

A

truxene
548-35-6

truxene

B

2,3-dihydro-3'H-[1,2']biindenyliden-1'-one
5706-06-9

2,3-dihydro-3'H-[1,2']biindenyliden-1'-one

Conditions
ConditionsYield
With zinc(II) chloride
With acetic acid; zinc(II) chloride at 140℃;
With sulfuric acid; water
1-indene
95-13-6

1-indene

truxene
548-35-6

truxene

Conditions
ConditionsYield
at 400℃; unter Druck;
With molybdenum oxide-coal at 300℃; unter 100 at Wasserstoff-Druck;
1-indene
95-13-6

1-indene

A

truxene
548-35-6

truxene

B

INDANE
496-11-7

INDANE

Conditions
ConditionsYield
beim Destillieren, Polymerisation;
1-(2-Cyan-phenyl)-pentanon-(3)
105104-77-6

1-(2-Cyan-phenyl)-pentanon-(3)

truxene
548-35-6

truxene

Conditions
ConditionsYield
With sulfuric acid In acetic acid
3,5-Diphenyl-2,4-thiophendimethanol
87694-21-1

3,5-Diphenyl-2,4-thiophendimethanol

A

truxene
548-35-6

truxene

B

6,11-Dihydrodiindeno<1,2-b:1',2'-d>thiophen
87292-48-6

6,11-Dihydrodiindeno<1,2-b:1',2'-d>thiophen

Conditions
ConditionsYield
With PPA In xylene for 3h; Ambient temperature; Yield given;
3-Phenylpropionic acid
501-52-0

3-Phenylpropionic acid

P2O5

P2O5

truxene
548-35-6

truxene

hydrogenchloride
7647-01-0

hydrogenchloride

inden-1-one
83-33-0

inden-1-one

A

truxene
548-35-6

truxene

B

2--indanone-(1)

2--indanone-(1)

Conditions
ConditionsYield
at 100℃;
...Expand
sulfuric acid
7664-93-9

sulfuric acid

inden-1-one
83-33-0

inden-1-one

A

truxene
548-35-6

truxene

B

2,3-dihydro-3'H-[1,2']biindenyliden-1'-one
5706-06-9

2,3-dihydro-3'H-[1,2']biindenyliden-1'-one

...Expand
bromo-truxone

bromo-truxone

truxene
548-35-6

truxene

Conditions
ConditionsYield
With phosphorus; hydrogen iodide at 180℃;
coumaroneresin

coumaroneresin

truxene
548-35-6

truxene

Conditions
ConditionsYield
bei der Destillation;
dichloroindene

dichloroindene

truxene
548-35-6

truxene

Conditions
ConditionsYield
With hydrogen iodide at 200℃;
polyindene

polyindene

truxene
548-35-6

truxene

Conditions
ConditionsYield
at 200 - 220℃; im Rohr;
at 400℃; unter Druck;
With calcium chloride at 270℃;
bei der Destillation;
With calcium chloride at 270℃;
polymer(ic) indene

polymer(ic) indene

truxene
548-35-6

truxene

Conditions
ConditionsYield
With hydrogen at 360℃; under 73550.8 Torr;
inden-1-one
83-33-0

inden-1-one

A

truxene
548-35-6

truxene

B

2--indanone-(1)

2--indanone-(1)

Conditions
ConditionsYield
With zinc(II) chloride auf Siedetemperatur;
With acetic acid; zinc(II) chloride at 140℃;
1-indene
95-13-6

1-indene

A

truxene
548-35-6

truxene

B

hydrindene and polymerization products of indene

hydrindene and polymerization products of indene

polymer(ic) indene

polymer(ic) indene

A

truxene
548-35-6

truxene

B

isotruxene
17509-71-6

isotruxene

Conditions
ConditionsYield
With hydrogen at 360℃; under 73550.8 Torr;
sulfuric acid
7664-93-9

sulfuric acid

2,3-dihydro-3'H-[1,2']biindenyliden-1'-one
5706-06-9

2,3-dihydro-3'H-[1,2']biindenyliden-1'-one

truxene
548-35-6

truxene

hydrogenchloride
7647-01-0

hydrogenchloride

2,3-dihydro-3'H-[1,2']biindenyliden-1'-one
5706-06-9

2,3-dihydro-3'H-[1,2']biindenyliden-1'-one

acetic acid
64-19-7

acetic acid

inden-1-one
83-33-0

inden-1-one

truxene
548-35-6

truxene

Conditions
ConditionsYield
at 180℃;
...Expand
2,3-dihydro-3'H-[1,2']biindenyliden-1'-one
5706-06-9

2,3-dihydro-3'H-[1,2']biindenyliden-1'-one

acetic acid
64-19-7

acetic acid

inden-1-one
83-33-0

inden-1-one

ZnCl2

ZnCl2

truxene
548-35-6

truxene

Conditions
ConditionsYield
at 140℃;
...Expand
truxene
548-35-6

truxene

α,α'-dibromo-o-xylene
91-13-4

α,α'-dibromo-o-xylene

C51H36

C51H36

Conditions
ConditionsYield
Stage #1: truxene In tetrahydrofuran for 0.5h; Heating;
Stage #2: With potassium hydroxide In tetrahydrofuran for 0.5h; Heating;
Stage #3: α,α'-dibromo-o-xylene In tetrahydrofuran for 15h; Heating; Further stages.;		100%
1-bromo-hexane
111-25-1

1-bromo-hexane

truxene
548-35-6

truxene

5,5,10,10,15,15-hexahexyltruxene
600172-85-8

5,5,10,10,15,15-hexahexyltruxene

Conditions
ConditionsYield
Stage #1: truxene With n-butyllithium In tetrahydrofuran at -78℃; for 2h;
Stage #2: 1-bromo-hexane In tetrahydrofuran at -78 - 20℃;		100%
Stage #1: truxene With n-butyllithium In tetrahydrofuran at -78℃; for 2h; Inert atmosphere;
Stage #2: 1-bromo-hexane In tetrahydrofuran at 20℃; Inert atmosphere;		95%
Stage #1: truxene With n-butyllithium In tetrahydrofuran; hexane at -78 - 20℃; for 2.5h; Inert atmosphere;
Stage #2: 1-bromo-hexane In tetrahydrofuran; hexane at -78 - 20℃; for 12h;		95%
1-bromo-butane
109-65-9

1-bromo-butane

truxene
548-35-6

truxene

5,5',10,10',15,15'-hexabutyltruxene
870772-59-1

5,5',10,10',15,15'-hexabutyltruxene

Conditions
ConditionsYield
Stage #1: truxene With n-butyllithium In diethyl ether at -78℃; for 2h;
Stage #2: 1-bromo-butane In diethyl ether at -78 - 20℃;		98%
Stage #1: truxene With n-butyllithium In tetrahydrofuran; hexane at 0 - 20℃; Inert atmosphere;
Stage #2: 1-bromo-butane In tetrahydrofuran; hexane at 0 - 20℃; for 17.25h; Inert atmosphere;		96.1%
With potassium tert-butylate In tetrahydrofuran for 17h; Inert atmosphere; Reflux;87%
truxene
548-35-6

truxene

2,7,12-tribromo-10,15-dihydro-5H-diindeno[1,2-a;1',2'-c]fluorene
353752-15-5

2,7,12-tribromo-10,15-dihydro-5H-diindeno[1,2-a;1',2'-c]fluorene

Conditions
ConditionsYield
With bromine In dichloromethane at 20℃; for 20h; Reagent/catalyst; Solvent;97%
With bromine In dichloromethane at 25℃; for 16h; Inert atmosphere; Darkness;95%
With bromine In dichloromethane at 23℃; for 16h; in the dark;92%
1-bromohexene
13154-12-6, 13154-13-7, 57855-22-8

1-bromohexene

truxene
548-35-6

truxene

5,5,10,10,15,15-hexahexyltruxene
600172-85-8

5,5,10,10,15,15-hexahexyltruxene

Conditions
ConditionsYield
With potassium hydroxide In tetrahydrofuran; water for 0.333333h; Reflux; Microwave irradiation;95%
truxene
548-35-6

truxene

4-cyanobenzyl bromide
17201-43-3

4-cyanobenzyl bromide

5,5,10,10,15,15-hexakis[(4-cyanophenyl)methyl]-10,15-dihydro-5H-diindeno[1,2-a;1',2'-c]fluorene

5,5,10,10,15,15-hexakis[(4-cyanophenyl)methyl]-10,15-dihydro-5H-diindeno[1,2-a;1',2'-c]fluorene

Conditions
ConditionsYield
With potassium tert-butylate In tetrahydrofuran for 16h; Heating;94%
truxene
548-35-6

truxene

truxenone
4430-15-3

truxenone

Conditions
ConditionsYield
With air; graphene-supported KOH composite In N,N-dimethyl-formamide at 20℃; for 36h;93%
With potassium hydroxide In N,N-dimethyl-formamide at 20℃; for 20h;87%
With chromic acid
truxene
548-35-6

truxene

1-bromomethyl-4-bromobenzene
589-15-1

1-bromomethyl-4-bromobenzene

5,5,10,10,15,15-hexakis[(4-bromophenyl)methyl]-10,15-dihydro-5H-diindeno[1,2-a;1',2'-c]fluorene

5,5,10,10,15,15-hexakis[(4-bromophenyl)methyl]-10,15-dihydro-5H-diindeno[1,2-a;1',2'-c]fluorene

Conditions
ConditionsYield
With potassium tert-butylate In tetrahydrofuran for 16h; Heating;92%
1-bromo dodecane
112-29-8

1-bromo dodecane

truxene
548-35-6

truxene

5,5',10,10',15,15'-hexadecyltruxene

5,5',10,10',15,15'-hexadecyltruxene

Conditions
ConditionsYield
Stage #1: truxene With n-butyllithium In tetrahydrofuran at -78℃; for 2h; Inert atmosphere;
Stage #2: 1-bromo dodecane In tetrahydrofuran at 20℃; Inert atmosphere;		92%
With potassium tert-butylate In tetrahydrofuran for 3.5h; Inert atmosphere; Reflux;
truxene
548-35-6

truxene

4-bromo-3-bromomethyl-p-terphenyl
1422181-28-9

4-bromo-3-bromomethyl-p-terphenyl

C84H57Br3

C84H57Br3

Conditions
ConditionsYield
Stage #1: truxene With n-butyllithium In tetrahydrofuran; hexane at -78 - 0℃; for 1h; Inert atmosphere;
Stage #2: 4-bromo-3-bromomethyl-p-terphenyl In tetrahydrofuran; hexane for 2h;		91%
truxene
548-35-6

truxene

methyl iodide
74-88-4

methyl iodide

5,5,10,10,15,15-hexamethyl-10,15-dihydro-5H-diindeno[1,2-a:1',2'-c]fluorene

5,5,10,10,15,15-hexamethyl-10,15-dihydro-5H-diindeno[1,2-a:1',2'-c]fluorene

Conditions
ConditionsYield
Stage #1: truxene With n-butyllithium In tetrahydrofuran; hexane at -60 - 20℃; Inert atmosphere;
Stage #2: methyl iodide In tetrahydrofuran; hexane at -60 - 20℃; Inert atmosphere;
Stage #3: methyl iodide With n-butyllithium In tetrahydrofuran; hexane at -60 - 20℃; for 14h; Inert atmosphere;		88%
With potassium tert-butylate In tetrahydrofuran at 20℃; for 0.166667h; Inert atmosphere; Cooling with ice;72%
Stage #1: truxene With potassium tert-butylate In tetrahydrofuran Cooling with ice; Inert atmosphere;
Stage #2: methyl iodide In tetrahydrofuran Reflux; Inert atmosphere;		69%
Stage #1: truxene With potassium tert-butylate In tetrahydrofuran at 0℃;
Stage #2: methyl iodide Reflux;
truxene
548-35-6

truxene

benzyl bromide
100-39-0

benzyl bromide

5,5,10,10,15,15-hexakis(phenylmethyl)-10,15-dihydro-5H-diindeno[1,2-a;1',2'-c]fluorene

5,5,10,10,15,15-hexakis(phenylmethyl)-10,15-dihydro-5H-diindeno[1,2-a;1',2'-c]fluorene

Conditions
ConditionsYield
With potassium tert-butylate In tetrahydrofuran for 16h; Heating;86%
truxene
548-35-6

truxene

1-methoxynaphthalen-2-ylmethylX

1-methoxynaphthalen-2-ylmethylX

syn-5,10,15-tris(1-methoxynaphthalen-2-ylmethyl)-10,15-dihydro-5H-diindeno[1,2-a;1',2'-c]fluorene

syn-5,10,15-tris(1-methoxynaphthalen-2-ylmethyl)-10,15-dihydro-5H-diindeno[1,2-a;1',2'-c]fluorene

Conditions
ConditionsYield
Stage #1: truxene With n-butyllithium In tetrahydrofuran at -78 - -10℃; for 4h;
Stage #2: 1-methoxynaphthalen-2-ylmethylX In tetrahydrofuran for 0.5h;
Stage #3: With potassium tert-butylate In tert-butyl alcohol for 12h; Heating; Further stages.;		85%
1-bromo-octane
111-83-1

1-bromo-octane

truxene
548-35-6

truxene

5,5',10,10',15,15'-hexaoctyltruxene

5,5',10,10',15,15'-hexaoctyltruxene

Conditions
ConditionsYield
With potassium tert-butylate In tetrahydrofuran for 16h; Inert atmosphere; Reflux;85%
truxene
548-35-6

truxene

meta-bromobenzyl bromide
823-78-9

meta-bromobenzyl bromide

5,5,10,10,15,15-hexakis[(3-bromophenyl)methyl]-10,15-dihydro-5H-diindeno[1,2-a;1',2'-c]fluorene

5,5,10,10,15,15-hexakis[(3-bromophenyl)methyl]-10,15-dihydro-5H-diindeno[1,2-a;1',2'-c]fluorene

Conditions
ConditionsYield
Stage #1: truxene With potassium hydroxide In tetrahydrofuran for 0.5h; Heating;
Stage #2: meta-bromobenzyl bromide In tetrahydrofuran for 24h; Heating; Further stages.;		84%
With potassium tert-butylate In tetrahydrofuran for 16h; Heating;81%
truxene
548-35-6

truxene

allyl bromide
106-95-6

allyl bromide

5,5,10,10,15,15-hexakis(3-buten-1-yl)-10,15-dihydro-5H-diindeno[1,2-a;1',2'-c]fluorene

5,5,10,10,15,15-hexakis(3-buten-1-yl)-10,15-dihydro-5H-diindeno[1,2-a;1',2'-c]fluorene

Conditions
ConditionsYield
With potassium tert-butylate In tetrahydrofuran for 16h; Heating;83%
With potassium tert-butylate In tetrahydrofuran for 16h; Reflux;62%
truxene
548-35-6

truxene

3-(bromomethyl)benzonitrile
28188-41-2

3-(bromomethyl)benzonitrile

A

5-(3-cyanophenylmethyl)-10,15-dihydro-5H-diindeno[1,2-a;1',2'-c]fluorene

5-(3-cyanophenylmethyl)-10,15-dihydro-5H-diindeno[1,2-a;1',2'-c]fluorene

syn-5,10-bis(3-cyanophenylmethyl)-10,15-dihydro-5H-diindeno[1,2-a;1',2'-c]fluorene

syn-5,10-bis(3-cyanophenylmethyl)-10,15-dihydro-5H-diindeno[1,2-a;1',2'-c]fluorene

anti-5,10-bis(3-cyanophenylmethyl)-10,15-dihydro-5H-diindeno[1,2-a;1',2'-c]fluorene

anti-5,10-bis(3-cyanophenylmethyl)-10,15-dihydro-5H-diindeno[1,2-a;1',2'-c]fluorene

anti-5,10,15-tris(3-cyanophenylmethyl)-10,15-dihydro-5H-diindeno[1,2-a;1',2'-c]fluorene

anti-5,10,15-tris(3-cyanophenylmethyl)-10,15-dihydro-5H-diindeno[1,2-a;1',2'-c]fluorene

Conditions
ConditionsYield
Stage #1: truxene With n-butyllithium In tetrahydrofuran at -20℃; for 3h;
Stage #2: m-(bromomethyl)benzonitrile In tetrahydrofuran for 0.5h;
Stage #3: With potassium tert-butylate In tert-butyl alcohol for 12h; Heating;		A 82%
B n/a
C n/a
D n/a
...Expand
truxene
548-35-6

truxene

1,3-dibromo-propane
109-64-8

1,3-dibromo-propane

trispiro[truxene-5,1':10,1'':15,1'''-tris(cyclobutane)]

trispiro[truxene-5,1':10,1'':15,1'''-tris(cyclobutane)]

Conditions
ConditionsYield
Stage #1: truxene With n-butyllithium In tetrahydrofuran; cyclohexane at 0℃; for 0.5h;
Stage #2: 1,3-dibromo-propane In tetrahydrofuran; cyclohexane at 20℃; for 0.5h;
Stage #3: With n-butyllithium In tetrahydrofuran; cyclohexane at 20℃; for 6h;		80%
truxene
548-35-6

truxene

MeX

MeX

syn-5,10,15-trimethyl-10,15-dihydro-5H-diindeno[1,2-a;1',2'-c]fluorene

syn-5,10,15-trimethyl-10,15-dihydro-5H-diindeno[1,2-a;1',2'-c]fluorene

Conditions
ConditionsYield
Stage #1: truxene With n-butyllithium In tetrahydrofuran at -78 - -10℃; for 4h;
Stage #2: MeX In tetrahydrofuran for 0.5h;
Stage #3: With potassium tert-butylate In tert-butyl alcohol for 12h; Heating; Further stages.;		79%
truxene
548-35-6

truxene

4-cyanobenzyl bromide
17201-43-3

4-cyanobenzyl bromide

A

5-(4-cyanophenylmethyl)-10,15-dihydro-5H-diindeno[1,2-a;1',2'-c]fluorene

5-(4-cyanophenylmethyl)-10,15-dihydro-5H-diindeno[1,2-a;1',2'-c]fluorene

syn-5,10-bis(4-cyanophenylmethyl)-10,15-dihydro-5H-diindeno[1,2-a;1',2'-c]fluorene

syn-5,10-bis(4-cyanophenylmethyl)-10,15-dihydro-5H-diindeno[1,2-a;1',2'-c]fluorene

anti-5,10-bis(4-cyanophenylmethyl)-10,15-dihydro-5H-diindeno[1,2-a;1',2'-c]fluorene

anti-5,10-bis(4-cyanophenylmethyl)-10,15-dihydro-5H-diindeno[1,2-a;1',2'-c]fluorene

anti-5,10,15-tris(4-cyanophenylmethyl)-10,15-dihydro-5H-diindeno[1,2-a;1',2'-c]fluorene

anti-5,10,15-tris(4-cyanophenylmethyl)-10,15-dihydro-5H-diindeno[1,2-a;1',2'-c]fluorene

Conditions
ConditionsYield
Stage #1: truxene With n-butyllithium In tetrahydrofuran at -20℃; for 3h;
Stage #2: 4-cyanobenzyl bromide In tetrahydrofuran for 0.5h;
Stage #3: With potassium tert-butylate In tert-butyl alcohol for 12h; Heating;		A 77%
B n/a
C n/a
D n/a
...Expand
truxene
548-35-6

truxene

EtX

EtX

syn-5,10,15-triethyl-10,15-dihydro-5H-diindeno[1,2-a;1',2'-c]fluorene

syn-5,10,15-triethyl-10,15-dihydro-5H-diindeno[1,2-a;1',2'-c]fluorene

Conditions
ConditionsYield
Stage #1: truxene With n-butyllithium In tetrahydrofuran at -78 - -10℃; for 4h;
Stage #2: EtX In tetrahydrofuran for 0.5h;
Stage #3: With potassium tert-butylate In tert-butyl alcohol for 12h; Heating; Further stages.;		76%
truxene
548-35-6

truxene

meta-bromobenzyl bromide
823-78-9

meta-bromobenzyl bromide

syn-5,10,15-tris(3-bromophenylmethyl)-10,15-dihydro-5H-diindeno[1,2-a;1',2'-c]fluorene

syn-5,10,15-tris(3-bromophenylmethyl)-10,15-dihydro-5H-diindeno[1,2-a;1',2'-c]fluorene

Conditions
ConditionsYield
Stage #1: truxene With n-butyllithium In tetrahydrofuran at -78 - -10℃; for 4h;
Stage #2: meta-bromobenzyl bromide In tetrahydrofuran for 0.5h;
Stage #3: With potassium tert-butylate In tert-butyl alcohol for 12h; Heating; Further stages.;		75%
truxene
548-35-6

truxene

9-bromoethylanthracene
2417-77-8

9-bromoethylanthracene

5,5,10,10,15,15-hexakis(9-methylanthracenyl)-10,15-dihydro-5H-diindeno[1,2-a;1',2'-c]fluorene

5,5,10,10,15,15-hexakis(9-methylanthracenyl)-10,15-dihydro-5H-diindeno[1,2-a;1',2'-c]fluorene

Conditions
ConditionsYield
With potassium tert-butylate In tetrahydrofuran for 16h; Heating;75%
truxene
548-35-6

truxene

3-(bromomethyl)benzonitrile
28188-41-2

3-(bromomethyl)benzonitrile

5,5,10,10,15,15-hexakis[(3-cyanophenyl)methyl]-10,15-dihydro-5H-diindeno[1,2-a;1',2'-c]fluorene
869963-19-9

5,5,10,10,15,15-hexakis[(3-cyanophenyl)methyl]-10,15-dihydro-5H-diindeno[1,2-a;1',2'-c]fluorene

Conditions
ConditionsYield
With potassium tert-butylate In tetrahydrofuran for 16h; Heating;75%
ethyl bromide
74-96-4

ethyl bromide

truxene
548-35-6

truxene

10,15-dihydro-5H-diindenol[1, 2-a:10, 20-c]-fluorene
913080-60-1

10,15-dihydro-5H-diindenol[1, 2-a:10, 20-c]-fluorene

Conditions
ConditionsYield
With n-butyllithium In tetrahydrofuran; hexane at 0 - 20℃;74%
With potassium tert-butylate51%
With n-butyllithium
truxene
548-35-6

truxene

CH2=CHCH2X

CH2=CHCH2X

syn-5,10,15-tris(1-prop-2-enyl)-10,15-dihydro-5H-diindeno[1,2-a;1',2'-c]fluorene

syn-5,10,15-tris(1-prop-2-enyl)-10,15-dihydro-5H-diindeno[1,2-a;1',2'-c]fluorene

Conditions
ConditionsYield
Stage #1: truxene With n-butyllithium In tetrahydrofuran at -78 - -10℃; for 4h;
Stage #2: CH2=CHCH2X In tetrahydrofuran for 0.5h;
Stage #3: With potassium tert-butylate In tert-butyl alcohol for 12h; Heating; Further stages.;		73%
truxene
548-35-6

truxene

C6H5CH2X

C6H5CH2X

syn-5,10,15-tris(phenylmethyl)-10,15-dihydro-5H-diindeno[1,2-a;1',2'-c]fluorene

syn-5,10,15-tris(phenylmethyl)-10,15-dihydro-5H-diindeno[1,2-a;1',2'-c]fluorene

Conditions
ConditionsYield
Stage #1: truxene With n-butyllithium In tetrahydrofuran at -78 - -10℃; for 4h;
Stage #2: C6H5CH2X In tetrahydrofuran for 0.5h;
Stage #3: With potassium tert-butylate In tert-butyl alcohol for 12h; Heating; Further stages.;		69%
truxene
548-35-6

truxene

2-BrC6H4CH2X

2-BrC6H4CH2X

syn-5,10,15-tris(2-bromophenylmethyl)-10,15-dihydro-5H-diindeno[1,2-a;1',2'-c]fluorene

syn-5,10,15-tris(2-bromophenylmethyl)-10,15-dihydro-5H-diindeno[1,2-a;1',2'-c]fluorene

Conditions
ConditionsYield
Stage #1: truxene With n-butyllithium In tetrahydrofuran at -78 - -10℃; for 4h;
Stage #2: 2-BrC6H4CH2X In tetrahydrofuran for 0.5h;
Stage #3: With potassium tert-butylate In tert-butyl alcohol for 12h; Heating; Further stages.;		68%

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